AGL Sugar Loaf 03 Soil Invest RPT Final

Soil Investigation Report
AGL Upstream Investments Pty Ltd Sugarloaf 03 Well Site Menangle NSW
24 JUNE 2011
Prepared for
AGL Upstream Investments Pty Ltd

Lot 35 Medhurst Road Menangle NSW 2568 PO BOX 67 Menangle NSW 2568
43177447
Sugarloaf Well Site - Soil Investigation
Project Manager: Adam Sullivan Senior Associate Environmental Scientist Author: Andrew Pettingell-Ward Environmental Scientist Reviewer: Date: Reference: Status: Gavan Butterfield Principal Scientist Document copyright of URS Australia Pty Limited. This report is submitted on the basis that it remains commercial-in-confidence. The contents of this report are and remain the intellectual property of URS and are not to be provided or disclosed to third parties without the prior written consent of URS. No use of the contents, concepts, designs, drawings, specifications, plans etc. included in this report is permitted unless and until they are the subject of a written contract between URS Australia and the addressee of this report. URS Australia accepts no liability of any kind for any unauthorised use of the contents of this report and URS reserves the right to seek compensation for any such unauthorised use. Document delivery URS Australia provides this document in either printed format, electronic format or both. URS considers the printed version to be binding. The electronic format is provided for the clients convenience and URS requests that the client ensures the integrity of this electronic information is maintained. Storage of this electronic information should at a minimum comply with the requirements of the Commonwealth Electronic Transactions Act (ETA) 2000. Where an electronic only version is provided to the client, a signed hard copy of this document is held on file by URS and a copy will be provided if requested. 24 June 2011 43177447/Rpt/01 Final URS Australia Pty Ltd Level 4, 407 Pacific Highway Artarmon NSW 2064 Australia T: 61 2 8925 5500 F: 61 2 8925 5555
j:\jobs\43177447\mttaurus_soilassess\gilead\final\agl sugarloaf03_soil invest_rpt_final.doc
Table of Contents
Executive Summary ..................................................................................................v 1 Introduction .......................................................................................................1
1.1 1.2 1.3 Background ........................................................................................................ 1 Objectives........................................................................................................... 1 Site Description.................................................................................................. 1
Methodology......................................................................................................3
2.1 2.2 2.3 Scope of Work.................................................................................................... 3 Sample Identification......................................................................................... 4 URS Field Quality Management........................................................................ 4
3 4
Assessment Criteria .........................................................................................5 Results ...............................................................................................................7

4.1
4.1.1 4.1.2 4.1.3
Analytical Data Validation ................................................................................. 7

Field QA/QC Results........................................................................................................7 Laboratory QA/QC Results .............................................................................................7 Overall Data Validity ........................................................................................................7
4.2
4.2.1 4.2.2
Analytical Results and Discussion .................................................................. 7

COPCs...............................................................................................................................7 Soil Quality .....................................................................................................................11
Conclusions.....................................................................................................13
5.1 Limitations........................................................................................................ 13
References.......................................................................................................15
Tables
Table 1 Table 2 Table 3 Table 4 Table 5 Soil Analytical Results (TPH, BTEX and Metals) Soil Analytical Results (PAHs) Soil Analytical Results (OP & OC Pesticides, Major Ions, General) Soil Analytical Results (VOCs) Soil Analytical Results (QA/QC Results)
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Tables (in text)

Table 4-1 Table 4-2 Summary of Soil Analytical Results for COPC at the Superfoam Spill Area and Background ....................................................................................................................... 9 Summary of Soil Quality Results at the Superfoam Spill and Down gradient Area and Background ..................................................................................................................... 11
Figures
Figure 1 SL03 foam release area - Soil Sampling Locations
Appendices
Appendix A Appendix B Appendix C Site Photography Laboratory Certificates Data Validation
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Abbreviations
Abbreviation
S/cm BTEX CoC COPC DECCW DPI EC EIL EPA HIL IL JSA LOR mg/kg NATA NEPM OH&S PAH RPD SB TOC TPH
Description
microSiemens per centimetre Benzene, Toluene, Ethyl-benzene, Xylenes Chain of Custody Constituents of Potential Concern Department of Environment Climate Change and Water Department of Primary Industries Electrical Conductivity Ecological Investigation Level Environmental Protection Authority Health-based Investigation Level Investigation Level Job Safety Analysis Limit of Reporting milligrams per kilogram National Association of Testing Laboratories National Environment Protection Measure Occupational Health and Safety Polycyclic Aromatic Hydrocarbons Relative Percentage Difference Soil Bore Total Organic Carbon Total Petroleum Hydrocarbons
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Executive Summary
URS Australia Pty Ltd (URS) was engaged by AGL Upstream Investments Pty Ltd (AGL) to undertake an investigation of shallow soil quality at the AGL Sugarloaf 03 (SL03) well site located in Menangle, NSW (the Site). The purpose of the work was to assess the soils in the immediate vicinity of the well site subsequent to a release of a foam compound (containing AMC Superfoam) during site work over operations on 17 May 2011. The objectives of the investigation were to: assess background quality of surface soils of the area; assess quality of the surface soils within the area of the foam release ; and assess whether the release of the foam has caused an adverse impact on the immediate area. The Site is located on an open rural grazing area. A coal seam gas well (SL03) and associated pipe work is in operation at the Site. A water storage dam and canal operated by Sydney Catchment Authority (SCA) is located approximately 200 m down slope (north) of the well site. The foam release was reported by AGL to have extended across an area approximately 40 m north of the well site. Based on the findings of this investigation, URS make the following conclusion: The analytical results indicate there is no evidence that the release of foam at the Sugarloaf 03 well has caused adverse environmental impacts on the immediate vicinity of the identified spill site. URS also consider it is unlikely that the release of foam would have carried to SCAs water storage dam, located down slope of the release area. URS make this conclusion based on there being no detection of COPC (above the LOR) in the release area. The conclusions made and all information in this Report is provided strictly in accordance with and subject to the limitations in Section 5.1.
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Introduction
Background
1.1
URS Australia Pty Ltd (URS) was engaged by AGL Upstream Investments Pty Ltd (AGL) to undertake an investigation of shallow soil quality at the AGL Sugarloaf 03 (SL03) well site located in Menangle, NSW (the Site). The location of the Site is shown on Figure 1. The purpose of the work was to assess the soils in the immediate vicinity of the well site subsequent to a release of a foam compound (containing AMC Superfoam) during site workover operations on 17 May 2011.
1.2
Objectives
The objectives of the investigation were to: assess background quality of surface soils of the area; assess quality of the surface soils within the area of the foam release ; and assess whether the release of the foam has caused an adverse impact on the immediate area.
1.3
Site Description
The Site is located on an open rural grazing area (Photos 1 and 5). A coal seam gas well (SL03) and associated pipe work is in operation at the Site (Photo 3). There is a shale access road leading to the well site which is situated on a shale covered work pad (Photos 1, 3 and 5). A water storage dam and canal operated by Sydney Catchment Authority (SCA) is located approximately 200 m down slope (north) of the well site (Photo 2). The foam release was reported by AGL to have extended across an area approximately 40 m north of the well site (refer to Figure 1) (Photo 4).
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Methodology
Scope of Work
2.1
URS were instructed by AGL to complete the following scope of work: An Occupational Health and Safety (OH&S) plan was prepared for field works that comprised task specific job safety analyses (JSAs), emergency response protocol, communication plan, hazards and controls, fatigue management, chemicals of potential concern (COPC) and job-specific, personal protective equipment (PPE). A URS field scientist was inducted onto the Site by AGLs site representative. The sampling area was inspected and surface soil sample locations were established. Sampling of surface soils was undertaken on 26 May 2011 between 1450 and 1555. 11 locations were sampled using a hand trowel to provide coverage of the footprint of the release area and the immediate down gradient area. Sampling locations are shown on Figure 1. Individual samples were collected from the four approximate corners and centre of the identified footprint of the foam release area as well as down gradient of this area. Sampling of surface soils was also carried out at two locations to the south and east of the well site, to assess background soil quality conditions. Two locations were considered appropriate for the collection of representative background samples. Surface soils were collected from a maximum depth of 0.1 m below ground level (mbgl). In addition to the samples URS collected, AGL also collected three surface samples in the immediate area of the foam release on 20 May 2011 at 4.30pm. The locations of these samples are shown on Figure 1. Soil samples were dispatched to ALS (the NATA accredited subcontracted environmental laboratory) for analysis for the following contaminants of potential concern (COPC) and soil quality indicators: o COPCs: Hydrocarbons (analysed as total petroleum hydrocarbons/total recoverable hydrocarbons (TPH/TRH)); benzene, toluene, ethylbenzene and xylene compounds (BTEX) Volatile organic compounds (VOCs); heavy metals (arsenic, cadmium, chromium, copper, lead, nickel, zinc, and mercury) organochlorine (OC) and organophosphorus (OP) pesticides polycyclic aromatic hydrocarbons (PAHs) anionic surfactants (as (Methylene Blue Active Substances - MBAS) o Soil quality indicators: pH electrical conductivity (EC) organic matter total nitrogen total phosphorus Total soluble salts major cations.
Anionic surfactants (as MBAS) were analysed as instructed by AGL on the basis that the foam contains the specific chemical. Other COPCs were selected based on a suite of common contaminants relative to assessing land contamination and recommended in NSW EPA and National
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Methodology
(i.e. NEPM) guideline documents (refer to section 3). These COPC have published Health-based and Ecological Investigation Levels (HILs) that can be used to assess potential impacts. Soil quality parameters were selected based on key quality indicators provided on the NSW Department of Primary Industries (DPI) web page for assessing soil health and fertility (www.dpi.nsw.gov.au/agriculture/resources/soils).
2.2
Sample Identification
Sampling locations were identified as follows: Identified foam release area: URS samples SB1, SB2, SB3, SB4 and SB11. AGL sample SL03.002. Down gradient of spill area: URS samples SB7, SB8, SB9 and SB10. AGL sample SL03.001 Background: URS samples SB5 and SB6 AGL sample SL03.003. For a detailed overview of soil sampling locations see Figure 1.
2.3
URS Field Quality Management
URS samples were collected using a stainless steel hand trowel at each location, which was decontaminated between each sampling location. URS field scientists used disposable nitrile gloves to handle and transfer sampling equipment and soil samples. URS samples were transferred directly into laboratory-prepared, acid-washed and solventrinsed, 250g glass jars. Each jar was filled, capped with a Teflon-lined lid and stored immediately in an insulated chest containing ice. URS collected soil samples were transported to ALS (the NATA accredited contracted environmental laboratory), using strict Chain-of-Custody procedures. Analyses were subsequently conducted on discrete (un-composited) samples for the analytical parameters listed in Section 2.1. Completed Chain-of-Custody documentation and a Sample Receipt Advice form, certifying the condition of the samples upon arrival at the laboratory, are presented in Appendix B. URS fieldwork Quality Control (QC) was maintained in the field during soil sampling, which included collection of one field duplicate sample. Analytical results for the field QC sample are discussed in Section 4.2.
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Assessment Criteria
Analytical results were assessed against environmental guidelines published or approved by the NSW Office of Environment and Heritage (as NSW EPA), which incorporated: NEPM 1999, Schedule B(1) Guideline on the Investigation Levels for Soil and Groundwater, National Environmental Protection (Assessment of Site Contamination) Measure 1999, National Environmental Protection Council; and NSW EPA 1994, Threshold Concentrations for Sensitive Land Use Soils, in Guidelines for Assessing Service Station Sites (1994), for contaminant parameters not addressed in the NEPC Assessing Service Station Sites, NSW Environment Protection Authority (EPA). The NEPM 1999 EILs were applied for inorganic analytes; however, the NSW EPA 1994 sensitive land use thresholds were used for total petroleum hydrocarbons (TPH), and BTEX, for which EILs were not available. Results for soil quality indicators were interpreted against guidance provided by NSW Department of Primary Industry (DPI) for assessing soil health and fertility (www.dpi.nsw.gov.au). For the purposes of this assessment, the adopted guideline thresholds will henceforth be referred to as the Soil Investigation Levels (SILs).
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4
Results
Analytical Data Validation
4.1
The analytical data produced by this investigation was validated in accordance with URS protocols. This process involved an evaluation of the quality assurance and quality control (QA/QC) procedures and results, which provided an indication of the accuracy and precision of the analytical data. URS assume that similar practices were followed during collection and transport of samples by AGL.
4.1.1
Field QA/QC Results
URS quality control in the field was assessed by collection of one field duplicate sample (QC100). Comparison of the data reported by the laboratory for the primary and secondary samples (Ref. Appendix B) showed that the data quality objectives were met.
4.1.2
Laboratory QA/QC Results
ALS carried out internal QA/QC testing on a number of sample types, which included the laboratory duplicates on URS and anonymous samples, as well as a number of method blanks, matrix spikes and other laboratory control samples. An assessment of laboratory QA/QC results indicated that all relevant data quality objectives, in terms of document completeness, data comparability, sample representativeness and data precision, were also adequately maintained. URS note that ALS is accredited by the National Association of Testing Authorities (NATA) for analytical testing methods for the selected analytes in Section 2.1, with the exception of anionic surfactants (as MBAS).
4.1.3
Overall Data Validity
On the basis of the analytical data validation procedure employed, the overall quality of the soil analytical data produced is considered to be of an acceptable standard valid for the purposes of the assessment.
4.2
Analytical Results and Discussion
Full results are presented in the Tables Appendix as Tables 1, 2, 3, 4 and 5 at the end of this report. Copies of the respective Laboratory Certificates and Data Validation summaries are provided in Appendices B and C, respectively.
4.2.1
COPCs
The upper, lower and mean concentrations for the tested analytes for both the foam release area and background soils are summarised in Table 4-1 below.
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4 Results
Table 4-1
Parameter
(mg/kg) Organics: TPH (C6-C9) TPH (C10-C36) BTEX Benzo(a)pyrene Total PAHs OCPs OPPs VOCs Heavy Metals: Arsenic Cadmium
Summary of Soil Analytical Results for COPC at the Foam Release Area and Background
SIL
(mg/kg)
Foam release area

Minimum Maximum Mean
Down gradient area

Background
65* 1,000* * 1* 20 NEPM NIL NIL
<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR
<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR
<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR
<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR
<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR
<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR
<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR
<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR
<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR
20 3 400 100 600 1 60 200 NIL
6 <1 15 23 19 <0.1 13 45 <100
8 <1 16 35 22 <0.1 16 55 <100
7.2 <1 15.5 29 20.4 <0.1 14.8 49.2 <100
6 <1 13 25 20 <0.1 12 48 <100
8 <1 15 27 44 <0.1 15 94 <100
6.75 <1 14.25 26 33 <0.1 13.75 69.25 <100
7 <1 15 25 19 <0.1 16 49 <100
8 <1 16 30 22 <0.1 17 79 <100
7.5 <1 15.5 27.5 20.5 <0.1 16.5 64 <100
Chromium (total) Copper Lead Mercury (inorganic) Nickel Zinc Anionic Surfactants
Notes:
NIL = no investigation level is currently published for the indicated analytical parameter.
SIL = Soil Investigation Levels, which are the NEPM 1999 Health or Ecological Investigation Levels, unless otherwise indicated. (*) NSW EPA 1994 Threshold Concentrations for Sensitive Land Use Soils. NA = Not Analysed. LOR = Limit of Reporting.
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Results
Heavy Metals Mean metals concentrations in surface soils at the foam release area and down gradient areas were comparable with background soil concentrations and all metal concentrations were within the same order of magnitude. All maximum soil concentrations were below the SILs, indicating no adverse impacts from site activities in relation to heavy metals. AGL samples taken from the gas well infrastructure (SL03.001, SL03.002 and SL03.003) were not analysed for heavy metals. Organics No detectable concentrations of the organic compound groups were identified in the tested soil samples collected by URS. This was considered to indicate that the foam release area was not subject to adverse impacts from site activities in relation to the tested organic compounds. Anionic Surfactants No detectable concentrations of anionic surfactants were present in the soil samples analysed from specific locations. This was considered to indicate that the foam release area had not adversely affected soil quality in the spill area or in the down gradient area.
4.2.2
Soil Quality
The upper, lower and mean concentrations of soil quality data for both the foam release area, down gradient area and background soils are summarised in Table 4-2.
Table 4-2 Summary of Soil Quality Results at the Foam release area and Down gradient area and Background Foam release area and Down gradient area Parameter EC (uS/cm) pH Total nitrogen Total phosphorus (mg/kg) Total soluble salts (mg/kg) Organic Carbon (%) Total Cations1 (mg/kg) Minimum 59 6.0 1,420 214 198 1.6 190 Maximum 117 8.1 6,580 960 2,240 7.0 930 Mean 88 7.2 2,991 446 637 4.26 328.9 Minimum 92 6.7 1,310 226 358 2.4 190 Maximum 92 7.1 4,920 532 452 9.6 320 Mean 92 6.9 3,183 411 405 6 255 Background
Notes: (1) refers to the sum of concentrations for major cations including calcium, magnesium, sodium and potassium.
The minimum and maximum values for soil quality parameters were comparable to those reported for background conditions and indicated a low risk of adverse impacts to site surface soils resulting from the foam release.
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Results
The mean electrical conductivity (EC) value in the foam release and down gradient areas (88 S/cm) was comparable with the mean background EC (92 S/cm) and consistent with the DPI-preferred EC of < 150 S/cm. The mean pH value in surface soils at the foam release area and down gradient area (pH 7.2) was comparable with the mean background value (pH 6.9). These pH levels indicated neutral pH conditions, which may be naturally occurring in the vicinity of the Site, although both areas were elevated above the DPI-preferred pH range of 5.8 6.3. The mean concentration of total nitrogen in surface soils at the foam release area and down gradient area (3,018 mg/kg) was comparable to the mean background concentration (3,105 mg/kg) and consistent with the DPI-preferred concentration of >20 mg/kg. The mean concentration of total phosphorus in surface soils at the foam release area and down gradient area (449 mg/kg) was comparable with the mean background concentration (379 mg/kg) and consistent with the DPI-preferred concentration of >50 mg/kg. The mean concentration of total soluble salts in the surface soils at the foam release area and down gradient area (637 mg/kg) is comparable to the background concentration (405 mg/kg). The mean concentration of organic carbon in surface soils at the foam release area and down gradient area (4.26%) was comparable with the mean background concentration (6%) and consistent with the DPI-preferred concentration of >2 %. The mean cation concentrations in surface soils at the foam release area and down gradient area were comparable with mean background concentrations, indicating soil cation exchange capacities (CEC) consistent with natural conditions.
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Conclusions
Based on the findings of this investigation, URS make the following conclusion: The analytical results indicate there is no evidence that the release of foam at the Sugarloaf 03 well has caused adverse environmental impacts on the immediate vicinity of the identified spill site. URS also consider it is unlikely that the release of foam would have carried to SCAs water storage dam, located down slope of the release area. URS make this conclusion based on there being no detection of COPC (above the LOR) in the release area.
5.1
Limitations
The conclusions made and all information in this Report is provided strictly in accordance with and subject to the following limitations:
a) This Report should be read in full and no excerpts are to be taken as representative of the findings. b) c) d) e)
f)
g) h) i)
j) k)
No responsibility is accepted by URS for use of any part of this Report in any other context. This conclusion is based solely on the information and findings contained in this Report. This conclusion is based solely on the scope of work agreed between URS and AGL and described in section 2.1 ("Scope of Works") of this Report. This Report has been prepared for the sole benefit of AGL and neither the whole nor any part of this Report may be used or relied upon by any party other than AGL. This Report is dated 23 June 2011 and is based on the conditions encountered during the site investigations conducted, and information reviewed, from 26 May 2011 to 23 June 2011. URS accepts no responsibility for any events arising from any changes in site conditions or in the information reviewed that have occurred after the completion of the site investigations. The investigations carried out for the purposes of the Report have been undertaken, and the Report has been prepared, in accordance with normal prudent practice and by reference to applicable environmental regulatory authority and industry standards, guidelines and assessment criteria in existence at the date of this Report. Where this Report indicates that information has been provided to URS by third parties, URS has made no independent verification of this information except as expressly stated in the Report. URS has tested only for those chemicals specifically referred to in this Report. URS makes no statement or representation as to the existence (or otherwise) of any other chemicals. Except as otherwise specifically stated in this Report, URS makes no warranty or representation as to the presence or otherwise of asbestos and/or asbestos containing materials (ACM) on the site. If fill has been imported on to the site at any time, or if any buildings constructed prior to 1970 have been demolished on the site or materials from such buildings disposed of on the site, the site may contain asbestos or ACM. Without limiting the generality of sub-clauses (h) and (m), even if asbestos was tested for and those test results did not reveal the presence of asbestos at specific points of sampling, asbestos may still be present at the site if fill has been imported at any time, or if any buildings constructed prior to 1970 have been demolished on the site or materials from such buildings disposed of on the site. No investigations have been undertaken into any off-site conditions, or whether any adjoining sites may have been impacted by contamination or other conditions originating from this site. Investigations undertaken in respect of this Report are constrained by the particular site conditions, such as the location of buildings, services and vegetation. As a result, not all relevant site features and contamination may have been identified in this Report.
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5 Conclusions
l)
m) n)
o)
p) q)
Subsurface conditions can vary across a particular site and cannot be exhaustively defined by the investigations described in this Report. It is unlikely therefore that the results and estimations expressed in this Report will represent conditions at any location removed from the specific points of sampling. A site which appears to be unaffected by contamination at the time the Report was prepared may later, due to natural phenomena or human intervention, become contaminated. Except as specifically stated above, URS makes no warranty, statement or representation of any kind concerning the suitability of the site for any purpose or the permissibility of any use, development or re-development of the site. Use, development or re-development of the site for any purpose may require planning and other approvals and, in some cases, environmental regulatory authority and accredited site auditor approvals. URS offers no opinion as to whether the current use has any or all approvals required, is operating in accordance with any approvals, the likelihood of obtaining any approvals for development or redevelopment of the site, or the conditions and obligations which such approvals may impose, which may include the requirement for additional environmental works. URS makes no determination or recommendation regarding a decision to provide or not to provide financing with respect to the site. The ongoing use of the site and/or the use of the site for any different purpose may require the owner/user to manage and/or remediate site conditions, such as contamination and other conditions, including but not limited to conditions referred to in this Report.
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References
National Environment Protection
6
Contaminated Sites:
National Environment Protection Council (NEPC) (1999). (Assessment of Site Contamination) Measure.
New South Wales South Wales Environment Protection Authority (1994). Guidelines for Assessing Service Station Sites.
New South Wales Environment Protection Authority (1995) Sampling Design Guidelines. New South Wales Department of Environment and Conservation (2006) Guidelines for the NSW Site Auditor Scheme (2nd Edition). New South Wales Department of Primary Industries (www.dpi.nsw.gov.au/agriculture/resources/soils)
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Tables
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Table 1: Soil Analytical Results - TPH, BTEX and Metals Sugarloaf 03 Well Site Menangle May 2011 URS Job No. 43177447
Location Sample ID Date Sampled Sample Type
Adopted ILs SB1 SB1_0.0-0.1 26/05/2011 PS SB2 SB2_0.0-0.1 26/05/2011 PS SB3 SB3_0.0-0.1 26/05/2011 PS SB4 SB4_0.0-0.1 26/05/2011 PS SB5 SB5_0.0-0.1 26/05/2011 PS SB6 SB6_0.0-0.1 26/05/2011 PS SB7 SB7_0.0-0.1 26/05/2011 PS SB8 SB8_0.0-0.1 26/05/2011 PS SB9 SB9_0.0-0.1 26/05/2011 PS SB10 SB10_0.0-0.1 26/05/2011 PS SB11 SB11_0.0-0.1 26/05/2011 PS Downgradient area SL03.001 19/05/2011 PS Foam release area SL03.002 19/05/2011 PS Background SL03.003 19/05/2011 PS
Analyte Total Petroleum Hydrocarbons

C6-C9 fraction C10-C14 fraction C15-C28 fraction C29-C36 fraction C10 - C36 Fraction
LOR
10 50 100 100 50 10 50 100 100 50 0.2 0.5 0.5 0.5 0.5 2 5 1 5 2 5 5 0.1 1.0
Units
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg % 25 400 20 3 600 60 200 100 1 1 130 50 1000 65 < 10 < 50 < 100 < 100 < 50 < 10 < 50 < 100 < 100 < 50 < 0.2 < 0.5 < 0.5 < 0.5 < 0.5 15 6 <1 20 13 47 23 < 0.1 18.0 < 10 < 50 < 100 < 100 < 50 < 10 < 50 < 100 < 100 < 50 < 0.2 < 0.5 < 0.5 < 0.5 < 0.5 16 8 <1 22 15 49 26 < 0.1 18.3 < 10 < 50 < 100 < 100 < 50 < 10 < 50 < 100 < 100 < 50 < 0.2 < 0.5 < 0.5 < 0.5 < 0.5 16 7 <1 22 15 50 25 < 0.1 14.7 < 10 < 50 < 100 < 100 < 50 < 10 < 50 < 100 < 100 < 50 < 0.2 < 0.5 < 0.5 < 0.5 < 0.5 15 8 <1 19 16 45 27 < 0.1 14.9 < 10 < 50 < 100 < 100 < 50 < 10 < 50 < 100 < 100 < 50 < 0.2 < 0.5 < 0.5 < 0.5 < 0.5 15 8 <1 22 17 79 25 < 0.1 15.1 < 10 < 50 < 100 < 100 < 50 < 10 < 50 < 100 < 100 < 50 < 0.2 < 0.5 < 0.5 < 0.5 < 0.5 16 7 <1 19 16 49 30 < 0.1 8.2 < 10 < 50 < 100 < 100 < 50 < 10 < 50 < 100 < 100 < 50 < 0.2 < 0.5 < 0.5 < 0.5 < 0.5 15 7 <1 20 15 48 27 < 0.1 8.3 < 10 < 50 < 100 < 100 < 50 < 10 < 50 < 100 < 100 < 50 < 0.2 < 0.5 < 0.5 < 0.5 < 0.5 13 6 <1 25 12 61 25 < 0.1 16.2 < 10 < 50 < 100 < 100 < 50 < 10 < 50 < 100 < 100 < 50 < 0.2 < 0.5 < 0.5 < 0.5 < 0.5 15 8 <1 44 14 74 25 < 0.1 14.7 < 10 < 50 < 100 < 100 < 50 < 10 < 50 < 100 < 100 < 50 < 0.2 < 0.5 < 0.5 < 0.5 < 0.5 14 6 <1 43 14 94 27 < 0.1 14.3 < 10 < 50 < 100 < 100 < 50 < 10 < 50 < 100 < 100 < 50 < 0.2 < 0.5 < 0.5 < 0.5 < 0.5 15 7 <1 19 15 55 35 < 0.1 18.0 < 10 < 50 < 100 < 100 < 50 < 10 < 50 < 100 < 100 < 50 < 0.2 < 0.5 < 0.5 < 0.5 < 0.5 < 10 < 50 < 100 < 100 < 50 < 10 < 50 < 100 < 100 < 50 < 0.2 < 0.5 < 0.5 < 0.5 < 0.5 < 10 < 50 < 100 < 100 < 50 < 10 < 50 < 100 < 100 < 50 < 0.2 < 0.5 < 0.5 < 0.5 < 0.5 -
TRH - NEPM 2010 DRAFT

C6 - C10 Fraction >C10 - C16 Fraction >C16 - C34 Fraction >C34 - C40 Fraction >C10 - C40 Fraction (sum)
BTEX Compounds
Benzene Toluene Ethylbenzene ortho-Xylene Total Xylenes
Metals (Total)
Chromium Arsenic Cadmium Lead Nickel Zinc Copper
Mercury
Mercury
Moisture Content
Moisture Content (dried @ 40C) Legend: PS = Primary Sample FD = Field Duplicate FT = Field Triplicate - = Not Analysed ND = Not Detected Exceeds the Adopted Soil Investigation Levels (ILs)
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URS Australia Pty Ltd Prepared By: AP Checked By: AS
Table 2: Soil Analytical Results - PAHs Sugarloaf 03 Well Site Menangle May 2011 URS Job No. 43177447
Adopted ILs SB1 SB1_0.0-0.1 26/05/2011 PS SB2 SB2_0.0-0.1 26/05/2011 PS SB3 SB3_0.0-0.1 26/05/2011 PS SB4 SB4_0.0-0.1 26/05/2011 PS SB5 SB5_0.0-0.1 26/05/2011 PS SB6 SB6_0.0-0.1 26/05/2011 PS SB7 SB7_0.0-0.1 26/05/2011 PS SB8 SB8_0.0-0.1 26/05/2011 PS SB9 SB9_0.0-0.1 26/05/2011 PS SB10 SB10_0.0-0.1 26/05/2011 PS SB11 SB11_0.0-0.1 26/05/2011 PS
Analyte LOR Polynuclear Aromatic Hydrocarbons

Acenaphthylene Acenaphthene Fluorene Phenanthrene Anthracene Fluoranthene Pyrene Benz(a)anthracene Chrysene Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(a)pyrene Indeno(1.2.3.cd)pyrene Dibenz(a.h)anthracene Benzo(g.h.i)perylene Naphthalene sum of polycyclic aromatic hydrocarbons Legend: PS = Primary Sample FD = Field Duplicate FT = Field Triplicate - = Not Analysed ND = Not Detected Exceeds the Adopted Soil Investigation Levels (ILs) 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5
Units
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 20 1 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
2 of 5
Table 3: Soil Analytical Results - OCP, OPP, Major Ions, Anionic Surfactants, General Sugarloaf 03 Well Site Menangle May 2011 URS Job No. 43177447
Adopted ILs SB1 SB1_0.0-0.1 26/05/2011 PS SB2 SB2_0.0-0.1 26/05/2011 PS SB3 SB3_0.0-0.1 26/05/2011 PS SB4 SB4_0.0-0.1 26/05/2011 PS SB5 SB5_0.0-0.1 26/05/2011 PS SB6 SB6_0.0-0.1 26/05/2011 PS SB7 SB7_0.0-0.1 26/05/2011 PS SB8 SB8_0.0-0.1 26/05/2011 PS SB9 SB9_0.0-0.1 26/05/2011 PS SB10 SB10_0.0-0.1 26/05/2011 PS SB11 SB11_0.0-0.1 26/05/2011 PS Downgradient area SL03.001 19/05/2011 PS Foam release area SL03.002 19/05/2011 PS Background SL03.003 19/05/2011 PS
Analyte OCPs
cis-Chlordane Endrin aldehyde Endrin ketone Methoxychlor trans-Chlordane alpha-BHC beta-BHC gamma-BHC delta-BHC Heptachlor Aldrin Heptachlor epoxide alpha-Endosulfan 4.4-DDE Dieldrin Endrin beta-Endosulfan 4.4-DDD Endosulfan sulfate 4.4-DDT Hexachlorobenzene (HCB)
LOR
0.05 0.05 0.05 0.2 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.2 0.05 0.05 0.05 0.2 0.05 0.05 0.05 0.2 0.05 0.05 0.05 0.2 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.5 0.1 20 0.1 20 2 5 1
Units
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg % pH units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 400 400 400 20 20 20 100 100 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 3.6 8.1 2450 < 0.1 2450 390 650 <1 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 4.5 8.0 1680 7.0 1690 274 663 <1 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 4.3 7.4 2120 < 0.1 2120 325 484 <1 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 1.6 7.8 1420 < 0.1 1420 214 497 <1 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 9.6 6.7 4900 16.2 4920 532 358 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 2.4 7.1 1310 < 0.1 1310 226 452 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 2.8 6.6 2360 < 0.1 2360 362 198 <1 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 5.9 6.3 3890 < 0.1 3890 533 221 <1 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 7.0 6.0 6410 171 6580 678 2240 <1 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 5.6 6.4 6040 < 0.1 6040 960 266 <1 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 3.0 7.9 2000 < 0.1 2000 333 520 <1
2120
2230
3320
OPPs
Dichlorvos Demeton-S-methyl Monocrotophos Dimethoate Diazinon Chlorpyrifos-methyl Parathion-methyl Malathion Fenthion Chlorpyrifos Parathion Pirimphos-ethyl Chlorfenvinphos Bromophos-ethyl Fenamiphos Prothiofos Ethion Carbophenothion Azinphos Methyl
Organic Matter
Organic Matter
pH
pH Value
Total Kjeldahl Nitrogen as N

Nitrite + Nitrate as N
Total Nitrogen as N
Total Nitrogen as N
Total Phosphorus as P
454
390
476
Total Soluble Salts

Total Soluble Salts
<1
<1
<1
Anionic Surfactants as MBAS

Anionic Surfactants as MBAS Legend: PS = Primary Sample FD = Field Duplicate FT = Field Triplicate - = Not Analysed ND = Not Detected Exceeds the Adopted Soil Investigation Levels (ILs) URS Australia Pty Ltd Prepared By: AP Checked By: AS
3 of 5
Table 4: Soil Analytical Results - VOCs Sugarloaf 03 Well Site Menangle May 2011 URS Job No. 43177447
Adopted ILs Downgradient area SL03.001 19/05/2011 PS Foam release area SL03.002 19/05/2011 PS Background SL03.003 19/05/2011 PS
Analyte Monocyclic Aromatic Compounds

Styrene Isopropylbenzene n-propylbenzene 1,3,5-trimethylbenzene sec-butylbenzene 1,2,4-trimethylbenzene tert-butylbenzene p-isopropylbenzene n-butylbenzene
LOR
0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 5 5 5 5 0.5 0.5 0.5 0.5 0.5 0.5 5 5 5 5 5 5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 1 1 20 2 1
Units
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg S/cm % mg/kg mg/kg mg/kg <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <5 <5 <5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 59 10.4 2120 454 <100 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <5 <5 <5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 117 19.5 2230 390 <100 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <5 <5 <5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 92 6.3 3320 476 <100
Oxygenated Compounds
Vinyl acetate 2-butanone (MEK) 4-methyl-2-pentanone (MIBK) 2-hexanone (MBK)
Sulfonated Compounds
Carbon disulfide
Fumigants
2,2-dichloropropane 1,2-dichloropropane cis-1,3-dichloropropylene trans-1,3-dichloropropylene 1,2-dibromoethane (EDB)
Halogenated Aliphatic Compounds

dichlorodifluoromethane chloromethane vinyl chlorides bromomethane chloroethane trichlorofluoromethane 1,1-dichloroethene iodomethane trans-1,2-dichloroethene 1,1-dichloroethene cis-1,2-dichloroethene 1,1,1-trichloroethane 1,1-dichloropropylene carbon tetrachloride 1,2-dichloroethane trichloroethene dibromomethane 1,1,2-trichloroethane 1,3-dichloropropane tetrachloroethene 1,1,1,2-tetrachloroethene trans-1,4-dichloro-2-butene cis-1,4-dichloro-2-butene 1,1,2,2-tetrachloroethane 1,2,3-trichloropropane pentachloroethane 1,2-dibromo-3-chloropropane hexachlorobutadiene
Halogenated Aromatic Compounds

chlorobenzene bromobenzene 2-chlorotoluene 4-chlorotoluene 1,3-dichlorobenzene 1,4-dichlorobenzene 1,2-dichlorobenzene 1,2,4-trichlorobenzene 1,2,3-trichlorobenzene
Trihalomethanes
chloroform bromodichloromethane dibromochloromethane bromoform
Electrical Conductivity Moisture Content Total Nitrogen as N Total Phosphorus as P Anionic Surfactants as MBAS
4 of 5
Table 5: Soil Analytical Results - QAQC Sugarloaf 03 Well Site Menangle May 2011 URS Job No. 43177447
Sample ID Date Sampled Sample Type
QC100 26/05/2011 FD QC100 26/05/2011 FD QC100 26/05/2011 FD
Adopted ILs
Adopted ILs
Adopted ILs
Analyte Total Petroleum Hydrocarbons

C6-C9 fraction C10-C14 fraction C15-C28 fraction C29-C36 fraction C10 - C36 Fraction
LOR
10 50 100 100 50 0.2 0.5 0.5 0.5 0.5 2 5 1 5 2 5 5 0.1 1.0
Units
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg % <10 < 50 < 100 < 100 <50 < 0.2 < 0.5 < 0.5 < 0.5 < 0.5 15 7 <1 20 16 60 27 <0.1 20.0
Analyte Polynuclear Aromatic Hydrocarbons

Acenaphthylene Acenaphthene Fluorene Phenanthrene Anthracene Fluoranthene Pyrene Benz(a)anthracene Chrysene Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(a)pyrene Indeno(1.2.3.cd)pyrene Dibenz(a.h)anthracene Benzo(g.h.i)perylene Naphthalene sum of polycyclic aromatic hydrocarbons
LOR
0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.05 0.05 0.05 0.2 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.2 0.05
Units
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05
Analyte OPPs
Dichlorvos Demeton-S-methyl Monocrotophos Dimethoate Diazinon Chlorpyrifos-methyl Parathion-methyl Malathion Fenthion Chlorpyrifos Parathion Pirimphos-ethyl Chlorfenvinphos Bromophos-ethyl Fenamiphos Prothiofos Ethion Carbophenothion Azinphos Methyl
LOR
0.05 0.05 0.2 0.05 0.05 0.05 0.2 0.05 0.05 0.05 0.2 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.5 0.1 20 0.1 20 2 5 1
Units
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg % pH units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 3.2 8.0 2080 < 0.1 2080 448 494 <1
BTEX Compounds
Benzene Toluene Ethylbenzene ortho-Xylene Total Xylenes
Metals (Total)
Chromium Arsenic Cadmium Lead Nickel Zinc Copper
OCPs
cis-Chlordane Endrin aldehyde Endrin ketone Methoxychlor trans-Chlordane alpha-BHC beta-BHC gamma-BHC delta-BHC Heptachlor Aldrin Heptachlor epoxide alpha-Endosulfan 4.4-DDE Dieldrin Endrin beta-Endosulfan 4.4-DDD Endosulfan sulfate 4.4-DDT Hexachlorobenzene (HCB)
Mercury
Mercury
Organic Matter
Organic Matter
Moisture Content
Moisture Content (dried @ 40C)
pH
pH Value

Total Nitrogen as N
Total Nitrogen as N
Total Soluble Salts

Total Soluble Salts

5 of 5
Figures
43177447/Rpt/01
17
D D D D D D SB9 SB9 SB9 SB9
D D D D D D SB10 SB10 SB10 SB10 SB10 SB10 D D D D D D SB2 SB2 SB2 SB2 D D D D D D SB1 SB1 SB1 SB1 SB1 SB1
D D D D D D SB7 SB7 SB7 SB7 SB7 SB7
SB8 SB8 SB8 D SB8 D SB8 D SB8 D D D D SB4 D SB4 D SB4 D SB4 D SB4 D SB4
D D D D D D D D D D D D SB3 SB3 SB3 SB3 SB3 SB3 SB11 SB11 SB11 SB11 SB11 SB11
This drawing is subject to COPYRIGHT.
Source: Aerial Photography from AGL AGL Drawing AGL Soil Sample Locations
Whilst every care is taken by URS to ensure the accuracy of the digital data, URS makes no representation or warranties about its accuracy, reliability, completeness, suitability for any particular purpose and disclaims all responsibility and liability (including without limitation, liability in negligence) for any expenses, losses, damages (including indirect or consequential damage) and costs which may be incurred as a result of data being inaccurate in any way for any reason. Electronic files are provided for information only. The data in these files is not controlled or subject to automatic updates for users outside of URS.
Legend:
D D &
Existing Wells (AGL) Soil Sample Locations (URS 2011) Soil Sample Locations (AGL)
Release Area
AGL
AGL MENANGLE
Draft
Site Locality Map
Figure:
001
A3
File No: 43177747.004.wor
Drawn: AY/SB
Approved: AS
Date: 24-06-2011
Rev. A
Appendix A Site Photography
Site photo 1: Gas well site looking east, foam release area past left of frame
Site Photo 2: Sydney Catchment Authority dam to the north
43177447/Rpt/01
Appendix A
Site photo 3: Gas well looking south east
Site photo 4: foam release area, grass stained orange
43177447/Rpt/01
Site photo 5: Gas well looking south
43177447/Rpt/01
Appendix B Laboratory Certificates
43177447/Rpt/01
ES1110639 False
CERTIFICATE OF ANALYSIS
Work Order :
ES1110639
Page Laboratory
: 1 of 6 : Environmental Division Sydney : Client Services : 277-289 Woodpark Road Smithfield NSW Australia 2164 : sydney@alsglobal.com : +61-2-8784 8555 : +61-2-8784 8500 : NEPM 1999 Schedule B(3) and ALS QCS3 requirement : 23-MAY-2011 : 27-MAY-2011 :3 :3
Client
: AGL ENERGY : TOM LAWLER : P.O BOX 67 MENANGLE : : : : : : : :
Contact
Address E-mail Telephone Facsimile Project Order number C-O-C number Sampler Site Quote number
Contact
Address E-mail Telephone Facsimile QC Level Date Samples Received Issue Date No. of samples received
MENANGLE NSW 2568 tlawler@agl.com.au 4633 5200 ---SUGARLOAF 09 SOIL TEST 4510002862 ---TOM LAWLER ----
: SY/456/10
No. of samples analysed
This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. All pages of this report have been checked and approved for release. This Certificate of Analysis contains the following information: l General Comments l Analytical Results l Surrogate Control Limits
NATA Accredited Laboratory 825 This document is issued in accordance with NATA accreditation requirements. Accredited for compliance with ISO/IEC 17025.
Signatories
This document has been electronically signed by the authorized signatories indicated below. Electronic signing has been carried out in compliance with procedures specified in 21 CFR Part 11.
Signatories Position Accreditation Category
Ankit Joshi Evie.Sidarta Pabi Subba Sarah Millington Stephen Hislop
Inorganic Chemist Inorganic Chemist Senior Organic Chemist Senior Inorganic Chemist Senior Inorganic Chemist
Sydney Inorganics Sydney Inorganics Sydney Organics Sydney Inorganics Brisbane Inorganics
Environmental Division Sydney

277-289 Woodpark Road Smithfield NSW Australia 2164 Tel. +61-2-8784 8555 Fax. +61-2-8784 8500 www.alsglobal.com
Page Work Order Client Project
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ES1110639 AGL ENERGY SUGARLOAF 09 SOIL TEST
General Comments
The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house developed procedures are employed in the absence of documented standards or by client request. Where moisture determination has been performed, results are reported on a dry weight basis. Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insuffient sample for analysis. Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference. When sampling time information is not provided by the client, sampling dates are shown without a time component. In these instances, the time component has been assumed by the laboratory for processing purposes. Key : CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society. LOR = Limit of reporting ^ = This result is computed from individual analyte detections at or above the level of reporting
EP050 (anionic surfactants as MBAS): Samples SL09.001, SL09.002 and SL09.003 were diluted due to matrix interference. LOR adjusted accordingly.
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Analytical Results
Sub-Matrix: SOIL
Client sample ID Client sampling date / time
SL09.001
20-MAY-2011 04:30
ES1110639-001
SL09.002
20-MAY-2011 04:30
ES1110639-002
SL09.003
20-MAY-2011 04:30
ES1110639-003
----------
----------
Compound
CAS Number
---------------100-42-5 98-82-8 103-65-1 108-67-8 135-98-8 95-63-6 98-06-6 99-87-6 104-51-8 108-05-4 78-93-3 108-10-1 591-78-6 75-15-0 594-20-7 78-87-5 10061-01-5 10061-02-6 106-93-4 75-71-8 74-87-3 75-01-4 74-83-9
LOR
1 1.0 20 2 1 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 5 5 5 5 0.5 0.5 0.5 0.5 0.5 0.5 5 5 5 5
Unit
S/cm % mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
EA010: Conductivity
Electrical Conductivity @ 25C 59 10.4 2120 454 117 19.5 2230 390 92 6.3 3320 476
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EA055: Moisture Content

^ Moisture Content (dried @ 103C)
EK062: Total Nitrogen as N (TKN + NOx)

^ Total Nitrogen as N Total Phosphorus as P
EK067G: Total Phosphorus as P by Discrete Analyser EP050: Anionic Surfactants as MBAS

<100 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <5 <5
<100 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <5 <5
<100 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <5 <5
EP074A: Monocyclic Aromatic Hydrocarbons

Styrene Isopropylbenzene n-Propylbenzene 1.3.5-Trimethylbenzene sec-Butylbenzene 1.2.4-Trimethylbenzene tert-Butylbenzene p-Isopropyltoluene n-Butylbenzene
EP074B: Oxygenated Compounds

Vinyl Acetate 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) 2-Hexanone (MBK)
EP074C: Sulfonated Compounds

Carbon disulfide
EP074D: Fumigants
2.2-Dichloropropane 1.2-Dichloropropane cis-1.3-Dichloropropylene trans-1.3-Dichloropropylene 1.2-Dibromoethane (EDB)
EP074E: Halogenated Aliphatic Compounds

Dichlorodifluoromethane Chloromethane Vinyl chloride Bromomethane
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Analytical Results
Sub-Matrix: SOIL
SL09.001
20-MAY-2011 04:30
ES1110639-001
SL09.002
20-MAY-2011 04:30
ES1110639-002
SL09.003
20-MAY-2011 04:30
ES1110639-003
----------
----------
Compound
Chloroethane Trichlorofluoromethane 1.1-Dichloroethene Iodomethane trans-1.2-Dichloroethene 1.1-Dichloroethane cis-1.2-Dichloroethene 1.1.1-Trichloroethane 1.1-Dichloropropylene Carbon Tetrachloride 1.2-Dichloroethane Trichloroethene Dibromomethane 1.1.2-Trichloroethane 1.3-Dichloropropane Tetrachloroethene 1.1.1.2-Tetrachloroethane trans-1.4-Dichloro-2-butene cis-1.4-Dichloro-2-butene 1.1.2.2-Tetrachloroethane 1.2.3-Trichloropropane Pentachloroethane 1.2-Dibromo-3-chloropropane Hexachlorobutadiene
CAS Number
75-00-3 75-69-4 75-35-4 74-88-4 156-60-5 75-34-3 156-59-2 71-55-6 563-58-6 56-23-5 107-06-2 79-01-6 74-95-3 79-00-5 142-28-9 127-18-4 630-20-6 110-57-6 1476-11-5 79-34-5 96-18-4 76-01-7 96-12-8 87-68-3 108-90-7 108-86-1 95-49-8 106-43-4 541-73-1 106-46-7 95-50-1 120-82-1 87-61-6 67-66-3 75-27-4 124-48-1
LOR
5 5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5
Unit
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
EP074E: Halogenated Aliphatic Compounds - Continued

<5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------
EP074F: Halogenated Aromatic Compounds

Chlorobenzene Bromobenzene 2-Chlorotoluene 4-Chlorotoluene 1.3-Dichlorobenzene 1.4-Dichlorobenzene 1.2-Dichlorobenzene 1.2.4-Trichlorobenzene 1.2.3-Trichlorobenzene
EP074G: Trihalomethanes
Chloroform Bromodichloromethane Dibromochloromethane
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Analytical Results
Sub-Matrix: SOIL
SL09.001
20-MAY-2011 04:30
ES1110639-001
SL09.002
20-MAY-2011 04:30
ES1110639-002
SL09.003
20-MAY-2011 04:30
ES1110639-003
----------
----------
Compound
CAS Number
75-25-2 ---------------------------------71-43-2 108-88-3 100-41-4 108-38-3 106-42-3 95-47-6 ---1330-20-7 91-20-3 17060-07-0 2037-26-5 460-00-4 17060-07-0 2037-26-5 460-00-4
LOR
0.5 10 50 100 100 50 10 10 50 100 100 50 0.2 0.5 0.5 0.5 0.5 0.2 0.5 1 0.1 0.1 0.1 0.1 0.1 0.1
Unit
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg % % % % % %
EP074G: Trihalomethanes - Continued

Bromoform
<0.5 <10 <50 <100 <100 <50 <10 <10 <50 <100 <100 <50 <0.2 <0.5 <0.5 <0.5 <0.5 <0.2 <0.5 <1
92.6 93.6 85.0 112 93.5 86.8
<0.5 <10 <50 <100 <100 <50 <10 <10 <50 <100 <100 <50 <0.2 <0.5 <0.5 <0.5 <0.5 <0.2 <0.5 <1
112 108 92.9 85.8 108 97.4
<0.5 <10 <50 <100 <100 <50 <10 <10 <50 <100 <100 <50 <0.2 <0.5 <0.5 <0.5 <0.5 <0.2 <0.5 <1
122 119 102 93.7 119 104
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EP080/071: Total Petroleum Hydrocarbons

C6 - C9 Fraction C10 - C14 Fraction C15 - C28 Fraction C29 - C36 Fraction ^ C10 - C36 Fraction (sum) C6 - C10 Fraction ^ C6 - C10 Fraction minus BTEX (F1) >C10 - C16 Fraction >C16 - C34 Fraction >C34 - C40 Fraction ^ >C10 - C40 Fraction (sum)
EP080/071: Total Recoverable Hydrocarbons - NEPM 2010 Draft
EP080: BTEX
Benzene Toluene Ethylbenzene meta- & para-Xylene ortho-Xylene
EP080: BTEXN
^ Sum of BTEX ^ Total Xylenes Naphthalene
EP074S: VOC Surrogates

1.2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene
EP080S: TPH(V)/BTEX Surrogates

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Surrogate Control Limits

Sub-Matrix: SOIL
Recovery Limits (%)
Compound
CAS Number
17060-07-0 2037-26-5 460-00-4 17060-07-0 2037-26-5 460-00-4
Low
High
EP074S: VOC Surrogates

70.1 66.3 60.3 72.8 73.9 71.6
130.9 137.7 136.3 133.2 132.1 130.0

False
QUALITY CONTROL REPORT

Work Order :
ES1110639
Page Laboratory
: 1 of 9 : Environmental Division Sydney : Client Services : 277-289 Woodpark Road Smithfield NSW Australia 2164
Client
: AGL ENERGY : TOM LAWLER : P.O BOX 67 MENANGLE
Contact
Address
Contact
Address
MENANGLE NSW 2568

E-mail Telephone Facsimile Project Site C-O-C number Sampler Order number Quote number : tlawler@agl.com.au : 4633 5200 : ---: SUGARLOAF 09 SOIL TEST : ---: ---: TOM LAWLER : 4510002862 No. of samples received : SY/456/10 No. of samples analysed :3 :3 Date Samples Received Issue Date : 23-MAY-2011 : 27-MAY-2011 E-mail Telephone Facsimile QC Level : sydney@alsglobal.com : +61-2-8784 8555 : +61-2-8784 8500 : NEPM 1999 Schedule B(3) and ALS QCS3 requirement
This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. All pages of this report have been checked and approved for release. This Quality Control Report contains the following information: l Laboratory Duplicate (DUP) Report ; Relative Percentage Difference (RPD) and Acceptance Limits l Method Blank (MB) and Laboratory Control Spike (LCS) Report ; Recovery and Acceptance Limits l Matrix Spike (MS) Report ; Recovery and Acceptance Limits
Signatories
Ankit Joshi Evie.Sidarta Pabi Subba Sarah Millington Stephen Hislop
Inorganic Chemist Inorganic Chemist Senior Organic Chemist Senior Inorganic Chemist Senior Inorganic Chemist
Sydney Inorganics Sydney Inorganics Sydney Organics Sydney Inorganics Brisbane Inorganics
: : : :
2 of 9
General Comments
The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house developed procedures are employed in the absence of documented standards or by client request. Where moisture determination has been performed, results are reported on a dry weight basis. Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insuffient sample for analysis. Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference. Key : Anonymous = Refers to samples which are not specifically part of this work order but formed part of the QC process lot CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society. LOR = Limit of reporting RPD = Relative Percentage Difference # = Indicates failed QC
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Laboratory Duplicate (DUP) Report

The quality control term Laboratory Duplicate refers to a randomly selected intralaboratory split. Laboratory duplicates provide information regarding method precision and sample heterogeneity. The permitted ranges for the Relative Percent Deviation (RPD) of Laboratory Duplicates are specified in ALS Method QWI -EN/38 and are dependent on the magnitude of results in comparison to the level of reporting: Result < 10 times LOR:No Limit; Result between 10 and 20 times LOR:- 0% - 50%; Result > 20 times LOR:- 0% - 20%. Sub-Matrix: SOIL
Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Laboratory Duplicate (DUP) Report Original Result Duplicate Result RPD (%) Recovery Limits (%)
EA010: Conductivity (QC Lot: 1801156)

ES1110629-001 ES1110632-010 ES1110341-001 ES1110423-022 ES1110639-002 ES1110775-008 ES1110639-001 ES1110639-001 ES1110639-001 Anonymous Anonymous Anonymous Anonymous SL09.002 Anonymous SL09.001 SL09.001 SL09.001 EA010: Electrical Conductivity @ 25C EA010: Electrical Conductivity @ 25C EA055-103: Moisture Content (dried @ 103C) EA055-103: Moisture Content (dried @ 103C) EA055-103: Moisture Content (dried @ 103C) EA055-103: Moisture Content (dried @ 103C) EK067G: Total Phosphorus as P EP050: Anionic Surfactants as MBAS EP074: Styrene EP074: Isopropylbenzene EP074: n-Propylbenzene EP074: 1.3.5-Trimethylbenzene EP074: sec-Butylbenzene EP074: 1.2.4-Trimethylbenzene EP074: tert-Butylbenzene EP074: p-Isopropyltoluene EP074: n-Butylbenzene 100-42-5 98-82-8 103-65-1 108-67-8 135-98-8 95-63-6 98-06-6 99-87-6 104-51-8 108-05-4 78-93-3 108-10-1 591-78-6 75-15-0 594-20-7 78-87-5 10061-01-5 10061-02-6 ---------------------1 1 1.0 1.0 1.0 1.0 2 1 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 5 5 5 5 0.5 0.5 0.5 0.5 0.5 S/cm S/cm % % % % mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 38 50 5.2 38.5 19.5 8.6 454 <100 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 34 51 5.9 40.7 17.9 9.8 463 <100 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 10.6 2.9 13.6 5.6 8.6 13.4 2.1 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0% - 20% 0% - 20% No Limit 0% - 20% 0% - 50% No Limit 0% - 20% No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit
EA055: Moisture Content (QC Lot: 1802515)
EK067G: Total Phosphorus as P by Discrete Analyser (QC Lot: 1800909) EP050: Anionic Surfactants as MBAS (QC Lot: 1801157) EP074A: Monocyclic Aromatic Hydrocarbons (QC Lot: 1800963)
EP074B: Oxygenated Compounds (QC Lot: 1800963)

ES1110639-001 SL09.001 EP074: Vinyl Acetate EP074: 2-Butanone (MEK) EP074: 4-Methyl-2-pentanone (MIBK) EP074: 2-Hexanone (MBK)
EP074C: Sulfonated Compounds (QC Lot: 1800963)

ES1110639-001 ES1110639-001 SL09.001 SL09.001 EP074: Carbon disulfide EP074: 2.2-Dichloropropane EP074: 1.2-Dichloropropane EP074: cis-1.3-Dichloropropylene EP074: trans-1.3-Dichloropropylene
EP074D: Fumigants (QC Lot: 1800963)
Page Work Order Client Project Sub-Matrix: SOIL

Laboratory sample ID
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Client sample ID
Method: Compound
CAS Number
LOR
Unit
Original Result
Duplicate Result
RPD (%)
Recovery Limits (%)
EP074D: Fumigants (QC Lot: 1800963) - continued

ES1110639-001 ES1110639-001 SL09.001 SL09.001 EP074: 1.2-Dibromoethane (EDB) EP074: 1.1-Dichloroethene EP074: Iodomethane EP074: trans-1.2-Dichloroethene EP074: 1.1-Dichloroethane EP074: cis-1.2-Dichloroethene EP074: 1.1.1-Trichloroethane EP074: 1.1-Dichloropropylene EP074: Carbon Tetrachloride EP074: 1.2-Dichloroethane EP074: Trichloroethene EP074: Dibromomethane EP074: 1.1.2-Trichloroethane EP074: 1.3-Dichloropropane EP074: Tetrachloroethene EP074: 1.1.1.2-Tetrachloroethane EP074: trans-1.4-Dichloro-2-butene EP074: cis-1.4-Dichloro-2-butene EP074: 1.1.2.2-Tetrachloroethane EP074: 1.2.3-Trichloropropane EP074: Pentachloroethane EP074: 1.2-Dibromo-3-chloropropane EP074: Hexachlorobutadiene EP074: Dichlorodifluoromethane EP074: Chloromethane EP074: Vinyl chloride EP074: Bromomethane EP074: Chloroethane EP074: Trichlorofluoromethane 106-93-4 75-35-4 74-88-4 156-60-5 75-34-3 156-59-2 71-55-6 563-58-6 56-23-5 107-06-2 79-01-6 74-95-3 79-00-5 142-28-9 127-18-4 630-20-6 110-57-6 1476-11-5 79-34-5 96-18-4 76-01-7 96-12-8 87-68-3 75-71-8 74-87-3 75-01-4 74-83-9 75-00-3 75-69-4 108-90-7 108-86-1 95-49-8 106-43-4 541-73-1 106-46-7 95-50-1 120-82-1 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 5 5 5 5 5 5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <5 <5 <5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <5 <5 <5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit
EP074E: Halogenated Aliphatic Compounds (QC Lot: 1800963)
EP074F: Halogenated Aromatic Compounds (QC Lot: 1800963)

ES1110639-001 SL09.001 EP074: Chlorobenzene EP074: Bromobenzene EP074: 2-Chlorotoluene EP074: 4-Chlorotoluene EP074: 1.3-Dichlorobenzene EP074: 1.4-Dichlorobenzene EP074: 1.2-Dichlorobenzene EP074: 1.2.4-Trichlorobenzene

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Client sample ID
Method: Compound
CAS Number
LOR
Unit
Original Result
Duplicate Result
RPD (%)
Recovery Limits (%)
EP074F: Halogenated Aromatic Compounds (QC Lot: 1800963) - continued

ES1110639-001 ES1110639-001 SL09.001 SL09.001 EP074: 1.2.3-Trichlorobenzene EP074: Chloroform EP074: Bromodichloromethane EP074: Dibromochloromethane EP074: Bromoform 87-61-6 67-66-3 75-27-4 124-48-1 75-25-2 ------------------------------------------71-43-2 108-88-3 100-41-4 108-38-3 106-42-3 95-47-6 91-20-3 0.5 0.5 0.5 0.5 0.5 100 100 50 100 100 50 10 100 100 50 100 100 50 10 0.2 0.5 0.5 0.5 0.5 1 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <0.5 <0.5 <0.5 <0.5 <0.5 <100 <100 <50 <100 <100 <50 <10 <100 <100 <50 <100 <100 <50 <10 <0.2 <0.5 <0.5 <0.5 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <100 <100 <50 <100 <100 <50 <10 <100 <100 <50 <100 <100 <50 <10 <0.2 <0.5 <0.5 <0.5 <0.5 <1 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit
EP074G: Trihalomethanes (QC Lot: 1800963)
EP080/071: Total Petroleum Hydrocarbons (QC Lot: 1800477)

ES1110202-139 Anonymous EP071: C15 - C28 Fraction EP071: C29 - C36 Fraction EP071: C10 - C14 Fraction ES1110549-004 Anonymous EP071: C15 - C28 Fraction EP071: C29 - C36 Fraction EP071: C10 - C14 Fraction

ES1110639-001 ES1110202-139 SL09.001 Anonymous EP080: C6 - C9 Fraction EP071: >C16 - C34 Fraction EP071: >C34 - C40 Fraction EP071: >C10 - C16 Fraction ES1110549-004 Anonymous EP071: >C16 - C34 Fraction EP071: >C34 - C40 Fraction EP071: >C10 - C16 Fraction
EP080/071: Total Recoverable Hydrocarbons - NEPM 2010 Draft (QC Lot: 1800477)
ES1110639-001 ES1110639-001 SL09.001 SL09.001 EP080: C6 - C10 Fraction EP080: Benzene EP080: Toluene EP080: Ethylbenzene EP080: meta- & para-Xylene EP080: ortho-Xylene EP080: Naphthalene
EP080: BTEXN (QC Lot: 1800962)
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Method Blank (MB) and Laboratory Control Spike (LCS) Report

The quality control term Method / Laboratory Blank refers to an analyte free matrix to which all reagents are added in the same volumes or proportions as used in standard sample preparation. The purpose of this QC parameter is to monitor potential laboratory contamination. The quality control term Laboratory Control Sample (LCS) refers to a certified reference material, or a known interference free matrix spiked with target analytes. The purpose of this QC parameter is to monitor method precision and accuracy independent of sample matrix. Dynamic Recovery Limits are based on statistical evaluation of processed LCS. Sub-Matrix: SOIL
Method: Compound CAS Number LOR Unit Method Blank (MB) Report Result Laboratory Control Spike (LCS) Report Spike Concentration Spike Recovery (%) LCS Recovery Limits (%) Low High
EA010: Conductivity (QCLot: 1801156)

EA010: Electrical Conductivity @ 25C EK067G: Total Phosphorus as P ------1 2 1 100-42-5 98-82-8 103-65-1 108-67-8 135-98-8 95-63-6 98-06-6 99-87-6 104-51-8 108-05-4 78-93-3 108-10-1 591-78-6 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 1 5 1 5 1 5 1 5 0.5 0.5 0.5 0.5 0.5 0.5 S/cm mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <1 <2 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ---<5 ---<5 ---<5 ---<5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1412 S/cm 442 mg/kg ---1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 10 mg/kg ---10 mg/kg ---10 mg/kg ---10 mg/kg ---1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 97.4 87.0 ---97.8 111 102 103 106 103 108 105 101 70.9 ---59.5 ---81.5 ---91.1 ---104 92.5 82.8 79.2 80.2 98.6 70 70 ---67 64 59 63 61 62 62 60 57 11 ---37 ---56 ---59 ---53 57 68 59 53 69 130 130 ---121 124 129 125 127 126 126 126 129 155 ---169 ---136 ---133 ---135 129 122 127 129 121
EK067G: Total Phosphorus as P by Discrete Analyser (QCLot: 1800909) EP050: Anionic Surfactants as MBAS (QCLot: 1801157)
EP050: Anionic Surfactants as MBAS
EP074A: Monocyclic Aromatic Hydrocarbons (QCLot: 1800963)

EP074: Styrene EP074: Isopropylbenzene EP074: n-Propylbenzene EP074: 1.3.5-Trimethylbenzene EP074: sec-Butylbenzene EP074: 1.2.4-Trimethylbenzene EP074: tert-Butylbenzene EP074: p-Isopropyltoluene EP074: n-Butylbenzene
EP074B: Oxygenated Compounds (QCLot: 1800963)

EP074: Vinyl Acetate EP074: 2-Butanone (MEK) EP074: 4-Methyl-2-pentanone (MIBK) EP074: 2-Hexanone (MBK)
EP074C: Sulfonated Compounds (QCLot: 1800963)

EP074: Carbon disulfide 75-15-0 594-20-7 78-87-5 10061-01-5 10061-02-6 106-93-4
EP074D: Fumigants (QCLot: 1800963)

EP074: 2.2-Dichloropropane EP074: 1.2-Dichloropropane EP074: cis-1.3-Dichloropropylene EP074: trans-1.3-Dichloropropylene EP074: 1.2-Dibromoethane (EDB)
EP074E: Halogenated Aliphatic Compounds (QCLot: 1800963)

Method: Compound
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Method Blank (MB) Report CAS Number LOR Unit Result Laboratory Control Spike (LCS) Report Spike Concentration Spike Recovery (%) LCS Recovery Limits (%) Low High
EP074E: Halogenated Aliphatic Compounds (QCLot: 1800963) - continued

EP074: Dichlorodifluoromethane EP074: Chloromethane EP074: Vinyl chloride EP074: Bromomethane EP074: Chloroethane EP074: Trichlorofluoromethane EP074: 1.1-Dichloroethene EP074: Iodomethane EP074: trans-1.2-Dichloroethene EP074: 1.1-Dichloroethane EP074: cis-1.2-Dichloroethene EP074: 1.1.1-Trichloroethane EP074: 1.1-Dichloropropylene EP074: Carbon Tetrachloride EP074: 1.2-Dichloroethane EP074: Trichloroethene EP074: Dibromomethane EP074: 1.1.2-Trichloroethane EP074: 1.3-Dichloropropane EP074: Tetrachloroethene EP074: 1.1.1.2-Tetrachloroethane EP074: trans-1.4-Dichloro-2-butene EP074: cis-1.4-Dichloro-2-butene EP074: 1.1.2.2-Tetrachloroethane EP074: 1.2.3-Trichloropropane EP074: Pentachloroethane EP074: 1.2-Dibromo-3-chloropropane EP074: Hexachlorobutadiene 75-71-8 74-87-3 75-01-4 74-83-9 75-00-3 75-69-4 75-35-4 74-88-4 156-60-5 75-34-3 156-59-2 71-55-6 563-58-6 56-23-5 107-06-2 79-01-6 74-95-3 79-00-5 142-28-9 127-18-4 630-20-6 110-57-6 1476-11-5 79-34-5 96-18-4 76-01-7 96-12-8 87-68-3 108-90-7 108-86-1 95-49-8 106-43-4 1 5 1 5 1 5 1 5 1 5 1 5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg ---<5 ---<5 ---<5 ---<5 ---<5 ---<5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 10 mg/kg ---10 mg/kg ---10 mg/kg ---10 mg/kg ---10 mg/kg ---10 mg/kg ---1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 127 ---126 ---115 ---112 ---120 ---114 ---106 93.2 92.2 94.5 95.1 87.7 91.3 85.3 85.4 95.8 84.8 99.4 91.6 121 99.3 87.4 74.2 96.2 97.4 91.6 91.1 107 104 102 98.1 101 28.9 ---43 ---40 ---44 ---49 ---53 ---57 48 62 64 66 61 62 56 70 65 67 70 71 61 57 45 56 57 62 26.4 51 48 67 68 63 64 146 ---140 ---146 ---152 ---149 ---139 ---133 134 128 126 124 125 128 128 124 129 123 122 121 139 125 137 128 127 126 144 133 136 125 122 127 126
EP074F: Halogenated Aromatic Compounds (QCLot: 1800963)

EP074: Chlorobenzene EP074: Bromobenzene EP074: 2-Chlorotoluene EP074: 4-Chlorotoluene

Method: Compound
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EP074F: Halogenated Aromatic Compounds (QCLot: 1800963) - continued

EP074: 1.3-Dichlorobenzene EP074: 1.4-Dichlorobenzene EP074: 1.2-Dichlorobenzene EP074: 1.2.4-Trichlorobenzene EP074: 1.2.3-Trichlorobenzene 541-73-1 106-46-7 95-50-1 120-82-1 87-61-6 67-66-3 75-27-4 124-48-1 75-25-2 ---------------------0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 50 100 100 10 50 100 100 50 10 0.2 0.5 0.5 0.5 0.5 1 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <50 <100 <100 <10 <50 <100 <100 ---<10 <0.2 <0.5 <0.5 <0.5 <0.5 <1 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 200 mg/kg 300 mg/kg 200 mg/kg 26 mg/kg 250 mg/kg 350 mg/kg ---150 mg/kg 31 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 2 mg/kg 1 mg/kg 1 mg/kg 104 99.3 98.8 106 100 77.9 81.9 99.1 85.8 103 134 112 102 113 133 ---72.2 86.4 91.4 77.0 83.2 79.3 84.0 80.3 66 64 67 54 58 67 60 58 57 59 74 63 68.4 59 74 ---63 68.4 63 69 61 62 63 63 124 126 121 134 132 123 126 124 121 131 138 131 128 131 138 ---131 128 121 122 117 118 117 131
EP074G: Trihalomethanes (QCLot: 1800963)

EP074: Chloroform EP074: Bromodichloromethane EP074: Dibromochloromethane EP074: Bromoform
EP080/071: Total Petroleum Hydrocarbons (QCLot: 1800477)

EP071: C10 - C14 Fraction EP071: C15 - C28 Fraction EP071: C29 - C36 Fraction

EP080: C6 - C9 Fraction EP071: >C10 - C16 Fraction EP071: >C16 - C34 Fraction EP071: >C34 - C40 Fraction
EP080/071: Total Recoverable Hydrocarbons - NEPM 2010 Draft (QCLot: 1800477)

EP080: C6 - C10 Fraction ---71-43-2 108-88-3 100-41-4 108-38-3 106-42-3 95-47-6 91-20-3
EP080: BTEXN (QCLot: 1800962)

EP080: Benzene EP080: Toluene EP080: Ethylbenzene EP080: meta- & para-Xylene EP080: ortho-Xylene EP080: Naphthalene
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Matrix Spike (MS) Report

The quality control term Matrix Spike (MS) refers to an intralaboratory split sample spiked with a representative set of target analytes. The purpose of this QC parameter is to monitor potential matrix effects on analyte recoveries. Static Recovery Limits as per laboratory Data Quality Objectives (DQOs). Ideal recovery ranges stated may be waived in the event of sample matrix interference. Sub-Matrix: SOIL
Spike Laboratory sample ID Client sample ID Method: Compound CAS Number Concentration Matrix Spike (MS) Report Spike Recovery (%) MS Recovery Limits (%) Low High
EK067G: Total Phosphorus as P by Discrete Analyser (QCLot: 1800909)

ES1110639-001 ES1110639-001 SL09.001 SL09.001 EK067G: Total Phosphorus as P EP074: 1.1-Dichloroethene EP074: Trichloroethene ---75-35-4 79-01-6 108-90-7 ------------------------71-43-2 108-88-3 100-41-4 108-38-3 106-42-3 95-47-6 91-20-3 100 mg/kg 2.5 mg/kg 2.5 mg/kg 2.5 mg/kg 640 mg/kg 3140 mg/kg 2860 mg/kg 32.5 mg/kg 850 mg/kg 4800 mg/kg 2400 mg/kg 37.5 mg/kg 2.5 mg/kg 2.5 mg/kg 2.5 mg/kg 2.5 mg/kg 2.5 mg/kg 2.5 mg/kg 88.3 109 76.6 73.5 99.4 77.2 95.9 82.1 96.3 78.8 99.7 75.5 72.1 83.0 79.6 74.9 73.4 74.4 70 70 70 70 73 53 52 70 73 53 52 70 70 70 70 70 70 70 130 130 130 130 137 131 132 130 137 131 132 130 130 130 130 130 130 130
EP074E: Halogenated Aliphatic Compounds (QCLot: 1800963)
EP074F: Halogenated Aromatic Compounds (QCLot: 1800963)

ES1110639-001 ES1110202-139 SL09.001 Anonymous EP074: Chlorobenzene EP071: C10 - C14 Fraction EP071: C15 - C28 Fraction EP071: C29 - C36 Fraction

ES1110639-001 ES1110202-139 SL09.001 Anonymous EP080: C6 - C9 Fraction EP071: >C10 - C16 Fraction EP071: >C16 - C34 Fraction EP071: >C34 - C40 Fraction

ES1110639-001 ES1110639-001 SL09.001 SL09.001 EP080: C6 - C10 Fraction EP080: Benzene EP080: Toluene EP080: Ethylbenzene EP080: meta- & para-Xylene EP080: ortho-Xylene EP080: Naphthalene
True
INTERPRETIVE QUALITY CONTROL REPORT

Work Order : ES1110639
Page Laboratory
: 1 of 6 : Environmental Division Sydney : Client Services : 277-289 Woodpark Road Smithfield NSW Australia 2164 : sydney@alsglobal.com : +61-2-8784 8555 : +61-2-8784 8500 : NEPM 1999 Schedule B(3) and ALS QCS3 requirement : 23-MAY-2011 : 27-MAY-2011 :3 :3
Client
Contact
Address
: AGL ENERGY : TOM LAWLER : P.O BOX 67 MENANGLE
Contact
Address
MENANGLE NSW 2568

E-mail Telephone Facsimile Project Site C-O-C number Sampler Order number Quote number : tlawler@agl.com.au : 4633 5200 : ---: SUGARLOAF 09 SOIL TEST : ---: ---: TOM LAWLER : 4510002862 : SY/456/10 E-mail Telephone Facsimile QC Level Date Samples Received Issue Date No. of samples received No. of samples analysed
This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. All pages of this report have been checked and approved for release. This Interpretive Quality Control Report contains the following information: l Analysis Holding Time Compliance
l Quality Control Parameter Frequency Compliance l Brief Method Summaries l Summary of Outliers

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Analysis Holding Time Compliance

The following report summarises extraction / preparation and analysis times and compares with recommended holding times. Dates reported represent first date of extraction or analysis and precludes subsequent dilutions and reruns. Information is also provided re the sample container (preservative) from which the analysis aliquot was taken. Elapsed period to analysis represents number of days from sampling where no extraction / digestion is involved or period from extraction / digestion where this is present. For composite samples, sampling date is assumed to be that of the oldest sample contributing to the composite. Sample date for laboratory produced leachates is assumed as the completion date of the leaching process. Outliers for holding time are based on USEPA SW 846, APHA, AS and NEPM (1999). A listing of breaches is provided in the Summary of Outliers. Holding times for leachate methods (excluding elutriates) vary according to the analytes being determined on the resulting solution. For non -volatile analytes, the holding time compliance assessment compares the leach date with the shortest analyte holding time for the equivalent soil method. These soil holding times are: Organics (14 days); Mercury (28 days) & other metals (180 days). A recorded breach therefore does not guarantee a breach for all non-volatile parameters. Matrix: SOIL
Method Container / Client Sample ID(s) Sample Date
Evaluation: = Holding time breach ; = Within holding time.

Extraction / Preparation
Date extracted
Analysis Evaluation
Date analysed
Due for extraction
Due for analysis
Evaluation
EA010: Conductivity Soil Glass Jar - Unpreserved SL09.001, SL09.003 EA055: Moisture Content Soil Glass Jar - Unpreserved SL09.001, SL09.003 EK067G: Total Phosphorus as P by Discrete Analyser Soil Glass Jar - Unpreserved SL09.001, SL09.003 EP050: Anionic Surfactants as MBAS Soil Glass Jar - Unpreserved SL09.001, SL09.003 EP074A: Monocyclic Aromatic Hydrocarbons Soil Glass Jar - Unpreserved SL09.001, SL09.003 EP074B: Oxygenated Compounds Soil Glass Jar - Unpreserved SL09.001, SL09.003 EP074C: Sulfonated Compounds Soil Glass Jar - Unpreserved SL09.001, SL09.003 EP074D: Fumigants Soil Glass Jar - Unpreserved SL09.001, SL09.003
SL09.002,
20-MAY-2011
24-MAY-2011
27-MAY-2011
24-MAY-2011
21-JUN-2011
SL09.002,
20-MAY-2011
----
----
----
24-MAY-2011
03-JUN-2011
SL09.002,
20-MAY-2011
24-MAY-2011
16-NOV-2011
24-MAY-2011
16-NOV-2011
SL09.002,
20-MAY-2011
24-MAY-2011
16-NOV-2011
25-MAY-2011
26-MAY-2011
SL09.002,
20-MAY-2011
24-MAY-2011
03-JUN-2011
26-MAY-2011
03-JUN-2011
SL09.002,
20-MAY-2011
24-MAY-2011
03-JUN-2011
26-MAY-2011
03-JUN-2011
SL09.002,
20-MAY-2011
24-MAY-2011
03-JUN-2011
26-MAY-2011
03-JUN-2011
SL09.002,
20-MAY-2011
24-MAY-2011
03-JUN-2011
26-MAY-2011
03-JUN-2011
Page Work Order Client Project Matrix: SOIL

Method
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ES1110639 AGL ENERGY SUGARLOAF 09 SOIL TEST Evaluation: = Holding time breach ; = Within holding time.
Sample Date
Date extracted
Analysis Evaluation
Date analysed
Container / Client Sample ID(s)
Due for extraction
Due for analysis
Evaluation
EP074E: Halogenated Aliphatic Compounds Soil Glass Jar - Unpreserved SL09.001, SL09.003 EP074F: Halogenated Aromatic Compounds Soil Glass Jar - Unpreserved SL09.001, SL09.003 EP074G: Trihalomethanes Soil Glass Jar - Unpreserved SL09.001, SL09.003 EP080/071: Total Petroleum Hydrocarbons Soil Glass Jar - Unpreserved SL09.001, SL09.003 Soil Glass Jar - Unpreserved SL09.001, SL09.003 Soil Glass Jar - Unpreserved SL09.001, SL09.003 Soil Glass Jar - Unpreserved SL09.001, SL09.003 EP080: BTEX Soil Glass Jar - Unpreserved SL09.001, SL09.003 EP080: BTEXN Soil Glass Jar - Unpreserved SL09.001, SL09.003
SL09.002,
20-MAY-2011
24-MAY-2011
03-JUN-2011
26-MAY-2011
03-JUN-2011
SL09.002,
20-MAY-2011
24-MAY-2011
03-JUN-2011
26-MAY-2011
03-JUN-2011
SL09.002,
20-MAY-2011
24-MAY-2011
03-JUN-2011
26-MAY-2011
03-JUN-2011
SL09.002,
20-MAY-2011
24-MAY-2011
03-JUN-2011
24-MAY-2011
03-JUL-2011
SL09.002,
20-MAY-2011
24-MAY-2011
03-JUN-2011
26-MAY-2011
03-JUN-2011
SL09.002,
20-MAY-2011
24-MAY-2011
03-JUN-2011
24-MAY-2011
03-JUL-2011
SL09.002,
20-MAY-2011
24-MAY-2011
03-JUN-2011
26-MAY-2011
03-JUN-2011
SL09.002,
20-MAY-2011
24-MAY-2011
03-JUN-2011
26-MAY-2011
03-JUN-2011
SL09.002,
20-MAY-2011
24-MAY-2011
03-JUN-2011
26-MAY-2011
03-JUN-2011
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Quality Control Parameter Frequency Compliance

The following report summarises the frequency of laboratory QC samples analysed within the analytical lot(s) in which the submitted sample(s) was(where) processed. Actual rate should be greater than or equal to the expected rate. A listing of breaches is provided in the Summary of Outliers. Matrix: SOIL
Quality Control Sample Type
Evaluation: = Quality Control frequency not within specification ; = Quality Control frequency within specification.
Count Method
EP050 EA010 EA055-103 EK067G EP071 EP080 EP074 EA010 EK067G EP071 EP080 EP074 EP050 EA010 EK067G EP071 EP080 EP074 EK067G EP071 EP080 EP074
Analytical Methods
Laboratory Duplicates (DUP) Anionic Surfactants as MBAS Electrical Conductivity (1:5) Moisture Content Total Phosporus By Discrete Analyser TPH - Semivolatile Fraction TPH Volatiles/BTEX Volatile Organic Compounds Laboratory Control Samples (LCS) Electrical Conductivity (1:5) Total Phosporus By Discrete Analyser TPH - Semivolatile Fraction TPH Volatiles/BTEX Volatile Organic Compounds Method Blanks (MB) Anionic Surfactants as MBAS Electrical Conductivity (1:5) Total Phosporus By Discrete Analyser TPH - Semivolatile Fraction TPH Volatiles/BTEX Volatile Organic Compounds Matrix Spikes (MS) Total Phosporus By Discrete Analyser TPH - Semivolatile Fraction TPH Volatiles/BTEX Volatile Organic Compounds
QC
1 2 4 1 2 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
Regular
3 20 26 3 18 10 4 20 3 18 10 4 3 20 3 18 10 4 3 18 10 4
Actual
33.3 10.0 15.4 33.3 11.1 10.0 25.0 5.0 33.3 5.6 10.0 25.0 33.3 5.0 33.3 5.6 10.0 25.0 33.3 5.6 10.0 25.0
Rate (%) Expected

10.0 10.0 10.0 10.0 10.0 10.0 10.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0
Quality Control Specification

Evaluation
NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999
Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement
ALS QCS3 requirement ALS QCS3 requirement ALS QCS3 requirement ALS QCS3 requirement
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Brief Method Summaries

The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the US EPA, APHA, AS and NEPM. In house developed procedures are employed in the absence of documented standards or by client request. The following report provides brief descriptions of the analytical procedures employed for results reported in the Certificate of Analysis. Sources from which ALS methods have been developed are provided within the Method Descriptions.
Analytical Methods
Method
EA010 EA055-103 EK059G EK061G EK062G EK067G EP050
Matrix
Method Descriptions
Electrical Conductivity (1:5) Moisture Content Nitrite and Nitrate as N (NOx)- Soluble by Discrete Analyser TKN as N By Discrete Analyser Total Nitrogen as N (TKN + NOx) By Discrete Analyser Total Phosporus By Discrete Analyser Anionic Surfactants as MBAS
SOIL SOIL SOIL SOIL SOIL SOIL SOIL
TPH - Semivolatile Fraction Volatile Organic Compounds
EP071 EP074
SOIL SOIL
TPH Volatiles/BTEX
EP080
SOIL
(APHA 21st ed., 2510) Conductivity is determined on soil samples using a 1:5 soil/water leach. This method is compliant with NEPM (1999) Schedule B(3) (Method 104) A gravimetric procedure based on weight loss over a 12 hour drying period at 103-105 degrees C. This method is compliant with NEPM (2010 Draft) Schedule B(3) Section 7.1 and Table 1 (14 day holding time). APHA 21st ed., 4500 NO3- F. Combined oxidised Nitrogen (NO2+NO3) in a water extract is determined by Cadmium Reduction, and direct colourimetry by Discrete Analyser. APHA 21st ed., 4500-Norg-D Soil samples are digested using Kjeldahl digestion followed by determination by Discrete Analyser. APHA 21st ed., 4500 Norg/NO3- Total Nitrogen is determined as the sum of TKN and Oxidised Nitrrogen, each determined seperately as N. APHA 21st ed., 4500 P-B&F This procedure involves sulfuric acid digestion and quantification using Discrete Analyser. APHA 21st ed., 5540 B & C. MBAS results determined following 1:5 solid / water leach. This method comprises three successive extractions from acid aqueous medium containing excess methylene blue, into chloroform, followed by an aqueous backwash and measurement of the colour by spectrophotometry at 625nm. ALS is not NATA accredited for this analysis. (USEPA SW 846 - 8015A) Sample extracts are analysed by Capillary GC/FID and quantified against alkane standards over the range C10 - C36. This method is compliant with NEPM (1999) Schedule B(3) (Method 506.1) (USEPA SW 846 - 8260B) Extracts are analysed by Purge and Trap, Capillary GC/MS. Quantification is by comparison against an established 5 point calibration curve. This method is compliant with NEPM (1999) Schedule B(3) (Method 501) (USEPA SW 846 - 8260B) Extracts are analysed by Purge and Trap, Capillary GC/MS. Quantification is by comparison against an established 5 point calibration curve. This method is compliant with NEPM (1999) Schedule B(3) (Method 501)
Method Descriptions
Preparation Methods
Method
EK061/EK067 EN34
Matrix
TKN/TP Digestion 1:5 solid / water leach for soluble analytes Methanolic Extraction of Soils for Purge and Trap Tumbler Extraction of Solids (Option B Non-concentrating)
SOIL SOIL SOIL SOIL
* ORG16
ORG17B
APHA 21st ed., 4500 Norg- D; APHA 21st ed., 4500 P - H. Macro Kjeldahl digestion. 10 g of soil is mixed with 50 mL of distilled water and tumbled end over end for 1 hour. Water soluble salts are leached from the soil by the continuous suspension. Samples are settled and the water filtered off for analysis. (USEPA SW 846 - 5030A) 5g of solid is shaken with surrogate and 10mL methanol prior to analysis by Purge and Trap - GC/MS. In-house, Mechanical agitation (tumbler). 10g of sample, Na2SO4 and surrogate are extracted with 20mL 1:1 DCM/Acetone by end over end tumble. The solvent is transferred directly to a GC vial for analysis.
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Summary of Outliers
Outliers : Quality Control Samples
The following report highlights outliers flagged in the Quality Control (QC) Report. Surrogate recovery limits are static and based on USEPA SW 846 or ALS-QWI/EN/38 (in the absence of specific USEPA limits). This report displays QC Outliers (breaches) only.
Duplicates, Method Blanks, Laboratory Control Samples and Matrix Spikes

l l l l
For all matrices, no Method Blank value outliers occur. For all matrices, no Duplicate outliers occur. For all matrices, no Laboratory Control outliers occur. For all matrices, no Matrix Spike outliers occur.
Regular Sample Surrogates

l
For all regular sample matrices, no surrogate recovery outliers occur.
Outliers : Analysis Holding Time Compliance

This report displays Holding Time breaches only. Only the respective Extraction / Preparation and/or Analysis component is/are displayed.
No Analysis Holding Time Outliers exist.
Outliers : Frequency of Quality Control Samples

The following report highlights breaches in the Frequency of Quality Control Samples.
No Quality Control Sample Frequency Outliers exist.
ES1111046 False
Work Order :
ES1111046
Page Laboratory
: 1 of 15 : Environmental Division Sydney : Client Services : 277-289 Woodpark Road Smithfield NSW Australia 2164 : sydney@alsglobal.com : +61-2-8784 8555 : +61-2-8784 8500 : NEPM 1999 Schedule B(3) and ALS QCS3 requirement : 26-MAY-2011 : 31-MAY-2011 : 12 : 12
Client
: URS AUSTRALIA : MR ADAM SULLIVAN : LEVEL 3, 116 MILLER STREET : : : : : : : :
Contact
Contact
NORTH SYDNEY NSW, AUSTRALIA 2060 adam_sullivan@urscorp.com +61 2 8925 5500 +61 2 8925 5555 43177447 ------AM ----
: EN/038/10
This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. All pages of this report have been checked and approved for release. This Certificate of Analysis contains the following information: l General Comments l Analytical Results l Surrogate Control Limits
Signatories
Ankit Joshi Evie.Sidarta Pabi Subba Sarah Millington Wisam.Marassa
Inorganic Chemist Inorganic Chemist Senior Organic Chemist Senior Inorganic Chemist Metals Coordinator
Sydney Inorganics Sydney Inorganics Sydney Organics Sydney Inorganics Sydney Inorganics

: : : :
2 of 15
ES1111046 URS AUSTRALIA 43177447
General Comments
: : : :
3 of 15
Analytical Results
Sub-Matrix: SOIL
SB1_0.0-0.1
26-MAY-2011 14:50
ES1111046-001
SB2_0.0-0.1
26-MAY-2011 14:55
ES1111046-002
SB3_0.0-0.1
26-MAY-2011 15:10
ES1111046-003
SB4_0.0-0.1
26-MAY-2011 15:05
ES1111046-004
SB5_0.0-0.1
26-MAY-2011 15:20
ES1111046-005
Compound
CAS Number
---------7440-70-2 7439-95-4 7440-23-5 7440-09-7 7440-38-2 7440-43-9 7440-47-3 7440-50-8 7439-92-1 7440-02-0 7440-66-6 7439-97-6 ---------------319-84-6 118-74-1 319-85-7 58-89-9 319-86-8
LOR
0.1 5 1.0 10 10 10 10 5 1 2 5 5 2 5 0.1 0.1 20 20 2 0.5 0.05 0.05 0.05 0.05 0.05
Unit
pH Unit mg/kg % mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg % mg/kg mg/kg mg/kg mg/kg mg/kg
EA002 : pH (Soils)
pH Value 8.1 650 18.0 10 10 230 60 6 <1 15 23 20 13 47 8.0 663 18.3 30 30 410 180 8 <1 16 26 22 15 49 7.4 484 14.7 10 10 130 80 7 <1 16 25 22 15 50 7.8 497 14.9 10 10 90 40 8 <1 15 27 19 16 45 6.7 358 15.1 40 20 20 110 8 <1 15 25 22 17 79
EA014 Total Soluble Salts

^ Total Soluble Salts

ED093S: Soluble Major Cations

Calcium Magnesium Sodium Potassium
EG005T: Total Metals by ICP-AES

Arsenic Cadmium Chromium Copper Lead Nickel Zinc
EG035T: Total Recoverable Mercury by FIMS

Mercury Nitrite + Nitrate as N (Sol.) Total Kjeldahl Nitrogen as N
<0.1 <5.0
2450 2450 390 3.6
<0.1
7.0 1680 1690 274 4.5
<0.1 <5.0
2120 2120 325 4.3
<0.1 <5.0
1420 1420 214 1.6
<0.1
16.2 4900 4920 532 9.6
EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser EK061G: Total Kjeldahl Nitrogen By Discrete Analyser EK062: Total Nitrogen as N (TKN + NOx)
EK067G: Total Phosphorus as P by Discrete Analyser EP004: Organic Matter

Organic Matter
EP068A: Organochlorine Pesticides (OC)

alpha-BHC Hexachlorobenzene (HCB) beta-BHC gamma-BHC delta-BHC
<0.05 <0.05 <0.05 <0.05 <0.05
<0.05 <0.05 <0.05 <0.05 <0.05
<0.05 <0.05 <0.05 <0.05 <0.05
<0.05 <0.05 <0.05 <0.05 <0.05
<0.05 <0.05 <0.05 <0.05 <0.05
: : : :
4 of 15
Analytical Results
Sub-Matrix: SOIL
SB1_0.0-0.1
26-MAY-2011 14:50
ES1111046-001
SB2_0.0-0.1
26-MAY-2011 14:55
ES1111046-002
SB3_0.0-0.1
26-MAY-2011 15:10
ES1111046-003
SB4_0.0-0.1
26-MAY-2011 15:05
ES1111046-004
SB5_0.0-0.1
26-MAY-2011 15:20
ES1111046-005
Compound
Heptachlor Aldrin Heptachlor epoxide trans-Chlordane alpha-Endosulfan cis-Chlordane Dieldrin 4.4`-DDE Endrin beta-Endosulfan 4.4`-DDD Endrin aldehyde Endosulfan sulfate 4.4`-DDT Endrin ketone Methoxychlor
CAS Number
76-44-8 309-00-2 1024-57-3 5103-74-2 959-98-8 5103-71-9 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 7421-93-4 1031-07-8 50-29-3 53494-70-5 72-43-5 62-73-7 919-86-8 6923-22-4 60-51-5 333-41-5 5598-13-0 298-00-0 121-75-5 55-38-9 2921-88-2 56-38-2 23505-41-1 470-90-6 4824-78-6 22224-92-6 34643-46-4 563-12-2 786-19-6 86-50-0 91-20-3
LOR
0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.2 0.05 0.2 0.05 0.05 0.2 0.05 0.05 0.05 0.2 0.05 0.05 0.05 0.2 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.5
Unit
EP068A: Organochlorine Pesticides (OC) - Continued

<0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.05 <0.2 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.5 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.05 <0.2 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.5 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.05 <0.2 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.5 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.05 <0.2 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.5 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.05 <0.2 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.5
EP068B: Organophosphorus Pesticides (OP)

Dichlorvos Demeton-S-methyl Monocrotophos Dimethoate Diazinon Chlorpyrifos-methyl Parathion-methyl Malathion Fenthion Chlorpyrifos Parathion Pirimphos-ethyl Chlorfenvinphos Bromophos-ethyl Fenamiphos Prothiofos Ethion Carbophenothion Azinphos Methyl Naphthalene
EP075(SIM)B: Polynuclear Aromatic Hydrocarbons
: : : :
5 of 15
Analytical Results
Sub-Matrix: SOIL
SB1_0.0-0.1
26-MAY-2011 14:50
ES1111046-001
SB2_0.0-0.1
26-MAY-2011 14:55
ES1111046-002
SB3_0.0-0.1
26-MAY-2011 15:10
ES1111046-003
SB4_0.0-0.1
26-MAY-2011 15:05
ES1111046-004
SB5_0.0-0.1
26-MAY-2011 15:20
ES1111046-005
Compound
Acenaphthylene Acenaphthene Fluorene Phenanthrene Anthracene Fluoranthene Pyrene Benz(a)anthracene Chrysene Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(a)pyrene Indeno(1.2.3.cd)pyrene Dibenz(a.h)anthracene Benzo(g.h.i)perylene ^ Sum of polycyclic aromatic hydrocarbons
CAS Number
208-96-8 83-32-9 86-73-7 85-01-8 120-12-7 206-44-0 129-00-0 56-55-3 218-01-9 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 ----
LOR
0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5
Unit
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
EP075(SIM)B: Polynuclear Aromatic Hydrocarbons - Continued

<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5

---------------------------------71-43-2 108-88-3 100-41-4 108-38-3 106-42-3 95-47-6 ----
10 50 100 100 50 10 10 50 100 100 50 0.2 0.5 0.5 0.5 0.5 0.2
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
<10 <50 <100 <100 <50 <10 <10 <50 <100 <100 <50 <0.2 <0.5 <0.5 <0.5 <0.5 <0.2
<10 <50 <100 <100 <50 <10 <10 <50 <100 <100 <50 <0.2 <0.5 <0.5 <0.5 <0.5 <0.2
<10 <50 <100 <100 <50 <10 <10 <50 <100 <100 <50 <0.2 <0.5 <0.5 <0.5 <0.5 <0.2
<10 <50 <100 <100 <50 <10 <10 <50 <100 <100 <50 <0.2 <0.5 <0.5 <0.5 <0.5 <0.2
<10 <50 <100 <100 <50 <10 <10 <50 <100 <100 <50 <0.2 <0.5 <0.5 <0.5 <0.5 <0.2
EP080: BTEX
EP080: BTEXN
^ Sum of BTEX
: : : :
6 of 15
Analytical Results
Sub-Matrix: SOIL
SB1_0.0-0.1
26-MAY-2011 14:50
ES1111046-001
SB2_0.0-0.1
26-MAY-2011 14:55
ES1111046-002
SB3_0.0-0.1
26-MAY-2011 15:10
ES1111046-003
SB4_0.0-0.1
26-MAY-2011 15:05
ES1111046-004
SB5_0.0-0.1
26-MAY-2011 15:20
ES1111046-005
Compound
CAS Number
1330-20-7 91-20-3 21655-73-2 78-48-8 13127-88-3 93951-73-6 118-79-6 321-60-8 1719-06-8 1718-51-0 17060-07-0 2037-26-5 460-00-4
LOR
0.5 1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1
Unit
mg/kg mg/kg % % % % % % % % % % %
EP080: BTEXN - Continued

^ Total Xylenes Naphthalene
<0.5 <1
102 107 107 106 111 106 107 118 88.1 76.4 73.8
<0.5 <1
95.2 113 108 106 110 106 106 115 88.6 91.3 82.9
<0.5 <1
102 106 107 106 111 114 109 117 86.1 93.6 81.4
<0.5 <1
100 102 112 104 106 113 110 117 82.1 87.0 79.5
<0.5 <1
99.0 104 110 104 98.6 113 108 116 90.2 97.4 86.4
EP068S: Organochlorine Pesticide Surrogate

Dibromo-DDE DEF
EP068T: Organophosphorus Pesticide Surrogate EP075(SIM)S: Phenolic Compound Surrogates

Phenol-d6 2-Chlorophenol-D4 2.4.6-Tribromophenol
EP075(SIM)T: PAH Surrogates

2-Fluorobiphenyl Anthracene-d10 4-Terphenyl-d14

: : : :
7 of 15
Analytical Results
Sub-Matrix: SOIL
SB6_0.0-0.1
26-MAY-2011 15:25
ES1111046-006
SB7_0.0-0.1
26-MAY-2011 15:30
ES1111046-007
SB8_0.0-0.1
26-MAY-2011 15:35
ES1111046-008
SB9_0.0-0.1
26-MAY-2011 15:40
ES1111046-009
SB10_0.0-0.1
26-MAY-2011 15:45
ES1111046-010
Compound
CAS Number
---------7440-70-2 7439-95-4 7440-23-5 7440-09-7 7440-38-2 7440-43-9 7440-47-3 7440-50-8 7439-92-1 7440-02-0 7440-66-6 7439-97-6 ---------------319-84-6 118-74-1 319-85-7 58-89-9 319-86-8
LOR
0.1 5 1.0 10 10 10 10 5 1 2 5 5 2 5 0.1 0.1 20 20 2 0.5 0.05 0.05 0.05 0.05 0.05
Unit
EA002 : pH (Soils)
pH Value 7.1 452 8.2 10 20 130 60 7 <1 16 30 19 16 49 6.6 198 8.3 20 20 30 60 7 <1 15 27 20 15 48 6.3 221 16.2 20 20 20 130 6 <1 13 25 25 12 61 6.0 2240 14.7 140 70 30 690 8 <1 15 25 44 14 74 6.4 266 14.3 20 20 20 120 6 <1 14 27 43 14 94





<0.1 <2.0
1310 1310 226 2.4
<0.1 <2.0
2360 2360 362 2.8
<0.1 <2.0
3890 3890 533 5.9
<0.1
171 6410 6580 678 7.0
<0.1 <5.0
6040 6040 960 5.6

Organic Matter

<0.05 <0.05 <0.05 <0.05 <0.05
<0.05 <0.05 <0.05 <0.05 <0.05
<0.05 <0.05 <0.05 <0.05 <0.05
<0.05 <0.05 <0.05 <0.05 <0.05
<0.05 <0.05 <0.05 <0.05 <0.05
: : : :
8 of 15
Analytical Results
Sub-Matrix: SOIL
SB6_0.0-0.1
26-MAY-2011 15:25
ES1111046-006
SB7_0.0-0.1
26-MAY-2011 15:30
ES1111046-007
SB8_0.0-0.1
26-MAY-2011 15:35
ES1111046-008
SB9_0.0-0.1
26-MAY-2011 15:40
ES1111046-009
SB10_0.0-0.1
26-MAY-2011 15:45
ES1111046-010
Compound
CAS Number
76-44-8 309-00-2 1024-57-3 5103-74-2 959-98-8 5103-71-9 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 7421-93-4 1031-07-8 50-29-3 53494-70-5 72-43-5 62-73-7 919-86-8 6923-22-4 60-51-5 333-41-5 5598-13-0 298-00-0 121-75-5 55-38-9 2921-88-2 56-38-2 23505-41-1 470-90-6 4824-78-6 22224-92-6 34643-46-4 563-12-2 786-19-6 86-50-0 91-20-3
LOR
0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.2 0.05 0.2 0.05 0.05 0.2 0.05 0.05 0.05 0.2 0.05 0.05 0.05 0.2 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.5
Unit

<0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.05 <0.2 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.5 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.05 <0.2 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.5 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.05 <0.2 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.5 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.05 <0.2 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.5 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.05 <0.2 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.5

: : : :
9 of 15
Analytical Results
Sub-Matrix: SOIL
SB6_0.0-0.1
26-MAY-2011 15:25
ES1111046-006
SB7_0.0-0.1
26-MAY-2011 15:30
ES1111046-007
SB8_0.0-0.1
26-MAY-2011 15:35
ES1111046-008
SB9_0.0-0.1
26-MAY-2011 15:40
ES1111046-009
SB10_0.0-0.1
26-MAY-2011 15:45
ES1111046-010
Compound
CAS Number
208-96-8 83-32-9 86-73-7 85-01-8 120-12-7 206-44-0 129-00-0 56-55-3 218-01-9 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 ----
LOR
0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5
Unit

<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5

---------------------------------71-43-2 108-88-3 100-41-4 108-38-3 106-42-3 95-47-6 ----
10 50 100 100 50 10 10 50 100 100 50 0.2 0.5 0.5 0.5 0.5 0.2
<10 <50 <100 <100 <50 <10 <10 <50 <100 <100 <50 <0.2 <0.5 <0.5 <0.5 <0.5 <0.2
<10 <50 <100 <100 <50 <10 <10 <50 <100 <100 <50 <0.2 <0.5 <0.5 <0.5 <0.5 <0.2
<10 <50 <100 <100 <50 <10 <10 <50 <100 <100 <50 <0.2 <0.5 <0.5 <0.5 <0.5 <0.2
<10 <50 <100 <100 <50 <10 <10 <50 <100 <100 <50 <0.2 <0.5 <0.5 <0.5 <0.5 <0.2
<10 <50 <100 <100 <50 <10 <10 <50 <100 <100 <50 <0.2 <0.5 <0.5 <0.5 <0.5 <0.2
EP080: BTEX
EP080: BTEXN
^ Sum of BTEX
: : : :
10 of 15
Analytical Results
Sub-Matrix: SOIL
SB6_0.0-0.1
26-MAY-2011 15:25
ES1111046-006
SB7_0.0-0.1
26-MAY-2011 15:30
ES1111046-007
SB8_0.0-0.1
26-MAY-2011 15:35
ES1111046-008
SB9_0.0-0.1
26-MAY-2011 15:40
ES1111046-009
SB10_0.0-0.1
26-MAY-2011 15:45
ES1111046-010
Compound
CAS Number
1330-20-7 91-20-3 21655-73-2 78-48-8 13127-88-3 93951-73-6 118-79-6 321-60-8 1719-06-8 1718-51-0 17060-07-0 2037-26-5 460-00-4
LOR
0.5 1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1
Unit
mg/kg mg/kg % % % % % % % % % % %

<0.5 <1
88.7 94.2 103 97.7 83.7 107 105 113 89.4 89.6 80.6
<0.5 <1
116 111 103 97.6 89.1 108 103 112 90.2 91.9 81.4
<0.5 <1
102 120 113 107 105 115 111 118 88.7 90.0 80.4
<0.5 <1
89.1 102 104 103 104 110 105 115 89.9 92.6 80.6
<0.5 <1
85.7 99.8 113 109 106 114 112 121 91.1 89.4 81.2

Dibromo-DDE DEF



: : : :
11 of 15
Analytical Results
Sub-Matrix: SOIL
SB11_0.0-0.1
26-MAY-2011 15:55
ES1111046-011
QC100
[26-MAY-2011]
ES1111046-012
----------
----------
----------
Compound
CAS Number
---------7440-70-2 7439-95-4 7440-23-5 7440-09-7 7440-38-2 7440-43-9 7440-47-3 7440-50-8 7439-92-1 7440-02-0 7440-66-6 7439-97-6 ---------------319-84-6 118-74-1 319-85-7 58-89-9 319-86-8
LOR
0.1 5 1.0 10 10 10 10 5 1 2 5 5 2 5 0.1 0.1 20 20 2 0.5 0.05 0.05 0.05 0.05 0.05
Unit
EA002 : pH (Soils)
pH Value 7.9 520 18.0 8.0 494 20.0
----------------------------------------------------------------------------
----------------------------------------------------------------------------
----------------------------------------------------------------------------



<10
10 120 60 7 <1 15 35 19 15 55
<10
10 140 60 7 <1 15 27 20 16 60


<0.1 <5.0
2000 2000 333 3.0
<0.1 <5.0
2080 2080 448 3.2

Organic Matter

<0.05 <0.05 <0.05 <0.05 <0.05
<0.05 <0.05 <0.05 <0.05 <0.05
: : : :
12 of 15
Analytical Results
Sub-Matrix: SOIL
SB11_0.0-0.1
26-MAY-2011 15:55
ES1111046-011
QC100
[26-MAY-2011]
ES1111046-012
----------
----------
----------
Compound
CAS Number
76-44-8 309-00-2 1024-57-3 5103-74-2 959-98-8 5103-71-9 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 7421-93-4 1031-07-8 50-29-3 53494-70-5 72-43-5 62-73-7 919-86-8 6923-22-4 60-51-5 333-41-5 5598-13-0 298-00-0 121-75-5 55-38-9 2921-88-2 56-38-2 23505-41-1 470-90-6 4824-78-6 22224-92-6 34643-46-4 563-12-2 786-19-6 86-50-0 91-20-3
LOR
0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.2 0.05 0.2 0.05 0.05 0.2 0.05 0.05 0.05 0.2 0.05 0.05 0.05 0.2 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.5
Unit

<0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.05 <0.2 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.5 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.05 <0.2 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.5 -------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------

: : : :
13 of 15
Analytical Results
Sub-Matrix: SOIL
SB11_0.0-0.1
26-MAY-2011 15:55
ES1111046-011
QC100
[26-MAY-2011]
ES1111046-012
----------
----------
----------
Compound
CAS Number
208-96-8 83-32-9 86-73-7 85-01-8 120-12-7 206-44-0 129-00-0 56-55-3 218-01-9 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 ----
LOR
0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5
Unit

<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -------------------------------------------------------------------------------------------------------------------------------------------------

---------------------------------71-43-2 108-88-3 100-41-4 108-38-3 106-42-3 95-47-6 ----
10 50 100 100 50 10 10 50 100 100 50 0.2 0.5 0.5 0.5 0.5 0.2
<10 <50 <100 <100 <50 <10 <10 <50 <100 <100 <50 <0.2 <0.5 <0.5 <0.5 <0.5 <0.2
<10 <50 <100 <100 <50 <10 <10 <50 <100 <100 <50 <0.2 <0.5 <0.5 <0.5 <0.5 <0.2
----------------------------------------------------
----------------------------------------------------
----------------------------------------------------
EP080: BTEX
EP080: BTEXN
^ Sum of BTEX
: : : :
14 of 15
Analytical Results
Sub-Matrix: SOIL
SB11_0.0-0.1
26-MAY-2011 15:55
ES1111046-011
QC100
[26-MAY-2011]
ES1111046-012
----------
----------
----------
Compound
CAS Number
1330-20-7 91-20-3 21655-73-2 78-48-8 13127-88-3 93951-73-6 118-79-6 321-60-8 1719-06-8 1718-51-0 17060-07-0 2037-26-5 460-00-4
LOR
0.5 1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1
Unit
mg/kg mg/kg % % % % % % % % % % %

<0.5 <1
120 115 107 104 107 109 106 115 99.3 97.9 88.0
<0.5 <1
70.8 95.3 108 103 107 110 105 113 86.2 85.4 79.4
----------------------------------------
----------------------------------------
----------------------------------------

Dibromo-DDE DEF



: : : :
15 of 15
Surrogate Control Limits

Sub-Matrix: SOIL
Recovery Limits (%)
Compound
CAS Number
21655-73-2 78-48-8 13127-88-3 93951-73-6 118-79-6 321-60-8 1719-06-8 1718-51-0 17060-07-0 2037-26-5 460-00-4
Low
High

Dibromo-DDE
19.5 22.7 56.3 53.8 23.1 58.9 55.0 54.0 72.8 73.9 71.6
167.0 163.5 133.3 133.8 134.9 132.7 137.6 147.8 133.2 132.1 130.0
EP068T: Organophosphorus Pesticide Surrogate

DEF
EP075(SIM)S: Phenolic Compound Surrogates



False

Work Order :
ES1111046
Page Laboratory
Client
: URS AUSTRALIA : MR ADAM SULLIVAN : LEVEL 3, 116 MILLER STREET
Contact
Address
Contact
Address
NORTH SYDNEY NSW, AUSTRALIA 2060

E-mail Telephone Facsimile Project Site C-O-C number Sampler Order number Quote number : adam_sullivan@urscorp.com : +61 2 8925 5500 : +61 2 8925 5555 : 43177447 : ---: ---: AM : ---No. of samples received : EN/038/10 No. of samples analysed : 12 : 12 Date Samples Received Issue Date : 26-MAY-2011 : 31-MAY-2011 E-mail Telephone Facsimile QC Level : sydney@alsglobal.com : +61-2-8784 8555 : +61-2-8784 8500 : NEPM 1999 Schedule B(3) and ALS QCS3 requirement
Signatories
Ankit Joshi Evie.Sidarta Pabi Subba Sarah Millington Wisam.Marassa
Inorganic Chemist Inorganic Chemist Senior Organic Chemist Senior Inorganic Chemist Metals Coordinator
Sydney Inorganics Sydney Inorganics Sydney Organics Sydney Inorganics Sydney Inorganics
: : : :
2 of 13
General Comments
: : : :
3 of 13

EA002 : pH (Soils) (QC Lot: 1807255)

ES1110904-001 ES1111046-010 ES1110915-020 ES1111046-008 ES1111046-001 Anonymous SB10_0.0-0.1 Anonymous SB8_0.0-0.1 SB1_0.0-0.1 EA002: pH Value EA002: pH Value EA055-103: Moisture Content (dried @ 103C) EA055-103: Moisture Content (dried @ 103C) ED093S: Calcium ED093S: Magnesium ED093S: Sodium ED093S: Potassium ES1111046-010 SB10_0.0-0.1 ED093S: Calcium ED093S: Magnesium ED093S: Sodium ED093S: Potassium ------------7440-70-2 7439-95-4 7440-23-5 7440-09-7 7440-70-2 7439-95-4 7440-23-5 7440-09-7 7440-43-9 7440-47-3 7440-02-0 7440-38-2 7440-50-8 7439-92-1 7440-66-6 7440-43-9 7440-47-3 7440-02-0 7440-38-2 7440-50-8 7439-92-1 7440-66-6 7439-97-6 7439-97-6 ------0.1 0.1 1.0 1.0 10 10 10 10 10 10 10 10 1 2 2 5 5 5 5 1 2 2 5 5 5 5 0.1 0.1 0.1 0.1 pH Unit pH Unit % % mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 7.1 6.4 4.8 16.2 10 10 230 60 20 20 20 120 <1 55 52 6 28 22 74 <1 16 15 7 25 22 50 <0.1 <0.1 <5.0 <5.0 7.0 6.3 5.4 17.7 10 10 260 70 20 10 20 110 <1 55 52 <5 28 18 77 <1 15 15 7 28 20 50 <0.1 <0.1 <5.0 <5.0 0.0 0.0 12.7 8.7 0.0 0.0 12.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 18.7 4.1 0.0 0.0 0.0 0.0 9.0 8.5 0.0 0.0 0.0 0.0 0.0 0% - 20% 0% - 20% No Limit 0% - 50% No Limit No Limit 0% - 20% No Limit No Limit No Limit No Limit 0% - 50% No Limit 0% - 20% 0% - 20% No Limit No Limit No Limit 0% - 50% No Limit No Limit No Limit No Limit No Limit No Limit 0% - 50% No Limit No Limit No Limit No Limit
ED093S: Soluble Major Cations (QC Lot: 1807256)
EG005T: Total Metals by ICP-AES (QC Lot: 1806656)

ES1110955-005 Anonymous EG005T: Cadmium EG005T: Chromium EG005T: Nickel EG005T: Arsenic EG005T: Copper EG005T: Lead EG005T: Zinc ES1111046-003 SB3_0.0-0.1 EG005T: Cadmium EG005T: Chromium EG005T: Nickel EG005T: Arsenic EG005T: Copper EG005T: Lead EG005T: Zinc
EG035T: Total Recoverable Mercury by FIMS (QC Lot: 1806657)

ES1110955-005 ES1111046-003 ES1111046-001 ES1111046-010 Anonymous SB3_0.0-0.1 SB1_0.0-0.1 SB10_0.0-0.1 EG035T: Mercury EG035T: Mercury EK059G: Nitrite + Nitrate as N (Sol.) EK059G: Nitrite + Nitrate as N (Sol.)
EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser (QC Lot: 1807257)

: : : :
4 of 13
Client sample ID
Method: Compound
CAS Number
LOR
Unit
Original Result
Duplicate Result
RPD (%)
Recovery Limits (%)
EK061G: Total Kjeldahl Nitrogen By Discrete Analyser (QC Lot: 1807646)

ES1110992-021 ES1111046-008 ES1110956-001 ES1111046-008 ES1111040-002 ES1111046-010 ES1111046-002 Anonymous SB8_0.0-0.1 Anonymous SB8_0.0-0.1 Anonymous SB10_0.0-0.1 SB2_0.0-0.1 EK061G: Total Kjeldahl Nitrogen as N EK061G: Total Kjeldahl Nitrogen as N EK067G: Total Phosphorus as P EK067G: Total Phosphorus as P EP004: Organic Matter EP004: Organic Matter EP068: alpha-BHC EP068: Hexachlorobenzene (HCB) EP068: beta-BHC EP068: gamma-BHC EP068: delta-BHC EP068: Heptachlor EP068: Aldrin EP068: Heptachlor epoxide EP068: trans-Chlordane EP068: alpha-Endosulfan EP068: cis-Chlordane EP068: Dieldrin EP068: 4.4`-DDE EP068: Endrin EP068: beta-Endosulfan EP068: 4.4`-DDD EP068: Endrin aldehyde EP068: Endosulfan sulfate EP068: Endrin ketone EP068: 4.4`-DDT EP068: Methoxychlor ES1111046-012 QC100 EP068: alpha-BHC EP068: Hexachlorobenzene (HCB) EP068: beta-BHC EP068: gamma-BHC EP068: delta-BHC EP068: Heptachlor EP068: Aldrin EP068: Heptachlor epoxide EP068: trans-Chlordane ------------------319-84-6 118-74-1 319-85-7 58-89-9 319-86-8 76-44-8 309-00-2 1024-57-3 5103-74-2 959-98-8 5103-71-9 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 7421-93-4 1031-07-8 53494-70-5 50-29-3 72-43-5 319-84-6 118-74-1 319-85-7 58-89-9 319-86-8 76-44-8 309-00-2 1024-57-3 5103-74-2 20 20 2 2 0.5 0.5 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.2 0.2 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 mg/kg mg/kg mg/kg mg/kg % % mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 2220 3890 Not Authorised 533 1.2 5.6 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 2020 4100 # Not Authorised 540 1.2 5.6 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 9.7 5.4 # 3.9 1.3 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0% - 20% 0% - 20% 0% - 20% 0% - 20% No Limit 0% - 50% No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit
EK067G: Total Phosphorus as P by Discrete Analyser (QC Lot: 1807645)
EP004: Organic Matter (QC Lot: 1807990)
EP068A: Organochlorine Pesticides (OC) (QC Lot: 1807982)

: : : :
5 of 13
Client sample ID
Method: Compound
CAS Number
LOR
Unit
Original Result
Duplicate Result
RPD (%)
Recovery Limits (%)
EP068A: Organochlorine Pesticides (OC) (QC Lot: 1807982) - continued

ES1111046-012 QC100 EP068: alpha-Endosulfan EP068: cis-Chlordane EP068: Dieldrin EP068: 4.4`-DDE EP068: Endrin EP068: beta-Endosulfan EP068: 4.4`-DDD EP068: Endrin aldehyde EP068: Endosulfan sulfate EP068: Endrin ketone EP068: 4.4`-DDT EP068: Methoxychlor 959-98-8 5103-71-9 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 7421-93-4 1031-07-8 53494-70-5 50-29-3 72-43-5 62-73-7 919-86-8 60-51-5 333-41-5 5598-13-0 121-75-5 55-38-9 2921-88-2 23505-41-1 470-90-6 4824-78-6 22224-92-6 34643-46-4 563-12-2 786-19-6 86-50-0 6923-22-4 298-00-0 56-38-2 62-73-7 919-86-8 60-51-5 333-41-5 5598-13-0 121-75-5 55-38-9 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.2 0.2 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.2 0.2 0.2 0.05 0.05 0.05 0.05 0.05 0.05 0.05 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.2 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.2 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit
EP068B: Organophosphorus Pesticides (OP) (QC Lot: 1807982)

ES1111046-002 SB2_0.0-0.1 EP068: Dichlorvos EP068: Demeton-S-methyl EP068: Dimethoate EP068: Diazinon EP068: Chlorpyrifos-methyl EP068: Malathion EP068: Fenthion EP068: Chlorpyrifos EP068: Pirimphos-ethyl EP068: Chlorfenvinphos EP068: Bromophos-ethyl EP068: Fenamiphos EP068: Prothiofos EP068: Ethion EP068: Carbophenothion EP068: Azinphos Methyl EP068: Monocrotophos EP068: Parathion-methyl EP068: Parathion ES1111046-012 QC100 EP068: Dichlorvos EP068: Demeton-S-methyl EP068: Dimethoate EP068: Diazinon EP068: Chlorpyrifos-methyl EP068: Malathion EP068: Fenthion

: : : :
6 of 13
Client sample ID
Method: Compound
CAS Number
LOR
Unit
Original Result
Duplicate Result
RPD (%)
Recovery Limits (%)
EP068B: Organophosphorus Pesticides (OP) (QC Lot: 1807982) - continued

ES1111046-012 QC100 EP068: Chlorpyrifos EP068: Pirimphos-ethyl EP068: Chlorfenvinphos EP068: Bromophos-ethyl EP068: Fenamiphos EP068: Prothiofos EP068: Ethion EP068: Carbophenothion EP068: Azinphos Methyl EP068: Monocrotophos EP068: Parathion-methyl EP068: Parathion 2921-88-2 23505-41-1 470-90-6 4824-78-6 22224-92-6 34643-46-4 563-12-2 786-19-6 86-50-0 6923-22-4 298-00-0 56-38-2 91-20-3 208-96-8 83-32-9 86-73-7 85-01-8 120-12-7 206-44-0 129-00-0 56-55-3 218-01-9 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 91-20-3 208-96-8 83-32-9 86-73-7 85-01-8 120-12-7 206-44-0 129-00-0 56-55-3 218-01-9 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.2 0.2 0.2 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.2 <0.2 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.2 <0.2 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit
EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QC Lot: 1807978)

ES1111046-002 SB2_0.0-0.1 EP075(SIM): Naphthalene EP075(SIM): Acenaphthylene EP075(SIM): Acenaphthene EP075(SIM): Fluorene EP075(SIM): Phenanthrene EP075(SIM): Anthracene EP075(SIM): Fluoranthene EP075(SIM): Pyrene EP075(SIM): Benz(a)anthracene EP075(SIM): Chrysene EP075(SIM): Benzo(b)fluoranthene EP075(SIM): Benzo(k)fluoranthene EP075(SIM): Benzo(a)pyrene EP075(SIM): Indeno(1.2.3.cd)pyrene EP075(SIM): Dibenz(a.h)anthracene EP075(SIM): Benzo(g.h.i)perylene ES1111046-012 QC100 EP075(SIM): Naphthalene EP075(SIM): Acenaphthylene EP075(SIM): Acenaphthene EP075(SIM): Fluorene EP075(SIM): Phenanthrene EP075(SIM): Anthracene EP075(SIM): Fluoranthene EP075(SIM): Pyrene EP075(SIM): Benz(a)anthracene EP075(SIM): Chrysene

: : : :
7 of 13
Client sample ID
Method: Compound
CAS Number
LOR
Unit
Original Result
Duplicate Result
RPD (%)
Recovery Limits (%)
EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QC Lot: 1807978) - continued

ES1111046-012 QC100 EP075(SIM): Benzo(b)fluoranthene EP075(SIM): Benzo(k)fluoranthene EP075(SIM): Benzo(a)pyrene EP075(SIM): Indeno(1.2.3.cd)pyrene EP075(SIM): Dibenz(a.h)anthracene EP075(SIM): Benzo(g.h.i)perylene 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 ------------------------------------------------71-43-2 108-88-3 100-41-4 108-38-3 106-42-3 95-47-6 91-20-3 71-43-2 108-88-3 100-41-4 108-38-3 106-42-3 0.5 0.5 0.5 0.5 0.5 0.5 10 10 100 100 50 100 100 50 10 10 100 100 50 100 100 50 0.2 0.5 0.5 0.5 0.5 1 0.2 0.5 0.5 0.5 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <10 <10 <100 <100 <50 <100 <100 <50 <10 <10 <100 <100 <50 <100 <100 <50 <0.2 <0.5 <0.5 <0.5 <0.5 <1 <0.2 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <10 <10 <100 <100 <50 <100 <100 <50 <10 <10 <100 <100 <50 <100 <100 <50 <0.2 <0.5 <0.5 <0.5 <0.5 <1 <0.2 <0.5 <0.5 <0.5 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit No Limit

ES1110777-001 ES1111046-005 ES1111046-002 Anonymous SB5_0.0-0.1 SB2_0.0-0.1 EP080: C6 - C9 Fraction EP080: C6 - C9 Fraction EP071: C15 - C28 Fraction EP071: C29 - C36 Fraction EP071: C10 - C14 Fraction ES1111046-012 QC100 EP071: C15 - C28 Fraction EP071: C29 - C36 Fraction EP071: C10 - C14 Fraction
ES1110777-001 ES1111046-005 ES1111046-002 Anonymous SB5_0.0-0.1 SB2_0.0-0.1 EP080: C6 - C10 Fraction EP080: C6 - C10 Fraction EP071: >C16 - C34 Fraction EP071: >C34 - C40 Fraction EP071: >C10 - C16 Fraction ES1111046-012 QC100 EP071: >C16 - C34 Fraction EP071: >C34 - C40 Fraction EP071: >C10 - C16 Fraction
EP080: BTEXN (QC Lot: 1806443)

ES1110777-001 Anonymous EP080: Benzene EP080: Toluene EP080: Ethylbenzene EP080: meta- & para-Xylene EP080: ortho-Xylene EP080: Naphthalene ES1111046-005 SB5_0.0-0.1 EP080: Benzene EP080: Toluene EP080: Ethylbenzene EP080: meta- & para-Xylene

: : : :
8 of 13
Client sample ID
Method: Compound
CAS Number
LOR
Unit
Original Result
Duplicate Result
RPD (%)
Recovery Limits (%)
EP080: BTEXN (QC Lot: 1806443) - continued

ES1111046-005 SB5_0.0-0.1 EP080: ortho-Xylene EP080: Naphthalene 95-47-6 91-20-3 0.5 1 mg/kg mg/kg <0.5 <1 <0.5 <1 0.0 0.0 No Limit No Limit
: : : :
9 of 13

ED093S: Soluble Major Cations (QCLot: 1807256)

ED093S: Calcium ED093S: Magnesium ED093S: Sodium ED093S: Potassium 7440-70-2 7439-95-4 7440-23-5 7440-09-7 7440-38-2 7440-43-9 7440-47-3 7440-50-8 7439-92-1 7440-02-0 7440-66-6 7439-97-6 ------------319-84-6 118-74-1 319-85-7 58-89-9 319-86-8 76-44-8 309-00-2 1024-57-3 5103-74-2 959-98-8 10 10 10 10 5 1 2 5 5 2 5 0.1 0.1 20 2 0.5 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg % mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <10 <10 <10 <10 <5 <1 <2 <5 <5 <2 <5 <0.1 <0.1 <20 <2 <0.5 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 250 mg/kg 250 mg/kg 250 mg/kg 250 mg/kg 13.11 mg/kg 2.76 mg/kg 60.93 mg/kg 54.68 mg/kg 54.76 mg/kg 55.23 mg/kg 103.88 mg/kg 1.4 mg/kg 4.8 mg/kg 1000 mg/kg 442 mg/kg 4.58 % 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 96.6 98.8 88.4 95.9 111 90.9 99.8 97.5 93.2 100 91.9 76.1 97.4 96.2 78.7 90.0 95.1 88.8 86.0 101 99.8 101 88.1 85.5 84.9 83.2 89.2 93.4 79.2 85.7 70 83.3 89.2 90.1 85.2 88.3 88.9 67 70 70 70 86 60.8 59.4 59.8 59.8 65.8 65.6 67 65.6 60.7 65.8 108 109 110 111 130 111 117 114 111 116 112 118 130 130 130 111 116 115 117 118 114 115 113 113 113 116
EG005T: Total Metals by ICP-AES (QCLot: 1806656)

EG005T: Arsenic EG005T: Cadmium EG005T: Chromium EG005T: Copper EG005T: Lead EG005T: Nickel EG005T: Zinc EG035T: Mercury EK059G: Nitrite + Nitrate as N (Sol.) EK061G: Total Kjeldahl Nitrogen as N EK067G: Total Phosphorus as P
EG035T: Total Recoverable Mercury by FIMS (QCLot: 1806657) EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser (QCLot: 1807257) EK061G: Total Kjeldahl Nitrogen By Discrete Analyser (QCLot: 1807646) EK067G: Total Phosphorus as P by Discrete Analyser (QCLot: 1807645) EP004: Organic Matter (QCLot: 1807990)
EP004: Organic Matter
EP068A: Organochlorine Pesticides (OC) (QCLot: 1807982)

EP068: alpha-BHC EP068: Hexachlorobenzene (HCB) EP068: beta-BHC EP068: gamma-BHC EP068: delta-BHC EP068: Heptachlor EP068: Aldrin EP068: Heptachlor epoxide EP068: trans-Chlordane EP068: alpha-Endosulfan

Method: Compound
: : : :
10 of 13
EP068A: Organochlorine Pesticides (OC) (QCLot: 1807982) - continued

EP068: cis-Chlordane EP068: Dieldrin EP068: 4.4`-DDE EP068: Endrin EP068: beta-Endosulfan EP068: 4.4`-DDD EP068: Endrin aldehyde EP068: Endosulfan sulfate EP068: 4.4`-DDT EP068: Endrin ketone EP068: Methoxychlor 5103-71-9 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 7421-93-4 1031-07-8 50-29-3 53494-70-5 72-43-5 62-73-7 919-86-8 6923-22-4 60-51-5 333-41-5 5598-13-0 298-00-0 121-75-5 55-38-9 2921-88-2 56-38-2 23505-41-1 470-90-6 4824-78-6 22224-92-6 34643-46-4 563-12-2 786-19-6 86-50-0 91-20-3 208-96-8 83-32-9 86-73-7 85-01-8 120-12-7 206-44-0 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.2 0.05 0.2 0.05 0.05 0.2 0.05 0.05 0.05 0.2 0.05 0.05 0.05 0.2 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.5 0.5 0.5 0.5 0.5 0.5 0.5 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.2 <0.05 <0.2 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.2 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 4 mg/kg 4 mg/kg 4 mg/kg 4 mg/kg 4 mg/kg 4 mg/kg 4 mg/kg 85.1 92.8 102 109 91.7 91.2 100 110 110 101 103 83.7 111 89.9 94.4 97.9 98.2 82.8 88.0 82.5 92.9 77.1 81.0 90.4 84.5 92.8 89.2 88.9 111 71.7 110 108 109 110 108 108 106 57.3 67.4 67.5 63 66.1 65.3 57.3 63.6 58.4 63.6 50.4 25.5 10.1 2.88 48.6 64.9 65.1 61.4 60.4 64.7 64.2 60 64.8 61.4 64.3 45.5 65.4 62 59.5 29.8 81.9 79.6 81.5 79.9 79.4 81.1 78.8 120 116 114 121 117 116 115 119 127 117 132 124 159 149 126 111 111 113 127 110 111 116 111 123 114 128 111 116 119 137 113 113 112 112 114 112 113
EP068B: Organophosphorus Pesticides (OP) (QCLot: 1807982)

EP068: Dichlorvos EP068: Demeton-S-methyl EP068: Monocrotophos EP068: Dimethoate EP068: Diazinon EP068: Chlorpyrifos-methyl EP068: Parathion-methyl EP068: Malathion EP068: Fenthion EP068: Chlorpyrifos EP068: Parathion EP068: Pirimphos-ethyl EP068: Chlorfenvinphos EP068: Bromophos-ethyl EP068: Fenamiphos EP068: Prothiofos EP068: Ethion EP068: Carbophenothion EP068: Azinphos Methyl EP075(SIM): Naphthalene EP075(SIM): Acenaphthylene EP075(SIM): Acenaphthene EP075(SIM): Fluorene EP075(SIM): Phenanthrene EP075(SIM): Anthracene EP075(SIM): Fluoranthene
EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QCLot: 1807978)

Method: Compound
: : : :
11 of 13
EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QCLot: 1807978) - continued

EP075(SIM): Pyrene EP075(SIM): Benz(a)anthracene EP075(SIM): Chrysene EP075(SIM): Benzo(b)fluoranthene EP075(SIM): Benzo(k)fluoranthene EP075(SIM): Benzo(a)pyrene EP075(SIM): Indeno(1.2.3.cd)pyrene EP075(SIM): Dibenz(a.h)anthracene EP075(SIM): Benzo(g.h.i)perylene 129-00-0 56-55-3 218-01-9 205-99-2 207-08-9 50-32-8 193-39-5 53-70-3 191-24-2 ------------------------0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 10 50 100 100 10 50 100 100 50 0.2 0.5 0.5 0.5 0.5 1 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <10 <50 <100 <100 <10 <50 <100 <100 ---<0.2 <0.5 <0.5 <0.5 <0.5 <1 4 mg/kg 4 mg/kg 4 mg/kg 4 mg/kg 4 mg/kg 4 mg/kg 4 mg/kg 4 mg/kg 4 mg/kg 26 mg/kg 200 mg/kg 300 mg/kg 200 mg/kg 31 mg/kg 250 mg/kg 350 mg/kg ---150 mg/kg 1 mg/kg 1 mg/kg 1 mg/kg 2 mg/kg 1 mg/kg 1 mg/kg 104 109 109 101 102 106 96.7 98.3 88.2 94.3 112 114 110 92.9 113 106 ---92.0 96.4 100 87.8 89.4 90.7 99.0 78.9 77.2 79.8 71.8 74.2 76.4 71 71.7 72.4 68.4 59 74 63 68.4 59 74 ---63 63 69 61 62 63 63 113 112 114 118 117 113 113 113 114 128 131 138 131 128 131 138 ---131 121 122 117 118 117 131

EP080: C6 - C9 Fraction

EP071: C10 - C14 Fraction EP071: C15 - C28 Fraction EP071: C29 - C36 Fraction EP080: C6 - C10 Fraction EP071: >C10 - C16 Fraction EP071: >C16 - C34 Fraction EP071: >C34 - C40 Fraction
EP080/071: Total Recoverable Hydrocarbons - NEPM 2010 Draft (QCLot: 1806443) EP080/071: Total Recoverable Hydrocarbons - NEPM 2010 Draft (QCLot: 1807977)

EP080: Benzene EP080: Toluene EP080: Ethylbenzene EP080: meta- & para-Xylene EP080: ortho-Xylene EP080: Naphthalene 71-43-2 108-88-3 100-41-4 108-38-3 106-42-3 95-47-6 91-20-3
: : : :
12 of 13

The quality control term Matrix Spike (MS) refers to an intralaboratory split sample spiked with a representative set of target analytes. The purpose of this QC parameter is to monitor potential matrix effects on analyte recoveries. Static Recovery Limits as per laboratory Data Quality Objectives (DQOs). Ideal recovery ranges stated may be waived in the event of sample matrix interference. Sub-Matrix: SOIL
Spike Laboratory sample ID Client sample ID Method: Compound CAS Number Concentration Matrix Spike (MS) Report Spike Recovery (%) MS Recovery Limits (%) Low High
EG005T: Total Metals by ICP-AES (QCLot: 1806656)

ES1110955-005 Anonymous EG005T: Arsenic EG005T: Cadmium EG005T: Chromium EG005T: Copper EG005T: Lead EG005T: Nickel EG005T: Zinc 7440-38-2 7440-43-9 7440-47-3 7440-50-8 7439-92-1 7440-02-0 7440-66-6 7439-97-6 ---------58-89-9 76-44-8 309-00-2 60-57-1 72-20-8 50-29-3 333-41-5 5598-13-0 23505-41-1 4824-78-6 34643-46-4 83-32-9 129-00-0 ---50 mg/kg 50 mg/kg 50 mg/kg 250 mg/kg 250 mg/kg 50 mg/kg 250 mg/kg 5 mg/kg 30 mg/kg 500 mg/kg 100 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 2 mg/kg 2 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 0.5 mg/kg 10 mg/kg 10 mg/kg 32.5 mg/kg 87.1 90.2 90.3 101 90.8 90.8 88.2 84.9 99.8 94.3 86.6 80.8 92.6 85.3 86.4 107 98.0 89.5 91.4 82.8 82.1 80.8 104 106 95.2 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 130 130 130 130 130 130 130 130 130 130 130 130 130 130 130 130 130 130 130 130 130 130 130 130 130
EG035T: Total Recoverable Mercury by FIMS (QCLot: 1806657)

ES1110955-005 ES1111046-001 ES1110992-021 ES1110956-001 ES1111046-002 Anonymous SB1_0.0-0.1 Anonymous Anonymous SB2_0.0-0.1 EG035T: Mercury EK059G: Nitrite + Nitrate as N (Sol.) EK061G: Total Kjeldahl Nitrogen as N EK067G: Total Phosphorus as P EP068: gamma-BHC EP068: Heptachlor EP068: Aldrin EP068: Dieldrin EP068: Endrin EP068: 4.4`-DDT
EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser (QCLot: 1807257) EK061G: Total Kjeldahl Nitrogen By Discrete Analyser (QCLot: 1807646) EK067G: Total Phosphorus as P by Discrete Analyser (QCLot: 1807645) EP068A: Organochlorine Pesticides (OC) (QCLot: 1807982)
EP068B: Organophosphorus Pesticides (OP) (QCLot: 1807982)

ES1111046-002 SB2_0.0-0.1 EP068: Diazinon EP068: Chlorpyrifos-methyl EP068: Pirimphos-ethyl EP068: Bromophos-ethyl EP068: Prothiofos
EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QCLot: 1807978)

ES1111046-002 SB2_0.0-0.1 EP075(SIM): Acenaphthene EP075(SIM): Pyrene

ES1111046-005 SB5_0.0-0.1 EP080: C6 - C9 Fraction
: : : :
13 of 13
Matrix Spike (MS) Report Spike Spike Recovery (%) MS Recovery Limits (%) Low High
Client sample ID
Method: Compound
CAS Number
Concentration

ES1111046-002 SB2_0.0-0.1 EP071: C10 - C14 Fraction EP071: C15 - C28 Fraction EP071: C29 - C36 Fraction ---------------------71-43-2 108-88-3 100-41-4 108-38-3 106-42-3 95-47-6 91-20-3 640 mg/kg 3140 mg/kg 2860 mg/kg 37.5 mg/kg 850 mg/kg 4800 mg/kg 2400 mg/kg 2.5 mg/kg 2.5 mg/kg 2.5 mg/kg 2.5 mg/kg 2.5 mg/kg 2.5 mg/kg 93.1 92.6 86.2 93.7 104 90.2 78.4 83.2 88.8 85.5 85.8 87.0 77.0 73 53 52 70 73 53 52 70 70 70 70 70 70 137 131 132 130 137 131 132 130 130 130 130 130 130

ES1111046-005 ES1111046-002 SB5_0.0-0.1 SB2_0.0-0.1 EP080: C6 - C10 Fraction EP071: >C10 - C16 Fraction EP071: >C16 - C34 Fraction EP071: >C34 - C40 Fraction

ES1111046-005 SB5_0.0-0.1 EP080: Benzene EP080: Toluene EP080: Ethylbenzene EP080: meta- & para-Xylene EP080: ortho-Xylene EP080: Naphthalene
True

Page Laboratory
: 1 of 10 : Environmental Division Sydney : Client Services : 277-289 Woodpark Road Smithfield NSW Australia 2164 : sydney@alsglobal.com : +61-2-8784 8555 : +61-2-8784 8500 : NEPM 1999 Schedule B(3) and ALS QCS3 requirement : 26-MAY-2011 : 31-MAY-2011 : 12 : 12
Client
Contact
Address
Contact
Address

E-mail Telephone Facsimile Project Site C-O-C number Sampler Order number Quote number : adam_sullivan@urscorp.com : +61 2 8925 5500 : +61 2 8925 5555 : 43177447 : ---: ---: AM : ---: EN/038/10 E-mail Telephone Facsimile QC Level Date Samples Received Issue Date No. of samples received No. of samples analysed

: : : :
2 of 10


Date extracted
Analysis Evaluation
Date analysed
Due for extraction
Due for analysis
Evaluation
EA002 : pH (Soils) Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1, EA055: Moisture Content Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1, ED093S: Soluble Major Cations Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1, EG005T: Total Metals by ICP-AES Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1,
SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100
26-MAY-2011
27-MAY-2011
02-JUN-2011
27-MAY-2011
27-MAY-2011
SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100
26-MAY-2011
----
----
----
26-MAY-2011
09-JUN-2011
SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100
26-MAY-2011
27-MAY-2011
22-NOV-2011
30-MAY-2011
22-NOV-2011
SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100
26-MAY-2011
27-MAY-2011
22-NOV-2011
27-MAY-2011
22-NOV-2011

Method
: : : :
3 of 10
ES1111046 URS AUSTRALIA 43177447 Evaluation: = Holding time breach ; = Within holding time.
Sample Date
Date extracted
Analysis Evaluation
Date analysed
Due for extraction
Due for analysis
Evaluation
EG035T: Total Recoverable Mercury by FIMS Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1, Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1, EK061G: Total Kjeldahl Nitrogen By Discrete Analyser Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1, EK067G: Total Phosphorus as P by Discrete Analyser Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1, EP004: Organic Matter Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1,
SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100
26-MAY-2011
27-MAY-2011
23-JUN-2011
27-MAY-2011
23-JUN-2011
EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser
SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100
26-MAY-2011
27-MAY-2011
22-NOV-2011
27-MAY-2011
22-NOV-2011
SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100
26-MAY-2011
30-MAY-2011
22-NOV-2011
30-MAY-2011
22-NOV-2011
SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100
26-MAY-2011
30-MAY-2011
22-NOV-2011
30-MAY-2011
22-NOV-2011
SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100
26-MAY-2011
27-MAY-2011
02-JUN-2011
27-MAY-2011
02-JUN-2011

Method
: : : :
4 of 10
Sample Date
Date extracted
Analysis Evaluation
Date analysed
Due for extraction
Due for analysis
Evaluation
EP068A: Organochlorine Pesticides (OC) Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1, EP068B: Organophosphorus Pesticides (OP) Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1, EP075(SIM)B: Polynuclear Aromatic Hydrocarbons Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1, EP080/071: Total Petroleum Hydrocarbons Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1, Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1,
SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100
26-MAY-2011
27-MAY-2011
09-JUN-2011
30-MAY-2011
06-JUL-2011
SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100
26-MAY-2011
27-MAY-2011
09-JUN-2011
30-MAY-2011
06-JUL-2011
SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100
26-MAY-2011
27-MAY-2011
09-JUN-2011
27-MAY-2011
06-JUL-2011
SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100 SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100
26-MAY-2011
26-MAY-2011
09-JUN-2011
29-MAY-2011
09-JUN-2011
26-MAY-2011
27-MAY-2011
09-JUN-2011
27-MAY-2011
06-JUL-2011

Method
: : : :
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Sample Date
Date extracted
Analysis Evaluation
Date analysed
Due for extraction
Due for analysis
Evaluation
EP080/071: Total Recoverable Hydrocarbons - NEPM 2010 Draft Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1, Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1, EP080: BTEX Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1, EP080: BTEXN Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB5_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1,
SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100 SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100
26-MAY-2011
26-MAY-2011
09-JUN-2011
29-MAY-2011
09-JUN-2011
26-MAY-2011
27-MAY-2011
09-JUN-2011
27-MAY-2011
06-JUL-2011
SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100
26-MAY-2011
26-MAY-2011
09-JUN-2011
29-MAY-2011
09-JUN-2011
SB2_0.0-0.1, SB4_0.0-0.1, SB6_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100
26-MAY-2011
26-MAY-2011
09-JUN-2011
29-MAY-2011
09-JUN-2011
: : : :
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Count Method
ED093S EA010 EA055-103 EK059G EP004 EP075(SIM) EP068 EA002 EK061G EG035T EG005T EK067G EP071 EP080 ED093S EA010 EK059G EP004 EP075(SIM) EP068 EK061G EG035T EG005T EK067G EP071 EP080 ED093S EA010 EK059G EP004 EP075(SIM) EP068 EK061G EG035T
Analytical Methods
Laboratory Duplicates (DUP) Cations - soluble by ICP-AES Electrical Conductivity (1:5) Moisture Content Nitrite and Nitrate as N (NOx)- Soluble by Discrete Analyser Organic Matter PAH/Phenols (SIM) Pesticides by GCMS pH (1:5) TKN as N By Discrete Analyser Total Mercury by FIMS Total Metals by ICP-AES Total Phosporus By Discrete Analyser TPH - Semivolatile Fraction TPH Volatiles/BTEX Laboratory Control Samples (LCS) Cations - soluble by ICP-AES Electrical Conductivity (1:5) Nitrite and Nitrate as N (NOx)- Soluble by Discrete Analyser Organic Matter PAH/Phenols (SIM) Pesticides by GCMS TKN as N By Discrete Analyser Total Mercury by FIMS Total Metals by ICP-AES Total Phosporus By Discrete Analyser TPH - Semivolatile Fraction TPH Volatiles/BTEX Method Blanks (MB) Cations - soluble by ICP-AES Electrical Conductivity (1:5) Nitrite and Nitrate as N (NOx)- Soluble by Discrete Analyser Organic Matter PAH/Phenols (SIM) Pesticides by GCMS TKN as N By Discrete Analyser Total Mercury by FIMS
QC
2 2 2 2 2 2 2 2 2 2 2 2 2 2 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
Regular
12 11 12 12 13 12 12 13 14 13 20 13 12 18 12 11 12 13 12 12 14 13 20 13 12 18 12 11 12 13 12 12 14 13
Actual
16.7 18.2 16.7 16.7 15.4 16.7 16.7 15.4 14.3 15.4 10.0 15.4 16.7 11.1 8.3 9.1 8.3 7.7 8.3 8.3 7.1 7.7 5.0 7.7 8.3 5.6 8.3 9.1 8.3 7.7 8.3 8.3 7.1 7.7
Rate (%) Expected

10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 9.5 10.0 10.0 10.0 10.0 10.0 5.0 5.0 5.0 5.0 5.0 5.0 4.8 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 4.8 5.0

Evaluation
NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999
Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement
NEPM 1999 Schedule B(3) and ALS QCS3 requirement NEPM 1999 Schedule B(3) and ALS QCS3 requirement NEPM 1999 Schedule B(3) and ALS QCS3 requirement NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement
NEPM 1999 Schedule B(3) and ALS QCS3 requirement NEPM 1999 Schedule B(3) and ALS QCS3 requirement NEPM 1999 Schedule B(3) and ALS QCS3 requirement NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999 Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement

: : : :
7 of 10
ES1111046 URS AUSTRALIA 43177447 Evaluation: = Quality Control frequency not within specification ; = Quality Control frequency within specification.
Count Method
EG005T EK067G EP071 EP080 EK059G EP075(SIM) EP068 EK061G EG035T EG005T EK067G EP071 EP080
Analytical Methods
Method Blanks (MB) - Continued Total Metals by ICP-AES Total Phosporus By Discrete Analyser TPH - Semivolatile Fraction TPH Volatiles/BTEX Matrix Spikes (MS) Nitrite and Nitrate as N (NOx)- Soluble by Discrete Analyser PAH/Phenols (SIM) Pesticides by GCMS TKN as N By Discrete Analyser Total Mercury by FIMS Total Metals by ICP-AES Total Phosporus By Discrete Analyser TPH - Semivolatile Fraction TPH Volatiles/BTEX
QC
1 1 1 1 1 1 1 1 1 1 1 1 1
Regular
20 13 12 18 12 12 12 14 13 20 13 12 18
Actual
5.0 7.7 8.3 5.6 8.3 8.3 8.3 7.1 7.7 5.0 7.7 8.3 5.6
Rate (%) Expected

5.0 5.0 5.0 5.0 5.0 5.0 5.0 4.8 5.0 5.0 5.0 5.0 5.0

Evaluation
NEPM 1999 NEPM 1999 NEPM 1999 NEPM 1999
Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement Schedule B(3) and ALS QCS3 requirement
ALS QCS3 requirement ALS QCS3 requirement ALS QCS3 requirement ALS QCS3 requirement ALS QCS3 requirement ALS QCS3 requirement ALS QCS3 requirement ALS QCS3 requirement ALS QCS3 requirement
: : : :
8 of 10

Analytical Methods
Method
EA002 EA010 EA014 EA055-103 ED093S
Matrix
Method Descriptions
pH (1:5) Electrical Conductivity (1:5) Total Soluble Salts Moisture Content Cations - soluble by ICP-AES
SOIL SOIL SOIL SOIL SOIL
Total Metals by ICP-AES
EG005T
SOIL
Total Mercury by FIMS
EG035T
SOIL
Nitrite and Nitrate as N (NOx)- Soluble by Discrete Analyser TKN as N By Discrete Analyser Total Nitrogen as N (TKN + NOx) By Discrete Analyser Total Phosporus By Discrete Analyser Organic Matter Pesticides by GCMS
EK059G EK061G EK062G EK067G EP004 EP068
SOIL SOIL SOIL SOIL SOIL SOIL
TPH - Semivolatile Fraction PAH/Phenols (SIM)
EP071 EP075(SIM)
SOIL SOIL
(APHA 21st ed., 4500H+) pH is determined on soil samples after a 1:5 soil/water leach. This method is compliant with NEPM (1999) Schedule B(3) (Method 103) (APHA 21st ed., 2510) Conductivity is determined on soil samples using a 1:5 soil/water leach. This method is compliant with NEPM (1999) Schedule B(3) (Method 104) In-house. The concentration of TSS in a soil is calculated from the Electrical conductivity of a water extract. This method is compliant with NEPM (1999) Schedule B(3) (Method 104) A gravimetric procedure based on weight loss over a 12 hour drying period at 103-105 degrees C. This method is compliant with NEPM (2010 Draft) Schedule B(3) Section 7.1 and Table 1 (14 day holding time). APHA 21st ed., 3120; USEPA SW 846 - 6010 (ICPAES) Water extracts of the soil are analyzed for major cations by ICPAES. The ICPAES technique ionises samples in a plasma, emitting a characteristic spectrum based on metals present. Intensities at selected wavelengths are compared against those of matrix matched standards. This method is compliant with NEPM (1999) Schedule B(3) (APHA 21st ed., 3120; USEPA SW 846 - 6010) (ICPAES) Metals are determined following an appropriate acid digestion of the soil. The ICPAES technique ionises samples in a plasma, emitting a characteristic spectrum based on metals present. Intensities at selected wavelengths are compared against those of matrix matched standards. This method is compliant with NEPM (1999) Schedule B(3) AS 3550, APHA 21st ed., 3112 Hg - B (Flow-injection (SnCl2)(Cold Vapour generation) AAS) FIM-AAS is an automated flameless atomic absorption technique. Mercury in solids are determined following an appropriate acid digestion. Ionic mercury is reduced online to atomic mercury vapour by SnCl2 which is then purged into a heated quartz cell. Quantification is by comparing absorbance against a calibration curve. This method is compliant with NEPM (1999) Schedule B(3) APHA 21st ed., 4500 NO3- F. Combined oxidised Nitrogen (NO2+NO3) in a water extract is determined by Cadmium Reduction, and direct colourimetry by Discrete Analyser. APHA 21st ed., 4500-Norg-D Soil samples are digested using Kjeldahl digestion followed by determination by Discrete Analyser. APHA 21st ed., 4500 Norg/NO3- Total Nitrogen is determined as the sum of TKN and Oxidised Nitrrogen, each determined seperately as N. APHA 21st ed., 4500 P-B&F This procedure involves sulfuric acid digestion and quantification using Discrete Analyser. AS1289.4.1.1 - 1997., Dichromate oxidation method after Walkley and Black. This method is compliant with NEPM (1999) Schedule B(3) (Method 105) (USEPA SW 846 - 8270B) Extracts are analysed by Capillary GC/MS and quantification is by comparison against an established 5 point calibration curve. This technique is compliant with NEPM (1999) Schedule B(3) (Method 504,505) (USEPA SW 846 - 8015A) Sample extracts are analysed by Capillary GC/FID and quantified against alkane standards over the range C10 - C36. This method is compliant with NEPM (1999) Schedule B(3) (Method 506.1) (USEPA SW 846 - 8270B) Extracts are analysed by Capillary GC/MS in Selective Ion Mode (SIM) and quantification is by comparison against an established 5 point calibration curve. This method is compliant with NEPM (1999) Schedule B(3) (Method 502 and 507)
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9 of 10
Analytical Methods
Method
EP080
Matrix
Method Descriptions
TPH Volatiles/BTEX
SOIL
(USEPA SW 846 - 8260B) Extracts are analysed by Purge and Trap, Capillary GC/MS. Quantification is by comparison against an established 5 point calibration curve. This method is compliant with NEPM (1999) Schedule B(3) (Method 501)
Method Descriptions
Preparation Methods
Method
EK061/EK067 EN34 EN69
Matrix
TKN/TP Digestion 1:5 solid / water leach for soluble analytes Hot Block Digest for metals in soils sediments and sludges
SOIL SOIL SOIL
Organic Matter Methanolic Extraction of Soils for Purge and Trap Tumbler Extraction of Solids (Option A Concentrating) Tumbler Extraction of Solids (Option B Non-concentrating)
EP004-PR
SOIL SOIL SOIL
* ORG16
ORG17A
ORG17B
SOIL
APHA 21st ed., 4500 Norg- D; APHA 21st ed., 4500 P - H. Macro Kjeldahl digestion. 10 g of soil is mixed with 50 mL of distilled water and tumbled end over end for 1 hour. Water soluble salts are leached from the soil by the continuous suspension. Samples are settled and the water filtered off for analysis. USEPA 200.2 Mod. Hot Block Acid Digestion 1.0g of sample is heated with Nitric and Hydrochloric acids, then cooled. Peroxide is added and samples heated and cooled again before being filtered and bulked to volume for analysis. Digest is appropriate for determination of selected metals in sludge, sediments, and soils. This method is compliant with NEPM (1999) Schedule B(3) (Method 202) AS1289.4.1.1 - 1997., Dichromate oxidation method after Walkley and Black. This method is compliant with NEPM (1999) Schedule B(3) (Method 105) (USEPA SW 846 - 5030A) 5g of solid is shaken with surrogate and 10mL methanol prior to analysis by Purge and Trap - GC/MS. In-house, Mechanical agitation (tumbler). 20g of sample, Na2SO4 and surrogate are extracted with 150mL 1:1 DCM/Acetone by end over end tumble. The solvent is decanted, dehydrated and concentrated (by KD) to the desired volume for analysis. In-house, Mechanical agitation (tumbler). 10g of sample, Na2SO4 and surrogate are extracted with 20mL 1:1 DCM/Acetone by end over end tumble. The solvent is transferred directly to a GC vial for analysis.
: : : :
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Summary of Outliers

l l l l

l


0.00
SAMPLE RECEIPT NOTIFICATION (SRN)

Comprehensive Report
Work Order :
ES1111046
Laboratory : Environmental Division Sydney : Client Services : 277-289 Woodpark Road Smithfield
Client
Contact
Address
Contact
Address

E-mail Telephone Facsimile Project Order number C-O-C number Site Sampler : adam_sullivan@urscorp.com : +61 2 8925 5500 : +61 2 8925 5555 : 43177447 : ---: ---: ---: AM QC Level Quote number E-mail Telephone Facsimile Page
NSW Australia 2164

: sydney@alsglobal.com : +61-2-8784 8555 : +61-2-8784 8500 : 1 of 2 : ES2011URSMAW0004 (EN/038/10) : NEPM
1999 Schedule QCS3 requirement
B(3)
and
ALS
Dates
Date Samples Received Client Requested Due Date : 26-MAY-2011 : 31-MAY-2011 Issue Date Scheduled Reporting Date : 26-MAY-2011 23:52 :
31-MAY-2011
Delivery Details
Mode of Delivery No. of coolers/boxes Security Seal : Carrier : 1 HARD : Not intact. Temperature No. of samples received No. of samples analysed : 2.1'C - Ice present : 12 : 12
General Comments
l
This report contains the following information:

Sample Container(s)/Preservation Non-Compliances Summary of Sample(s) and Requested Analysis Requested Deliverables
l l
Samples received in appropriately pretreated and preserved containers. Sample(s) have been received within recommended holding times. l Sample(s) requiring volatile organic compound analysis received in airtight containers (ZHE). l MBAS analysis split into ES1111055
l l l
Please direct any queries you have regarding this work order to the above ALS laboratory contact. Analytical work for this work order will be conducted at ALS Sydney. Sample Disposal - Aqueous (14 days), Solid (90 days) from date of completion of work order.

Issue Date Page Work Order Client
: : : :
26-MAY-2011 23:52 ES1111046
2 of 2
URS AUSTRALIA
Sample Container(s)/Preservation Non-Compliances

All comparisons are made against pretreatment/preservation AS, APHA, USEPA standards.
l No sample container / preservation non-compliance exist.
Summary of Sample(s) and Requested Analysis

Some items described below may be part of a laboratory process neccessary for the execution of client requested tasks. Packages may contain additional analyses, such as the determination of moisture content and preparation tasks, that are included in the package. When sampling time information is not provided by the client, sampling dates are shown without a time component. In these instances, the time component has been assumed by the laboratory for processing purposes.
Matrix: SOIL SOIL - EA002 pH (1:5)
SOIL - NT-1S Major Cations (Ca, Mg, Na, K)
SOIL - EP004 (Carbon) Total Organic Carbon (Calc.)
ES1111046-001 ES1111046-002 ES1111046-003 ES1111046-004 ES1111046-005 ES1111046-006 ES1111046-007 ES1111046-008 ES1111046-009 ES1111046-010 ES1111046-011 ES1111046-012
Client sampling date / time

26-MAY-2011 14:50 26-MAY-2011 14:55 26-MAY-2011 15:10 26-MAY-2011 15:05 26-MAY-2011 15:20 26-MAY-2011 15:25 26-MAY-2011 15:30 26-MAY-2011 15:35 26-MAY-2011 15:40 26-MAY-2011 15:45 26-MAY-2011 15:55 [ 26-MAY-2011 ]
Client sample ID
SB1_0.0-0.1 SB2_0.0-0.1 SB3_0.0-0.1 SB4_0.0-0.1 SB5_0.0-0.1 SB6_0.0-0.1 SB7_0.0-0.1 SB8_0.0-0.1 SB9_0.0-0.1 SB10_0.0-0.1 SB11_0.0-0.1 QC100
Requested Deliverables
ACCOUNTS PAYABLE ALL INVOICES - A4 - AU Tax Invoice ( INV ) EQUIS URS_EDMS - EDI Format - EQUIS V5 URS ( EQUV5_URS ) MR ADAM SULLIVAN - *AU Certificate of Analysis - NATA ( COA ) - *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) ( QCI ) - *AU QC Report - DEFAULT (Anon QC Rep) - NATA ( QC ) - A4 - AU Sample Receipt Notification - Environmental ( SRN ) - A4 - AU Tax Invoice ( INV ) - Chain of Custody (CoC) ( COC ) - Chromatogram ( CHROM ) - EDI Format - ENMRG ( ENMRG ) - EDI Format - EQUIS V5 URS ( EQUV5_URS ) - EDI Format - MRED ( MRED )
Email Email Email Email Email Email Email Email Email Email Email Email
sydney_accounts@urscorp.com urs_edms@urscorp.com adam_sullivan@urscorp.com adam_sullivan@urscorp.com adam_sullivan@urscorp.com adam_sullivan@urscorp.com adam_sullivan@urscorp.com adam_sullivan@urscorp.com adam_sullivan@urscorp.com adam_sullivan@urscorp.com adam_sullivan@urscorp.com adam_sullivan@urscorp.com
SOIL - S-26 8 metals/TPH/BTEX/PAH
SOIL - EA014 Total Soluble Salts
SOIL - S-12 OC/OP Pesticides
SOIL - NT-11S Total N + Total P
ES1111055 False
Work Order :
ES1111055
Page Laboratory
: 1 of 4 : Environmental Division Sydney : Client Services : 277-289 Woodpark Road Smithfield NSW Australia 2164 : sydney@alsglobal.com : +61-2-8784 8555 : +61-2-8784 8500 : NEPM 1999 Schedule B(3) and ALS QCS3 requirement : 26-MAY-2011 : 03-JUN-2011 : 10 : 10
Client
: URS AUSTRALIA : MR ADAM SULLIVAN : LEVEL 3, 116 MILLER STREET : : : : : : : :
Contact
Contact
NORTH SYDNEY NSW, AUSTRALIA 2060 adam_sullivan@urscorp.com +61 2 8925 5500 +61 2 8925 5555 43177447 ------AM ----
: EN/038/10
This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. All pages of this report have been checked and approved for release. This Certificate of Analysis contains the following information: l General Comments l Analytical Results
Signatories
Kim McCabe
Senior Inorganic Chemist
Brisbane Inorganics

: : : :
2 of 4
General Comments
EP050 (anionic surfactants as MBAS): Samples SB1_0.0-0.1, SB2_0.0-0.1, SB3_0.0-0.1, SB4_0.0-0.1, SB7_0.0-0.1, SB8_0.0-0.1, SB9_0.0-0.1, SB10_0.0-0.1, SB11_0.0-0.1, QC100 were diluted due to matrix interference. LOR adjusted accordingly.
: : : :
3 of 4
Analytical Results
Sub-Matrix: SOIL
SB1_0.0-0.1
26-MAY-2011 14:50
ES1111055-001
SB2_0.0-0.1
26-MAY-2011 14:55
ES1111055-002
SB3_0.0-0.1
26-MAY-2011 15:10
ES1111055-003
SB4_0.0-0.1
26-MAY-2011 15:05
ES1111055-004
SB7_0.0-0.1
26-MAY-2011 15:30
ES1111055-005
Compound
CAS Number
----
LOR
1
Unit
mg/kg

<100
<100
<100
<100
<100
: : : :
4 of 4
Analytical Results
Sub-Matrix: SOIL
SB8_0.0-0.1
26-MAY-2011 15:35
ES1111055-006
SB9_0.0-0.1
26-MAY-2011 15:40
ES1111055-007
SB10_0.0-0.1
26-MAY-2011 15:45
ES1111055-008
SB11_0.0-0.1
26-MAY-2011 15:55
ES1111055-009
QC100
26-MAY-2011 15:00
ES1111055-010
Compound
CAS Number
----
LOR
1
Unit
mg/kg

<100
<100
<100
<50
<50
False

Work Order :
ES1111055
Page Laboratory
Client
Contact
Address
Contact
Address

E-mail Telephone Facsimile Project Site C-O-C number Sampler Order number Quote number : adam_sullivan@urscorp.com : +61 2 8925 5500 : +61 2 8925 5555 : 43177447 : ---: ---: AM : ---No. of samples received : EN/038/10 No. of samples analysed : 10 : 10 Date Samples Received Issue Date : 26-MAY-2011 : 03-JUN-2011 E-mail Telephone Facsimile QC Level : sydney@alsglobal.com : +61-2-8784 8555 : +61-2-8784 8500 : NEPM 1999 Schedule B(3) and ALS QCS3 requirement
Signatories
Kim McCabe
Senior Inorganic Chemist
Brisbane Inorganics
: : : :
2 of 5
General Comments
: : : :
3 of 5

EP050: Anionic Surfactants as MBAS (QC Lot: 1812969)

ES1111055-004 ES1111055-010 SB4_0.0-0.1 QC100 EP050: Anionic Surfactants as MBAS EP050: Anionic Surfactants as MBAS 1 1 mg/kg mg/kg <100 <50 <100 <50 0.0 0.0 No Limit No Limit
: : : :
4 of 5

EP050: Anionic Surfactants as MBAS (QCLot: 1812969)

EP050: Anionic Surfactants as MBAS 1 mg/kg <1 -------------
: : : :
5 of 5

The quality control term Matrix Spike (MS) refers to an intralaboratory split sample spiked with a representative set of target analytes. The purpose of this QC parameter is to monitor potential matrix effects on analyte recoveries. Static Recovery Limits as per laboratory Data Quality Objectives (DQOs). Ideal recovery ranges stated may be waived in the event of sample matrix interference.
l No Matrix Spike (MS) Results are required to be reported.
True

Page Laboratory
: 1 of 5 : Environmental Division Sydney : Client Services : 277-289 Woodpark Road Smithfield NSW Australia 2164 : sydney@alsglobal.com : +61-2-8784 8555 : +61-2-8784 8500 : NEPM 1999 Schedule B(3) and ALS QCS3 requirement : 26-MAY-2011 : 03-JUN-2011 : 10 : 10
Client
Contact
Address
Contact
Address

E-mail Telephone Facsimile Project Site C-O-C number Sampler Order number Quote number : adam_sullivan@urscorp.com : +61 2 8925 5500 : +61 2 8925 5555 : 43177447 : ---: ---: AM : ---: EN/038/10 E-mail Telephone Facsimile QC Level Date Samples Received Issue Date No. of samples received No. of samples analysed

: : : :
2 of 5


Date extracted
Analysis Evaluation
Date analysed
Due for extraction
Due for analysis
Evaluation
EP050: Anionic Surfactants as MBAS Soil Glass Jar - Unpreserved SB1_0.0-0.1, SB3_0.0-0.1, SB7_0.0-0.1, SB9_0.0-0.1, SB11_0.0-0.1,
SB2_0.0-0.1, SB4_0.0-0.1, SB8_0.0-0.1, SB10_0.0-0.1, QC100
26-MAY-2011
01-JUN-2011
22-NOV-2011
03-JUN-2011
03-JUN-2011
: : : :
3 of 5

Count Method
EP050 EP050
Analytical Methods
Laboratory Duplicates (DUP) Anionic Surfactants as MBAS Method Blanks (MB) Anionic Surfactants as MBAS
QC
2 1
Regular
10 10
Actual
20.0 10.0
Rate (%) Expected

10.0 5.0

Evaluation
NEPM 1999 Schedule B(3) and ALS QCS3 requirement NEPM 1999 Schedule B(3) and ALS QCS3 requirement
: : : :
4 of 5

Analytical Methods
Method
EP050
Matrix
Method Descriptions
SOIL
APHA 21st ed., 5540 B & C. MBAS results determined following 1:5 solid / water leach. This method comprises three successive extractions from acid aqueous medium containing excess methylene blue, into chloroform, followed by an aqueous backwash and measurement of the colour by spectrophotometry at 625nm. ALS is not NATA accredited for this analysis.
Method Descriptions
Preparation Methods
Method
EN34
Matrix
1:5 solid / water leach for soluble analytes
SOIL
10 g of soil is mixed with 50 mL of distilled water and tumbled end over end for 1 hour. Water soluble salts are leached from the soil by the continuous suspension. Samples are settled and the water filtered off for analysis.
: : : :
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Summary of Outliers

l l l l

l


0.00
SAMPLE RECEIPT NOTIFICATION (SRN)

Comprehensive Report
Work Order :
ES1111055
Laboratory : Environmental Division Sydney : Client Services : 277-289 Woodpark Road Smithfield
Client
Contact
Address
Contact
Address

E-mail Telephone Facsimile Project Order number C-O-C number Site Sampler : adam_sullivan@urscorp.com : +61 2 8925 5500 : +61 2 8925 5555 : 43177447 : ---: ---: ---: AM QC Level Quote number E-mail Telephone Facsimile Page
NSW Australia 2164

: sydney@alsglobal.com : +61-2-8784 8555 : +61-2-8784 8500 : 1 of 2 : ES2011URSMAW0004 (EN/038/10) : NEPM
1999 Schedule QCS3 requirement
B(3)
and
ALS
Dates
Date Samples Received Client Requested Due Date : 26-MAY-2011 : 02-JUN-2011 Issue Date Scheduled Reporting Date : 31-MAY-2011 22:04 :
02-JUN-2011
Delivery Details
Mode of Delivery No. of coolers/boxes Security Seal : Carrier : 1 HARD : Not intact. Temperature No. of samples received No. of samples analysed : 2.1'C - Ice present : 10 : 10
General Comments
l
This report contains the following information:

Sample Container(s)/Preservation Non-Compliances Summary of Sample(s) and Requested Analysis Requested Deliverables
l l
Samples received in appropriately pretreated and preserved containers. Sample(s) have been received within recommended holding times. l MBAS analysis split from ES1111046
l l l
Please direct any queries you have regarding this work order to the above ALS laboratory contact. Analytical work for this work order will be conducted at ALS Sydney. Sample Disposal - Aqueous (14 days), Solid (90 days) from date of completion of work order.

Issue Date Page Work Order Client
: : : :
31-MAY-2011 22:04 ES1111055
2 of 2
URS AUSTRALIA
Sample Container(s)/Preservation Non-Compliances

All comparisons are made against pretreatment/preservation AS, APHA, USEPA standards.
l No sample container / preservation non-compliance exist.
Summary of Sample(s) and Requested Analysis

Some items described below may be part of a laboratory process neccessary for the execution of client requested tasks. Packages may contain additional analyses, such as the determination of moisture content and preparation tasks, that are included in the package. When sampling time information is not provided by the client, sampling dates are shown without a time component. In these instances, the time component has been assumed by the laboratory for processing purposes.
Matrix: SOIL
ES1111055-001 ES1111055-002 ES1111055-003 ES1111055-004 ES1111055-005 ES1111055-006 ES1111055-007 ES1111055-008 ES1111055-009 ES1111055-010
Client sampling date / time

26-MAY-2011 14:50 26-MAY-2011 14:55 26-MAY-2011 15:10 26-MAY-2011 15:05 26-MAY-2011 15:30 26-MAY-2011 15:35 26-MAY-2011 15:40 26-MAY-2011 15:45 26-MAY-2011 15:55 26-MAY-2011 15:00
Client sample ID
SB1_0.0-0.1 SB2_0.0-0.1 SB3_0.0-0.1 SB4_0.0-0.1 SB7_0.0-0.1 SB8_0.0-0.1 SB9_0.0-0.1 SB10_0.0-0.1 SB11_0.0-0.1 QC100
Requested Deliverables
ACCOUNTS PAYABLE ALL INVOICES - A4 - AU Tax Invoice ( INV ) EQUIS URS_EDMS - EDI Format - EQUIS V5 URS ( EQUV5_URS ) MR ADAM SULLIVAN - *AU Certificate of Analysis - NATA ( COA ) - *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) ( QCI ) - *AU QC Report - DEFAULT (Anon QC Rep) - NATA ( QC ) - A4 - AU Sample Receipt Notification - Environmental ( SRN ) - A4 - AU Tax Invoice ( INV ) - Chain of Custody (CoC) ( COC ) - EDI Format - ENMRG ( ENMRG ) - EDI Format - EQUIS V5 URS ( EQUV5_URS ) - EDI Format - MRED ( MRED )
SOIL - EP050 Anionic Surfactants as MBAS
Email Email Email Email Email Email Email Email Email Email Email
sydney_accounts@urscorp.com urs_edms@urscorp.com adam_sullivan@urscorp.com adam_sullivan@urscorp.com adam_sullivan@urscorp.com adam_sullivan@urscorp.com adam_sullivan@urscorp.com adam_sullivan@urscorp.com adam_sullivan@urscorp.com adam_sullivan@urscorp.com adam_sullivan@urscorp.com
Appendix C Data Validation
43177447/Rpt/01
Project Name: Primary Laboratory: Secondary Laboratory: Date Sampled:
AGL Soil Assessment ALS None 23/05/2011
DATA VALIDATION SUMMARY Note: Data validation assesses each analyte in terms of all the data validation variables and only the exceedances and outliers are reported in this form. 43177447 Project/Task Number: Batch/Ref. Number(s): Sample Type: Yes/No Yes Yes No Yes Yes Yes No Yes Method EP050 Anionic Surfactants as MBAS. ES1110639 Water Comments
Sample Handling, Receipt and Holding Times COC completed adequately All requested analysis conducted Samples received intact and chilled Samples analysed within appropriate holding times per analytical methods. Samples volumes sufficient for QC analysis? Are there any non-NATA accredited methods used? Have chromatograms for positive TPH been supplied? Laboratory reports signed by an authorised person
No SRN provided with lab certificates
# of Primary Samples # of QAQC # of FD # of FT 3 0 0 0 Samples taken in the field were sent to ALS by AGL staff. URS is not aware of or evaluating QAQC procedures undertaken in the field. Method Blank (MB), Rinsate Blank (RB), Trip Blank (TB), Field Blank (FB) Type Comments All MB were less than LOR. MB Laboratory Control Samples (LCS) Analyte Comments All LCS recoveries were within acceptable control limits Water Matrix Spike (MS) Analyte Comments Water Trip Spike /Control Trip Spike Analyte NA MS were reported on sample SL09.001for Total Phosphorous, HACs, TPH C6-C9 and BTEX. TPH C10-C36 was reported on an anonymous sample. All results were within acceptable control limits. No other analytes were reported. % Recovery Comments
URS Australia Pty Ltd
J:\JOBS\43177447\MtTaurus_SoilAssess\Gilead\Lab Data\AGL soil results\Data Validation AGL analytical results ES1110639_SH.xls
Project Name: Primary Laboratory: Secondary Laboratory: Date Sampled: Duplicates Laboratory Duplicates Analyte Water
AGL Soil Assessment ALS None 23/05/2011
DATA VALIDATION SUMMARY Note: Data validation assesses each analyte in terms of all the data validation variables and only the exceedances and outliers are reported in this form. 43177447 Project/Task Number: Batch/Ref. Number(s): Sample Type: ES1110639 Water
Comments LD's were reported on anonymous samples for all specified methods with the exception TPHC10-C36. All LD's were within acceptable laboratory RPD control limits Comments
Intra-Laboratory Duplicates Analyte N/A Inter-Laboratory Duplicates Analyte N/A Surrogate Monitoring Compound Analyses Analyte Water
Comments
Comments All surrogate recoveries were within acceptable control limits Overall Comments *As stated by ALS: EP050 (anionic surfactants as MBAS): Samples SL09.001, SL09.002 and SL09.003 were diluted due to matrix interference. LOR adjusted accordingly. This should be noted for reporting purposes to ensure LOR is not above adopted guideline concentrations.
This batch is considered to be acceptable for environmental interpretative use. Note: When concentrations are less than LOR for both the primary and secondary results, no RPDs are calculated. Performed By: Date: Andrew Pettingell-Ward 17-Jun-11 Checked By: Date: S.Higgs 17-Jun-11
URS Australia Pty Ltd
J:\JOBS\43177447\MtTaurus_SoilAssess\Gilead\Lab Data\AGL soil results\Data Validation AGL analytical results ES1110639_SH.xls
DATA VALIDATION SUMMARY Note: Data validation assesses each analyte in terms of all the data validation variables and only the exceedances and outliers are reported in this form. AGL Soil Assessment Project/Task Number: 43177447 ALS None 26/05/2011 Batch/Ref. Number(s): Sample Type: Yes/No Yes Yes Yes Yes Yes No No Yes # of FT ES1111046 split with batch ES1111055 Soil Comments
Sample Handling, Receipt and Holding Times COC completed adequately All requested analysis conducted Samples received intact and chilled Samples analysed within appropriate holding times per analytical methods. Samples volumes sufficient for QC analysis? Are there any non-NATA accredited methods used? Have chromatograms for positive TPH been supplied? Laboratory reports signed by an authorised person
Samples received at 2.1C, ice present, security seal not intact
# of Primary Samples # of QAQC # of FD 11 0 1 Method Blank (MB), Rinsate Blank (RB), Trip Blank (TB), Field Blank (FB) Comments Type MB Laboratory Control Samples (LCS) Analyte Soil Matrix Spike (MS) Analyte Soil Trip Spike /Control Trip Spike Analyte NA All MB were less than LOR.
Comments All LCS recoveries were within acceptable control limits
Comments MS were reported on URS and anonymous samples for all methods with the exception of Total Metals and Mercury, Total Phosphorous as P, Nitrogen as N, all were within acceptable control limits.
% Recovery
Comments
URS Australia Pty Ltd J:\JOBS\43177447\MtTaurus_SoilAssess\Gilead\Lab Data\soil URS\Data Validation URS analytical results general ES1111046_SH.xls
Project Name: Primary Laboratory: Secondary Laboratory: Date Sampled: Duplicates Laboratory Duplicates Analyte
DATA VALIDATION SUMMARY Note: Data validation assesses each analyte in terms of all the data validation variables and only the exceedances and outliers are reported in this form. AGL Soil Assessment Project/Task Number: 43177447 ALS None 26/05/2011 Batch/Ref. Number(s): Sample Type: ES1111046 split with batch ES1111055 Soil
Comments LD's were reported on URS and anonymous samples for all specified methods. All LD's returned results within acceptable control limits, however total phosporus as P original and duplicate results were reported as "not authorised" and an RPD of 3.9% for an anonymous sample.
Soil
Intra-Laboratory Duplicates Analyte SB2_0.0-0.1/QC100
Comments RPD for all analytes are within acceptable limits with the following exceptions: Total Nitrogen as N (197.6%), potassium (100%), sodium (98%), total phosphorus as P (48.2%)
Inter-Laboratory Duplicates Analyte NA Surrogate Monitoring Compound Analyses Analyte Soil
Comments
Comments All surrogate recovereis were within acceptable control limits.
Overall Comments RPD results for total nitrogen as N (197.6%), potassium (100%), sodium (98%), total phosphorus as P (48.2%) have most likely occurred as a result of sample/matrix heterogeneity. This should be noted when interpreting the data. This batch is considered to be acceptable for environmental interpretative use. Note: When concentrations are less than LOR for both the primary and secondary results, no RPDs are calculated. Performed By: Date: Andrew Pettingell-Ward 17-Jun-11 Checked By Date: Shannon Higgs 17-Jun-11
URS Australia Pty Ltd J:\JOBS\43177447\MtTaurus_SoilAssess\Gilead\Lab Data\soil URS\Data Validation URS analytical results general ES1111046_SH.xls
Matrix:
SO
Location: Sample ID: Date Sampled: Sample Type: LOR2 1 10 0.05 0.05 0.05 10 0.2 0.1 10 10 20 20 2 5 0.05 0.2 10 0.05 0.5 0.05 0.05 0.5 50 0.5 0.05 0.5 0.2 100 0.05 0.5 0.05 100 0.05 0.05 0.5 50 0.5 0.05 0.05 0.05 0.5 0.2 0.05 0.05 0.5 0.05 0.5 0.05 0.05 0.05 0.5 0.5 0.05 0.5 0.2 0.5 0.05 0.05 0.5 0.05 0.05 0.5 0.05 0.05 0.5 0.5 0.05 0.05 0.2 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
SB2_0.0-0.1 SB2_0.0-0.1 26/05/2011 Primary < 0.5 30 < 0.03 < 0.03 < 0.03 30 < 0.1 7.0 180 410 1680 1690 274 663 < 0.03 < 0.1 <5 < 0.03 < 0.3 < 0.03 < 0.03 < 0.3 < 20 < 0.3 < 0.03 < 0.3 < 0.1 < 50 < 0.03 < 0.3 < 0.03 < 50 < 0.03 < 0.03 < 0.3 < 20 < 0.3 < 0.03 < 0.03 < 0.03 < 0.3 < 0.1 < 0.03 < 0.03 < 0.3 < 0.03 < 0.3 < 0.03 < 0.03 < 0.03 < 0.3 < 0.3 < 0.03 < 0.3 < 0.1 < 0.3 < 0.03 < 0.03 < 0.3 < 0.03 < 0.03 < 0.3 < 0.03 < 0.03 < 0.3 < 0.3 < 0.03 < 0.03 < 0.1
SB2_0.0-0.1 QC100 26/05/2011 Secondary < 0.5 <5 < 0.03 < 0.03 < 0.03 10 < 0.1 < 0.05 60 140 2080 2080 448 494 < 0.03 < 0.1 <5 < 0.03 < 0.3 < 0.03 < 0.03 < 0.3 < 20 < 0.3 < 0.03 < 0.3 < 0.1 < 50 < 0.03 < 0.3 < 0.03 < 50 < 0.03 < 0.03 < 0.3 < 20 < 0.3 < 0.03 < 0.03 < 0.03 < 0.3 < 0.1 < 0.03 < 0.03 < 0.3 < 0.03 < 0.3 < 0.03 < 0.03 < 0.03 < 0.3 < 0.3 < 0.03 < 0.3 < 0.1 < 0.3 < 0.03 < 0.03 < 0.3 < 0.03 < 0.03 < 0.3 < 0.03 < 0.03 < 0.3 < 0.3 < 0.03 < 0.03 < 0.1 Primary vs. Duplicate 0.00% 142.86% 0.00% 0.00% 0.00% 100.00% 0.00% 197.16% 100.00% 98.18% 21.28% 20.69% 48.20% 29.21% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 0.00% Category1 Pass Pass-1 Pass Pass Pass Pass-1 Pass Fail Fail Fail Pass Pass Fail Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass
Analyte Anionic Surfactants as MBAS Calcium cis-Chlordane Endrin aldehyde Endrin ketone Magnesium Methoxychlor Nitrite + Nitrate as N Potassium Sodium Total Kjeldahl Nitrogen as N Total Nitrogen as N Total Phosphorus as P Total Soluble Salts trans-Chlordane Benzene C6 - C10 Fraction Dichlorvos Acenaphthylene alpha-BHC Demeton-S-methyl Toluene >C10 - C16 Fraction Acenaphthene beta-BHC Ethylbenzene Monocrotophos >C16 - C34 Fraction Dimethoate Fluorene gamma-BHC >C34 - C40 Fraction delta-BHC Diazinon Phenanthrene >C10 - C40 Fraction (sum) Anthracene Chlorpyrifos-methyl Heptachlor Aldrin Fluoranthene Parathion-methyl Heptachlor epoxide Malathion Pyrene alpha-Endosulfan Benz(a)anthracene Fenthion 4.4-DDE Chlorpyrifos Chrysene Benzo(b)fluoranthene Dieldrin ortho-Xylene Parathion Benzo(k)fluoranthene Endrin Pirimphos-ethyl Benzo(a)pyrene beta-Endosulfan Chlorfenvinphos Total Xylenes 4.4-DDD Bromophos-ethyl Indeno(1.2.3.cd)pyrene Dibenz(a.h)anthracene Endosulfan sulfate Fenamiphos 4.4-DDT
LOR1 1 10 0.05 0.05 0.05 10 0.2 0.1 10 10 20 20 2 5 0.05 0.2 10 0.05 0.5 0.05 0.05 0.5 50 0.5 0.05 0.5 0.2 100 0.05 0.5 0.05 100 0.05 0.05 0.5 50 0.5 0.05 0.05 0.05 0.5 0.2 0.05 0.05 0.5 0.05 0.5 0.05 0.05 0.05 0.5 0.5 0.05 0.5 0.2 0.5 0.05 0.05 0.5 0.05 0.05 0.5 0.05 0.05 0.5 0.5 0.05 0.05 0.2
J:\JOBS\43177447\MtTaurus_SoilAssess\Gilead\Lab Data\soil URS\Data Validation URS analytical results general ES1111046_SH.xls Prepared By:AP URS Australia Pty Ltd 3 of 4 Checked By:SH
Matrix:
SO
Location: Sample ID: Date Sampled: Sample Type: LOR2 0.5 0.05 2 0.05 5 0.05 0.05 1 5 5 2 5 0.05 0.5 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
SB2_0.0-0.1 SB2_0.0-0.1 26/05/2011 Primary < 0.3 < 0.03 16 < 0.03 8 < 0.03 < 0.03 < 0.5 26 22 15 49 < 0.03 < 0.3
SB2_0.0-0.1 QC100 26/05/2011 Secondary < 0.3 < 0.03 15 < 0.03 7 < 0.03 < 0.03 < 0.5 27 20 16 60 < 0.03 < 0.3 Primary vs. Duplicate 0.00% 0.00% 6.45% 0.00% 13.33% 0.00% 0.00% 0.00% 3.77% 9.52% 6.45% 20.18% 0.00% 0.00% Category1 Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass
Analyte Benzo(g.h.i)perylene Prothiofos Chromium, T Ethion Arsenic, T Carbophenothion Azinphos Methyl Cadmium, T Copper, T Lead , T Nickel, T Zinc, T Hexachlorobenzene (HCB) Naphthalene
LOR1 0.5 0.05 2 0.05 5 0.05 0.05 1 5 5 2 5 0.05 0.5
RPD Control Limits Pass - RPD <= 30% Pass-1 - RPD > 30%, Analysis results < 10 times Detection Limit Pass-2 - RPD > 30% and RPD <= 50%, Analysis result > 10 times Detection Limit and < 20 times Detection Limit Exceeds RPD Control Limits
J:\JOBS\43177447\MtTaurus_SoilAssess\Gilead\Lab Data\soil URS\Data Validation URS analytical results general ES1111046_SH.xls Prepared By:AP URS Australia Pty Ltd 4 of 4 Checked By:SH
DATA VALIDATION SUMMARY Note: Data validation assesses each analyte in terms of all the data validation variables and only the exceedances and outliers are reported in this form. AGL Soil Assessment Project/Task Number: 43177447 ALS None 26/05/2011 Batch/Ref. Number(s): Sample Type: Yes/No Yes Yes Yes Yes Yes Yes No Yes # of FD 1 ES1111055 split batch with ES1111046 Soil Comments
Sample Handling, Receipt and Holding Times COC completed adequately All requested analysis conducted Samples received intact and chilled Samples analysed within appropriate holding times per analytical methods. Samples volumes sufficient for QC analysis? Are there any non-NATA accredited methods used? Have chromatograms for positive TPH been supplied? Laboratory reports signed by an authorised person # of Primary Samples 9 # of QAQC 0
Samples received at 2.1C, ice present, security seal not intact
EP050 Anionic Surfactants as MBAS.
# of FT 0
Method Blank (MB), Rinsate Blank (RB), Trip Blank (TB), Field Blank (FB) Comments Type All MB were less than LOR. MB Laboratory Control Samples (LCS) Analyte
Comments No LCS were analysed.
Matrix Spike (MS) Analyte Trip Spike /Control Trip Spike Analyte NA
Comments No matrix spike results are required to be reported % Recovery Comments
J:\JOBS\43177447\MtTaurus_SoilAssess\Gilead\Lab Data\soil anionic surfactants URS\Data Validation URS analytical results anionic surfactants URS Australia Pty Ltd ES1111055_SH.xls
Project Name: Primary Laboratory: Secondary Laboratory: Date Sampled: Duplicates Laboratory Duplicates Analyte Anionic Surfactants Intra-Laboratory Duplicates Analyte SB2_0.-0.1/QC100 Inter-Laboratory Duplicates Analyte NA
DATA VALIDATION SUMMARY Note: Data validation assesses each analyte in terms of all the data validation variables and only the exceedances and outliers are reported in this form. AGL Soil Assessment Project/Task Number: 43177447 ALS None 26/05/2011 Batch/Ref. Number(s): Sample Type: ES1111055 split batch with ES1111046 Soil
Comments LDs were within acceptable control limits. Comments All results were less than LOR, no RPDs were calculated. Comments
Surrogate Monitoring Compound Analyses Analyte
Comments No surrogates were analysed.
Overall Comments *As stated by ALS: EP050 (anionic surfactants as MBAS): Samples SB1_0.0-0.1, SB2_0.0-0.1, SB3_0.0-0.1, SB4_0.0-0.1, SB7_0.00.1, SB8_0.0-0.1, SB9_0.0-0.1, SB10_0.0-0.1, SB11_0.0-0.1, QC100 were diluted due to matrix interference. LOR adjusted accordingly. This batch is considered to be acceptable for environmental interpretative use. Note: When concentrations are less than LOR for both the primary and secondary results, no RPDs are calculated. Performed By: Date: Andrew Pettingell-Ward 16-Jun-11 Checked By: Date: S.Higgs 17-Jun-11
J:\JOBS\43177447\MtTaurus_SoilAssess\Gilead\Lab Data\soil anionic surfactants URS\Data Validation URS analytical results anionic surfactants URS Australia Pty Ltd ES1111055_SH.xls
URS Australia Pty Ltd Level 4, 407 Pacific Highway Artarmon NSW 2064 Australia T: 61 2 8925 5500 F: 61 2 8925 5555
www.ap.urscorp.com

AGL Sugar Loaf 03 Soil Invest RPT Final

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AGL Sugar Loaf 03 Soil Invest RPT Final

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Soil Investigation Report

AGL Upstream Investments Pty Ltd

Sugarloaf Well Site - Soil Investigation

j:\jobs\43177447\mttaurus_soilassess\gilead\final\agl sugarloaf03_soil invest_rpt_final.doc

Sugarloaf Well Site - Soil Investigation

Assessment Criteria .........................................................................................5 Results ...............................................................................................................7

Analytical Data Validation ................................................................................. 7

Analytical Results and Discussion .................................................................. 7

Sugarloaf Well Site - Soil Investigation

Tables (in text)

Sugarloaf Well Site - Soil Investigation

Sugarloaf Well Site - Soil Investigation

Sugarloaf Well Site - Soil Investigation

Sugarloaf Well Site - Soil Investigation

Sugarloaf Well Site - Soil Investigation

URS Field Quality Management

Sugarloaf Well Site - Soil Investigation

Sugarloaf Well Site - Soil Investigation

Field QA/QC Results

Laboratory QA/QC Results

Overall Data Validity

Analytical Results and Discussion

Sugarloaf Well Site - Soil Investigation

Foam release area

Down gradient area

65* 1,000* * 1* 20 NEPM NIL NIL

<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR

<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR

<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR

<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR

<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR

<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR

<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR

<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR

<10 <50 <0.2 <0.5 <LOR <LOR <LOR <LOR

20 3 400 100 600 1 60 200 NIL

6 <1 15 23 19 <0.1 13 45 <100

8 <1 16 35 22 <0.1 16 55 <100

7.2 <1 15.5 29 20.4 <0.1 14.8 49.2 <100

6 <1 13 25 20 <0.1 12 48 <100

8 <1 15 27 44 <0.1 15 94 <100

6.75 <1 14.25 26 33 <0.1 13.75 69.25 <100

7 <1 15 25 19 <0.1 16 49 <100

8 <1 16 30 22 <0.1 17 79 <100

7.5 <1 15.5 27.5 20.5 <0.1 16.5 64 <100

Sugarloaf Well Site - Soil Investigation

Sugarloaf Well Site - Soil Investigation

Sugarloaf Well Site - Soil Investigation

Sugarloaf Well Site - Soil Investigation

Sugarloaf Well Site - Soil Investigation

Sugarloaf Well Site - Soil Investigation

Analyte Total Petroleum Hydrocarbons

TRH - NEPM 2010 DRAFT

J:\JOBS\43177447\MtTaurus_SoilAssess\Gilead\Final\Appendices\Gilead tables - Final.xls

URS Australia Pty Ltd Prepared By: AP Checked By: AS

Analyte LOR Polynuclear Aromatic Hydrocarbons

J:\JOBS\43177447\MtTaurus_SoilAssess\Gilead\Final\Appendices\Gilead tables - Final.xls

URS Australia Pty Ltd Prepared By: AP Checked By: AS

Total Kjeldahl Nitrogen as N

Total Soluble Salts

Anionic Surfactants as MBAS

J:\JOBS\43177447\MtTaurus_SoilAssess\Gilead\Final\Appendices\Gilead tables - Final.xls