II 10.

9 C
"/ I '/
II

)f'h

R
1;»

Ic b -"

f (....

L; L

b ~ \,...
I~

In

.r. I J

r: I

nJ~IUC'+/ +:; /
I_

vlL

"

-1-_ -+----I----II-+----+--f--+---~-+-f---I__--_i---+---_j--~J

f' \

1-,

I-l-'F--"-

.+----

"r-

(i(\V\

[; bU, h IJ.., (

p.~

.p

h ,\,

IJ_~

,\1\

r~

.~ 'VI~

f-

~~.
\ ) pl\
h
\

I----/I~-I--~---I--~~--I---~-f----~-!~~-_+-r-r~~--r---I--r----~-l----l-_t----I--I_jI
~
-4 '7

1-1-

~b_

/".1

__[L~~"

_f_

I":J
1"-

_ ....

I"~ ""'r

I
I

P p(
----,

v,
_
I~

J ('"
It r~

<

Ie_.~
) 0

iJ\IJ,-r·
,,.. I

,...

v
/t

Ir',-""

'"

1\

.r-

r: ')

"/

l..J
/

..._ ,
/

L~c.)

H- 1 10
I~

I- 1--I---l-":!:::o.1

t-l

v-

u..

'<;1 e

'I "'"

I 1 _

___
._-_._--_._------------_._.- _._~- -·,..·-,----1--,--,--~-~---

- - - - .__ .--,_ -_----_._-_._-

.-- ---r--

f---I---=I-t

____
f-.

IL=~---±. \! Ir'\ ___ .---t---t--I-.J--.I-J__L -r---+--1--I-':__~I-L.~( (' u :l_ (_,.a.::>1I j "T r.:::1-=l'f \
I

_:=- ~)k~
~ ~ _

CH_ C(~lJt'-i~_)CJ'),.oll...rc. --il--j--i---1f-+___j----+--L-L

I""",, "

=r=r-r--lb,v
j_)

__

.-.--.--.-----------J

..

_-

.1~!&..

1c..Y~.

I ";i~';:" ~QP-~----t-t-f--+-+--+-V-1--I-t-+---+-l---I---).--J--c::-

.L'~r~1(,111r~frdfjL.t++-h~-~-L
r------

UI,~I, \

_.+-+-I--J....-I...-I--r-r-Ir--r-~+++--~~-U--j__ , ,
_
---1--- -

_-=:~I-_~~'~ t-- __
______
__

_g;r='
..J__:_ _.

--~,~-

------c---

-'-T~---~.~
1

f~.~1---_
__.__

__

l1:--f:-r-' =-1.1~~~0-T~l--.--:t~.;-t-;-- 1.C=r--f~./\:....lj··~JQI£~'"/ ...--ft-'tjt---rir--;t--+-I--~"--':~' +-+-+-W--LJ t

---.i--~+_-./-e----L-~ t:L

-I--t-+--l---l-__j ---c---I---I--l__j -1--1-1-1

./ \

'-r-

~--_

'c-I

..

~~~~J i'lt!:- c;m)J:<p;\_~ -t -l-f---.-f---_ ..

c----

-:=- '~-1f~__

t-t;~.r:
C

t: ~

I' / rIP.i, -

--iJ/-/.~ /
-- -I-I--t---l---j-__j_j
.. --~---

it
..

;1} (

(1/

P-~'PJ,-*'_{LfJJlQ,.~-·-'>-><-I--------f/, ..... l-/

~_~:_

-_._-_.- .... _._--------'"-j-I·---I·_·I

-).. _--_._---_ - eli'·· -::Pt%;--'-:__I---t,.J-!, LV ()_-+-b-(-"l' _ -.J_'L;F:'7 IT

L [T
/

-----c---f---I--

c_-

-----c----r--+--+--~--I--LJ

-1-

..-

-1---

ITt'

I ,

~~~~~==~ _

r-[I-r-+-+- f-l-L-J-

[--+--+--1

_l_~_L_L_l_l_lj_JLj_~~

fJ·
.

"

ANALiTiK . KiMY.A-I-: 'I'e~k-FiN~

CEVAPLARI r.. a) 1[){}gn-~Il'~elti~~ll'h:tcmt-:.... Molarite= .. , . Mol.g x Eft:rr, '. iHCiTarite

s.m.A¥1-

.',

5.· Q..:1..19SJ.S.__

Gram

i;Eh'795:g'~i-1-mt-iS'e100 Cf·." ? ml : :::) 100/1,0695 .

= 93,50 ml

= :,

1074,5 x 0,0935 Gram

= r,4356 LYr

olur,

Bu ~o:zeltinin ~oziicii. aglrhgl

Molalite»

(100 - 10 =) 90 grnrndrr, 0 halde:

. '.

Moi.g xtpz .ag.(gram)

7.:f,5x9fJ"

xfovrr
" hulunur,

MoIalite

10

x16oo=
.

1,4914 ~ol:l1

b) hlO-lIYl Cu(N.oj);: cdzeltisinde .. 2xlO~ :r..63.5,=UJ'x.iO·~ ~[J, .Cll:~ ~a.z::dlr.: 1,.17:r1(;';: gIL ::::;. 2,7 mgfL Cu:!+ ve => 12~7 ppm Cu:!" olur. 1
c) I -'1/2

-r '21.: 10'~+·2t12;. lO=:!)l=-3xl(f:! =O;fT3-

V'e'

r::> O;o-i-

otcinganciJ:ll

'+ 10g'/;\I~~

.,

= - . . .' IT

O.5.Z.:1.JT

ve ,,/:...r/'" , log'!C1'=

= lO-O.:!S'o=1 0.. .1 o
1

u -n

0,5.2
.
D.11 0=

1+..;0,03

r;:;-;:;;

.,[0,03..

-O,-79tr 0,513 oIur .. Ayni sekilde , '\

5,129;dO·1";' ve·

0;5.1:1..JO,03 .

Yc,'= 10.
IT. n)

1+.j0Ji3
1

-0,0726

0 01 6 •:

=10· .10°.9:m::=

0,8459= 0,846 olarak bulunur.

"Na::'~OJ:

Zayif Baz ..

N~:HPO~·:

Bazik Amfolit

~~ ..

I
,

H~S04 : ., Kuvvetli .. ~it .•...... A

I'

Na.. ..: -_. .Zavif Bai:.. _._..

.';

. 'f

1 HeN:

=. ~~~lfAsit

N:B:o.+N&CL:..-.- .Taznncn .._.__

. ..__

b):1._ 1- pH'lnn belli bi;'slmra kadar seyrelmeyle degi§mez.· • '1- 2- B elirli' .sirnrl azi.asmayacak.s e.kild.e... uxve.ili:as it.yeja..~ az.ilave.edil di ~ i0 eli.. k pH'Iarindn finemli bir degijiklik olmaz, . . . " ( 3-lQ::l.iy.i ta.rripon.~ilzelti..za..yIf,a.ill.ye...b.un.u.n..tn.zll.kllll1lilllar~!l{ yaprlan; -, tampondur, ve pH~pKa durumun da tampon gii~ maksimurn olur, . . ('-4: Po:. tampou.~Qzel~kl!"andabilm.e.arah~I pH:=pKn+l .rlir., .
........... _

..

"

'._

.\
--< ..
-/1.
0 ,

::) :'/1"r

rt.
.
......

.~ _' ".
.'

....

'

.,.

--.----- .... ~

...

_,.

...

-._

.....

~'-' . .'2.. ;...;~;(

i t_.::' 2

'

".
...
,

ANALiTil(, KIMy..A-I.: 'I'e~k-FiN~ CEVAPLARI

SJNAVI:-

,',

TI. a)

I
I'

H~SO.j :..•. Kuvvetli ..A~it

/ HeN:

NH,:;. .. : __ ·4yliBai:... ~--_. ~+~Cl;_._.Ta.mpQD. ..... __ ••__ b) ~1.. 1- p.H'lari belli hir smrra kadar seyrelmeyle degi$mez. . 'L- 2- B eIirI1.s irnrlari, ~m.n.Yacak_~ ekilde, knzvetli.as it yeja..~ ?:Z-ilaY e.edil d i~n di_ i p'H'Jnz:1.nda 5nemli hir degi§iklik olmaz. '.' .. I 3- ~.iy.i t.arripOD..~5z_elti.za...ylf.asiLye.b.U!Ul.ll..t.u.zJikIlll:li1l1arak ya.p.lian.. -,tamporidur, ve pH~pKa dururnunda tampon gii~ m.aksimum oIur.·· . ("4: Poi. tampon .-;:5zel~k!"Iamlabilme.arah~I pH:=pKa+J .dir. : .

~~~lfA.sit

.................•...•...

.
.

'-. -'.

",.

"-

run)'

NHJ =17g/mol· 'C=4,25! 17 :=O,25lYf 1 ~Cl ='S3~5 gluiO! ... C= 6';4z-t$",s-=cr,~" b) Tampon c;:oze1ti; oIduguna.g5.re..;., ", t, pH pKa;l-l~g r NEJII j'N:EG +J = 9,24+Iog 0,25" 0,12 == 9,56 7. c) NHj+ B; -;..NEt . " NEfJ!- azalad.. , I- Nfu<:1- xrt:rcakttr." :1.00xO,25 15xO,Ol 15xO,Ol

:1

P H =9 2...+ Dc
A • ' b

I'

[JOO:r-IJ,25-15xO,Ol)IJJ5 9'2' 7 24,85·'9--.rz_ ::;: "I + log-- = ,.)) (JOOxO;12'+ J5rO,O'J)/ 115-' 12,15--' . , ;.~NR.t~ a.z.ahca.1c,.~t-t~,,~'.'L· . /.. . 15"0,01

0) N&:+O!;L ...,....,. N&-+.;EI:Q.

HlG'{),12 15xO,\n

GO

FOTOKOpi

33934 60

@.:..
,

t-":«

."
.

=)',{"1/
:

!.L_ .

'"

.'.:.sc... :':').~ . " ..

.
"

'_

,~.

. - .,.

..

:._ ". :__.c (.,

-_....

. :.'
'

-_ _
..

-_ .

__ - _ _-_-.
...

..

,;.~ ..• , ,

•. (:-:.

• J'

pE ==9 2::+[00' .1._ O(lOO;cO.12-15:dJ,Ol)IJJ5

.

. '( 1.DOxO.25.-7: 15xO,Ol) /115

:::

9 :.,., r .25,159---;-+ ,0'7'--::: J I

~"j

.!

..

On,C)5

'.,

e! 9,00
-

= 9,24+1og ,.

0,25 _ rt: z, ""'1 L 1\rt-.Jt,. I

:::::>

- O'''~==- Icz

,_::NHJ;1 l :I

or ,_J

/jY'H:Ct. '.t

= (fA3'<f~r,_.~rriralI>
r

L..
iL1_Ye,edilmelidir,

O;434-0,12'~_ 0,314, 1\1 d~b.~ ~yaD.i 0,314::63,5

= 16,80

gram

daha .fl~CI

n:..

IlYr~~+ S" 1== 1,4:r.1Q-is oldugundan 1-.1 CdS .~5kecegi' anI~~i!fr. a) MnS'ii.o.. ~61-aIleJ'ebaslamasr.icin.gereken asgari pH;' .: .ortamdaki IlYIn::!+ = 1M oIdug~ndan 'j S~ l,4::t10,1: NI' oIur ... . .' I:r;,lO .... --:r
. IV.

. I Cd~+ 1.'1 S~ I = 5,01.10-:!1 ve

burada

once

I:;;

I HJO+ I :::.(1,4x.lO,I,5)=lxlO·::J've

' buradan

I :8::;0+ I""

l,-fxl 0-:'- .

S,45ilO-s

M ve 'pR=4,CJi

1 l·~cin" ortamdan.Jcantitatif .' Is-I der#i rni .. 1 '?' , I s] =' (5'<10''')'1

) ,

olur, '. . b). Cd:+

S:I-I~:,r
.

. aynlmasi

:. . ., yam CdS·iin.~ tam s:5kclmesL icin, gerekli., (I O~) = 5<10:" M d.r.

'.

"~'

, ~

~C'

B u nokta daki

I R,O +1

d erisirni

'\:._

.0

.c C

, ,pH = 1,35 bulunur. " "'\ ',', . ..,', c) .pH=3,ya da,·1 H;;O":{=H).:Ji\l- durumuada : = lQ.·:!Jf 10--6::; 10:17 lYI o-lHF_Ort.am-daki1T C.c!:!-t-deri~j.mi ise Cd::'" ~ ~(5xl.0-::1) I filO- ,= 5x1o.~lU aIue... ~ratikp! slfl~dlr. , M .'

IHlO"'/:!=(O,b:10;=)/5i10'Zl=

a;d9·J"·ye

Ise

·/B.:JO+-/=4,47xio·::M o!t:;r.Budur~rr{d:ld~

'-...:.

;IJi~.~-I,~S::"JI Qi' J'd en, = 1x1

. ·./f:;, ',J

Is-1~

Vl

V. a).B rind tepkimenin indirgenrne istegi lkinci tepkimenin indirgenme istegi.nden . buyiik 0 dtigundan birinci' tepkime aynen kata:cak,iKinci tepkime ters cevrilip thr::r.f--, ,tarafa planacaknr. ' ,. o '_ X;'O-, ~- -k 14K. +' -:;.:=:! zx" 4: 7~O, . E ;(.= t,lEb,¥o . y::+ .;:::=:: ,y:}+ +e ' ·E y =-0;90 v

5~:

K =10m

,.u'

,"10(6;<0.;95)10.0;59.=,10.30

"

bulunur,

,b) Y~ettge~~~,~~~j
Etilalkol' (3p)-

C.:lHsOH,.L:.=4--G~&g_~
' ....:::,,;_~~~4 +:!H

en.kwnlr;g~lp )'i.:Ici~,~~,~,~~~:~ .. ~X~~~,!l!!!~i (~ ~

'~'-" .--.~ -~ -0

.(,'....Rt~., .. ~
•

..

).

: ... El:ifa~f:

asetilC asif

'.

c) A$aglCI.aki.bo~(~.dol.d~u;z;:Standart hidrojenyari pi! gerilimi :.••'l"Atm ..•.... basmc altmda ,,:e ...1M_: E", .derisiminde - .......sifir....:.... - almzz., . ..... (2p)- ~lektrokimyasa1 (redoks) pillerinde denge duriirnuna pil geriliminin ..•• sifrr ..•.•_. oldtigiii:ld:f uIa.~tllf. '+ _, 0 0 + . 0 . (lp)-Ag- ,+ e Ag ..,. E = O,80,:y-, ise,-, 2A.g +e~·--.--? -lAg; .. Eo =...080 v''d' Ir.
I .

.. .
'

_'.

.. ~ . '" .

ANALITIK KIMYA-l· Tee-rik- B-UTUNLEME

SINA¥J
I ,----I ---'

O·D· 0 -

..,;_imZ:t_·

ogunlugu 1,80 olan .%98 'Iik siilfiirik asit ~oze1tisinin molarite ve ' .hesaplaymrz, (R~SO.;.. = 98 glmo} ). .... a'daki derisik siilfiirik asitten-hareketla, 250 ml 1,44 N konsantrasyonda bir . ........u.w.........,......... lfin_ derisik,a sitteo ~ ml.alin m ah d.tr? . •c) b' . hazrrianan asit ~9zeltisi~in iyonlk kuvvetini buIunuz .

...a!:!l~~~,,~,

,41\'1 HeODR ve lLYf.RCOONa: hulunan bit; ~ozelti ele al.1ruyor.HCOOR a=· ,75 olduguna gore: . -'f '-IN'-F--J<"":'j::£U ~ozeltin.in pH'lUl bulunuz. . :$('4 S +-- 0 C?c y b),Bn ~ozeI1j 59 defa seyreltiIirse , cJ 'Bu. s:;ozdti .10000 defa, seyrelrilirse, oze1ligioi korur mu? .Resap_yap.2..rak osteriniz. "

GUm iJ}iin '~~J'nyahla v~l=digi ko'R'lpkkskrla. kararhhk ·samtJ.eri K1-;2:101o! : ve.: =81.10 olduguna gore; I.NEJI = IlYI clan. bir ~ozeltide ,saf sudaki ~oriinurliik 'rIHID1 ~ =1:5.1:10-16 olan' giim U$ iyodiiriin s:oziinifrfiigfinu hesaplayip sar SUOaKf' 'ziiniirIiiguyle karstlastrrinzz, . , IO b)'2S(lC da f giimu¥ kkI:riiriJ.n sm: sudaki. y01:~;nUT!ii~ puplUn ~ = 1,56:do.: oIdng-una.· gore O,OlM ~ozeltisindeki AgO 'fin molar: s:oziiniirlugu~i.i hesaplayxoxz.
3

3tlp);a)

xxo,

~ ~
)

1.

~~E.g:d.s. yarr.pil reaksiyonlan, veziliyor ; _ ..,.-y+ • _ ~ ....,..:i::, -_ EIS:; =J.,59 V X 0" + 8.u .,..:J e+===!=.·,?\, -r- 4.ttl V J~. • "Ul+ £1)7 =1:,00 ':"" 0) ..,.. e-....---. L. Y sonra L\_E0 ve K· Kendiliginden olusan reaksiyonu bulduktan

denge sahitinl

. ulunuz,

I f
I

,j

.. .. :. b)(4p). YUkseltgen;yiiJweltgeum.e. terirolecini ~otnek vererek aciklaynnz,

. .c) (6p) Nernst bagmtlsllH ,bftgmtJdaki te~nr1eri. aciklayarak yazmrz, .

. £'

.;:::.. ~ ri:
;

:;;:-0 .' {) 'ott4: [0 _,___.

I

.!"\

1\.."

{Ii e.Z6I(
___

i\

'.

:."'!.'

.1

}{J1 ...J>.;d-.NALiTiK KjiYlTA I Teartk Find

CEVAPLARI:
L(l5p) a) 1ml cozelti
SlnflJll

-S:Jj/0.
21 .1. 1997

1,0309 gram olduguna gore:

500/1,0309
'-.ih

500 g cozelti hacrni ..... , Cozeltinin Iviolari:esi .....

_

= 485
--"--

ml
5

= 0,435
'

L.

!y -

gram mol gxl:

IOIxOAS5

. 5/

Cczeltinin Molalitesi ...... b),l LitredeO,10:21

grcmrlOOO . idO(]O ,n= llIol.gxf 6::a if, = 10 1.r(5CO-5)

m=O,lOOO mala! olur

.'

5/
':l

mol }-:NOj olduguna.gore

llitrede

..... O,102Ix39=3.9819g1Ll'Cve

.z.,

3,9819 gIL K" _. 3981,9 rng/L K+ 398 I 9 porn K+ olur. II. (12p) HNO) :Kuvvetli asit 2/ (HCOOH+RCDONa):' llimpon . CH:;CQONa: Zayif baz ..::.n·h2f:1PQ : ..-Bazik arnfolit.; . HeN: Zayif asit ..2/ KOH: Kuvvetli baz, _ . III. (lSp) a) C6HjCOOH 122 g/mol "; M - 1,83) 122x 1 0,0'15 iVI ASlt Csli:sCOONa ~144 g/ .I' M = 4,32/ 144x l. =0,030 M Tuz(=baz) b) Tampon yozeltidir = Ka+1og[tuz I asit =4,2+1og(0,03/0,O 15)= 4,5 olur. c) CoHsCOOH + OK -7 C6Hj~OQ.: +H:!O IOOxO,015 10xO,10 10xO,10.
->,

pH= 4,2

10g[(1 OOxO,03+ 1OxO, 10)/11 O]l[(100xO,015-1 OxO, 10)/11 0] =4,2+log( 4,0/0,5)=5,1 d) C6HjCOO- + H30+ -7 CJi5COOH + H20 100xO,030 lOxO,l 10xO,W.

olur.

':'!

pH= 4,2+ log[( 100xO,030-1 OxO,1 0)/11 0] / [(IOOxO,015+1 OxO, 10)/11 0]=4,2+1og(21:2,5)=4, IV.(:20p) a) 1Cd:!·' Is-I = 5x10·21 ve I Mn:-l I s-l = I, 4xlO·l~ 1f6~e.r. Cd:Z~run kantitatif olarak cokmesi icin gerekli S' derisirni

1 olur.

V.

,./'-

oldugundan

once CdS

I s -I = (5x:l O·:!1)11 0'" =5xl0·:1 M dtr. H1Siyin Ka=clH30+11 Js-I)l!H:zsJ == Kal.Ka2=(9,lx10.a).(I.lxIO·lj)=lxlO·:!2~ ve iHzsl =0,1 M oldugundan Cd2" rim tamarnen ,;okmesi icin gerekli Is-I =5xlO-21
derisimi IH]of!=(I-hS).(lxlO·:!:!)/(S-)=(O,l veiHJO+I=4,47xlO- M ; pH=-log4,47xlO,z=1.35 OIUf.
2

noktasmdaki

IH:;oi

M c>: xlxlO·~)/5xlO·z. =2xl0'~

b) Mn2"

=lM

oldugundan

·IMn2+I!S~'=1.4xlO·l;I ;

bulunur.IH:zSl=o,lM
=(lxlO·:!2.0: 1)11,4xl0'
1$ •

ve

IH;;o···i== 3.45xl0·~

Is"'I=(1,4xlO·I.5)I1=l,4xtO,uM (iH;o+I:Z.ls-I)/IH:zsl=l:do':!:! ve lH;:o12

ve M : pH == 4,07 bulunur .

. V.CIOp) a) C;ozeltideki denge

Ag(CN)2' 6 Ag~ + 2CN"

Denge durumunda
.....

IAg"l;;;;:
'\

5,6;.;:1o' M

;I CN"' = 21

Ag+ J == 2x 5.6xlO·1I =11 ,2x1 O·:!M

_;...;...!!...:_···_w:..............

..

1 Ag(CN); 1~ 1 Toplam

Ag(CN);

1 -I

Aynsrrus Ag(CN);

1~

0,05 - 5, 6x 10-' ;; 0,05 M

K== [Ag) [CN"]2/ [Ag(CN):r']:::;(5,6xlO-Z) (l I,2xlO'?! b) K =(AgJ [NHJf! x=[Brl=(Ag(NH:;):rl [Ag(NHJ)::!"] = 6,8x10' olur. ~=[Agl[Br] s

0,05 == l,4xlO':!o

bulunur.

ve cozunen AgBr mol sayisi x olsun, dan [Agl=(5,OxlO-13)lx den

olur,

Aynsrna sabiti denkleminde yerine konursa : 6,SxlO":::: [(5x 1O·':;/X).2:!] / x

=19,4xlO..o ve x =5,41xIO'3 M olur, Yani 5,41xlO-) mol AgBr ya da -5,42xl0·J rnol/L x188 glmo! = 1,01 g/L' AuBr ~6:;::unGr. x2 =(5xlO·13 x4)/6,8xlO'& VI.(15p)

Q) _Mtl+ + /3;
--4 II..:; -+0

a3~ ----:'7 Iv/nuy

_"';>

o
. -:

\Ji'
.' I

1-1

I-A: i" ~

iVf.n_ 'I' + :; n :

+ 8; 3

of-

;" / .. I

rl·!

f ..

r . If

.I uPI? jyt

t i.~ "

\. II

I,. l.k:

5/

~/
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1-)NUMUNE,ANALiTCOZELTi VE GUVENiRLiK NEDiR? 2-)VOLHARD YONTEMiNi ACIKLAYINIZ?(ANALiTiKLABKiTABrNDAKi. GiBi iSiTIVOR) . . 3-)DEFTERDEKi VOLHARD SORUSU Ag+CI. .. ~.~ AgCI Ag+SCN ... ;.. AgSCN Fe+3+SCN(FeSCNt2 4-Potonsiyemetride kullamlan elekrotlatlar snnflandmn ve aciklaymiz.) 5-Gravimetrik faktor hesaplamasi 6-Defterdeki ve kitaptaki KMn04 redoks tepkime sorusu. 7-1.2 grram ornekte safsizhk bulunrnaktadir.O'.l N HC1sozeitisi yardimiyla 25 ml ornek ffile titrasyonda 30 ml HCI sarfiyat aym yozeltiyemetil oranj konuldugunda 5 ml sarfiyat harcadlgml gore.Safsizhk nedir? .8-Deri~imi 0.05 olan KAg(CN)2 90zeltiside [Ag+] denge deri~imi5.6*1 0-8 oldugtina gore Ag(CN)2- iyonun aynsma sabiti nedir..(Emrahhocanm notunda varkompleksmedengeleri) 9-0.1 N50ml NaOH ileO)N HCItitrasyon tepkimesi a-45ml sar. Ph .. b-51 mlrsar Ph .. c-iridikatorun hatapaYl %0.1 oldugunda ph nedir hesapayiniz.

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