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basic heat treatment procedure, its principles and why it is necessary to heat treat the steel. The previous articles have reviewed "What is Steel" and the "Influence of Alloying Elements on Steel." This article and the next three articles will focus on the basic principles of heat treatment such as:
The definitions of processes. Their meanings and selection. Quenching. Surface treatments, including nitriding up to thin-film depositions. Quality control. Troubleshooting.
It is stable at room temperature. It is magnetic. It can have a shiny finish. In other words, it polishes to a bright shine. It has a high density (it is heavy). It is ductile (it can bend or be shaped easily).
Consider a straight vertical line as being an iron and temperature line combined. If we look at the line in the vertical configuration at room temperature, the iron is stable. To understand what happens to iron when heat is applied, you must first know about ferrite, a condition in iron that has a number of inherent properties at room temperature such as a large grain size, a low hardness, good ductility and is easily machinable. The ferrite condition exists in a particular crystal form and will exist at low temperatures. Iron is therefore made up of millions of tiny crystals much like sugar or salt. Those crystals are bound together in what is called a lattice structure. The ferrite condition of iron can be compared to water, or H2O to be more precise. H2O exists in three forms: ice, liquid and vapor. Each of the three phases or conditions is still H2O, but they each exist in a different crystal form. Similarly, ferrite is one of the conditions of iron. As heat is applied to iron, a number of things begin to happen to the shiny piece of steel that is being heated. The oxygen in the air will begin to react with the shiny surface of the iron to form Iron Oxide. As the temperature is
increased, the reaction between the iron and oxygen becomes more aggressive, and a visible product begins to form on the surface of the iron, which is known as scale. Once the steel reaches an approximate temperature of 1,350xF, a change in the structure takes place as well as the phase. The phase changes from ferrite to austenite. In addition to this, the crystal structure changes from bodycentered cubic to face-centered cubic. An indication of the change occurring is that the ion will lose its magnetic property, which can be seen by testing the surface of the steel with a magnet. Protect your hand and fingers when testing for the loss of magnetism from the hot steel (see Figure 2)
What Is Annealing?
Annealing is the process of heating the steel to a particular temperature in the austenite region and cooling down the steel very slowly. There are many derivatives of the annealing process, but generally the process is a slow cool process. Another derivative of the annealing process is known as sub-critical anneal. This process involves soaking at a temperature below the lower transformation line, in the region of 1,200xF to 1,300xF, until the steel has equalized across its cross-section in temperature, followed by a slow cool. Slow cooling can mean a cooling rate between 5xF per hour up to 50xF per hour. As can be imagined, the cooling period can be a considerable amount of time. It should be noted that the nickel alloyed steels and the A series tool steels should be cooled very slowly, as nickel will cause an air-hardening effect.
Bright Anneal. This method is a method of annealing which uses a protective atmosphere to prevent the steel surface from oxidation.
Process Anneal. This procedure is done at a temperature close to the lower critical line on the iron carbon diagram. Sometimes confused with sub-critical annealing, it is used when considerable cold working is to follow. Recrystallization Anneal. Once again, this is a process often mistaken for subcritical annealing. It is used after cold working to produce a specific grain structure. Sub-Critical Anneal. This method is used on cold-worked steel and is carried out below the lower critical line on the iron carbon equilibrium diagram. It is sometimes applied to tool steels that have been over tempered and require annealing before hardening and tempering. Spheroidize Anneal. This process is a controlled heating and cooling procedure to produce spheroidal or globular cementite particles. It is usually applied on high carbon steels for good machining characteristics such as high alloy steels and tool steels. Isothermal Annealing. The process temperature of this procedure is determined by knowledge of the steel's carbon content. The steel is then taken to that temperature and cooled down to a holding temperature that allows the steel to transform isothermally. Full Anneal. This is a process that involves raising the steel's temperature up to the sustenite region followed by a slow cool.
What Is Normalizing?
Normalizing is a process that makes the grain size normal. This process is usually carried out after forging, extrusion, drawing or heavy bending operations. When steel is heated to elevated temperatures to complete the above operations, the grain of the steel will grow. In other words, the steel experiences a phenomenon called "grain growth." This leaves the steel with a very coarse and erratic grain structure. Furthermore, when the steel is mechanically deformed by the aforementioned operations, the grain becomes elongated. There are mechanical property changes that take place as a result of normalizing - inasmuch as the normalized steel is soft, but not as soft as a fully annealed steel. Its grain structure is not as coarse as an annealed steel, simply because the cooling rate is faster than that of annealing. Usually the steel is cooled in still air and free from air drafts. The process temperature is virtually the same as for annealing, but the results are different due to the cooling rate. The process is designed to:
Give improved machining characteristics. Ensure a homogenous structure. Reduce residual stresses from rolling and forging. Reduce the risk of "banding." Help to give a more even response to the steel when hardening.