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Jothinathan
Project Consultant
Centre for NonDestructive Evaluation-MDS
Dept. of Mechanical Engineering
Indian Institute of Technology, Madras, Chennai 600 036
Email gj@iitm.ac.in
Ph. 4218 4781
Cell 98411 07465
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PT
Fundamentals:
Interaction of penetrants and discontinuity
openings (properties required of penetrants)
Fluorescence and contrast (Types of penetrants)
Liquid penetrant testing:
Penetrant processes
Test equipment and system factors
Test result interpretation; discontinuity indications
Applications-
castings,
welds,
wrought metals,
machined parts,
leaks and
field inspections. Standard Blocks
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PT involves developing an indication of a
discontinuity and the indications width is
very much larger than the actual width of the
surface open discontinuities so as to be seen
or be detected by the unaided human eye
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PT can be classifed as a Surface NDT method
This method is not restricted to ferromagnetic
materials only like MT. It can be applied on all
materials ferrous and nonferrous metals and
also on nonmetals like rubber, plastics, ceramics
etc.
This is the major advantage over MT
But this method can detect only defects that are
on the surface and open to the surface
Cannot detect subsurface defects. This is one major disadvantage
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Used to locate cracks, porosity and other
defects that break the surface of a material.
Liquid penetrant testing is used to find flaws
in a large veriety of materials and in parts
ranging from spark plugs to jet engine fan blades
All defects that are open to the surface.
Rolled products-- cracks, seams, laminations.
Castings--cold shuts, hot tears, porosity, blow
holes, shrinkage.
Forgings cracks, laps, external bursts.
Welds cracks, porosity, undercut, overlap, lack
of fusion, lack of penetration.
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PT MT
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Penetrant Inspection
Penetrating
fluid applied
to clean surface of
component
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Penetrant Inspection
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Penetrant Inspection
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Penetrant Inspection
Developer applied to
surface
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Penetrant Inspection
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Advantages of Penetrant Inspection
Applicable to all materials metals and nonmetals
Able to test large parts with portable kit
Suitable for batch testing
May not require electricity or water
Applicable to small parts with complex geometry
Simple, cheap and easy to interpret
Sensitivity
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Disadvantages of Penetrant Inspection
Will only detect defects open to the surface
(Inclusion,segregation even on surface cannot be
detected-surface opening is required)
Requires careful surface preparation
Not normally applicable to porous surfaces(Filtered
particle P)
Mention some components that may be porous
Temperature dependant ( 4-49deg.C) Outside this
temperature say at 65 deg. C, how to go about
Cannot retest indefinitely- why
Compatibility of chemicals(penetrant and plastics
alkaline developer and Al)
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Penetrant Inspection
Types of Penetrant
Fluorescent Type I
Colour contrast-Type II
Dual- Type III
Based on the dye that is incorporated in penetrant
Dual- Type III
Contain both the dyes
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Types of Penetrant
Type Some details Remarks
Type I:Fluorescent dye Fluorescence Highly sensitive
(Brightness contrast) Emitting light Needs black light
/colour & dark room booth
Can be viewed Not that suitable
only under for field
black light (?) in applications
dark ambience
Type II Visible dye Visible red Sensitivity is low
Colour contrast colour in normal Good for field
light applications
Type III Dual Inspection Convenient to
Both the dyes under ambient operators for
light for gross immediate
discontinuities acceptance
Black light for /rejection
fine
discontinuities
1.White light for gross discontinuities-?-Decision-a or r
Black light and inspection for fine discontinuities
2. Large tanks and gun barrels inside fluorescent
Outside visible
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Visible Vs Fluorescent PT
Inspection can be
performed using visible (or
red dye) or fluorescent
penetrant materials.
Visible PT is performed under
white light while fluorescent
PT must be performed using
an ultraviolet light in a
darkened area. All are all in
the level 1 sensitivity range Photo Courtesy of Contesco
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Types are further classified into methods
Each of these are further classified as methods
1. Water washable WW ( Method A)
2. Post emulsifiable PE lippophilic (Method B)
3. Solvent removable SR (Method C )
4. Post emulsifiable Hydrophilic ( Method D)
-classification is based on the method by which the
excess penetrant is removed in the excess penetrant
removal step.
Simple water washing water washable A
Solvent wiping solvent removable C
Emulsifying &removing post emulsifiable B & D
Simple water washing is not possible as the
penetrant is organic oil base and hence the
penetrant contains one more constituent
namely emulsifier that is this is self emulsifying
compared to post emulsifing
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3. Removal of Excess Penetrant
Penetrating fluid removed from component surface
(but not from defect)
Water washable
Solvent Removable
Post Emulsifiable
Water washable single step advantage - simple
Post emulsifiable two steps close control of e.time
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Sensitivity levels
Classes of removers
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When the liquid will be penetrating
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Two main properties
Wettability- ability to spread over the surfac
Capillarity ability to rise in capillary
ability to enter into small openings
Where or on what
Summary
Penetrant required properties for
1.Penetration of dye into small openings ( T & )
2. Penetration in a reasonable time ( )
3.Safety of the operator(Flash point& nontoxicity)
4.Inertness towards materials (organic oils)-except
plastics
5. Long life and economy (stabilisers)
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Surface preparation
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Preparation of parts
3.1.2 The possible contaminants on the components are
1.Oil and grease
2. Rust or scales (Oxidation products)
3. Paints and conversion coatings
4. Carbon, Varnish etc
5. water
3.1.3 Sources
1. Surface protection against corrosion
2. Surface treatment for improvement of properties
3. Fabrication processes and subsequent treatment
3.1.4 Interference by contaminants
1.physical blocking of the discontinuity (eg
Rust or scale paint or conversion coatings)
2.disturbing the balanced composition of the
penetrant (eg. Oil, water etc)
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3. Entering and occupying the discontinuities. Oil, water etc)
Simple wiping Organic contaminants
Solvent Cleaning
Vapour degreasing like oil, grease etc
Ultrasonic cleaning
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Some machining, surface finishing and cleaning operations
(sand blasting, grit blasting) can cause a thin layer of metal to
smear on the surface and prevent penetrant from entering any
flaws that may be present.
Etching of the surface prior to inspection is sometimes required.
A
3 in
3/8 in.
2 in
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Table 2.4: Factors influencing the dwell time
6.Temperature of the
parts and penetrant
T , and
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How to remove an oil base penetrant from the surface oil in
shirt - same way oil base penetrant can be removed from the
surface
By use of solvents making a solution-solvent removable- petrol wash
By use of dispersants making a dispersion so as to be removed by
water- PE -detergents Wash- soap & use of detergent powder
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Removal of excess penetrant
The excess surface penetrant on the surface is
carefully removed without affecting the penetrant
that is residing in the discontinuity.
This is an important step as the unremoved excess
surface penetrant will affect subsequently by
affecting the contrast of the indication and if any
penetrant in the discontinuity is disturbed the volume
of the penetrant indication will get reduced (The
volume of penetrant is already very small)
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Solvent removable
In this method the excess surface penetrant is removed by solvent
action by using organic solvents that have solvent action on
the oil base penetrants.
.
Assessing Effectiveness of removal of
Visible & Fluorescent dye
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2.5.2.3 Post emulsifiable penetrants
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Development of hydrophilic Rolls royce - why
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2.6.3 Application of emulsifiers
Lipophilic emulsifier are applied using dipping or
flowing and never by brushing. This is due to the
fact that forced mixing with the penetrant affects
the control of emulsification time and also forcing
of emulsifier in the discontinuity thereby
emulsifying the penetrant in the discontinuity.
Spraying is also not permitted for the same
reason. Brushes can be used for flowing.
Hydrophilic emulsifier is applied by immersion or
spray. In the case of immersion some agitation is
required for effective emulsification
Emulsification time & improper
emulsification
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2.7 Developing
After the removal of the excess surface penetrant , in developing
step, the penetrant from the discontinuity is brought to the surface
so as to form an visible indication.
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Developers
The role of the developer is to pull trapped
penetrant out of defects and to spread it out on the
surface so that it can be seen.
Alos provides a proper background to increase
contrast when visible penetrant is used.
Developer materials are available in several different
forms
Dry Powder is a mix of light fluffy powder that
clumps together where penetrant bleeds back to
the surface to produces very defined indications.
Wet, Water Suspendable is a powder that is suspended in a water that
covers the surface with a relatively uniform layer of developer when
the water is evaporated. The solution is somewhat difficult to
maintain as the powder settles out over time.
Wet, Water Soluble is a crystalline powder that forms a clear solution
when mixed with water. The solution recrystallizes on the surface
when the water is driven off. Indications sometimes lack definition
and look milky. Not recommended for use with water-washable
penetrants.
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Wet, Non-Aqueous - is supplied in a spray can and is the most
Natural seepage
Reverse capillary
Concentration gradient Developer Particles
Absorbed Penetrant
No Developer
Thickness
Increased
Width is more
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2.7.5 Application of developers
Table 2.9: Mode of application and surface condition for the application
The state of surface is different for different type of developers. The wet
developers are applied in wet condition and specimen is dried subsequently.
In the case of dry and non-aqueous dry developers. The specimen is dried
and then the developer is applied. This is summarized in the table.
Dipping
Spraying
3. Pouring
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Inspection, interpretation and evaluation
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2.8.1 Inspection environment
Visible dye penetrant indications are inspected under
white light and fluorescent dye penetrant ndications
are viewed under black light (ultraviolet light?)
Black light
Yellowish green
light
Fluorescent dye
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Environment and others Visible Dye Fluorescent Dye
Penetrant Penetrant
.9 evaluation of test
3 sensitivity, test
pieces for comparison
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Equipments
Penetrant Test kit aerosol cans
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PT & MT Comparison
PT MT
Materials All including nonmetals Limited to ferromagnetic
plastic and rubber materials - magnetised
Surface Rigorous Not that much scale,
condition rust & paint coatings
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Comparison of Visible dye and Fluorescent dye penetrant
Visible Fluorescent
Sensitivity less high
Viewing Good white light Black light & dark ambience
Application Because of 2 convenient Not that good as black light and
& useful for spot examination dark are
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Comparison of Water washable, Solvent Removable and
Post Emulsifiable dye penetrants
WW SR Fluorescent
Sensitivity Low Med. high High Control of emulsification
Overwahing time- overwashing tend. reduced
Shallow D Not good Can be adjusted Can detect
Others Convenience Two step process
1 Step process
Design Good Not good
features
Press fits
Surfaces Good for rough Not good
surfaces
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Comparison of Dry, aqueous wet and Nonaqueous wet
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Comparison of Visible dye and Fluorescent dye penetrant
Visible Fluorescent
Sensitivity less high
Viewing Good white light Black light & dark ambience
Application Because of 2 convenient Not that good as black light and
& useful for spot examination dark are
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Choices of Penetrant Materials
Penetrant Type
I Fluorescent
II Visible
Method
A Water Washable
B Postemulsifiable Lipophilic
D Postemulsifiable - Hydrophilic
C Solvent Removable
Developer Form
Dry Powder
Wet, Water Soluble
Wet, Water Suspendable
Wet, Non-Aqueous(suspendible)
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