SCOPE OF ACCREDITATION

Bodycote Materials Testing Canada Inc. Drayton Valley Laboratory 7407 Twp Road 485 P.O. Box 7706 Drayton Valley, AB T7A 1R7 Accredited Laboratory No. 296 (Conforms with requirements of CANP4E (ISO/IEC 17025:2005))

CONTACT: TEL: FAX: EMAIL: CLIENTS SERVED: FIELDS OF TESTING:

Mr. Michael Hooey (780) 5426812 (780) 5424844 michael.hooey@bodycote.com All interested parties Chemical/Physical

PROGRAM SPECIALTY Environmental AREA: ISSUED ON: VALID TO: 20080520 20110707

ENVIRONMENTAL AND OCCUPATIONAL HEALTH AND SAFETY

Environmental Soil/Sediment (Boron Soil [035])

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Standards Council of Canada Accredited Laboratory No. 296

SC20; based on MCKEAGUE 4.61; STANDARD METHODS; ICP APHA 3120 Boron (Conductivity Paste [064]) SC5/WC15; based on APHA CONDUCTIVITY METER 2510 B Conductivity (Major Ions Paste [061]) SC5/WC75; based on APHA ICP 3102B; EPA 6010 Calcium Magnesium Potassium Sodium (Major Ions Paste [062]) SC5/WC25; based on USEPA ION CHROMATOGRAPHY 300.0 Chloride Sulfate (Major Ions Soil [041]) SC5/WC25; based on MCKEAGUE 3.21 AND 4.13; ION CHROMATOGRAPHY EXTRACTION USEPA 300.7; USEPA 300.0; APHA 3120; APHA 450H+B Chloride Sulfate (Metals Soil [032]) SC15; based on EPA 3050; APHA 3120 B; EPA 6010 B ICP DIGESTION Antimony Barium Beryllium Cadmium Chromium
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Standards Council of Canada Accredited Laboratory No. 296

Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thallium Tin Vanadium Zinc (pH Paste [063]) SC5/WC10; based on APHA pH METER 4500H+B pH Soil/Sludge (BTEX Soil/Sludge [056]) GC50+SC70/SC75; based on SPME VARIAN APPLICATION GCFID (LEACHABLE) NOTE1+NOTE3 ANDSYPEKO APPLICATION NOTE Benzene Ethyl Benzene m,pxylene oxylene Toluene (Metals Soil/Sludge [057]) SC75, SC70, WC70, WC80; based on USEPA 1311: TOXICITY ICP (LEACHABLE) CHARACTERISTIC LEACHATE PROCEDURES Antimony Arsenic Barium Beryllium Boron Cadmium
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Standards Council of Canada Accredited Laboratory No. 296

Chromium Cobalt Copper Iron Lead Mercury Nickel Selenium Silver Thallium Uranium Vanadium Zinc Zirconium (Microtox Soil/Sludge [033]) SC6/SC55; based on AECV94G1 BIO LUMINESCENCE Microtox EC20 (15 min) Microtox EC20 (5 min) Microtox EC50 (5 min) Microtox EC50( 15 min) (pH Soil/Sludge [055]) SC6; based on USEPA VOLUME IC CHAPTER 6, METHOD 9045C15

SOIL+WASTE pH 1:1 EXTRACTION pH

Water (Inorganic) (Alkalinity Water [014]) WC5; based on APHA 2320 B AUTO TITRIMETRIC Alkalinity (pH 4.5) (Chemical Oxygen Demand (COD) Water) WC60; based on APHA 5220 COLORIMETRIC D COD (Chromium (Hexavalent) Water)
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Standards Council of Canada Accredited Laboratory No. 296

WC85; based on APHA 3500 COLORIMETRIC Cr D Chromium (Hexavalent) (Conductivity Water [008]) WC15; based on APHA 2510 CONDUCTIVITY METER B Conductivity (25C) (Dissolved Metals Water [010]) WC80,WC70; based on APHA 3030B/3120 B; EPA 6010 B

ICP Dissolved Aluminum (High) Dissolved Barium (High) Dissolved Chromium (High) Dissolved Cobalt (High) Dissolved Copper (High) Dissolved Iron (High) Dissolved Lead (High) Dissolved Manganese (High) Dissolved Molybdenum (High) Dissolved Nickel (High) Dissolved Thallium (High)

(Fluoride Water [047]) WC11; based on APHA 4500 SELECTIVE ION ELECTRODE FC Fluoride (Major Ions Water [002]) WC25; based on USEPA 300.0 ION CHROMATOGRAPHY Chloride Sulfate (Metals Water [009]) WC75; based on APHA 3120 ICP B; EPA 6010 Calcium Magnesium Potassium
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Standards Council of Canada Accredited Laboratory No. 296

Sodium (pH Water [007]) WC10; based on APHA 4500H+B pH METER pH (Total Suspended Solids (TSS) Water [012]) WC35; based on APHA 2540 GRAVIMETRIC D Total Suspended Solids Water (Organic) (BTEX Water [046]) GC15 rev. 2.0; based on ASTM652000 GC/FID EXTRACTION Benzene Ethylbenzene m/pxylene oxylene Toluene Water (Toxicology) (Microtox Water [006]) WC65+WC10; based on AECV94G1 BIO LUMINESCENCE Microtox EC 20 (15min.) Microtox EC 20 (5min.) Microtox EC 50 (15min.) Microtox EC 50 (5min.) Microtox IC50 (15 min)

NON METALLIC MINERALS AND PRODUCTS Petroleum Crudes and Natural Gas: (Gas) GC105
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Standards Council of Canada Accredited Laboratory No. 296

Determination of Hydrogen Sulfide (H2S) in Gas by Tutweiler (Glycol) GC65; based on ASTM E20294a Analysis of Glycol Compounds by Gas Chromatography: Ethylene Glycol; Diethylene Glycol; Triethylene Glycol; Tetraethylene Glycol

OC55, based on ASTM Freeze Point 117794 WC105, Based on APHA 4110 Ion ChromatographyDionex 100Glycol: Chloride CCB content (ppm) (Liquid/Fluid) GC25 AmineGC: Monoethanolamine, Diethanolamine, Triethanolamine, and Methyldiethanolamine

(Natural Gas) GC95, based on DS 651 Gas Analysis by Gas Chromatography: Hydrogen, Helium, Oxygen, and Nitrogen GC95; based on GPA 226195 Gas Analysis by Gas Chromatography Hydrocarbons: Carbon Dioxide, Air, Methane, Ethane, Propane, iButane, nbutane, iPentane, nPentane, Hexane, Heptane. (Oil) GC70; based on ASTM D5307 GC75; based on ASTM D5307 OC10; based on ASTM 1298 OC15; based on ASTM 4294 OC20; based on ASTM D97 OC25; based on ASTM D445 OC30; based on ASTM D86 OC40; based on ASTM D128 OC45; based on UOP 46 OC5; based on ASTM D9694 (Soil Sludge) SC 51; Based on ASTMD93 (Water) WC100; based on ASTM Refractive Index
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Hydrocarbons C2 > C30+ Hydrocarbons C10 > C60+ Oil Density by Digital Density Meter Total Sulfur Content in Oil Pour Point Viscosity (Saybolt 20 to 50) Distillation of Hydrocarbons Asphalthenes in Hydrocarbons Wax Content in Hydrocarbons Basic Solids and Water: Sediment %; Water %

Closed Cup Flash Point

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Standards Council of Canada Accredited Laboratory No. 296

D1218 (Water, Oil) OC35; based on ASTM D93 Flash Point Closed Cup

Notes: CANP4E (ISO/IEC 17025): General Requirements for the Competence of Testing and Calibration Laboratories (ISO/IEC 170252005) CANP1585 Guidelines for the Accreditation of Environmental Testing Laboratories GC#, OC#, WC#, SC#: Subject Laboratory inhouse Test Methods.

P. Paladino, P. Eng., Director, Conformity Assessment Date: 20080520 Number of Scope Listings: 42 SCC 100315/361 Partner File #0 Partner: SCC

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