Professional Documents
Culture Documents
HPLC Accessories
Choice of Congurations
The SLIPFREE connector is available in both single and double congurations. The double SLIPFREE is useful when frequent connections and disconnections will be made between HPLC columns and injectors or detectors. The single SLIPFREE connector is useful when only the column is changed. SLIPFREE connectors are available in exible 1/32" OD tubing as well as standard 1/16" OD tubing, in various lengths. SLIPFREE connectors come in 0.010" ID for routine work, 0.005" ID for use with small-bore and microbore columns, and 0.020" ID for semi preparative and preparative connections, or for connections ahead of the injector. PEEKcollared SLIPFREE connectors are ideal for higher temperature applications such as SFC. Long-neck SLIPFREE connectors have an extra long nut on the end which allows improved reach into tight spaces. SLIPFREE connectors come standard with Vespel ferrules. SLIPFREE sample loops are compatible with Rheodyne and Valco injectors. PEEK and Kel-F ferrules are available for applications where Vespel is not suitable, such as with strong acids or bases.
130
Accessories
Ordering Information
Description Length 0.005" ID 0.010" ID 0.020" ID
Single
6 cm 10 cm 20 cm 30 cm
30106 30110 30120 30130 30206 30210 30220 30230 30111-FLEX 30115-FLEX 30128-FLEX 30140-FLEX 30211-FLEX 30215-FLEX 30228-FLEX 30240-FLEX 30306 30310 30320 30406 30410 30420 30510 30520 31710 31720
31106 31110 31120 31130 31206 31210 31220 31230 39111-FLEX 39115-FLEX 39128-FLEX 39140-FLEX 39211-FLEX 39215-FLEX 39228-FLEX 39240-FLEX 31306 31310 31320 31406 31410 31420 31510 31520 32710 32720
32106 32110 32120 32130 32206 32210 32220 32230 N/A N/A N/A N/A N/A N/A N/A N/A 32306 32310 32320 32406 32410 32420 N/A N/A N/A N/A
Double
6 cm 10 cm 20 cm 30 cm
Single Flexible
10.5 cm 15 cm 28 cm 40 cm
Double Flexible
10.5 cm 15 cm 28 cm 40 cm
6 cm 10 cm 20 cm
6 cm 10 cm 20 cm
10 cm 20 cm 10 cm 20 cm
10 L Long-neck Loop 20 L Long-neck Loop 50 L Long-neck Loop 100 L Long-neck Loop 250 L Long-neck Loop
20 cm 40 cm 25 cm 50 cm 125 cm
SLIPFREE Ferrule
Description Part Number
131
HPLC Accessories
Ordering Information
Description Part Number
60170-370
132
Accessories
Ordering Information
Description Part Number
Solvent Inlet Filter with 1/16" O.D. tube to slip into 1/8" O.D. plastic tubing,10 m lter Solvent Inlet Filter with 1/8" polypropylene nut to t 1/8" O.D. tubing, 10 m lter 100% PEEK Bottom-of-the-Bottle Solvent Inlet Filter for 1/8" O.D. tubing, helium sparge, 2 m lter 100% PEEK Bottom-of-the-Bottle Solvent Inlet Filter for 3/16" O.D. tubing, helium sparge, 2 m lter (typically for Waters systems)
A-302
A-302A
A-437
A-436
133
HPLC Accessories
Ordering Information
Stainless Steel Fittings
Description Quantity Part Number
Two piece SS Fingerlok 10-32 nut with PEEK ferrule, 1/16" Replacement PEEK ferrules Universal SS 10-32 male hex nut Universal SS ferrule, 1/16" Valco SS 10-32 male hex nut Valco SS ferrule, 1/16" Waters compatible SS 10-32 male hex nut Waters SS ferrule, 1/16" RheFlex SS 10-32, 1/16" short ttings set RheFlex SS 10-32, 1/16" long ttings set RheFlex SS 10-32, 1/16" extra long ttings set RheFlex SS ferrule, 1/16" RheFlex SS ferrule, 0.5 mm (for Model 8125 only)
1 10 10 10 10 10 10 10 5 10 5 10 5 10 5 10 1
F-190 F-192x U-400x U-401x U-320x U-321x U-410x U-401x 6000-109 6000-209 6000-111 6000-211 6000-162 6000-262 6000-110 6000-210 8125-084
One piece PEEK ngertight tting, 1/16", 0.37" head One piece PEEK long ngertight tting, 1/16", 0.37" head One piece PEEK ngertight tting, 1/32", 0.25" head Two piece PEEK ngertight wing nut with PEEK ferrule, 1/16"
10 10 10 10
Replacement PEEK ferrules Column end plugs, 1/16", 10-32 coned, Delrin, black Column end plugs, 1/16", 10-32 coned, Delrin, red
10 10 10
60182-357
134
Accessories
Ordering Information
Stainless Steel Unions, Tees and Crosses
Description Through Hole Swept Volume Part Number
Union, stainless steel, Upchurch Scientic/Parker ttings compatible, includes 2 stainless steel nuts and ferrules Union, stainless steel, Upchurch Scientic/Parker ttings compatible, includes 2 stainless steel nuts and ferrules Union, stainless steel, Upchurch Scientic/Parker ttings compatible, includes 2 stainless steel nuts and ferrules Union, stainless steel, Upchurch Scientic/Parker ttings compatible, includes 2 stainless steel nuts and ferrules Union, stainless steel, Waters ttings compatible, includes 2 stainless steel nuts and ferrules Union, stainless steel, Valco ttings compatible, includes 2 stainless steel nuts and ferrules Tee, stainless steel, 10-32 ttings for use with 1/16" OD tubing
Cross, stainless steel, 10-32 ttings for use with 1/16" OD tubing
0.020"
< 0.72 L
U-430
Union, PEEK polymer, includes two PEEK 2-piece ttings Union, PEEK polymer, includes two PEEK 2-piece ttings
0.010" 0.020"
0.070 L 0.28 L
P-742 P-704
Tee, PEEK, 10-32 ttings for use with 1/16" OD tubing, includes three 10-32 PEEK double-winged nuts
0.020"
< 0.57 L
P-727
PEEK, 10-32 ttings for use with 1/16" OD tubing, includes four 10-32 PEEK double-winged nuts
0.020"
< 0.72 L
P-729
135
HPLC Accessories
Ordering Information
1/16" OD Precut PEEK Tubing
Description Length (cm) Color Part Number
0.003"
5 10 20 30 50 100
Natural Natural Natural Natural Natural Natural Red Red Red Red Red Red Yellow Yellow Yellow Yellow Yellow Yellow Blue Blue Blue Blue Blue Blue Orange Orange Orange Orange Orange Orange
37003-5 37003-10 37003-20 37003-30 37003-50 37003-100 37005-5 37005-10 37005-20 37005-30 37005-50 37005-100 37007-5 37007-10 37007-20 37007-30 37007-50 37007-100 37010-5 37010-10 37010-20 37010-30 37010-50 37010-100 37020-5 37020-10 37020-20 37020-30 37020-50 37020-100
0.005"
5 10 20 30 50 100
0.007"
5 10 20
PEEK tubing is designed to work in most HPLC applications, particularly reversed phase with aqueous mobile phases. It is supplied in pre-cut lengths, but is easily cut to a desired length. PEEK tubing is available in a range of internal diameters and can be used with standard ngertight ttings. PEEK tubing is resistant to most organic solvents. However, nitric acid, sulfuric acid, dichloromethane, THF and DMSO are not recommended.
Part Number
Ordering Information
Description Part Number
0.040"
Polymer tubing cutter (for 1/16" and 1/8" OD) Replacement blades (5/pk)
A-327 A-328
136
Accessories
Ordering Information
Description Length (cm)* Quantity Part Number
0.002" (50 m)
10 20 50
5 5 2 5 5 2 5 5 2
0.004" (100 m)
10 20 50
0.007" (175 m)
10 20 50
* It is recommended that PEEKsil tubing be used in the lengths provided, as damage may occur upon cutting.
0.008
PEEKsil fused silica lined PEEK tubing is manufactured using precision bore fused silica tubing coated with a 1/16" OD PEEK covering. The tubing can withstand high pressures, which makes it an ideal choice for capillary HPLC and LC/MS. The tubing has a very smooth internal surface for excellent ow characteristics, which leads to improved reproducibility and resolution, and higher efciency.
PEEKsil tubing is quite stiff and is difcult to bend without damaging the fused silica core. As such, it is not recommended for sections of the system where tubing bends are required. The tubing cannot be cut in the laboratory and is therefore limited to pre-cut lengths only.
137
HPLC Accessories
in 1/16" and 1/32" OD for ultra high pressure applications Wide chemical compatibility
Ordering Information
1/16" OD Precut 316 Stainless Steel Tubing
Description Length (cm) Color Part Number
0.005"
5 10 20 30 50 100
Red Red Red Red Red Red Black Black Black Black Black Black Blue Blue Blue Blue Blue Blue
U-152 U-153 U-154 U-155 U-156 U-157 U-126 U-127 U-128 U-129 U-130 U-131 U-111 U-112 U-113 U-114 U-132 U-133
0.007"
5 10 20 30 50 100
Stainless steel tubing is available in a range of precut lengths and IDs. Each length of tubing has pre-nished, square, burr-free ends and interiors to ensure minimum dead volume connections. It is cleaned and passivated and ready for immediate installation. Stainless steel tubing is required for ultra high pressure applications where plastic or hybrid tubing will not work. Stainless steel tubing is reasonably exible, but is best when bends are kept to a minimum. The tubing also has a rough internal surface, which could lead to sample carry-over. Stainless steel tubing is not recommended for biological samples .
0.010"
5 10 20 30 50 100
0.005"
10.5 15 28 40
0.007"
10.5 15 28 40
Description
Part Number
This tool cuts 1/16" or 1/8" stainless steel tubing, producing a clean, 90 cut.
Description Part Number
60182-509 60182-510
Straight cut tubing from Poorly cut tubing Terry Tool cutter
138
Accessories
The Click-On Inline gas ltering system is designed with ease of use and gas quality (99.9999% or 6.0 grade) in mind. Re-useable end ttings remain installed on the gas line during lter replacement, reducing the cost of clean gas. These unique patented end
ttings incorporate needle valves that close the lines and prevent contamination. Filters are available to remove oxygen, moisture, hydrocarbons, including a Click-On inline Combi lter to remove moisture and oxygen, or a Triple lter to remove all three.
Capacity
Useable Gases
Color Change
Moisture Oxygen Hydrocarbons Combi (H2O, O2) Triple (H2O, O2, HC) Indicating Triple (H2O, O2, HC)
> 6.0 > 6.0 > 6.0 > 6.0 > 6.0 > 6.0
15 g H2O 2000 mL O2 24 g HCs 7 g H2O 4 g H20, 1000 mL O2, 8 g HCs 3 g H20, 400 mL O2, 5 g HCs
Yellow to transparent Green to gray N/A Moisture and O2 See Combi See Combi
Ordering Information
Description Quantity Part Number
Click-On Inline Moisture Filter Click-On Inline Oxygen Filter Click-On Inline Hydrocarbon Filter Click-On Inline Combi (Oxygen & Moisture) Click-On Inline Triple, (Oxygen, Moisture & Hydrocarbons) Click-On Inline Triple (He preconditioned) Click-On Inline Indicating Triple Click-On Inline Indicating Triple (He preconditioned) 1/8" Brass Re-useable End Fittings 1/8" Steel Re-useable End Fittings 1/4" Brass Re-useable End Fittings 1/4" Steel Re-useable End Fittings Double-ended Cartridge Connector to connect lter to indicator Wall Mounting Clamp Replacement O-rings
1 1 1 1 1 1 1 1 2 2 2 2 1 4 10
60180-801 60180-802 60180-803 60180-804 60180-805 60180-806 60180-807 60180-808 60180-809 60180-810 60180-811 60180-812 60180-813 60180-834 60180-833
145
GC Accessories
The Thermo Super Clean range of cartridge gas ltering systems is designed with ease of use and gas quality (99.9999% or 6.0 grade) in mind. The lter base plate is a one-time installation procedure and can be congured to the individual requirements of the user. Needle valves ensure the gas line is not contaminated during cartridge change.
Capacity
Useable Gases
Color Change
Moisture Oxygen Hydrocarbons Combi (H2O, HC) Triple (H2O, O2, HC)
> 6.0 > 6.0 > 6.0 > 6.0 > 6.0
7.2 g H2O 1000 mL O2 12 g (n-butane) hydrocarbons 3.5 g H2O 6 g HCs 1.8 g H2O 500 mL O2 4 g HCs
Inert; Air; H2, He Inert Inert; Air; H2 Inert; Air; H2, He Inert N/A Moisture and O2 See Combi
Description
Contains
Use
Carrier gas only Air & fuel gas Carrier, make up and fuel High capacity carrier, fuel & make up
Ordering Information
Description Quantity Part Number
Base plate for 1 lter Base plate for 2 lters High ow 2 lter base plate for N2 in LC/MS or H2O in H2/air-generators Base plate for 3 lters Base plate for 4 lters Moisture cartridge with indicator Oxygen cartridge with indicator Hydrocarbon cartridge GC cartridge bundle of 3 (Triple + 2x HC/H2O Combi) GC cartridge bundle of 4 (O2, H2O + 2x HC) GC cartridge triple (O2 + H2O + HC) GC cartridge triple (O2/H2O/HC) He preconditioned GC cartridge combi (HC/H2O) 4 cartridges (O2/H2O/2x HC + Base) 3 cartridge kit (Triple + 2x Combi + Base) He preconditioned kit (Base + Triple Cartridge Gas lter kit (Base + Triple Cartridge) Twin HC lters for high ow base plate (LC/MS) (No indicator) High ow twin H2O lters (air generators) Replacement O-rings for base plates Flush cap (allows gas ow without lter) High ow bundle (2x HC) no indicator for LCMS High ow bundle (2x HC) with indicator for LCMS High ow bundle (2x H20) with indicator for LCMS
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
60180-814 60180-815 60180-816 60180-817 60180-818 60180-819 60180-820 60180-821 60180-822 60180-823 60180-824 60180-825 60180-826 60180-827 60180-828 60180-829 60180-830 60180-831 60180-832 60180-837 60180-838 60180-839 60180-840 60180-841
146
Accessories
Capillary Accessories
Ordering Information
Retention Gap Kits
Description Part Number
Retention gap kit, ID 0.22-0.32 mm, 2 m (includes connectors) Retention gap kit, ID 0.53 mm, 2 m (includes connectors) Deactivated silica tubing, ID 0.32 mm, 2 m Deactivated silica tubing, ID 0.53 mm, 2 m
1* 1*
290GU498 290GU499
Column End Caps Reusable universal capillary end caps t all capillary column IDs and eliminate column contamination caused by leaving the column unsealed or sealed with a septum. The ttings are color coordinated to ensure that column is re-installed the same way it came out, preventing detector contamination.
Description Quantity Part Number
10 pairs
260EC111
147
GC Accessories
GC Injection Liners
Improved, reproducible vaporization
Full range for Thermo and other GCs Highly deactivated borsilicate glass FocusLiner injection liner for improved vaporization providing 10 times the reproducibility The injection liners from Thermo are highly deactivated, and produced to exacting tolerances to ensure the high level of reproducibility required in todays separation laboratory. A full range of liners is available for Thermo and other manufacturers instruments.
improvements. The FocusLiner secures the quartz wool between two restrictions preventing movement during syringe needle injection. The quartz wool consistently wipes the dispensed liquid away from the end of
the syringe needle during the injection process, resulting in less carryover and greatly improved precision. With these liners, a Relative Standard Deviation (RSD) of less than 1% can be achieved.
Please also see septa on page 154.
Injection Type
Quantity
Part Number
5 x 8 x 105
Splitless Use 70 mm Needle Splitless Use 50 mm Needle Split Use 50 mm Needle Split Split Splitless Splitless PTV PTV-LVI PTV PTV Split Split/Splitless Split
453T2895
5 x 8 x 105
453T2999
5 x 8 x 105
453T1905
TRACE & FOCUS SSL TRACE & FOCUS SSL TRACE & FOCUS SSL TRACE & FOCUS SSL TRACE PTV TRACE PTV TRACE PTV TRACE PTV Mega 4000, 5000, 6000 Mega 4000, 5000, 6000 Mega 4000, 5000, 6000
3 x 8 x 105 5 x 8 x 105 3 x 8 x 105 5 x 8 x 105 1 x 2.75 x 125 2 x 2.75 x 120 2 x 2.75 x 120 1 x 2.75 x 120 3 x 5 x 79.5 5 x 5 x 79.5 2 x 5 x 79.5
5 5 5 5 5 5 5 5 5 5 5
45350031 45350030 45350032 45350033 45352054 45352060 45352057 45352062 45350400 453T2955 45350300
148
Accessories
Other Liners
Instrument I.D. x O.D. x Length (mm) Quantity of 5 Quantity of 25
Agilent Agilent Agilent Agilent Agilent Agilent Agilent Agilent Agilent Agilent Agilent Agilent Agilent Varian 1078/1079 Varian 1078/1079 Varian 1078/1079 Varian 1078/1079 Varian 1078/1079 Varian 1078/1079 Shimadzu 2010 Shimadzu 2010 Shimadzu 2010 Shimadzu 17A Shimadzu 17A Shimadzu 17A Shimadzu 17A
4.0 x 6.3 x 78.5 2.3 x 6.3 x 78.5 2.3 x 6.3 x 78.5 4.0 x 6.3 x 78.5 4.0 x 6.3 x 78.5 4.0 x 6.3 x 78.5 4.0 x 6.3 x 78.5 4.0 x 6.3 x 78.5 4.0 x 6.3 x 78.5 4.0 x 6.3 x 78.5 1.2 x 6.3 x 78.5 2.0 x 6.1 x 78.5 2.0 x 6.3 x 78.5 0.75 x 5 x 54 2 x 5 x 54 3.4 x 5 x 54 0.5 x 5 x 54 3.4 x 5 x 54 3.4 x 5 x 54 3.4 x 5 x 95 3.4 x 5 x 95 2.6 x 5 x 95 3.4 x 5 x 95 3.4 x 5 x 95 3.4 x 5 x 95 3.4 x 5 x 95
453A1255 453A1285 453A2375 453A1925 453A2265 453A1345 453A1305 453A1355 453A1315 453A1295 453A1335 453A2275 453A2325 453V2995 453V2545 453V1535 453V2885 453V1515 453V2525 453S2985 453S2615 453S1645 453S1605 453S1625 453S2595 453S2615
149
GC Accessories
Other Liners
Instrument I.D. x O.D. x Length (mm) Quantity of 5
Shimadzu 17A Shimadzu 17A Shimadzu 17A PE Clarus PE Clarus PE Clarus PE Clarus PE Clarus PE Clarus PE Clarus
3.4 x 5 x 95 2.6 x 5 x 95 0.75 x 5 x 95 2 x 4 x 86.2 4 x 6.2 x 92 4 x 6.2 x 92 4 x 6.2 x 92 2 x 6.2 x 92 2 x 4 x 86.2 3 x 6 x 112
453S2635 453S1645 453S1665 453P1795 453P1755 453P2765 453P2785 453P2805 453P1775 453P1815
Ordering Information
Liner Sealing Rings
Instrument Liner Material Quantity Part Number
8 mm O.D. liners 453A1335, 453A1355, 453A2332, 453A2352 453A2265, 453A1255, 453A1315, 453A1285, 453A1295, 453A2282, 453A1305, 453A1312, 453A2325, 453A1345, 453A2375, 453A1372, 453A1252, 453A1262, 453A2292, 453A2302, 453A2342 453A2275 All above Agilent liners 453P1755, 453P2765, 453P2785, 453P2805, 453P1815 453S2985 All 17A liners All liners
10 10 10
Graphite Ring Viton O-Ring Viton O-Ring Viton O-Ring Graphite Ring Graphite Ring
10 10 10 10 10 10
150
Accessories
Ferrules
Wide range of choices for a wide range of instruments and applications
Ferrules from Thermo are available in three different materials and various dimensions to match the instrument and capillary column ID. The choice of material is dependent upon the use; guidelines are given in the table.
Material Type Suitable for GC/MS Temp Limit (C) Re-usable
No Yes Yes
Yes No No
All varieties of ferrules are supplied in contaminant-free, individual blister packs, allowing removal of an individual item without risk of contamination to the other supplied items.
Ordering Information
Thermo Instruments
Description Uses Ferrule Size (Column ID) Quantity Part Number
0.1 0.25 mm 0.32 mm 0.53 mm Packed Column 1/8" OD Packed Column 1/4" OD
29033461 29033460 29033471 290VT168 290VT165 290VT186 290VT187 290VT188 290BT239 29033496 29033497 29053488 29053487 29053486 290MT229 290MT230 290MT231 290MT221 290MT222 290MT223 290MT211
Brass Nut GC/MS Interface 100% Graphite Ferrules Injectors & Detectors at Atmospheric Pressure (Not for GC/MS) GC/MS Interface 0.1 0.25 mm 0.32 mm 0.1 0.25 mm 0.32 mm 0.53 mm SilTite Kit 0.1 0.25 mm 0.32 mm 0.53 mm Replacement SilTite Ferrules 0.1 0.25 mm 0.32 mm 0.53 mm Replacement SilTite Nuts
* Must be used in conjunction with brass nut PN 290BT239 ** Kit contains 2 SilTite nuts and 10 ferrules Equivalent to PN 29013488, 29013487 & 29013486 previously sold in quantities of two
151
GC Accessories
0.1 0.25 mm 0.32 mm 0.53 mm Packed Column 1/8" OD Packed Column 1/4" OD
290VA191 290VA192 290VA193 290VT168 290VT165 29033496 29033497 290VP144 290GA139 290GA140 290GA108 290GA107 290MA194 290MA195 290MA196 290MA215 290MA216 290MA217 290MA201 290MA202 290MA203 290MA205 290MA207 290MA227 290MA228
GC/MS Interface
0.1 0.32 mm 0.45 0.53 mm Packed Column 1/8" OD Packed Column 1/4" OD
SilTite Kits
GC/MS Interface
SilTite Nuts
* Kits contain 2 nuts and 10 ferrules ** Contains 2 nuts, 10 ferrules and 2 base seals
Varian Instruments
Description Uses Ferrule Size (Column ID) Quantity Part Number
0.1 0.25 mm 0.32 mm 0.53 mm Packed Column 1/4" OD Packed Column 1/8" OD
10 10 10 10 10 10 10 10 10 1* 1* 1* 10 10 10 5
29033496 29033497 290VP144 290VT165 290VT168 290GP132 290GP131 290GT128 29033405 290MV218 290MV219 290MV220 290MA201 290MA202 290MA203 290MV212
100% Graphite
0.1 0.32 mm 0.45 0.53 mm Packed Column 1/8" OD Packed Column 1/4" OD
SilTite Kit
152
Accessories
Shimadzu Instruments
Description Uses Ferrule Size (Column ID) Quantity Part Number
100% Graphite
Injectors & Detectors at Atmospheric Pressure (Not for GC/MS ) 2010 Injector
SilTite Kit
Shimadzu Direct GC/MS Interface (check interface is tapered) Jet Separator & 2010
Shimadzu Jet Separator GC/MS Interface, 2010/MS GC/MS Interface and Injector. (check interface is at) All injectors except 2010
0.1 0.25 mm 0.32 mm 0.1 0.25 mm 0.32 mm 0.1 0.25 mm 0.32 mm 0.53 mm 0.1 0.32 mm 0.45 0.53 mm 5 mm OD Packed Columns 0.1 .032 mm 0.45 0.53 mm 0.1 0.25 mm 0.32 mm 0.53 mm 0.1 0.25 mm 0.32 mm 0.53 mm 0.1 0.25 mm 0.32 mm 0.53 mm 0.1 0.25 mm 0.32 mm 0.53 mm Replacement Nuts 0.1 0.25 mm 0.32 mm 0.53 mm Replacement Nuts 0.1 0.25 mm 0.32 mm 0.53 mm Replacement Nuts
10 10 10 10 10 10 10 10 10 10 10 10 1* 1* 1* 1* 1* 1* 1* 1* 1* 10 10 10 5 10 10 10 5 10 10 10 5
290VS148 290VS149 290VS146 290VS147 29033496 29033497 290VP144 290GS115 290GS116 290GS101 290GA139 290GA140 290MS198 290MS199 290MS200 290MA194 290MA195 290MA196 290MS224 290MS225 290MS226 290MS208 290MS209 290MS210 290MS214 290MA201 290MA202 290MA203 290MA205 290MA201 290MS209 290MS210 290MU240
PerkinElmer Instruments
Description Uses Ferrule Size (Column ID) Quantity Part Number
100% Graphite
SilTite Kit
GC/MS Interface
Replacement Ferrules
0.1 0.2 5 mm (1/16" Nut) 0.32 mm (1/16" Nut) 0.53 mm (1/16" Nut) 0.1 0.25 mm (1/8" Nut) 0.32 mm (1/8" Nut) 0.53 mm (1/8" Nut) 0.1 0.32 mm (1/16" Nut) 0.45 0.53 mm (1/16" Nut) 0.1 0.32 mm (1/8" Nut) 0.45 0.53 mm (1/8" Nut) Packed Column 1/8" OD Packed Column 1/4" OD 0.1 0.25 mm 0.32 mm 0.53 mm 0.1 0.25 mm 0.32 mm 0.53 mm
SilTite Nuts
10 10 10 10 10 10 10 10 10 10 10 10 1* 1* 1* 10 10 10 5
29033496 29033497 290VP144 290VP173 290VP172 290VP174 290GP132 290GP131 290GP130 290GP135 290GT128 29033405 290MA194 290MA195 290MA196 290MA201 290MA202 290MA203 290MA205
153
GC Accessories
Septa
Wide range of septa to cover most applications
Variety of materials and temperature limits for all applications For use with Thermo TRACE and FOCUS GCs and instruments from other manufacturers Septa Materials Characteristics
Septa Type Description Temperature Limit (C)
Triple layer with Teon Silicone with Teon High Grade Silicone High Grade Silicone with Teon Low Bleed Silicone
Ordering Information
Septa Materials Diameter (mm) Quantity Part Number
17 11 9 12.7 5 9.5 11 12.5 9.5 11 12.5 17 9.5 11 9.5 9.5 11 11 12.5 17 Shimadzu plug
50 50 50 50 50 50 50 50 50 50 50 50 25 25 25 100 25 100 25 25 50
31303211 31303230 31303240 31313228 313C500A 313C950M 313C110M 313C125A 313T950M 313T110M 313T125A 313T170T 313A950M 313A110V 313S950M 313S959M 313S110M 313S119M 313S125A 313A170T 313B201S
Septa are an important part of the GC instrument and require durability, resealability and low bleed for optimal performance of your instrument. Septa from Thermo are available in several types of materials that t in Thermo and other manufacturers instruments. All septa are supplied in contaminant-free, individual blister packs, allowing removal of an individual item without risk of contamination to the other supplied items.
CS TCS TCS TCS TCS Auto-Sep Auto-Sep Auto-Sep T Auto-Sep T Auto-Sep T Auto-Sep T Auto-Sep T Auto-Sep T Enduro
154
Accessories
General GC Tools
Additional quality GC accessories
Thermo offers a variety of tools for use in any lab with a GC, from forceps to a complete kit of commonly used items. Using a rotation diamond scribe, the Shortix Capillary cutter gives a far Shortix superior column end than a column cutter ceramic or pen type cutter. This leads to better seals in column joints, leading to less leakage and more reproducible results.
Please also see gas lters on page 145-146.
Ordering Information
Description Part Number
Straight tipped forceps Angle tipped forceps Pin vice for drilling holes in ferrules Magnifying glass Probes Inspection mirror Needle le Pick-up tool Ceramic column cutter Shortix capillary column cutter Shortix cutter repair kit Adjustable wrench 0.35 mm drill bit 0.45 mm drill bit 0.70 mm drill bit
60180-770 60180-771 60180-772 60180-773 60180-774 60180-775 60180-776 60180-777 60201-318 60180-835 60180-836 60180-782 60180-779 60180-780 60180-781
155
Syringes
HPLC Syringes
Easy and reproducible manual injection
Square tip to prevent damage to injector Wide range of volumes and styles Accurate and reproducible The range of Thermo syringes covers a wide range of volumes for manual injection. The syringes are precision made from borosilicate glass and stainless steel. The range of PTFE tipped syringes is ideal for dirty samples as the sample is cleaned more completely from the barrel with every injection. Long lifetimes are provided by the robust design and the easy-to-read markings make reproducible manual injection far easier. The range of autosampler syringes has been tested on a range of Thermo instruments to ensure the accuracy and reliability of performance over long analysis sequences. For accuracy and reproducibility information please see page 158.
Ordering Information
Standard Fixed Needle for Rheodyne/Valco
Volume Gauge Needle Quantity Part Number
22 22 22 22 22 22 22
1 1 1 1 1 1 1
22 22 22 22 22 22
1 1 1 1 1 1
2" 2"
22 22
5 5
365RNL15 365RNL25
1 mL 2.5 mL 5 mL 10 mL 25 mL 50 mL
1 1 1 1 1 1
156
Accessories
All
22
2"
365RNL22
X X X X X X X X
22 22
2" RN 2" RN
1 1 1 1 1
For LCQ XP, DECA, Advantage For LCQ MS For LCQ XSQ
1 1 1
157
Syringes
GC Syringes
Improved designs for a range of instruments
Accurate and reproducible over a range of volumes Manual and autosampler varieties Range of needle tips Robustness from improved design Syringe Specications (Autosampler and Manual)
Temperature Limits Volume Reproducibility (displaced) Volume Accuracy Maximum Safe Working Pressure 5 115 C for removable needle syringes; 5 70 C for xed needle syringes 1% (2% for plunger-in-needle syringes) 1% (2% for plunger-in-needle syringes) 5 L to 100 L 1000 psi 250 L and 500 L 500 psi 1 mL to 5 mL 400 psi 10 mL 200 psi 25 mL, 50 mL and 100 mL 100 psi Maximum Functional Pressure 100 psi
The accuracy and precision of the GC sample syringe is critical to your GC results. Thermos syringes are designed, manufactured and inspected to ensure the expected volume is transferred every time. Our syringes are made by chromatographers who are familiar with the requirements of the entire GC system, not just syringe manufacturing. All Thermo syringes use borosilicate glass with metal anges of either stainless steel or nickel-plated brass. Your syringe choices include xed and removable needles as well as standard and gas-tight plungers for convenience. The needles and plungers are stainless steel; gas-tight plunger tips are PTFE. The table summarizes the specications of all available syringes.
Autosampler Syringes
Thermo is the source for all your GC autosampler syringes, no matter what GC you use. Thermo offers a wide variety of needle tips including cone point which can help prevent the plunger binding with dirty samples. The eld proven syringe designs are optimized for septum piercing, and come in a range of volumes.
Manual Syringes
Thermo manual syringes come in industry standard sizes, ensuring you of a consistent t with your GC. The white scale backing makes markings easy-to-read, improving reproducibility, and the markings are resistant to solvents. Syringe volumes range from 0.5 L to 1.0 mL, covering most sample take up and delivery requirements.
For syringe accessories and replacement parts, see page 161.
158
Accessories
Ordering Information
Autosampler Syringes for Thermo Instruments
Volume Needle Type Length (mm) Needle Gauge Tip Style Quantity Thermo Instrument TriPlus AS3000 AS2000 AS200/AS800 Notes Part Number
0.5 L 0.5 L 0.5 L 5.0 L 5.0 L 5.0 L 5.0 l 5.0L 10 L 10 L 10 L 10 L 10 L 10 L 10 L 10 L 10 L 10 L 10 L 10 L 50 L 50 L 100 L 100 L 100 L 100 L 250 L 250 L 250 L 250 L 500 L 1.0 mL
Plunger-in-Needle Plunger-in-Needle Plunger-in-Needle Fixed Needle Fixed Needle Fixed Needle Removable Needle Fixed Needle Removable Needle Fixed Needle Fixed Needle Fixed Needle Fixed Needle Removable Needle Removable Needle Fixed Needle Fixed Needle Fixed Needle, Gas Tight Fixed Needle Removable Needle, Gas Tight Removable Needle, Gas Tight Removable Needle Removable Needle Removable Needle, Gas Tight Removable Needle, Gas Tight Removable Needle, Gas Tight Removable Needle, Gas Tight Removable Needle, Gas Tight Removable Needle, Gas Tight Removable Needle, Gas Tight Removable Needle Removable Needle, Gas Tight
50 75 80 50 50 50 75 80 42 50 50 50 50 50 50 80 50 50 80 75 50 50 50 50 50 50 50 50 80 50 50 50
23 31 26 26 23 26 31 26 23 26 26 25 23 26 23 23 23 - 26 23 26 31 25 23 25 23 25 23 25 25 26 23 23 23
Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Bevel Cone Bevel Side Hole Bevel Cone Bevel Bevel Cone Side Hole Side Hole Bevel
1 1 1 1 1 1 1 1 1 1 6 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
X X X
Split/PTV Manual OC Splitless & OC Split/PTV X X X Split/PTV Manual OC Splitless & OC X X X X X X Merlin Valve SSL Splitless OC in PTV Merlin Valve OC & Splitless Manual OC X X X LV Splitless
X X X X X X X X X
X X
X X X
X X X X X X X X X X
X X
X X X
X X
36504045 36500500 36504046 36504047 365C3701 36500505 36500510 36502025 365D1611 365D3711 365D1856 36500525 36520060 365D1841 365D3731 36520061 36500580 365D3741 36502019 36500520 365G2161 36503015 365H2301 36520050 365H2381 36500495 365I2561 365I2611 36500490 36520051 36520055 365K3041
1. Specic syringe to be used when performing PTV/LVI injections with dedicated liner for thermo labile compounds (p/n 45352060). Compatible with Merlin Microseal device installed on BEST PTV and with AS2000 and TriPlus autosamplers for liquids.
Agilent
Removable Needle Removable Needle Removable Needle Fixed Needle Fixed Needle Fixed Needle Fixed Needle Fixed Needle Fixed Needle Fixed Needle Fixed Needle Fixed Needle, Gas Tight Fixed Needle Fixed Needle Removable Needle, Gas Tight Fixed Needle Fixed Needle
42 42 42 42 42 42 42 42 42 42 42 42 42 42 42 42 42
26 23 23 26 26 26 23 23 23 26 23 26 26 26 23 26 23 23 23 23 26 23 26
Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone
1 1 1 1 6 1 6 1 6 1 6 1 1 6 1 1 6
365A0411 365A0421 365A0431 365C0921 365C0926 365C0951 365C0956 365C0971 365C0976 365D1521 365D1526 365D1561 365D1571 365D1576 365D1611 365D1621 365D1636
159
Syringes
PerkinElmer
0.5 L 0.5 L 5 L 5 L 5 L 5 L
Removable Needle Removable Needle Fixed Needle Fixed Needle Fixed Needle, Gas Tight Fixed Needle, Gas Tight Removable Needle Removable Needle Removable Needle, Gas Tight Removable Needle Fixed Needle
70 70 70 70 70 70 42 42 42 53 50
26 23 26 23 26 23 26 23 23 25 26
Cone Cone Cone Cone Cone Cone Cone Cone Cone Side Hole Bevel
1 1 1 1 1 1 1 1 1 1 1
365A0471 365A0481 365C1011 365C1021 365C1031 365C1041 365D1771 365D1781 365D1791 365D1811 365D1831
Shimadzu
10 L 10 L 10 L
Varian
10 L 10 L
Manual Syringes
Volume Needle Type Needle Length (mm) Gauge Tip Style Quantity Part Number
0.5 L 1.0 L 1.0 L 5.0 L 5.0 L 10 L 10 L 10 L 25 L 25 L 25 L 25 L 50 L 50 L 50 L 50 L 100 L 100 L 100 L 100 L 250 L 250 L 250 L 500 L 500 L 1.0 mL 1.0 mL
Plunger-in-Needle Plunger-in-Needle Plunger-in-Needle Fixed Needle Removable Needle Fixed Needle Fixed Needle Removable Needle Fixed Needle Removable Needle Fixed Needle, Gas Tight Removable Needle, Gas Tight Fixed Needle Removable Needle Fixed Needle, Gas Tight Removable Needle, Gas Tight Fixed Needle Removable Needle Fixed Needle, Gas Tight Removable Needle, Gas Tight Fixed Needle Fixed Needle, Gas Tight Removable Needle, Gas Tight Fixed Needle, Gas Tight Removable Needle, Gas Tight Removable Needle, Gas Tight Fixed Needle, Gas Tight
50 50 70 50 50 50 50 50 50 50 50 70 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50
23 23 23 26 26 26 26 26 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 23 22
Cone Cone Cone Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel
1 1 1 1 1 1 6 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
365A0331 365B0511 365B0531 365C0741 365C0761 365D1091 365D1096 365D1171 365F1891 365F1901 365F1921 365F1931 365G2081 365G2091 365G2111 365G2161 365H2291 365H2301 365H2321 365H2381 365I2541 365I2561 365I2611 365J2831 365J2881 365K3041 365K3051
160
Accessories
GC Syringe Accessories
To increase the life of your Thermo syringes, Thermo carries a line of replacement needles, plungers, and repair kits.
Ordering Information
Replacement Needles
For Syringe Part Number Quantity Part Number
365D1611 365D1841 365D1771 365D3731 365H2301, 365F1931, 365G2161, 365H2381, 365I2611, 365F1901, 365G2091, 365J2881 365K3041 36500495, 36503015 36500490, 36520050, 36520051, 36520055 365D1811 365C0761 365D1171 365D1781, 365D1791 36500510 36500520
2 2 2 2 5 5 5 5 2 1 5 5 2 2 2
365RN252 365RN362 365RN272 365RN372 365RN225 365RN235 36566485 36566480 36550040 365RN351 365RN555 365RN215 365RN282 36550045 36550046
Replacement Plungers
For Syringe Part Number Quantity Part Number
365F1921, 365F1931 365G2111, 365G2161 365H2321, 365H2381 365I2561, 365I2611 365J2831, 365J2881 365K3041, 365K3051 365D1811 365D1561 365C1041 365D1791 365D3741 365D1611 365H3771 36500500 Replacement seal for all 0.5 L syringes Replacement seal for all 1 L syringes
1 1 1 1 1 1 1 2 2 2 2 2 1 1 1 1
365RP421 365RP451 365RP461 365RP481 365RP491 365RP511 365RP441 365RP392 365RP382 365RP522 365RP532 365RP412 365RP471 365RK351 365RK561 365RK563
Repair Kits
For Syringe Part Number Quantity Part Number
1 1 1 1 1 1 1 1
161
Vials
Thermo Vials
Compatible with a wide range of HPLC and GC instruments
Convenient clam shell packs include 100 vials and caps Vials and caps also available separately Head space vials also available Thermo provides a range of vials tested on our GC and LC instruments; they are also compatible with many other manufacturers instruments such as Agilent, PerkinElmer and Varian. Made from highly pure borosilicate glass, the vials meet the high standards required by such bodies as the US and European Pharmacopoeia, and ASTM for hydrolytic extraction.
1 2 3 4 5 6 7 8
Ordering Information
Vial Combination Packs
Cap Type Vial Type Dimensions (mm x mm) Quantity Instrument Compatibility (please refer to reference table) Part Number
Blue cap with blue silicone/ red PTFE seal Cap with white silicone/ red PTFE seal 9 mm screw cap (blue) pretted silicone/PTFE seal 8 mm screw cap (black) with silicone/PTFE seal
2.0 mL crimp top vial, clear borosilicate glass 33 2.0 mL crimp top vial, clear borosilicate glass 33 2.0 mL screw top vial, clear borosilicate glass 33 2.0 mL screw top vial, clear borosilicate glass 33
12 x 32 12 x 32 12 x 32 12 x 32
Autosampler Vials
Description Dimensions (mm x mm) Quantity Instrument Compatibility (please refer to reference table) Part Number
Crimp top vial, 1 mL, 8 mm nish Requires 8 mm aluminum caps and seals (60180-525) and plastic reducer (60180-524) Crimp top vial, 1.2 mL, 8 mm nish Requires 8 mm aluminum caps and seals (60180-525) and plastic reducer (60180-524) Crimp top vial, 2 mL, 11 mm nish Requires 11 mm aluminum caps and seals (60180-526) and spacers (60180-523)* Crimp top vial, 10 mL, 20 mm nish Requires 20 mm aluminum caps and seals (60180-513 or 60180-511) Crimp top amber vial, 10 mL, 20 mm nish Requires 20 mm aluminum caps and seals (60180-513 or 60180-511) Crimp top vial, 20 mL, 20 mm nish Requires 20 mm aluminum caps and seals (60180-513 or 60180-511) 300 L micro-volume sampling vial Requires screw top cap with septa (60180-516) Screw top vial, 2 mL, 8 mm nish, clear glass Requires 8 mm plastic screw caps (60180-514), Teon faced seals (60180-515) and plastic spacers (60180-523)* Screw top vial, 2 mL, clear glass Requires screw top cap with septa (60180-516) Solvent vial, 4 mL Requires screw top cap with septa (60180-516) Screw top vial, 2 mL, 8 mm nish, amber glass Requires 8 mm plastic screw caps (60180-514), Teon faced seals (60180-515) and plastic spacers (60180-523)* Screw top vial, 2 mL, amber glass Requires screw top cap with septa (60180-516) Crimp top vial, 2.5 mL, 11 mm nish. Requires 11 mm aluminum Caps and Seals (60180-526) and Spacers (60180-523)*
8 x 40
125
2,6
60180-500
8 x 40
125
2,6
60180-501
12 x 32
100
2,6,8
60180-502
22 x 45
125
2,3,4,5,6
60180-504
22 x 45
125
2,3,4,5,6
60180-505
22 x 75
125
3,4,5
60180-506
12 x 32 12 x 32
100 100
1,8 2,6,7,8
60180-507 60180-508
12 x 32 15 x 46 12 x 32
1,6,7,8 1 2,6,7,8
12 x 32
100
1,6,7,8
60180-561
12 x 32
100
2,6
60180-503
162
Accessories
Ordering Information
Caps and Septa
Description Quantity Part Number
Aluminum crimp cap with silicone/PTFE seal Aluminum crimp cap with chlorobutyl/PTFE seal Plastic screw caps, 8 mm 8 mm seal, red PTFE/white silicone 8 mm seal, blue silicone/PTFE Screw top caps for 2 mL, 4 mL and 300 mL vials complete with septa Plastic spacer for 2 mL screw top vials (compatible with AS800/AS2000) Plastic reducer for 1 and 1.2 mL vials (compatible with TriPlus AS) Aluminum caps, 8 mm with Teon faced septa Aluminum crimp cap, 11 mm with Teon faced septa 9 mm magnetic cover and screw cap, pretted with a soft silicone/PTFE seal Blank cap, tin plate, magnetic Composite blue magnetic cap, for 20 mm crimp top vials Composite blue magnetic cap with blue chlorobutyl/PTFE seal, for 20 mm crimp top vials Blue silicone/PTFE seal, for 20 mm crimp top vials Red silicone/PTFE seal, for 20 mm crimp top vials
100 100 100 100 500 100 100 10 100 100 100 100 100 100 100 100
60180-511 60180-513 60180-514 60180-562 60180-515 60180-516 60180-523 60180-524 60180-525 60180-526 60180-517 60180-518 60180-519 60180-520 60180-521 60180-522
Other vials and caps are also available. Please call customer service for more information.
Crimpers
Description North America United Kingdom Europe Japan
60180-527 60180-531
60180-528 60180-532
60180-529 60180-533
60180-530 60180-534
Decappers
Description North America United Kingdom Europe Japan
60180-535 60180-539
60180-536 60180-540
60180-537 60180-541
60180-538 60180-542
163