RRC Water Samples 2

ANALYTICAL REPORT
March 13, 2019
Terracon - Austin, TX
Sample Delivery Group: L1075168
Samples Received: 03/04/2019
Project Number: 96187C01
Description: Boundary Ventures, Inc.
Report To: Brian Mann

5307 Industrial Oaks, Suite 160
Austin, TX 78735
Entire Report Reviewed By:

[Preliminary Report]
Chris McCord
Jason Romer
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National
is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com

TABLE OF CONTENTS ONE LAB. NATIONWIDE.
Cp: Cover Page 1 1

Cp
Tc: Table of Contents 2
2
Ss: Sample Summary 4 Tc
Cn: Case Narrative 11
3
Tr: TRRP Summary 12 Ss
TRRP form R 13 4
Cn
TRRP form S 15
5
TRRP Exception Reports 16 Tr
Sr: Sample Results 17
6
MW-1 L1075168-01 17 Sr
MW-2 L1075168-02 19 7
Qc
MW-3 L1075168-03 21
8
MW-4 L1075168-04 25 Gl
MW-5 L1075168-05 27
9
MW-6 L1075168-06 29 Al
MW-7 L1075168-07 31 10
Sc
MW-8 L1075168-08 33
MW-9 L1075168-09 35
MW-10 L1075168-10 37
MW-11 L1075168-11 39
MW-12 L1075168-12 41
MW-13 L1075168-13 45
PSW-1 L1075168-14 49
PSW-2 L1075168-15 53
PSW-3 L1075168-16 57
PSW-4 L1075168-17 61
SK-1 L1075168-18 65
DUPLICATE 1 L1075168-19 69
PS-1 L1075168-20 73
PS-2 L1075168-21 77
PS-3 L1075168-22 81
PS-4 L1075168-23 85
PS-5 L1075168-24 89
Qc: Quality Control Summary 93
Gravimetric Analysis by Method 2540 C-2011 93
Total Solids by Method 2540 G-2011 96
Wet Chemistry by Method 2320 B-2011 98
Wet Chemistry by Method 300.0 99
Wet Chemistry by Method 9040C 101
Wet Chemistry by Method 9050A 103
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

Terracon - Austin, TX 96187C01 L1075168 03/13/19
03/13/19 15:42
16:10 2 of 161
ONE LAB. NATIONWIDE.
Wet Chemistry by Method 9050AMod 104 1

Cp
Wet Chemistry by Method 9056A 105
2
Mercury by Method 7470A 106 Tc
Mercury by Method 7471A 107
3
Metals (ICP) by Method 6010B 108 Ss
Metals (ICPMS) by Method 6020 109 4
Cn
Volatile Organic Compounds (GC) by Method 8021B 111
5
Volatile Organic Compounds (GC/MS) by Method 8260B 114 Tr
Volatile Organic Compounds (GC/MS) by Method 8260C 126
6
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 134 Sr
Semi Volatile Organic Compounds (GC/MS) by Method 8270C 138 7
Qc
Semi Volatile Organic Compounds (GC/MS) by Method 8270D 145
8
Gl: Glossary of Terms 155 Gl
Al: Accreditations & Locations 157
9
Sc: Sample Chain of Custody 158 Al
10
Sc

03/13/19 15:42
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SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time

MW-1 L1075168-01 GW Cody 03/01/19 14:45 03/04/19 09:00 1
Cp
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time 2
Tc
Gravimetric Analysis by Method 2540 C-2011 WG1246056 1 03/07/19 19:53 03/07/19 23:39 AEC Mt. Juliet, TN
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 14:32 03/07/19 14:32 GB Mt. Juliet, TN 3
Wet Chemistry by Method 300.0 WG1245159 1 03/06/19 09:41 03/06/19 09:41 ELN Mt. Juliet, TN Ss
Wet Chemistry by Method 300.0 WG1245159 50 03/06/19 02:30 03/06/19 02:30 ELN Mt. Juliet, TN
4
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN
Cn
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 09:41 ABL Mt. Juliet, TN 5
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 20:39 LD Mt. Juliet, TN Tr
Volatile Organic Compounds (GC) by Method 8021B WG1245228 1 03/05/19 18:46 03/05/19 18:46 BMB Mt. Juliet, TN
6
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1246143 1 03/06/19 23:14 03/07/19 18:03 FM Mt. Juliet, TN
Sr
Collected by Collected date/time Received date/time 7
Cody 03/01/19 15:15 03/04/19 09:00

Qc
MW-2 L1075168-02 GW
Method Batch Dilution Preparation Analysis Analyst Location 8
date/time date/time
Gl
Gravimetric Analysis by Method 2540 C-2011 WG1246056 1 03/07/19 19:53 03/07/19 23:39 AEC Mt. Juliet, TN 9
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 14:44 03/07/19 14:44 GB Mt. Juliet, TN Al
Wet Chemistry by Method 9040C WG1245130 1 03/05/19 11:55 03/05/19 11:55 TH Mt. Juliet, TN 10
Sc
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 09:48 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 20:43 LD Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245479 1 03/05/19 17:08 03/06/19 06:05 DMW Mt. Juliet, TN

MW-3 L1075168-03 GW Cody 03/01/19 15:45 03/04/19 09:00

date/time date/time
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 14:51 03/07/19 14:51 GB Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260C WG1245356 1 03/05/19 20:32 03/05/19 20:32 GLN Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1246279 1 03/07/19 07:27 03/07/19 16:39 JF Mt. Juliet, TN

MW-4 L1075168-04 GW Cody 03/01/19 16:30 03/04/19 09:00

date/time date/time

03/13/19 15:42
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MW-4 L1075168-04 GW Cody 03/01/19 16:30 03/04/19 09:00 1
Cp
Tc
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245479 1 03/05/19 17:08 03/06/19 06:37 DMW Mt. Juliet, TN 3
Ss
4
MW-5 L1075168-05 GW Cody 03/01/19 16:15 03/04/19 09:00 Cn
5
date/time date/time Tr
Sr
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN Qc
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 21:07 LD Mt. Juliet, TN 8
Gl
Volatile Organic Compounds (GC) by Method 8021B WG1245643 1 03/06/19 04:13 03/06/19 04:13 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1246143 1 03/06/19 23:14 03/07/19 18:20 FM Mt. Juliet, TN 9
Al
10
MW-6 L1075168-06 GW Cody 03/01/19 16:00 03/04/19 09:00 Sc
date/time date/time

MW-7 L1075168-07 GW Cody 03/01/19 12:45 03/04/19 09:00

date/time date/time

MW-8 L1075168-08 GW Cody 03/01/19 11:35 03/04/19 09:00

date/time date/time

03/13/19 15:42
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MW-8 L1075168-08 GW Cody 03/01/19 11:35 03/04/19 09:00 1
Cp
Tc
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN 3
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 10:08 ABL Mt. Juliet, TN Ss
4
Volatile Organic Compounds (GC) by Method 8021B WG1248019 1 03/11/19 13:24 03/11/19 13:24 ACG Mt. Juliet, TN
Cn
5

Tr
MW-9 L1075168-09 GW Cody 03/01/19 11:15 03/04/19 09:00
6

Sr
date/time date/time
7
Gravimetric Analysis by Method 2540 C-2011 WG1246058 1 03/07/19 19:43 03/07/19 23:09 AEC Mt. Juliet, TN Qc
Wet Chemistry by Method 300.0 WG1245159 1 03/06/19 05:35 03/06/19 05:35 ELN Mt. Juliet, TN 8
Gl
Wet Chemistry by Method 9050A WG1245735 1 03/07/19 13:22 03/07/19 13:22 BAM Mt. Juliet, TN 9
Mercury by Method 7470A WG1245002 1 03/04/19 19:15 03/05/19 10:10 ABL Mt. Juliet, TN Al
Volatile Organic Compounds (GC) by Method 8021B WG1245643 1 03/06/19 05:38 03/06/19 05:38 DWR Mt. Juliet, TN 10
Sc

MW-10 L1075168-10 GW Cody 03/01/19 12:15 03/04/19 09:00

date/time date/time

MW-11 L1075168-11 GW Cody 03/01/19 13:15 03/04/19 09:00

date/time date/time

03/13/19 15:42
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MW-12 L1075168-12 GW Cody 03/01/19 13:45 03/04/19 09:00 1
Cp
Tc
4
Cn
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 21:39 LD Mt. Juliet, TN Tr
6
Sr
7

Qc
MW-13 L1075168-13 GW Cody 03/01/19 14:15 03/04/19 09:00
8

Gl
date/time date/time
9
Gravimetric Analysis by Method 2540 C-2011 WG1246058 1 03/07/19 19:43 03/07/19 23:09 AEC Mt. Juliet, TN Al
Wet Chemistry by Method 300.0 WG1245159 1 03/06/19 10:59 03/06/19 10:59 ELN Mt. Juliet, TN 10
Sc

PSW-1 L1075168-14 GW Cody 03/01/19 17:10 03/04/19 09:00

date/time date/time

PSW-2 L1075168-15 GW Cody 03/01/19 17:15 03/04/19 09:00

date/time date/time

03/13/19 15:42
16:10 7 of 161

PSW-2 L1075168-15 GW Cody 03/01/19 17:15 03/04/19 09:00 1
Cp
Tc
Volatile Organic Compounds (GC/MS) by Method 8260C WG1245979 1 03/06/19 16:03 03/06/19 16:03 GLN Mt. Juliet, TN Ss
4
Cn
Cody 03/01/19 17:20 03/04/19 09:00

Tr
PSW-3 L1075168-16 GW
date/time date/time
Sr
Gravimetric Analysis by Method 2540 C-2011 WG1246059 1 03/07/19 20:03 03/08/19 01:53 AEC Mt. Juliet, TN 7
Wet Chemistry by Method 2320 B-2011 WG1245955 1 03/07/19 16:34 03/07/19 16:34 GB Mt. Juliet, TN Qc
Gl
Metals (ICPMS) by Method 6020 WG1245245 1 03/05/19 17:13 03/06/19 22:25 LD Mt. Juliet, TN Al
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1245678 1 03/06/19 07:51 03/06/19 19:31 DMW Mt. Juliet, TN 10
Sc

PSW-4 L1075168-17 GW Cody 03/01/19 17:25 03/04/19 09:00

date/time date/time
Wet Chemistry by Method 9040C WG1245737 1 03/06/19 09:50 03/06/19 09:50 SJM Mt. Juliet, TN

SK-1 L1075168-18 GW Cody 03/01/19 17:50 03/04/19 09:00

date/time date/time

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DUPLICATE 1 L1075168-19 GW Cody 03/01/19 00:00 03/04/19 09:00 1
Cp
Tc
4
Cn
Volatile Organic Compounds (GC/MS) by Method 8260C WG1245979 1 03/06/19 17:21 03/06/19 17:21 GLN Mt. Juliet, TN Tr
6
Sr
Cody 03/01/19 09:15 03/04/19 09:00

Qc
PS-1 L1075168-20 Solid
date/time date/time
Gl
Total Solids by Method 2540 G-2011 WG1245367 1 03/06/19 13:46 03/06/19 14:08 JD Mt. Juliet, TN 9
Wet Chemistry by Method 9050AMod WG1245948 1 03/06/19 15:35 03/06/19 21:03 RDW Mt. Juliet, TN Al
Wet Chemistry by Method 9056A WG1245719 1 03/06/19 17:00 03/06/19 18:51 ST Mt. Juliet, TN
Sc
Metals (ICP) by Method 6010B WG1245191 1 03/05/19 10:59 03/07/19 20:41 TRB Mt. Juliet, TN
Metals (ICP) by Method 6010B WG1245191 5 03/05/19 10:59 03/08/19 10:03 CCE Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG1245869 1 03/05/19 23:41 03/06/19 19:43 BMB Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1246136 1 03/06/19 19:07 03/10/19 16:33 TJD Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG1244658 2 03/04/19 21:24 03/05/19 05:28 JNJ Mt. Juliet, TN

PS-2 L1075168-21 Solid Cody 03/01/19 09:30 03/04/19 09:00

date/time date/time
Total Solids by Method 2540 G-2011 WG1245367 1 03/06/19 13:46 03/06/19 14:08 JD Mt. Juliet, TN
Wet Chemistry by Method 9050AMod WG1245948 1 03/06/19 15:35 03/06/19 21:03 RDW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B WG1245896 1 03/05/19 23:41 03/06/19 12:03 DWR Mt. Juliet, TN

PS-3 L1075168-22 Solid Cody 03/01/19 09:45 03/04/19 09:00

date/time date/time
Wet Chemistry by Method 9050AMod WG1245948 1 03/06/19 15:35 03/06/19 21:03 RDW Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1246136 1 03/06/19 19:07 03/09/19 23:30 KME Mt. Juliet, TN

03/13/19 15:42
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PS-4 L1075168-23 Solid Cody 03/01/19 10:00 03/04/19 09:00 1
Cp
Tc
Wet Chemistry by Method 9050AMod WG1245948 1 03/06/19 15:35 03/06/19 21:03 RDW Mt. Juliet, TN 3
Wet Chemistry by Method 9056A WG1245719 1 03/06/19 17:00 03/06/19 19:34 ST Mt. Juliet, TN Ss
4
Cn
Volatile Organic Compounds (GC/MS) by Method 8260B WG1245896 1 03/05/19 23:41 03/06/19 14:30 DWR Mt. Juliet, TN 5
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1246136 1 03/06/19 19:07 03/09/19 01:11 DMW Mt. Juliet, TN Tr
6
Sr
PS-5 L1075168-24 Solid Cody 03/01/19 17:00 03/04/19 09:00 7
Qc
Gl
Wet Chemistry by Method 9050AMod WG1245948 1 03/06/19 15:35 03/06/19 21:03 RDW Mt. Juliet, TN 9
Wet Chemistry by Method 9056A WG1245719 1 03/06/19 17:00 03/06/19 19:59 ST Mt. Juliet, TN Al
Metals (ICP) by Method 6010B WG1245191 1 03/05/19 10:59 03/07/19 20:53 TRB Mt. Juliet, TN 10
Sc
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 WG1246136 5 03/06/19 19:07 03/09/19 23:58 KME Mt. Juliet, TN

03/13/19 15:42
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CASE NARRATIVE ONE LAB. NATIONWIDE.
1
Cp
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within 2
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples Tc
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form 3
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my Ss
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been 4
knowingly withheld that would affect the quality of the data. Cn
5
Tr
6
Sr
7
Qc
Chris McCord
Jason Romer 8
Project Manager Gl
9
Al
10
Sc

03/13/19 15:42
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RG-366/TRRP-13
Revised May 2010 Laboratory Data Package Cover Page ONE LAB. NATIONWIDE.
This data package consists of this signature page, the laboratory review checklist, and the following
reportable data as applicable:
R1 - Field chain-of-custody documentation;
R2 - Sample identification cross-reference;
R3 - Test reports (analytical data sheets) for each environmental sample that includes:
a. Items consistent with NELAC Chapter 5,
b. dilution factors,
c. preparation methods,
d. cleanup methods, and
e. if required for the project, tentatively identified compounds (TICs).
R4 - Surrogate recovery data including:
a. Calculated recovery (%R), and
b. The laboratory’s surrogate QC limits.
R5 - Test reports/summary forms for blank samples;
R6 - Test reports/summary forms for laboratory control samples (LCSs) including:
a. LCS spiking amounts,
b. Calculated %R for each analyte, and
c. The laboratory’s LCS QC limits.
R7 - Test reports for project matrix spike/matrix spike duplicates (MS/MSDs) including:
a. Samples associated with the MS/MSD clearly identified,
b. MS/MSD spiking amounts,
c. Concentration of each MS/MSD analyte measured in the parent and spiked samples,
d. Calculated %Rs and relative percent differences (RPDs), and
e. The laboratory’s MS/MSD QC limits
R8 - Laboratory analytical duplicate (if applicable) recovery and precision:
a. The amount of analyte measured in the duplicate,
b. The calculated RPD, and
c. The laboratory’s QC limits for analytical duplicates.
R9 - List of method quantitation limits (MQLs) and detectability check sample results for each analyte
for each method and matrix.
R10 - Other problems or anomalies.
Release Statement: I am responsible for the release of this laboratory data package. This laboratory is
NELAC accredited under the Texas Laboratory Accreditation Program for all the methods, analytes, and
matrices reported in this data package except as noted in the Exception Reports. The data have been
reviewed and are technically compliant with the requirements of the methods used, except where
noted by the laboratory in the Exception Reports. By my signature below, I affirm to the best of my
knowledge all problems/anomalies observed by the laboratory have been identified in the Laboratory
Review Checklist, and no information affecting the quality of the data has been knowingly withheld.
Chris McCord
Jason Romer
Project Manager

03/13/19 15:42
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RG-366/TRRP-13
Revised May 2010 Laboratory Review Checklist: Reportable Data ONE LAB. NATIONWIDE.
Laboratory Name: Pace Analytical National LRC Date: 03/13/2019 16:10

15:42
Laboratory Job Number: L1075168-01, 02, 03, 04, 05, 06, 07, 08, 09, 10, 11, 12, 13, 14,
Project Name: Boundary Ventures, Inc. 15, 16, 17, 18, 19, 20, 21, 22, 23 and 24
Prep Batch Number(s): WG1244658, WG1245047, WG1245002, WG1245130,
WG1245228, WG1245356, WG1245479, WG1245737, WG1245159, WG1245869,
WG1245948, WG1245245, WG1245719, WG1245896, WG1245476, WG1245678,
Reviewer Name: Jason
Chris McCord
Romer WG1245367, WG1245670, WG1245979, WG1245735, WG1246279, WG1245955,
WG1246143, WG1246136, WG1245191, WG1246058, WG1246059, WG1246056,
WG1245643 and WG1248019
#¹ A² Description Yes No NA³ NR⁴ ER#⁵
R1 OI Chain-of-custody (C-O-C)
Did samples meet the laboratory’s standard conditions of sample acceptability upon receipt? X
Were all departures from standard conditions described in an exception report? X
R2 OI Sample and quality control (QC) identification
Are all field sample ID numbers cross-referenced to the laboratory ID numbers? X
Are all laboratory ID numbers cross-referenced to the corresponding QC data? X
R3 OI Test reports
Were all samples prepared and analyzed within holding times? X 1
Other than those results < MQL, were all other raw values bracketed by calibration standards? X
Were calculations checked by a peer or supervisor? X
Were all analyte identifications checked by a peer or supervisor? X
Were sample detection limits reported for all analytes not detected? X
Were all results for soil and sediment samples reported on a dry weight basis? X
Were % moisture (or solids) reported for all soil and sediment samples? X
Were bulk soils/solids samples for volatile analysis extracted with methanol per SW846 Method 5035? X
If required for the project, are TICs reported? X
R4 O Surrogate recovery data
Were surrogates added prior to extraction? X
Were surrogate percent recoveries in all samples within the laboratory QC limits? X 2
R5 OI Test reports/summary forms for blank samples
Were appropriate type(s) of blanks analyzed? X
Were blanks analyzed at the appropriate frequency? X
Were method blanks taken through the entire analytical process, including preparation and, if applicable, X
cleanup procedures?
Were blank concentrations < MQL? X
R6 OI Laboratory control samples (LCS):
Were all COCs included in the LCS? X
Was each LCS taken through the entire analytical procedure, including prep and cleanup steps? X
Were LCSs analyzed at the required frequency? X
Were LCS (and LCSD, if applicable) %Rs within the laboratory QC limits? X 3
Does the detectability check sample data document the laboratory’s capability to detect the COCs at the MDL X
used to calculate the SDLs?
Was the LCSD RPD within QC limits? X 4
R7 OI Matrix spike (MS) and matrix spike duplicate (MSD) data
Were the project/method specified analytes included in the MS and MSD? X
Were MS/MSD analyzed at the appropriate frequency? X
Were MS (and MSD, if applicable) %Rs within the laboratory QC limits? X 5
Were MS/MSD RPDs within laboratory QC limits? X 6
R8 OI Analytical duplicate data
Were appropriate analytical duplicates analyzed for each matrix? X
Were analytical duplicates analyzed at the appropriate frequency? X
Were RPDs or relative standard deviations within the laboratory QC limits? X 7
R9 OI Method quantitation limits (MQLs):
Are the MQLs for each method analyte included in the laboratory data package? X
Do the MQLs correspond to the concentration of the lowest non-zero calibration standard? X
Are unadjusted MQLs and DCSs included in the laboratory data package? X
R10 OI Other problems/anomalies
Are all known problems/anomalies/special conditions noted in this LRC and ER? X
Was applicable and available technology used to lower the SDL to minimize the matrix interference effects on X
the sample results?
Is the laboratory NELAC-accredited under the Texas Laboratory Accreditation Program for the analytes, matrices X
and methods associated with this laboratory data package?

03/13/19 15:42
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RG-366/TRRP-13
Revised May 2010 Laboratory Review Checklist: Reportable Data ONE LAB. NATIONWIDE.

15:42
WG1245228, WG1245356, WG1245479, WG1245737, WG1245159, WG1245869,
WG1245948, WG1245245, WG1245719, WG1245896, WG1245476, WG1245678,
Chris McCord
WG1246143, WG1246136, WG1245191, WG1246058, WG1246059, WG1246056,
WG1245643 and WG1248019
1. Items identified by the letter “R” must be included in the laboratory data package submitted in the TRRP-required report(s). Items identified by the letter “S”
should be retained and made available upon request for the appropriate retention period.
2. O = organic analyses; I = inorganic analyses (and general chemistry, when applicable);
3. NA = Not applicable;
4. NR = Not reviewed;
5. ER# = Exception Report identification number (an Exception Report should be completed for an item if “NR” or “No” is checked).

03/13/19 15:42
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RG-366/TRRP-13
Revised May 2010 Laboratory Review Checklist: Supporting Data ONE LAB. NATIONWIDE.

15:42
WG1245228, WG1245356, WG1245479, WG1245737, WG1245159, WG1245869,
WG1245948, WG1245245, WG1245719, WG1245896, WG1245476, WG1245678,
Chris McCord
WG1246143, WG1246136, WG1245191, WG1246058, WG1246059, WG1246056,
WG1245643 and WG1248019
S1 OI Initial calibration (ICAL)
Were response factors and/or relative response factors for each analyte within QC limits? X
Were percent RSDs or correlation coefficient criteria met? X
Was the number of standards recommended in the method used for all analytes? X
Were all points generated between the lowest and highest standard used to calculate the curve? X
Are ICAL data available for all instruments used? X
Has the initial calibration curve been verified using an appropriate second source standard? X
S2 OI Initial and continuing calibration verification (ICCV and CCV) and continuing calibration blank (CCB):
Was the CCV analyzed at the method-required frequency? X
Were percent differences for each analyte within the method-required QC limits? X
Was the ICAL curve verified for each analyte? X
Was the absolute value of the analyte concentration in the inorganic CCB < MDL? X
S3 O Mass spectral tuning
Was the appropriate compound for the method used for tuning? X
Were ion abundance data within the method-required QC limits? X
S4 O Internal standards (IS)
Were IS area counts and retention times within the method-required QC limits? X
S5 OI Raw data (NELAC Section 5.5.10)
Were the raw data (for example, chromatograms, spectral data) reviewed by an analyst? X
Were data associated with manual integrations flagged on the raw data? X
S6 O Dual column confirmation
Did dual column confirmation results meet the method-required QC? X
S7 O Tentatively identified compounds (TICs)
If TICs were requested, were the mass spectra and TIC data subject to appropriate checks? X
S8 I Interference Check Sample (ICS) results
Were percent recoveries within method QC limits? X
S9 I Serial dilutions, post digestion spikes, and method of standard additions
Were percent differences, recoveries, and the linearity within the QC limits specified in the method? X 8
S10 OI Method detection limit (MDL) studies
Was a MDL study performed for each reported analyte? X
Is the MDL either adjusted or supported by the analysis of DCSs? X
S11 OI Proficiency test reports
Was the laboratory's performance acceptable on the applicable proficiency tests or evaluation studies? X
S12 OI Standards documentation
Are all standards used in the analyses NIST-traceable or obtained from other appropriate sources? X
S13 OI Compound/analyte identification procedures
Are the procedures for compound/analyte identification documented? X
S14 OI Demonstration of analyst competency (DOC)
Was DOC conducted consistent with NELAC Chapter 5? X
Is documentation of the analyst’s competency up-to-date and on file? X
S15 OI Verification/validation documentation for methods (NELAC Chapter 5)
Are all the methods used to generate the data documented, verified, and validated, where applicable? X
S16 OI Laboratory standard operating procedures (SOPs)
Are laboratory SOPs current and on file for each method performed X

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RG-366/TRRP-13
Revised May 2010 Laboratory Review Checklist: Exception Reports ONE LAB. NATIONWIDE.

15:42
WG1245228, WG1245356, WG1245479, WG1245737, WG1245159, WG1245869,
WG1245948, WG1245245, WG1245719, WG1245896, WG1245476, WG1245678,
Chris McCord
WG1246143, WG1246136, WG1245191, WG1246058, WG1246059, WG1246056,
WG1245643 and WG1248019
ER #¹ Description
9040C WG1245130 L1075168-15, 06, 10, 01, 03, 02, 04, 05, 07, 12, 08, 16, 13, 09, 11 and 14: Prepared and/or analyzed
past recommended holding time. Concentrations should be considered minimum values.
1 9040C WG1245737 L1075168-18, 17 and 19: Prepared and/or analyzed past recommended holding time. Concentrations
should be considered minimum values.
TCEQ Method 1005 WG1246136 o-Terphenyl L1075168-24 and 21: Percent Recovery is outside of established control
limits.
2 8270C WG1244658 2,4,6-Tribromophenol, 2-Fluorophenol, Phenol-d5, Nitrobenzene-d5, p-Terphenyl-d14,
2-Fluorobiphenyl L1075168-21, 24 and 23: Percent Recovery is outside of established control limits.
8260C WG1245979 4-Bromofluorobenzene L1075168-16: Percent Recovery is outside of established control limits.
8260B WG1245869 Dibromomethane, 1,1,2,2-Tetrachloroethane: Percent Recovery is outside of established control
3 limits.
8270C WG1244658 Benzidine: Percent Recovery is outside of established control limits.
8021B WG1245643 Ethylbenzene, Total Xylene: Relative Percent Difference is outside of established control limits.
4 8270D WG1245476 Benzidine: Relative Percent Difference is outside of established control limits.
8270D WG1246279 Pentachlorophenol: Relative Percent Difference is outside of established control limits.
8260B WG1245869 1,2,4-Trimethylbenzene: Percent Recovery is outside of established control limits.
6020 WG1245245 Barium, Calcium, Sodium: Percent Recovery is outside of established control limits.
TCEQ Method 1005 WG1246136 TPH C12 - C28, TPH C6 - C35: Percent Recovery is outside of established control limits.
8260B WG1245869 Ethylbenzene, p-Isopropyltoluene, Naphthalene, Toluene, 1,2,3-Trimethylbenzene,
1,3,5-Trimethylbenzene, Xylenes, Total: Percent Recovery is outside of established control limits.
8260B WG1245896 Chloroethane, Tetrachloroethene, 1,1,1-Trichloroethane: Percent Recovery is outside of established
5 control limits.
8021B WG1245643 Total Xylene: Percent Recovery is outside of established control limits.
8270D WG1246279 Benzidine: Percent Recovery is outside of established control limits.
8270C WG1244658 Benzidine, 3,3-Dichlorobenzidine, Hexachlorocyclopentadiene, n-Nitrosodimethylamine,
n-Nitrosodiphenylamine, Diethyl phthalate, 4,6-Dinitro-2-methylphenol, 2,4-Dinitrophenol, Pentachlorophenol: Percent
Recovery is outside of established control limits.
7470A WG1245002 Mercury: Percent Recovery is outside of established control limits.
TCEQ Method 1005 WG1246136 TPH C12 - C28: Relative Percent Difference is outside of established control limits.
8260B WG1245896 Bromomethane, sec-Butylbenzene, tert-Butylbenzene, Chloroethane, p-Isopropyltoluene,
n-Propylbenzene, 1,1,2-Trichlorotrifluoroethane, Trichlorofluoromethane, Vinyl chloride: Relative Percent Difference is
outside of established control limits.
8021B WG1245228 Benzene, Toluene, Ethylbenzene, Total Xylene: Relative Percent Difference is outside of established
6 control limits.
8270D WG1246279 3,3-Dichlorobenzidine, 2,4-Dimethylphenol: Relative Percent Difference is outside of established
control limits.
8270C WG1244658 2,4-Dinitrotoluene, 2,6-Dinitrotoluene, Hexachlorobenzene, Hexachloro-1,3-butadiene,
Hexachloroethane, 2-Nitrophenol, Pentachlorophenol: Relative Percent Difference is outside of established control
limits.
9056A WG1245719 Chloride: Relative Percent Difference is outside of established control limits.
7 2540 C-2011 WG1246058 Dissolved Solids: Relative Percent Difference is outside of established control limits.
2540 C-2011 WG1246059 Dissolved Solids: Relative Percent Difference is outside of established control limits.
6010B WG1245191 Barium, Chromium, Lead: Post Spike Percent Recovery and/or Serial Dilution Relative Percent
8 Difference was outside of established control limits.

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MW-1 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/time: 03/01/19 14:45 L1075168
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch

Cp
Analyte mg/l mg/l mg/l mg/l date / time
2
Dissolved Solids 2960 14.1 50.0 50.0 1 03/07/2019 23:39 WG1246056 Tc
3
Wet Chemistry by Method 2320 B-2011 Ss
Analyte mg/l mg/l mg/l mg/l date / time 4
Cn
Alkalinity 157 2.71 20.0 20.0 1 03/07/2019 14:32 WG1245955
5
Sample Narrative: Tr
L1075168-01 WG1245955: Endpoint pH 4.5 headspace
6
Sr
Wet Chemistry by Method 300.0
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch 7

Qc
Chloride 1510 2.60 1.00 50.0 50 03/06/2019 02:30 WG1245159 8
Sulfate 2.85 J 0.0774 5.00 5.00 1 03/06/2019 09:41 WG1245159 Gl
9
Wet Chemistry by Method 9040C Al
Result Qualifier Dilution Analysis Batch
Analyte su date / time 10
Sc
pH 6.54 T8 1 03/05/2019 11:55 WG1245130
Sample Narrative:
L1075168-01 WG1245130: 6.54 at 11.6C
Wet Chemistry by Method 9050A

Result Qualifier Unadj. MQL MQL Dilution Analysis Batch
Analyte umhos/cm umhos/cm umhos/cm date / time
Specific Conductance 4510 10.0 10.0 1 03/07/2019 13:22 WG1245735
Mercury by Method 7470A

Mercury U J6 0.0000490 0.000200 0.000200 1 03/05/2019 09:41 WG1245002
Metals (ICPMS) by Method 6020

Arsenic 0.104 0.000250 0.00200 0.00200 1 03/06/2019 20:39 WG1245245
Barium 0.812 0.000360 0.00500 0.00500 1 03/06/2019 20:39 WG1245245
Cadmium 0.000204 J 0.000160 0.00100 0.00100 1 03/06/2019 20:39 WG1245245
Calcium 252 0.0460 1.00 1.00 1 03/06/2019 20:39 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 20:39 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 20:39 WG1245245
Magnesium 43.7 0.100 1.00 1.00 1 03/06/2019 20:39 WG1245245
Potassium 6.10 0.0370 1.00 1.00 1 03/06/2019 20:39 WG1245245
Selenium 0.000561 J 0.000380 0.00200 0.00200 1 03/06/2019 20:39 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 20:39 WG1245245
Sodium 496 0.110 1.00 1.00 1 03/06/2019 20:39 WG1245245

03/13/19 15:42
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Volatile Organic Compounds (GC) by Method 8021B

1
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Cp
2
Benzene U 0.000190 0.000500 0.000500 1 03/05/2019 18:46 WG1245228
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/05/2019 18:46 WG1245228
Ethylbenzene U 0.000160 0.000500 0.000500 1 03/05/2019 18:46 WG1245228 3
Total Xylene U 0.000510 0.00150 0.00150 1 03/05/2019 18:46 WG1245228 Ss
(S) a,a,a-Trifluorotoluene(PID) 99.8 79.0-125 03/05/2019 18:46 WG1245228
4
Cn
Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005
Tr
TPH C6 - C12 U 0.600 0.900 0.900 1 03/07/2019 18:03 WG1246143 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/07/2019 18:03 WG1246143 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/07/2019 18:03 WG1246143
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/07/2019 18:03 WG1246143
Qc
(S) o-Terphenyl 85.2 70.0-130 03/07/2019 18:03 WG1246143
8
Gl
9
Al
10
Sc

03/13/19 15:42
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Cp
2
3
Cn
Alkalinity 285 2.71 20.0 20.0 1 03/07/2019 14:44 WG1245955
5
6
Sr

Qc
Chloride 487 0.519 1.00 10.0 10 03/06/2019 02:45 WG1245159 8
Sulfate 99.3 0.774 5.00 50.0 10 03/06/2019 02:45 WG1245159 Gl
9
Sc
pH 6.67 T8 1 03/05/2019 11:55 WG1245130
Sample Narrative:
L1075168-02 WG1245130: 6.67 at 11.2C


Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 09:48 WG1245002

Arsenic 0.00617 0.000250 0.00200 0.00200 1 03/06/2019 20:43 WG1245245
Barium 0.755 0.000360 0.00500 0.00500 1 03/06/2019 20:43 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 20:43 WG1245245
Calcium 160 0.0460 1.00 1.00 1 03/06/2019 20:43 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 20:43 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 20:43 WG1245245
Magnesium 43.0 0.100 1.00 1.00 1 03/06/2019 20:43 WG1245245
Potassium 6.16 0.0370 1.00 1.00 1 03/06/2019 20:43 WG1245245
Selenium 0.000593 J 0.000380 0.00200 0.00200 1 03/06/2019 20:43 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 20:43 WG1245245
Sodium 176 0.110 1.00 1.00 1 03/06/2019 20:43 WG1245245

03/13/19 15:42
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1
2
Benzene U 0.000190 0.000500 0.000500 1 03/05/2019 19:07 WG1245228
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/05/2019 19:07 WG1245228
4
Cn
Tr
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 06:05 WG1245479 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 06:05 WG1245479 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 06:05 WG1245479
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 06:05 WG1245479
Qc
(S) o-Terphenyl 89.0 70.0-130 03/06/2019 06:05 WG1245479
8
Gl
9
Al
10
Sc

03/13/19 15:42
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Cp
2
3
Cn
Alkalinity 214 2.71 20.0 20.0 1 03/07/2019 14:51 WG1245955
5
6
Sr

Qc
Chloride 1630 2.60 1.00 50.0 50 03/06/2019 03:32 WG1245159 8
Sulfate 200 0.774 5.00 50.0 10 03/06/2019 09:57 WG1245159 Gl
9
Sc
pH 6.57 T8 1 03/05/2019 11:55 WG1245130
Sample Narrative:
L1075168-03 WG1245130: 6.57 at 12C


Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 09:56 WG1245002

Arsenic 0.00412 0.000250 0.00200 0.00200 1 03/06/2019 20:48 WG1245245
Barium 0.478 0.000360 0.00500 0.00500 1 03/06/2019 20:48 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 20:48 WG1245245
Calcium 436 0.0460 1.00 1.00 1 03/06/2019 20:48 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 20:48 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 20:48 WG1245245
Magnesium 49.7 0.100 1.00 1.00 1 03/06/2019 20:48 WG1245245
Potassium 8.67 0.0370 1.00 1.00 1 03/06/2019 20:48 WG1245245
Selenium U 0.000380 0.00200 0.00200 1 03/06/2019 20:48 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 20:48 WG1245245
Sodium 367 0.110 1.00 1.00 1 03/06/2019 20:48 WG1245245

03/13/19 15:42
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Volatile Organic Compounds (GC/MS) by Method 8260C

1
2
Acetone U 0.0100 0.0500 0.0500 1 03/05/2019 20:32 WG1245356
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/05/2019 20:32 WG1245356
Acrylonitrile U 0.00187 0.0100 0.0100 1 03/05/2019 20:32 WG1245356 3
Benzene U 0.000331 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 Ss
Bromobenzene U 0.000352 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
4
Bromodichloromethane U 0.000380 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Cn
Bromoform U 0.000469 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Bromomethane U 0.000866 0.00500 0.00500 1 03/05/2019 20:32 WG1245356 5
n-Butylbenzene U 0.000361 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 Tr
sec-Butylbenzene U 0.000365 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
6
tert-Butylbenzene U 0.000399 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Sr
Carbon tetrachloride U 0.000379 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Chlorobenzene U 0.000348 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 7
Chlorodibromomethane U 0.000327 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 Qc
Chloroethane U 0.000453 0.00500 0.00500 1 03/05/2019 20:32 WG1245356
8
Chloroform U 0.000324 0.00500 0.00500 1 03/05/2019 20:32 WG1245356
Gl
Chloromethane U 0.000276 0.00250 0.00250 1 03/05/2019 20:32 WG1245356
2-Chlorotoluene U 0.000375 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 9
4-Chlorotoluene U 0.000351 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 Al
1,2-Dibromo-3-Chloropropane U 0.00133 0.00500 0.00500 1 03/05/2019 20:32 WG1245356
10
1,2-Dibromoethane U 0.000381 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Sc
Dibromomethane U 0.000346 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,2-Dichlorobenzene U 0.000349 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Dichlorodifluoromethane U 0.000551 0.00500 0.00500 1 03/05/2019 20:32 WG1245356
1,1-Dichloroethane U 0.000259 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,1-Dichloroethene U 0.000398 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
cis-1,2-Dichloroethene U 0.000260 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
trans-1,2-Dichloroethene U 0.000396 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,2-Dichloropropane U 0.000306 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,1-Dichloropropene U 0.000352 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
cis-1,3-Dichloropropene U 0.000418 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
trans-1,3-Dichloropropene U 0.000419 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Di-isopropyl ether U 0.000320 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Ethylbenzene U 0.000384 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Hexachloro-1,3-butadiene U 0.000256 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Isopropylbenzene U 0.000326 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
p-Isopropyltoluene U 0.000350 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
2-Butanone (MEK) U 0.00393 0.0100 0.0100 1 03/05/2019 20:32 WG1245356
Methylene Chloride U 0.00100 0.00500 0.00500 1 03/05/2019 20:32 WG1245356
4-Methyl-2-pentanone (MIBK) U 0.00214 0.0100 0.0100 1 03/05/2019 20:32 WG1245356
Methyl tert-butyl ether U 0.000367 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Naphthalene U 0.00100 0.00500 0.00500 1 03/05/2019 20:32 WG1245356
n-Propylbenzene U 0.000349 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Styrene U 0.000307 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,1,1,2-Tetrachloroethane U 0.000385 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,1,2-Trichlorotrifluoroethane U 0.000303 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Tetrachloroethene U 0.000372 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Toluene U 0.000412 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
1,2,3-Trichlorobenzene U 0.000230 0.00100 0.00100 1 03/05/2019 20:32 WG1245356

03/13/19 15:42
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1
2
1,1,1-Trichloroethane U 0.000319 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Tc
Trichloroethene U 0.000398 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 3
Trichlorofluoromethane U 0.00120 0.00500 0.00500 1 03/05/2019 20:32 WG1245356 Ss
1,2,3-Trichloropropane U 0.000807 0.00250 0.00250 1 03/05/2019 20:32 WG1245356
4
1,2,4-Trimethylbenzene U 0.000373 0.00100 0.00100 1 03/05/2019 20:32 WG1245356
Cn
1,3,5-Trimethylbenzene U 0.000387 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 5
Vinyl chloride U 0.000259 0.00100 0.00100 1 03/05/2019 20:32 WG1245356 Tr
Xylenes, Total U 0.00106 0.00300 0.00300 1 03/05/2019 20:32 WG1245356
6
(S) Toluene-d8 106 80.0-120 03/05/2019 20:32 WG1245356
Sr
(S) 4-Bromofluorobenzene 104 77.0-126 03/05/2019 20:32 WG1245356
(S) 1,2-Dichloroethane-d4 105 70.0-130 03/05/2019 20:32 WG1245356 7
Qc
8
Result Qualifier SDL Unadj. MQL MQL Dilution Analysis Batch Gl
9
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 06:21 WG1245479
Al
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 06:21 WG1245479
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 06:21 WG1245479 10
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 06:21 WG1245479 Sc
(S) o-Terphenyl 86.9 70.0-130 03/06/2019 06:21 WG1245479
Semi Volatile Organic Compounds (GC/MS) by Method 8270D

Acenaphthene U 0.000316 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Acenaphthylene U 0.000309 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Anthracene U 0.000291 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Benzidine U 0.00432 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Benzo(a)anthracene U 0.0000975 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Benzo(b)fluoranthene U 0.0000896 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Benzo(k)fluoranthene U 0.000355 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Benzo(g,h,i)perylene U 0.000161 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Benzo(a)pyrene U 0.000340 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Bis(2-chlorethoxy)methane U 0.000329 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Bis(2-chloroethyl)ether U 0.00162 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Bis(2-chloroisopropyl)ether U 0.000445 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
4-Bromophenyl-phenylether U 0.000335 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
2-Chloronaphthalene U 0.000330 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
4-Chlorophenyl-phenylether U 0.000303 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Chrysene U 0.000332 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Dibenz(a,h)anthracene U 0.000279 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
3,3-Dichlorobenzidine U 0.00202 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
2,4-Dinitrotoluene U 0.00165 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Fluoranthene U 0.000310 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Fluorene U 0.000323 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Hexachlorobenzene U 0.000341 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Hexachlorocyclopentadiene U 0.00233 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Hexachloroethane U 0.000365 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
Isophorone U 0.000272 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Naphthalene U 0.000372 0.00100 0.00100 1 03/07/2019 16:39 WG1246279

03/13/19 15:42
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1
2
Nitrobenzene U 0.000367 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Tc
n-Nitrosodimethylamine U 0.00126 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
n-Nitrosodiphenylamine U 0.00119 0.0100 0.0100 1 03/07/2019 16:39 WG1246279 3
n-Nitrosodi-n-propylamine U 0.000403 0.0100 0.0100 1 03/07/2019 16:39 WG1246279 Ss
Phenanthrene U 0.000366 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
4
Benzylbutyl phthalate U 0.000275 0.00300 0.00300 1 03/07/2019 16:39 WG1246279
Cn
Bis(2-ethylhexyl)phthalate U 0.000709 0.00300 0.00300 1 03/07/2019 16:39 WG1246279
Di-n-butyl phthalate U 0.000266 0.00300 0.00300 1 03/07/2019 16:39 WG1246279 5
Diethyl phthalate 0.000716 J 0.000282 0.00300 0.00300 1 03/07/2019 16:39 WG1246279 Tr
Dimethyl phthalate U 0.000283 0.00300 0.00300 1 03/07/2019 16:39 WG1246279
6
Di-n-octyl phthalate U 0.000278 0.00300 0.00300 1 03/07/2019 16:39 WG1246279
Sr
Pyrene U 0.000330 0.00100 0.00100 1 03/07/2019 16:39 WG1246279
1,2,4-Trichlorobenzene U 0.000355 0.0100 0.0100 1 03/07/2019 16:39 WG1246279 7
4-Chloro-3-methylphenol U 0.000263 0.0100 0.0100 1 03/07/2019 16:39 WG1246279 Qc
2-Chlorophenol U 0.000283 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
8
2,4-Dichlorophenol U 0.000284 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Gl
2,4-Dimethylphenol U 0.000264 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
4,6-Dinitro-2-methylphenol U 0.00262 0.0100 0.0100 1 03/07/2019 16:39 WG1246279 9
2,4-Dinitrophenol U 0.00325 0.0100 0.0100 1 03/07/2019 16:39 WG1246279 Al
2-Nitrophenol U 0.000320 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
10
4-Nitrophenol U 0.00201 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Sc
Pentachlorophenol U J3 0.000313 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
Phenol 0.00266 J 0.000334 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
2,4,6-Trichlorophenol U 0.000297 0.0100 0.0100 1 03/07/2019 16:39 WG1246279
(S) 2-Fluorophenol 38.4 10.0-120 03/07/2019 16:39 WG1246279
(S) Phenol-d5 22.9 10.0-120 03/07/2019 16:39 WG1246279
(S) Nitrobenzene-d5 53.5 10.0-127 03/07/2019 16:39 WG1246279
(S) 2-Fluorobiphenyl 61.5 10.0-130 03/07/2019 16:39 WG1246279
(S) 2,4,6-Tribromophenol 77.5 10.0-155 03/07/2019 16:39 WG1246279
(S) p-Terphenyl-d14 76.2 10.0-128 03/07/2019 16:39 WG1246279

03/13/19 15:42
16:10 24 of 161

Cp
2
3
Cn
Alkalinity 382 2.71 20.0 20.0 1 03/07/2019 14:58 WG1245955
5
6
Sr

Qc
Chloride 682 1.04 1.00 20.0 20 03/06/2019 03:47 WG1245159 8
Sulfate 16.3 0.0774 5.00 5.00 1 03/06/2019 10:12 WG1245159 Gl
9
Sc
pH 6.78 T8 1 03/05/2019 11:55 WG1245130
Sample Narrative:
L1075168-04 WG1245130: 6.78 at 11.8C


Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 09:58 WG1245002

Arsenic 0.00198 J 0.000250 0.00200 0.00200 1 03/06/2019 20:20 WG1245245
Barium 2.43 V 0.000360 0.00500 0.00500 1 03/06/2019 20:20 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 20:20 WG1245245
Calcium 211 V 0.0460 1.00 1.00 1 03/06/2019 20:20 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 20:20 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 20:20 WG1245245
Magnesium 22.8 0.100 1.00 1.00 1 03/06/2019 20:20 WG1245245
Potassium 1.78 0.0370 1.00 1.00 1 03/06/2019 20:20 WG1245245
Selenium U 0.000380 0.00200 0.00200 1 03/06/2019 20:20 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 20:20 WG1245245
Sodium 279 V 0.110 1.00 1.00 1 03/06/2019 20:20 WG1245245

03/13/19 15:42
16:10 25 of 161

1
2
Benzene U 0.000190 0.000500 0.000500 1 03/05/2019 19:28 WG1245228
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/05/2019 19:28 WG1245228
4
Cn
Tr
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 06:37 WG1245479 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 06:37 WG1245479 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 06:37 WG1245479
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 06:37 WG1245479
Qc
(S) o-Terphenyl 83.6 70.0-130 03/06/2019 06:37 WG1245479
8
Gl
9
Al
10
Sc

03/13/19 15:42
16:10 26 of 161

Cp
2
Dissolved Solids 5200 28.2 100 100 1 03/07/2019 23:09 WG1246058 Tc
3
Cn
Alkalinity 295 2.71 20.0 20.0 1 03/07/2019 15:05 WG1245955
5
6
Sr

Qc
Chloride 2360 2.60 1.00 50.0 50 03/06/2019 04:02 WG1245159 8
Sulfate 443 3.87 5.00 250 50 03/06/2019 04:02 WG1245159 Gl
9
Sc
pH 6.62 T8 1 03/05/2019 11:55 WG1245130
Sample Narrative:
L1075168-05 WG1245130: 6.62 at 11.9C


Mercury 0.0000675 J 0.0000490 0.000200 0.000200 1 03/05/2019 10:00 WG1245002

Arsenic 0.00189 J 0.000250 0.00200 0.00200 1 03/06/2019 21:07 WG1245245
Barium 0.156 0.000360 0.00500 0.00500 1 03/06/2019 21:07 WG1245245
Cadmium 0.000194 J 0.000160 0.00100 0.00100 1 03/06/2019 21:07 WG1245245
Calcium 628 0.0460 1.00 1.00 1 03/06/2019 21:07 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 21:07 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 21:07 WG1245245
Magnesium 75.1 0.100 1.00 1.00 1 03/06/2019 21:07 WG1245245
Potassium 29.2 0.0370 1.00 1.00 1 03/06/2019 21:07 WG1245245
Selenium 0.00199 J 0.000380 0.00200 0.00200 1 03/06/2019 21:07 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:07 WG1245245
Sodium 688 0.110 1.00 1.00 1 03/06/2019 21:07 WG1245245

03/13/19 15:42
16:10 27 of 161

1
2
Benzene 0.000248 J 0.000190 0.000500 0.000500 1 03/06/2019 04:13 WG1245643
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/06/2019 04:13 WG1245643
Ethylbenzene U J3 0.000160 0.000500 0.000500 1 03/06/2019 04:13 WG1245643 3
Total Xylene U J3 0.000510 0.00150 0.00150 1 03/06/2019 04:13 WG1245643 Ss
(S) a,a,a-Trifluorotoluene(PID) 100 79.0-125 03/06/2019 04:13 WG1245643
4
Cn
Tr
TPH C6 - C12 U 0.600 0.900 0.900 1 03/07/2019 18:20 WG1246143 6
TPH C12 - C28 0.674 J 0.600 0.900 0.900 1 03/07/2019 18:20 WG1246143 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/07/2019 18:20 WG1246143
7
TPH C6 - C35 0.674 J 0.600 0.900 0.900 1 03/07/2019 18:20 WG1246143
Qc
(S) o-Terphenyl 89.8 70.0-130 03/07/2019 18:20 WG1246143
8
Gl
9
Al
10
Sc

03/13/19 15:42
16:10 28 of 161

Cp
2
Dissolved Solids 1120 J3 5.64 20.0 20.0 1 03/07/2019 23:09 WG1246058 Tc
3
Cn
Alkalinity 416 2.71 20.0 20.0 1 03/07/2019 15:12 WG1245955
5
6
Sr

Qc
Chloride 267 0.260 1.00 5.00 5 03/06/2019 04:18 WG1245159 8
Sulfate 135 0.387 5.00 25.0 5 03/06/2019 04:18 WG1245159 Gl
9
Sc
pH 6.90 T8 1 03/05/2019 11:55 WG1245130
Sample Narrative:
L1075168-06 WG1245130: 6.9 at 11.4C


Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 10:03 WG1245002

Arsenic 0.00161 J 0.000250 0.00200 0.00200 1 03/06/2019 21:11 WG1245245
Barium 0.125 0.000360 0.00500 0.00500 1 03/06/2019 21:11 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 21:11 WG1245245
Calcium 144 0.0460 1.00 1.00 1 03/06/2019 21:11 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 21:11 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 21:11 WG1245245
Magnesium 19.4 0.100 1.00 1.00 1 03/06/2019 21:11 WG1245245
Potassium 4.00 0.0370 1.00 1.00 1 03/06/2019 21:11 WG1245245
Selenium 0.00186 J 0.000380 0.00200 0.00200 1 03/06/2019 21:11 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:11 WG1245245
Sodium 212 0.110 1.00 1.00 1 03/06/2019 21:11 WG1245245

03/13/19 15:42
16:10 29 of 161

1
2
Benzene U 0.000190 0.000500 0.000500 1 03/06/2019 04:34 WG1245643
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/06/2019 04:34 WG1245643
4
Cn
Tr
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 07:10 WG1245479 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 07:10 WG1245479 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 07:10 WG1245479
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 07:10 WG1245479
Qc
(S) o-Terphenyl 86.9 70.0-130 03/06/2019 07:10 WG1245479
8
Gl
9
Al
10
Sc

03/13/19 15:42
16:10 30 of 161

Cp
2
3
Cn
Alkalinity 432 2.71 20.0 20.0 1 03/07/2019 15:19 WG1245955
5
6
Sr

Qc
Chloride 804 1.04 1.00 20.0 20 03/06/2019 04:33 WG1245159 8
Sulfate 127 1.55 5.00 100 20 03/06/2019 04:33 WG1245159 Gl
9
Sc
pH 6.76 T8 1 03/05/2019 11:55 WG1245130
Sample Narrative:
L1075168-07 WG1245130: 6.76 at 11C


Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 10:05 WG1245002

Arsenic 0.0174 0.000250 0.00200 0.00200 1 03/06/2019 21:16 WG1245245
Barium 0.692 0.000360 0.00500 0.00500 1 03/06/2019 21:16 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 21:16 WG1245245
Calcium 277 0.0460 1.00 1.00 1 03/06/2019 21:16 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 21:16 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 21:16 WG1245245
Magnesium 28.7 0.100 1.00 1.00 1 03/06/2019 21:16 WG1245245
Potassium 3.59 0.0370 1.00 1.00 1 03/06/2019 21:16 WG1245245
Selenium U 0.000380 0.00200 0.00200 1 03/06/2019 21:16 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:16 WG1245245
Sodium 319 0.110 1.00 1.00 1 03/06/2019 21:16 WG1245245

03/13/19 15:42
16:10 31 of 161

1
2
Benzene U 0.000190 0.000500 0.000500 1 03/06/2019 04:55 WG1245643
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/06/2019 04:55 WG1245643
4
Cn
Tr
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 07:26 WG1245479 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 07:26 WG1245479 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 07:26 WG1245479
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 07:26 WG1245479
Qc
(S) o-Terphenyl 79.2 70.0-130 03/06/2019 07:26 WG1245479
8
Gl
9
Al
10
Sc

03/13/19 15:42
16:10 32 of 161

Cp
2
3
Cn
Alkalinity 176 2.71 20.0 20.0 1 03/07/2019 15:26 WG1245955
5
6
Sr

Qc
Chloride 13.3 0.0519 1.00 1.00 1 03/06/2019 04:49 WG1245159 8
Sulfate 10.7 0.0774 5.00 5.00 1 03/06/2019 04:49 WG1245159 Gl
9
Sc
pH 7.23 T8 1 03/05/2019 11:55 WG1245130
Sample Narrative:
L1075168-08 WG1245130: 7.23 at 11.1C


Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 10:08 WG1245002

Arsenic 0.00720 0.000250 0.00200 0.00200 1 03/06/2019 21:21 WG1245245
Barium 0.472 0.000360 0.00500 0.00500 1 03/06/2019 21:21 WG1245245
Cadmium 0.000219 J 0.000160 0.00100 0.00100 1 03/06/2019 21:21 WG1245245
Calcium 39.8 0.0460 1.00 1.00 1 03/06/2019 21:21 WG1245245
Chromium 0.0137 0.000540 0.00200 0.00200 1 03/06/2019 21:21 WG1245245
Lead 0.00947 0.000240 0.00200 0.00200 1 03/06/2019 21:21 WG1245245
Magnesium 8.83 0.100 1.00 1.00 1 03/06/2019 21:21 WG1245245
Potassium 2.54 0.0370 1.00 1.00 1 03/06/2019 21:21 WG1245245
Selenium 0.00155 J 0.000380 0.00200 0.00200 1 03/06/2019 21:21 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:21 WG1245245
Sodium 39.8 0.110 1.00 1.00 1 03/06/2019 21:21 WG1245245

03/13/19 15:42
16:10 33 of 161

1
2
Benzene U 0.000190 0.000500 0.000500 1 03/11/2019 13:24 WG1248019
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/11/2019 13:24 WG1248019
4
Cn
Tr
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 07:43 WG1245479 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 07:43 WG1245479 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 07:43 WG1245479
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 07:43 WG1245479
Qc
(S) o-Terphenyl 91.3 70.0-130 03/06/2019 07:43 WG1245479
8
Gl
9
Al
10
Sc

03/13/19 15:42
16:10 34 of 161

Cp
2
3
Cn
Alkalinity 231 2.71 20.0 20.0 1 03/07/2019 15:42 WG1245955
5
6
Sr

Qc
Chloride 13.0 0.0519 1.00 1.00 1 03/06/2019 05:35 WG1245159 8
Sulfate 19.9 0.0774 5.00 5.00 1 03/06/2019 05:35 WG1245159 Gl
9
Sc
pH 7.12 T8 1 03/05/2019 11:55 WG1245130
Sample Narrative:
L1075168-09 WG1245130: 7.12 at 13.3C


Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 10:10 WG1245002

Arsenic 0.00114 J 0.000250 0.00200 0.00200 1 03/06/2019 21:25 WG1245245
Barium 0.142 0.000360 0.00500 0.00500 1 03/06/2019 21:25 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 21:25 WG1245245
Calcium 14.8 0.0460 1.00 1.00 1 03/06/2019 21:25 WG1245245
Chromium 0.000997 BJ 0.000540 0.00200 0.00200 1 03/06/2019 21:25 WG1245245
Lead 0.000395 J 0.000240 0.00200 0.00200 1 03/06/2019 21:25 WG1245245
Magnesium 4.26 0.100 1.00 1.00 1 03/06/2019 21:25 WG1245245
Potassium 0.423 J 0.0370 1.00 1.00 1 03/06/2019 21:25 WG1245245
Selenium 0.000484 J 0.000380 0.00200 0.00200 1 03/06/2019 21:25 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:25 WG1245245
Sodium 95.9 0.110 1.00 1.00 1 03/06/2019 21:25 WG1245245

03/13/19 15:42
16:10 35 of 161

1
2
Benzene U 0.000190 0.000500 0.000500 1 03/06/2019 05:38 WG1245643
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/06/2019 05:38 WG1245643
4
Cn
Tr
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 08:00 WG1245479 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 08:00 WG1245479 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 08:00 WG1245479
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 08:00 WG1245479
Qc
(S) o-Terphenyl 82.9 70.0-130 03/06/2019 08:00 WG1245479
8
Gl
9
Al
10
Sc

03/13/19 15:42
16:10 36 of 161

Cp
2
3
Cn
Alkalinity 277 2.71 20.0 20.0 1 03/07/2019 15:50 WG1245955
5
6
Sr

Qc
Chloride 10.9 0.0519 1.00 1.00 1 03/06/2019 05:50 WG1245159 8
Sulfate 5.99 0.0774 5.00 5.00 1 03/06/2019 05:50 WG1245159 Gl
9
Sc
pH 7.46 T8 1 03/05/2019 11:55 WG1245130
Sample Narrative:
L1075168-10 WG1245130: 7.46 at 13.7C


Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 10:13 WG1245002

Arsenic 0.00397 0.000250 0.00200 0.00200 1 03/06/2019 21:30 WG1245245
Barium 0.546 0.000360 0.00500 0.00500 1 03/06/2019 21:30 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 21:30 WG1245245
Calcium 58.4 0.0460 1.00 1.00 1 03/06/2019 21:30 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 21:30 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 21:30 WG1245245
Magnesium 11.1 0.100 1.00 1.00 1 03/06/2019 21:30 WG1245245
Potassium 0.277 J 0.0370 1.00 1.00 1 03/06/2019 21:30 WG1245245
Selenium U 0.000380 0.00200 0.00200 1 03/06/2019 21:30 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:30 WG1245245
Sodium 46.8 0.110 1.00 1.00 1 03/06/2019 21:30 WG1245245

03/13/19 15:42
16:10 37 of 161

1
2
Benzene U 0.000190 0.000500 0.000500 1 03/06/2019 05:59 WG1245643
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/06/2019 05:59 WG1245643
4
Cn
Tr
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 17:54 WG1245678 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 17:54 WG1245678 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 17:54 WG1245678
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 17:54 WG1245678
Qc
(S) o-Terphenyl 89.2 70.0-130 03/06/2019 17:54 WG1245678
8
Gl
9
Al
10
Sc

03/13/19 15:42
16:10 38 of 161

Cp
2
3
Cn
Alkalinity 298 2.71 20.0 20.0 1 03/07/2019 15:58 WG1245955
5
6
Sr

Qc
Chloride 858 1.04 1.00 20.0 20 03/06/2019 06:37 WG1245159 8
Sulfate 14.9 0.0774 5.00 5.00 1 03/06/2019 10:28 WG1245159 Gl
9
Sc
pH 6.95 T8 1 03/05/2019 11:55 WG1245130
Sample Narrative:
L1075168-11 WG1245130: 6.95 at 12.9C


Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 10:15 WG1245002

Arsenic 0.0199 0.000250 0.00200 0.00200 1 03/06/2019 21:35 WG1245245
Barium 3.06 0.000360 0.00500 0.00500 1 03/06/2019 21:35 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 21:35 WG1245245
Calcium 265 0.0460 1.00 1.00 1 03/06/2019 21:35 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 21:35 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 21:35 WG1245245
Magnesium 27.9 0.100 1.00 1.00 1 03/06/2019 21:35 WG1245245
Potassium 4.83 0.0370 1.00 1.00 1 03/06/2019 21:35 WG1245245
Selenium U 0.000380 0.00200 0.00200 1 03/06/2019 21:35 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:35 WG1245245
Sodium 270 0.110 1.00 1.00 1 03/06/2019 21:35 WG1245245

03/13/19 15:42
16:10 39 of 161

1
2
Benzene U 0.000190 0.000500 0.000500 1 03/06/2019 06:20 WG1245643
Tc
Toluene U 0.000412 0.00100 0.00100 1 03/06/2019 06:20 WG1245643
Total Xylene 0.000570 J J6 0.000510 0.00150 0.00150 1 03/06/2019 06:20 WG1245643 Ss
4
Cn
Tr
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 18:10 WG1245678 6
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 18:10 WG1245678 Sr
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 18:10 WG1245678
7
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 18:10 WG1245678
Qc
(S) o-Terphenyl 93.1 70.0-130 03/06/2019 18:10 WG1245678
8
Gl
9
Al
10
Sc

03/13/19 15:42
16:10 40 of 161

Cp
2
3
Cn
Alkalinity 361 2.71 20.0 20.0 1 03/07/2019 16:05 WG1245955
5
6
Sr

Qc
Chloride 885 1.04 1.00 20.0 20 03/06/2019 06:52 WG1245159 8
Sulfate 18.5 0.0774 5.00 5.00 1 03/06/2019 10:43 WG1245159 Gl
9
Sc
pH 6.88 T8 1 03/05/2019 11:55 WG1245130
Sample Narrative:
L1075168-12 WG1245130: 6.88 at 12.3C


Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 10:17 WG1245002

Arsenic 0.00129 J 0.000250 0.00200 0.00200 1 03/06/2019 21:39 WG1245245
Barium 3.57 0.000360 0.00500 0.00500 1 03/06/2019 21:39 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 21:39 WG1245245
Calcium 260 0.0460 1.00 1.00 1 03/06/2019 21:39 WG1245245
Chromium U 0.000540 0.00200 0.00200 1 03/06/2019 21:39 WG1245245
Lead U 0.000240 0.00200 0.00200 1 03/06/2019 21:39 WG1245245
Magnesium 27.0 0.100 1.00 1.00 1 03/06/2019 21:39 WG1245245
Potassium 3.88 0.0370 1.00 1.00 1 03/06/2019 21:39 WG1245245
Selenium U 0.000380 0.00200 0.00200 1 03/06/2019 21:39 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:39 WG1245245
Sodium 307 0.110 1.00 1.00 1 03/06/2019 21:39 WG1245245

03/13/19 15:42
16:10 41 of 161

1
2
Acetone U 0.0100 0.0500 0.0500 1 03/05/2019 20:52 WG1245356
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/05/2019 20:52 WG1245356
Benzene U 0.000331 0.00100 0.00100 1 03/05/2019 20:52 WG1245356 Ss
4
Cn
Bromoform U 0.000469 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
6
Sr
8
Chloroform U 0.000324 0.00500 0.00500 1 03/05/2019 20:52 WG1245356
Gl
10
Sc
Ethylbenzene U 0.000384 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
2-Butanone (MEK) U 0.00393 0.0100 0.0100 1 03/05/2019 20:52 WG1245356
Naphthalene U 0.00100 0.00500 0.00500 1 03/05/2019 20:52 WG1245356
Styrene U 0.000307 0.00100 0.00100 1 03/05/2019 20:52 WG1245356
Toluene U 0.000412 0.00100 0.00100 1 03/05/2019 20:52 WG1245356

03/13/19 15:42
16:10 42 of 161

1
2
Tc
4
Cn
1,3,5-Trimethylbenzene U 0.000387 0.00100 0.00100 1 03/05/2019 20:52 WG1245356 5
Xylenes, Total U 0.00106 0.00300 0.00300 1 03/05/2019 20:52 WG1245356
6
(S) Toluene-d8 108 80.0-120 03/05/2019 20:52 WG1245356
Sr
Qc
8
9
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 18:26 WG1245678
Al
TPH C12 - C28 U 0.600 0.900 0.900 1 03/06/2019 18:26 WG1245678
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 18:26 WG1245678 10
TPH C6 - C35 U 0.600 0.900 0.900 1 03/06/2019 18:26 WG1245678 Sc
(S) o-Terphenyl 93.0 70.0-130 03/06/2019 18:26 WG1245678

Anthracene U 0.000291 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
Benzidine U 0.00432 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
Chrysene U 0.000332 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
Fluorene U 0.000323 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
Isophorone U 0.000272 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
Naphthalene U 0.000372 0.00100 0.00100 1 03/07/2019 17:03 WG1246279

03/13/19 15:42
16:10 43 of 161

1
2
Tc
4
Cn
Diethyl phthalate 0.000491 J 0.000282 0.00300 0.00300 1 03/07/2019 17:03 WG1246279 Tr
6
Sr
Pyrene U 0.000330 0.00100 0.00100 1 03/07/2019 17:03 WG1246279
8
Gl
2-Nitrophenol U 0.000320 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
10
4-Nitrophenol U 0.00201 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
Sc
Phenol 0.00127 J 0.000334 0.0100 0.0100 1 03/07/2019 17:03 WG1246279
(S) Phenol-d5 21.1 10.0-120 03/07/2019 17:03 WG1246279
(S) p-Terphenyl-d14 66.6 10.0-128 03/07/2019 17:03 WG1246279

03/13/19 15:42
16:10 44 of 161

Cp
2
Dissolved Solids 15600 56.4 200 200 1 03/07/2019 23:09 WG1246058 Tc
3
Cn
Alkalinity 123 2.71 20.0 20.0 1 03/07/2019 16:12 WG1245955
5
6
Sr

Qc
Chloride 7610 5.19 1.00 100 100 03/06/2019 07:23 WG1245159 8
Sulfate 0.291 J 0.0774 5.00 5.00 1 03/06/2019 10:59 WG1245159 Gl
9
Sc
pH 6.16 T8 1 03/05/2019 11:55 WG1245130
Sample Narrative:
L1075168-13 WG1245130: 6.16 at 12.4C


Mercury 0.0000566 J 0.0000490 0.000200 0.000200 1 03/05/2019 10:25 WG1245002

Arsenic 0.0582 0.000250 0.00200 0.00200 1 03/06/2019 21:44 WG1245245
Barium 28.9 0.00180 0.00500 0.0250 5 03/06/2019 22:44 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 21:44 WG1245245
Calcium 1480 0.230 1.00 5.00 5 03/06/2019 22:44 WG1245245
Chromium 0.00140 BJ 0.000540 0.00200 0.00200 1 03/06/2019 21:44 WG1245245
Lead 0.000647 J 0.000240 0.00200 0.00200 1 03/06/2019 21:44 WG1245245
Magnesium 4.00 0.100 1.00 1.00 1 03/06/2019 21:44 WG1245245
Potassium 156 0.0370 1.00 1.00 1 03/06/2019 21:44 WG1245245
Selenium 0.00172 J 0.000380 0.00200 0.00200 1 03/06/2019 21:44 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:44 WG1245245
Sodium 2670 0.550 1.00 5.00 5 03/06/2019 22:44 WG1245245

03/13/19 15:42
16:10 45 of 161

1
2
Acetone 0.0360 J 0.0100 0.0500 0.0500 1 03/05/2019 21:13 WG1245356
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/05/2019 21:13 WG1245356
Benzene 0.00547 0.000331 0.00100 0.00100 1 03/05/2019 21:13 WG1245356 Ss
4
Cn
Bromoform U 0.000469 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
6
Sr
8
Chloroform U 0.000324 0.00500 0.00500 1 03/05/2019 21:13 WG1245356
Gl
10
Sc
Ethylbenzene 0.00434 0.000384 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Isopropylbenzene 0.000430 J 0.000326 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
2-Butanone (MEK) 0.00713 J 0.00393 0.0100 0.0100 1 03/05/2019 21:13 WG1245356
4-Methyl-2-pentanone (MIBK) 0.0656 0.00214 0.0100 0.0100 1 03/05/2019 21:13 WG1245356
Methyl tert-butyl ether 0.00101 0.000367 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Naphthalene 0.0249 0.00100 0.00500 0.00500 1 03/05/2019 21:13 WG1245356
n-Propylbenzene 0.000559 J 0.000349 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Styrene U 0.000307 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Toluene 0.00360 0.000412 0.00100 0.00100 1 03/05/2019 21:13 WG1245356

03/13/19 15:42
16:10 46 of 161

1
2
Tc
4
1,2,4-Trimethylbenzene 0.00261 0.000373 0.00100 0.00100 1 03/05/2019 21:13 WG1245356
Cn
1,3,5-Trimethylbenzene 0.000880 J 0.000387 0.00100 0.00100 1 03/05/2019 21:13 WG1245356 5
Xylenes, Total 0.0113 0.00106 0.00300 0.00300 1 03/05/2019 21:13 WG1245356
6
(S) Toluene-d8 105 80.0-120 03/05/2019 21:13 WG1245356
Sr
Qc
8
9
TPH C6 - C12 1.39 0.600 0.900 0.900 1 03/06/2019 18:42 WG1245678
Al
TPH C12 - C28 14.4 0.600 0.900 0.900 1 03/06/2019 18:42 WG1245678
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 18:42 WG1245678 10
TPH C6 - C35 15.8 0.600 0.900 0.900 1 03/06/2019 18:42 WG1245678 Sc
(S) o-Terphenyl 89.6 70.0-130 03/06/2019 18:42 WG1245678

Anthracene U 0.000291 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
Benzidine U 0.00432 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
Chrysene U 0.000332 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
Fluorene U 0.000323 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
Isophorone U 0.000272 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
Naphthalene 0.00168 0.000372 0.00100 0.00100 1 03/07/2019 22:11 WG1246279

03/13/19 15:42
16:10 47 of 161

1
2
Tc
4
Cn
Diethyl phthalate U 0.000282 0.00300 0.00300 1 03/07/2019 22:11 WG1246279 Tr
6
Sr
Pyrene U 0.000330 0.00100 0.00100 1 03/07/2019 22:11 WG1246279
8
Gl
2,4-Dimethylphenol 0.00584 J 0.000264 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
2-Nitrophenol U 0.000320 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
10
4-Nitrophenol U 0.00201 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
Sc
Phenol 0.00244 J 0.000334 0.0100 0.0100 1 03/07/2019 22:11 WG1246279
(S) Phenol-d5 23.5 10.0-120 03/07/2019 22:11 WG1246279
(S) p-Terphenyl-d14 58.4 10.0-128 03/07/2019 22:11 WG1246279

03/13/19 15:42
16:10 48 of 161
PSW-1 SAMPLE RESULTS - 14 ONE LAB. NATIONWIDE.

Cp
2
3
Cn
Alkalinity 346 2.71 20.0 20.0 1 03/07/2019 16:18 WG1245955
5
6
Sr

Qc
Chloride 584 0.519 1.00 10.0 10 03/06/2019 07:38 WG1245159 8
Sulfate 105 0.774 5.00 50.0 10 03/06/2019 07:38 WG1245159 Gl
9
Sc
pH 7.77 T8 1 03/05/2019 11:55 WG1245130
Sample Narrative:
L1075168-14 WG1245130: 7.77 at 12.2C


Mercury 0.0000997 J 0.0000490 0.000200 0.000200 1 03/05/2019 10:27 WG1245002

Arsenic 0.0250 0.000250 0.00200 0.00200 1 03/06/2019 21:49 WG1245245
Barium 1.70 0.000360 0.00500 0.00500 1 03/06/2019 21:49 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 21:49 WG1245245
Calcium 102 0.0460 1.00 1.00 1 03/06/2019 21:49 WG1245245
Chromium 0.00374 B 0.000540 0.00200 0.00200 1 03/06/2019 21:49 WG1245245
Lead 0.00526 0.000240 0.00200 0.00200 1 03/06/2019 21:49 WG1245245
Magnesium 7.58 0.100 1.00 1.00 1 03/06/2019 21:49 WG1245245
Potassium 17.7 0.0370 1.00 1.00 1 03/06/2019 21:49 WG1245245
Selenium 0.00166 J 0.000380 0.00200 0.00200 1 03/06/2019 21:49 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 21:49 WG1245245
Sodium 433 0.110 1.00 1.00 1 03/06/2019 21:49 WG1245245

03/13/19 15:42
16:10 49 of 161

1
2
Acetone 0.228 0.0100 0.0500 0.0500 1 03/05/2019 21:33 WG1245356
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/05/2019 21:33 WG1245356
Benzene 0.000375 J 0.000331 0.00100 0.00100 1 03/05/2019 21:33 WG1245356 Ss
4
Cn
Bromoform U 0.000469 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
6
Sr
8
Chloroform U 0.000324 0.00500 0.00500 1 03/05/2019 21:33 WG1245356
Gl
10
Sc
Ethylbenzene 0.00254 0.000384 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
2-Butanone (MEK) 0.00707 J 0.00393 0.0100 0.0100 1 03/05/2019 21:33 WG1245356
Naphthalene 0.00147 J 0.00100 0.00500 0.00500 1 03/05/2019 21:33 WG1245356
Styrene U 0.000307 0.00100 0.00100 1 03/05/2019 21:33 WG1245356
Toluene 0.00750 0.000412 0.00100 0.00100 1 03/05/2019 21:33 WG1245356

03/13/19 15:42
16:10 50 of 161

1
2
Tc
4
Cn
Xylenes, Total 0.0214 0.00106 0.00300 0.00300 1 03/05/2019 21:33 WG1245356
6
(S) Toluene-d8 108 80.0-120 03/05/2019 21:33 WG1245356
Sr
Qc
8
9
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 18:59 WG1245678
Al
TPH C12 - C28 9.56 0.600 0.900 0.900 1 03/06/2019 18:59 WG1245678
TPH C28 - C35 0.749 J 0.600 0.900 0.900 1 03/06/2019 18:59 WG1245678 10
TPH C6 - C35 10.3 0.600 0.900 0.900 1 03/06/2019 18:59 WG1245678 Sc
(S) o-Terphenyl 86.7 70.0-130 03/06/2019 18:59 WG1245678

Anthracene U 0.00291 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
Benzidine U J3 0.0432 0.0100 0.100 10 03/07/2019 07:37 WG1245476
Chrysene U 0.00332 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
Fluorene U 0.00323 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
Isophorone U 0.00272 0.0100 0.100 10 03/07/2019 07:37 WG1245476
Naphthalene U 0.00372 0.00100 0.0100 10 03/07/2019 07:37 WG1245476

03/13/19 15:42
16:10 51 of 161

1
2
Tc
4
Cn
6
Sr
Pyrene U 0.00330 0.00100 0.0100 10 03/07/2019 07:37 WG1245476
8
Gl
2-Nitrophenol U 0.00320 0.0100 0.100 10 03/07/2019 07:37 WG1245476
10
4-Nitrophenol U 0.0201 0.0100 0.100 10 03/07/2019 07:37 WG1245476
Sc
Pentachlorophenol U 0.00313 0.0100 0.100 10 03/07/2019 07:37 WG1245476
Phenol U 0.00334 0.0100 0.100 10 03/07/2019 07:37 WG1245476
(S) Phenol-d5 33.4 10.0-120 03/07/2019 07:37 WG1245476
(S) p-Terphenyl-d14 87.1 10.0-128 03/07/2019 07:37 WG1245476
Sample Narrative:
L1075168-14 WG1245476: Dilution due to viscosity.

03/13/19 15:42
16:10 52 of 161

Cp
2
3
Cn
Alkalinity 348 2.71 20.0 20.0 1 03/07/2019 16:26 WG1245955
5
6
Sr

Qc
Chloride 595 0.519 1.00 10.0 10 03/06/2019 07:54 WG1245159 8
Sulfate 107 0.774 5.00 50.0 10 03/06/2019 07:54 WG1245159 Gl
9
Sc
pH 7.88 T8 1 03/05/2019 11:55 WG1245130
Sample Narrative:
L1075168-15 WG1245130: 7.88 at 12.5C


Mercury 0.0000997 J 0.0000490 0.000200 0.000200 1 03/05/2019 10:30 WG1245002

Arsenic 0.0249 0.000250 0.00200 0.00200 1 03/06/2019 22:20 WG1245245
Barium 1.40 0.000360 0.00500 0.00500 1 03/06/2019 22:20 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 22:20 WG1245245
Calcium 102 0.0460 1.00 1.00 1 03/06/2019 22:20 WG1245245
Chromium 0.00370 B 0.000540 0.00200 0.00200 1 03/06/2019 22:20 WG1245245
Lead 0.00392 0.000240 0.00200 0.00200 1 03/06/2019 22:20 WG1245245
Magnesium 7.70 0.100 1.00 1.00 1 03/06/2019 22:20 WG1245245
Potassium 17.8 0.0370 1.00 1.00 1 03/06/2019 22:20 WG1245245
Selenium 0.00153 J 0.000380 0.00200 0.00200 1 03/06/2019 22:20 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 22:20 WG1245245
Sodium 439 0.110 1.00 1.00 1 03/06/2019 22:20 WG1245245

03/13/19 15:42
16:10 53 of 161

1
2
Acetone 0.244 0.0100 0.0500 0.0500 1 03/06/2019 16:03 WG1245979
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/06/2019 16:03 WG1245979
Benzene 0.000379 J 0.000331 0.00100 0.00100 1 03/06/2019 16:03 WG1245979 Ss
4
Cn
Bromoform U 0.000469 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
6
Sr
8
Chloroform U 0.000324 0.00500 0.00500 1 03/06/2019 16:03 WG1245979
Gl
10
Sc
Ethylbenzene 0.00215 0.000384 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
2-Butanone (MEK) 0.0122 0.00393 0.0100 0.0100 1 03/06/2019 16:03 WG1245979
Naphthalene 0.00118 J 0.00100 0.00500 0.00500 1 03/06/2019 16:03 WG1245979
Styrene U 0.000307 0.00100 0.00100 1 03/06/2019 16:03 WG1245979
Toluene 0.00635 0.000412 0.00100 0.00100 1 03/06/2019 16:03 WG1245979

03/13/19 15:42
16:10 54 of 161

1
2
Tc
4
Cn
Xylenes, Total 0.0182 0.00106 0.00300 0.00300 1 03/06/2019 16:03 WG1245979
6
(S) Toluene-d8 98.9 80.0-120 03/06/2019 16:03 WG1245979
Sr
Qc
8
9
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 19:15 WG1245678
Al
TPH C12 - C28 10.3 0.600 0.900 0.900 1 03/06/2019 19:15 WG1245678
TPH C28 - C35 0.817 J 0.600 0.900 0.900 1 03/06/2019 19:15 WG1245678 10
TPH C6 - C35 11.1 0.600 0.900 0.900 1 03/06/2019 19:15 WG1245678 Sc
(S) o-Terphenyl 93.3 70.0-130 03/06/2019 19:15 WG1245678

Anthracene U 0.00291 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
Benzidine U J3 0.0432 0.0100 0.100 10 03/07/2019 08:00 WG1245476
Chrysene U 0.00332 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
Fluorene U 0.00323 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
Isophorone U 0.00272 0.0100 0.100 10 03/07/2019 08:00 WG1245476
Naphthalene U 0.00372 0.00100 0.0100 10 03/07/2019 08:00 WG1245476

03/13/19 15:42
16:10 55 of 161

1
2
Tc
4
Cn
6
Sr
Pyrene U 0.00330 0.00100 0.0100 10 03/07/2019 08:00 WG1245476
8
Gl
2-Nitrophenol U 0.00320 0.0100 0.100 10 03/07/2019 08:00 WG1245476
10
4-Nitrophenol U 0.0201 0.0100 0.100 10 03/07/2019 08:00 WG1245476
Sc
Phenol U 0.00334 0.0100 0.100 10 03/07/2019 08:00 WG1245476
(S) Phenol-d5 32.0 10.0-120 03/07/2019 08:00 WG1245476
(S) 2,4,6-Tribromophenol 111 10.0-155 03/07/2019 08:00 WG1245476
(S) p-Terphenyl-d14 95.5 10.0-128 03/07/2019 08:00 WG1245476
Sample Narrative:

03/13/19 15:42
16:10 56 of 161

Cp
2
3
Cn
Alkalinity 347 2.71 20.0 20.0 1 03/07/2019 16:34 WG1245955
5
6
Sr

Qc
Chloride 601 0.519 1.00 10.0 10 03/06/2019 08:09 WG1245159 8
Sulfate 107 0.774 5.00 50.0 10 03/06/2019 08:09 WG1245159 Gl
9
Sc
pH 7.91 T8 1 03/05/2019 11:55 WG1245130
Sample Narrative:
L1075168-16 WG1245130: 7.91 at 13.3C


Mercury 0.000104 J 0.0000490 0.000200 0.000200 1 03/05/2019 10:32 WG1245002

Arsenic 0.0258 0.000250 0.00200 0.00200 1 03/06/2019 22:25 WG1245245
Barium 2.82 0.000360 0.00500 0.00500 1 03/06/2019 22:25 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 22:25 WG1245245
Calcium 108 0.0460 1.00 1.00 1 03/06/2019 22:25 WG1245245
Chromium 0.00475 B 0.000540 0.00200 0.00200 1 03/06/2019 22:25 WG1245245
Lead 0.00803 0.000240 0.00200 0.00200 1 03/06/2019 22:25 WG1245245
Magnesium 7.87 0.100 1.00 1.00 1 03/06/2019 22:25 WG1245245
Potassium 17.7 0.0370 1.00 1.00 1 03/06/2019 22:25 WG1245245
Selenium 0.00167 J 0.000380 0.00200 0.00200 1 03/06/2019 22:25 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 22:25 WG1245245
Sodium 438 0.110 1.00 1.00 1 03/06/2019 22:25 WG1245245

03/13/19 15:42
16:10 57 of 161

1
2
Acetone 0.266 0.0100 0.0500 0.0500 1 03/06/2019 16:22 WG1245979
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/06/2019 16:22 WG1245979
Benzene 0.000338 J 0.000331 0.00100 0.00100 1 03/06/2019 16:22 WG1245979 Ss
4
Cn
Bromoform U 0.000469 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
6
Sr
8
Chloroform U 0.000324 0.00500 0.00500 1 03/06/2019 16:22 WG1245979
Gl
10
Sc
Ethylbenzene 0.00222 0.000384 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
2-Butanone (MEK) 0.0123 0.00393 0.0100 0.0100 1 03/06/2019 16:22 WG1245979
Naphthalene 0.00124 J 0.00100 0.00500 0.00500 1 03/06/2019 16:22 WG1245979
Styrene U 0.000307 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Toluene 0.00691 0.000412 0.00100 0.00100 1 03/06/2019 16:22 WG1245979

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1
2
Tc
4
Cn
1,2,3-Trimethylbenzene 0.000975 J 0.000321 0.00100 0.00100 1 03/06/2019 16:22 WG1245979
Xylenes, Total 0.0200 0.00106 0.00300 0.00300 1 03/06/2019 16:22 WG1245979
6
(S) Toluene-d8 96.2 80.0-120 03/06/2019 16:22 WG1245979
Sr
(S) 4-Bromofluorobenzene 129 J1 77.0-126 03/06/2019 16:22 WG1245979
Qc
8
9
TPH C6 - C12 0.641 J 0.600 0.900 0.900 1 03/06/2019 19:31 WG1245678
Al
TPH C12 - C28 9.26 0.600 0.900 0.900 1 03/06/2019 19:31 WG1245678
TPH C28 - C35 0.762 J 0.600 0.900 0.900 1 03/06/2019 19:31 WG1245678 10
TPH C6 - C35 10.7 0.600 0.900 0.900 1 03/06/2019 19:31 WG1245678 Sc
(S) o-Terphenyl 85.1 70.0-130 03/06/2019 19:31 WG1245678

Anthracene U 0.00291 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
Benzidine U J3 0.0432 0.0100 0.100 10 03/07/2019 08:24 WG1245476
Chrysene U 0.00332 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
Fluorene U 0.00323 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
Isophorone U 0.00272 0.0100 0.100 10 03/07/2019 08:24 WG1245476
Naphthalene U 0.00372 0.00100 0.0100 10 03/07/2019 08:24 WG1245476

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1
2
Tc
4
Cn
6
Sr
Pyrene U 0.00330 0.00100 0.0100 10 03/07/2019 08:24 WG1245476
8
Gl
2-Nitrophenol U 0.00320 0.0100 0.100 10 03/07/2019 08:24 WG1245476
10
4-Nitrophenol U 0.0201 0.0100 0.100 10 03/07/2019 08:24 WG1245476
Sc
Phenol U 0.00334 0.0100 0.100 10 03/07/2019 08:24 WG1245476
(S) Phenol-d5 29.5 10.0-120 03/07/2019 08:24 WG1245476
(S) p-Terphenyl-d14 76.0 10.0-128 03/07/2019 08:24 WG1245476
Sample Narrative:

03/13/19 15:42
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Cp
2
3
Cn
Alkalinity 348 2.71 20.0 20.0 1 03/07/2019 16:42 WG1245955
5
6
Sr

Qc
Chloride 601 0.519 1.00 10.0 10 03/06/2019 08:24 WG1245159 8
Sulfate 111 0.774 5.00 50.0 10 03/06/2019 08:24 WG1245159 Gl
9
Sc
pH 7.86 T8 1 03/06/2019 09:50 WG1245737
Sample Narrative:
L1075168-17 WG1245737: 7.86 at 17.6C


Mercury 0.000109 J 0.0000490 0.000200 0.000200 1 03/05/2019 10:35 WG1245002

Arsenic 0.0260 0.000250 0.00200 0.00200 1 03/06/2019 22:30 WG1245245
Barium 3.17 0.000360 0.00500 0.00500 1 03/06/2019 22:30 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 22:30 WG1245245
Calcium 110 0.0460 1.00 1.00 1 03/06/2019 22:30 WG1245245
Chromium 0.00612 0.000540 0.00200 0.00200 1 03/06/2019 22:30 WG1245245
Lead 0.00902 0.000240 0.00200 0.00200 1 03/06/2019 22:30 WG1245245
Magnesium 8.27 0.100 1.00 1.00 1 03/06/2019 22:30 WG1245245
Potassium 18.0 0.0370 1.00 1.00 1 03/06/2019 22:30 WG1245245
Selenium 0.00225 0.000380 0.00200 0.00200 1 03/06/2019 22:30 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 22:30 WG1245245
Sodium 442 0.110 1.00 1.00 1 03/06/2019 22:30 WG1245245

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1
2
Acetone 0.0999 0.0100 0.0500 0.0500 1 03/06/2019 16:42 WG1245979
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/06/2019 16:42 WG1245979
Benzene 0.000368 J 0.000331 0.00100 0.00100 1 03/06/2019 16:42 WG1245979 Ss
4
Cn
Bromoform U 0.000469 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
6
Sr
8
Chloroform U 0.000324 0.00500 0.00500 1 03/06/2019 16:42 WG1245979
Gl
10
Sc
Ethylbenzene 0.00222 0.000384 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
2-Butanone (MEK) 0.00894 J 0.00393 0.0100 0.0100 1 03/06/2019 16:42 WG1245979
Naphthalene 0.00116 J 0.00100 0.00500 0.00500 1 03/06/2019 16:42 WG1245979
Styrene U 0.000307 0.00100 0.00100 1 03/06/2019 16:42 WG1245979
Toluene 0.00697 0.000412 0.00100 0.00100 1 03/06/2019 16:42 WG1245979

03/13/19 15:42
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1
2
Tc
4
Cn
1,3,5-Trimethylbenzene 0.00103 0.000387 0.00100 0.00100 1 03/06/2019 16:42 WG1245979 5
Xylenes, Total 0.0186 0.00106 0.00300 0.00300 1 03/06/2019 16:42 WG1245979
6
(S) Toluene-d8 103 80.0-120 03/06/2019 16:42 WG1245979
Sr
(S) 4-Bromofluorobenzene 94.6 77.0-126 03/06/2019 16:42 WG1245979
Qc
8
9
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 19:48 WG1245678
Al
TPH C12 - C28 9.96 0.600 0.900 0.900 1 03/06/2019 19:48 WG1245678
TPH C28 - C35 0.754 J 0.600 0.900 0.900 1 03/06/2019 19:48 WG1245678 10
TPH C6 - C35 10.7 0.600 0.900 0.900 1 03/06/2019 19:48 WG1245678 Sc
(S) o-Terphenyl 90.7 70.0-130 03/06/2019 19:48 WG1245678

Anthracene U 0.00291 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
Benzidine U J3 0.0432 0.0100 0.100 10 03/07/2019 08:48 WG1245476
Chrysene U 0.00332 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
Fluorene U 0.00323 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
Isophorone U 0.00272 0.0100 0.100 10 03/07/2019 08:48 WG1245476
Naphthalene U 0.00372 0.00100 0.0100 10 03/07/2019 08:48 WG1245476

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1
2
Tc
4
Cn
6
Sr
Pyrene U 0.00330 0.00100 0.0100 10 03/07/2019 08:48 WG1245476
8
Gl
2-Nitrophenol U 0.00320 0.0100 0.100 10 03/07/2019 08:48 WG1245476
10
4-Nitrophenol U 0.0201 0.0100 0.100 10 03/07/2019 08:48 WG1245476
Sc
Phenol 0.00646 J 0.00334 0.0100 0.100 10 03/07/2019 08:48 WG1245476
(S) Phenol-d5 26.8 10.0-120 03/07/2019 08:48 WG1245476
(S) p-Terphenyl-d14 78.6 10.0-128 03/07/2019 08:48 WG1245476
Sample Narrative:

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SK-1 SAMPLE RESULTS - 18 ONE LAB. NATIONWIDE.

Cp
2
Dissolved Solids 116 J3 2.82 10.0 10.0 1 03/08/2019 01:53 WG1246059 Tc
3
Cn
Alkalinity 34.0 2.71 20.0 20.0 1 03/07/2019 16:49 WG1245955
5
6
Sr

Qc
Chloride 15.7 0.0519 1.00 1.00 1 03/06/2019 11:14 WG1245159 8
Sulfate 4.61 J 0.0774 5.00 5.00 1 03/06/2019 11:14 WG1245159 Gl
9
Sc
pH 6.89 T8 1 03/06/2019 09:50 WG1245737
Sample Narrative:
L1075168-18 WG1245737: 6.89 at 17.6C


Mercury U 0.0000490 0.000200 0.000200 1 03/05/2019 10:37 WG1245002

Arsenic 0.00178 J 0.000250 0.00200 0.00200 1 03/06/2019 22:34 WG1245245
Barium 0.282 0.000360 0.00500 0.00500 1 03/06/2019 22:34 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 22:34 WG1245245
Calcium 10.8 0.0460 1.00 1.00 1 03/06/2019 22:34 WG1245245
Chromium 0.00337 B 0.000540 0.00200 0.00200 1 03/06/2019 22:34 WG1245245
Lead 0.00231 0.000240 0.00200 0.00200 1 03/06/2019 22:34 WG1245245
Magnesium 2.55 0.100 1.00 1.00 1 03/06/2019 22:34 WG1245245
Potassium 3.00 0.0370 1.00 1.00 1 03/06/2019 22:34 WG1245245
Selenium 0.000734 J 0.000380 0.00200 0.00200 1 03/06/2019 22:34 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 22:34 WG1245245
Sodium 12.1 0.110 1.00 1.00 1 03/06/2019 22:34 WG1245245

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1
2
Acetone U 0.0100 0.0500 0.0500 1 03/06/2019 17:01 WG1245979
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/06/2019 17:01 WG1245979
Benzene 0.00382 0.000331 0.00100 0.00100 1 03/06/2019 17:01 WG1245979 Ss
4
Cn
Bromoform 0.00345 0.000469 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
n-Butylbenzene 0.000593 J 0.000361 0.00100 0.00100 1 03/06/2019 17:01 WG1245979 Tr
sec-Butylbenzene 0.000517 J 0.000365 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
6
Sr
8
Chloroform U 0.000324 0.00500 0.00500 1 03/06/2019 17:01 WG1245979
Gl
2-Chlorotoluene 0.000869 J 0.000375 0.00100 0.00100 1 03/06/2019 17:01 WG1245979 9
10
Sc
Dibromomethane 0.000372 J 0.000346 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Ethylbenzene 0.0281 0.000384 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Isopropylbenzene 0.00155 0.000326 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
2-Butanone (MEK) U 0.00393 0.0100 0.0100 1 03/06/2019 17:01 WG1245979
Methyl tert-butyl ether 0.000432 J 0.000367 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Naphthalene 0.00525 0.00100 0.00500 0.00500 1 03/06/2019 17:01 WG1245979
n-Propylbenzene 0.00394 0.000349 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Styrene 0.000574 J 0.000307 0.00100 0.00100 1 03/06/2019 17:01 WG1245979
Toluene 0.0605 0.000412 0.00100 0.00100 1 03/06/2019 17:01 WG1245979

03/13/19 15:42
16:10 66 of 161

1
2
Tc
4
Cn
1,3,5-Trimethylbenzene 0.00712 0.000387 0.00100 0.00100 1 03/06/2019 17:01 WG1245979 5
Xylenes, Total 0.213 0.00106 0.00300 0.00300 1 03/06/2019 17:01 WG1245979
6
(S) Toluene-d8 104 80.0-120 03/06/2019 17:01 WG1245979
Sr
Qc
8
9
TPH C6 - C12 0.622 J 0.600 0.900 0.900 1 03/06/2019 20:04 WG1245678
Al
TPH C12 - C28 0.816 J 0.600 0.900 0.900 1 03/06/2019 20:04 WG1245678
TPH C28 - C35 U 0.600 0.900 0.900 1 03/06/2019 20:04 WG1245678 10
TPH C6 - C35 1.44 0.600 0.900 0.900 1 03/06/2019 20:04 WG1245678 Sc
(S) o-Terphenyl 86.8 70.0-130 03/06/2019 20:04 WG1245678

Anthracene U 0.000291 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
Benzidine U J3 0.00432 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
Chrysene U 0.000332 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
Fluoranthene 0.000367 J 0.000310 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
Fluorene 0.000370 J 0.000323 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
Isophorone U 0.000272 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
Naphthalene U 0.000372 0.00100 0.00100 1 03/07/2019 04:26 WG1245476

03/13/19 15:42
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1
2
Tc
4
Cn
6
Sr
Pyrene U 0.000330 0.00100 0.00100 1 03/07/2019 04:26 WG1245476
8
Gl
2-Nitrophenol U 0.000320 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
10
4-Nitrophenol U 0.00201 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
Sc
Phenol 0.00140 J 0.000334 0.0100 0.0100 1 03/07/2019 04:26 WG1245476
(S) Phenol-d5 23.8 10.0-120 03/07/2019 04:26 WG1245476
(S) p-Terphenyl-d14 59.3 10.0-128 03/07/2019 04:26 WG1245476

03/13/19 15:42
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DUPLICATE 1 SAMPLE RESULTS - 19 ONE LAB. NATIONWIDE.

Cp
2
3
Cn
Alkalinity 339 2.71 20.0 20.0 1 03/07/2019 17:04 WG1245955
5
6
Sr

Qc
Chloride 606 0.519 1.00 10.0 10 03/06/2019 08:55 WG1245159 8
Sulfate 118 0.774 5.00 50.0 10 03/06/2019 08:55 WG1245159 Gl
9
Sc
pH 7.70 T8 1 03/06/2019 09:50 WG1245737
Sample Narrative:
L1075168-19 WG1245737: 7.7 at 17.8C


Mercury 0.0000943 J 0.0000490 0.000200 0.000200 1 03/05/2019 10:39 WG1245002

Arsenic 0.0257 0.000250 0.00200 0.00200 1 03/06/2019 22:39 WG1245245
Barium 1.52 0.000360 0.00500 0.00500 1 03/06/2019 22:39 WG1245245
Cadmium U 0.000160 0.00100 0.00100 1 03/06/2019 22:39 WG1245245
Calcium 102 0.0460 1.00 1.00 1 03/06/2019 22:39 WG1245245
Chromium 0.00390 B 0.000540 0.00200 0.00200 1 03/06/2019 22:39 WG1245245
Lead 0.00436 0.000240 0.00200 0.00200 1 03/06/2019 22:39 WG1245245
Magnesium 7.74 0.100 1.00 1.00 1 03/06/2019 22:39 WG1245245
Potassium 17.9 0.0370 1.00 1.00 1 03/06/2019 22:39 WG1245245
Selenium 0.00153 J 0.000380 0.00200 0.00200 1 03/06/2019 22:39 WG1245245
Silver U 0.000310 0.00200 0.00200 1 03/06/2019 22:39 WG1245245
Sodium 436 0.110 1.00 1.00 1 03/06/2019 22:39 WG1245245

03/13/19 15:42
16:10 69 of 161

1
2
Acetone 0.118 0.0100 0.0500 0.0500 1 03/06/2019 17:21 WG1245979
Tc
Acrolein U 0.00887 0.0500 0.0500 1 03/06/2019 17:21 WG1245979
Benzene U 0.000331 0.00100 0.00100 1 03/06/2019 17:21 WG1245979 Ss
4
Cn
Bromoform U 0.000469 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
6
Sr
8
Chloroform U 0.000324 0.00500 0.00500 1 03/06/2019 17:21 WG1245979
Gl
10
Sc
Ethylbenzene 0.00193 0.000384 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
2-Butanone (MEK) 0.00701 J 0.00393 0.0100 0.0100 1 03/06/2019 17:21 WG1245979
Naphthalene 0.00110 J 0.00100 0.00500 0.00500 1 03/06/2019 17:21 WG1245979
Styrene U 0.000307 0.00100 0.00100 1 03/06/2019 17:21 WG1245979
Toluene 0.00576 0.000412 0.00100 0.00100 1 03/06/2019 17:21 WG1245979

03/13/19 15:42
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1
2
Tc
4
Cn
Xylenes, Total 0.0162 0.00106 0.00300 0.00300 1 03/06/2019 17:21 WG1245979
6
(S) Toluene-d8 105 80.0-120 03/06/2019 17:21 WG1245979
Sr
Qc
8
9
TPH C6 - C12 U 0.600 0.900 0.900 1 03/06/2019 20:21 WG1245678
Al
TPH C12 - C28 8.96 0.600 0.900 0.900 1 03/06/2019 20:21 WG1245678
TPH C28 - C35 0.683 J 0.600 0.900 0.900 1 03/06/2019 20:21 WG1245678 10
TPH C6 - C35 9.64 0.600 0.900 0.900 1 03/06/2019 20:21 WG1245678 Sc
(S) o-Terphenyl 91.1 70.0-130 03/06/2019 20:21 WG1245678

Anthracene U 0.00291 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
Benzidine U J3 0.0432 0.0100 0.100 10 03/07/2019 09:13 WG1245476
Chrysene U 0.00332 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
Fluorene U 0.00323 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
Isophorone U 0.00272 0.0100 0.100 10 03/07/2019 09:13 WG1245476
Naphthalene U 0.00372 0.00100 0.0100 10 03/07/2019 09:13 WG1245476

03/13/19 15:42
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1
2
Tc
4
Cn
6
Sr
Pyrene U 0.00330 0.00100 0.0100 10 03/07/2019 09:13 WG1245476
8
Gl
2-Nitrophenol U 0.00320 0.0100 0.100 10 03/07/2019 09:13 WG1245476
10
4-Nitrophenol U 0.0201 0.0100 0.100 10 03/07/2019 09:13 WG1245476
Sc
Phenol U 0.00334 0.0100 0.100 10 03/07/2019 09:13 WG1245476
(S) Phenol-d5 25.7 10.0-120 03/07/2019 09:13 WG1245476
(S) p-Terphenyl-d14 76.7 10.0-128 03/07/2019 09:13 WG1245476
Sample Narrative:

03/13/19 15:42
16:10 72 of 161
PS-1 SAMPLE RESULTS - 20 ONE LAB. NATIONWIDE.

Cp
Analyte % date / time
2
Total Solids 63.3 1 03/06/2019 14:08 WG1245367 Tc
3
Wet Chemistry by Method 9050AMod Ss
Analyte umhos/cm umhos/cm umhos/cm umhos/cm date / time 4
Cn
Specific Conductance 933 10.0 10.0 10.0 1 03/06/2019 21:03 WG1245948
5
Wet Chemistry by Method 9056A Tr
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch
6
Analyte mg/kg mg/kg mg/kg mg/kg date / time Sr
Chloride 265 1.26 10.0 15.8 1 03/06/2019 18:51 WG1245719
7
Qc
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch 8
Analyte mg/kg mg/kg mg/kg mg/kg date / time

Gl
Mercury 0.748 0.00442 0.0200 0.0316 1 03/05/2019 09:02 WG1245047 9
Al
Metals (ICP) by Method 6010B
10
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Sc
Arsenic 17.2 0.726 2.00 3.16 1 03/07/2019 20:41 WG1245191
Barium 23500 1.34 0.500 3.95 5 03/08/2019 10:03 WG1245191
Cadmium U 0.553 0.500 3.95 5 03/08/2019 10:03 WG1245191
Chromium 28.0 0.221 1.00 1.58 1 03/07/2019 20:41 WG1245191
Lead 61.3 0.300 0.500 0.790 1 03/07/2019 20:41 WG1245191
Selenium 1.10 J 0.979 2.00 3.16 1 03/07/2019 20:41 WG1245191
Silver U 0.190 1.00 1.58 1 03/07/2019 20:41 WG1245191
Volatile Organic Compounds (GC/MS) by Method 8260B

Acetone 0.120 0.0216 0.0250 0.0395 1 03/06/2019 19:43 WG1245869
Acrylonitrile U 0.00300 0.0125 0.0197 1 03/06/2019 19:43 WG1245869
Benzene 0.00171 0.000632 0.00100 0.00158 1 03/06/2019 19:43 WG1245869
Bromoform U 0.00944 0.0250 0.0395 1 03/06/2019 19:43 WG1245869
Bromomethane U 0.00584 0.0125 0.0197 1 03/06/2019 19:43 WG1245869
n-Butylbenzene U 0.00606 0.0125 0.0197 1 03/06/2019 19:43 WG1245869
Chlorobenzene U 0.000905 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Chlorodibromomethane U 0.000711 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Chloroform U 0.000655 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
2-Chlorotoluene U 0.00145 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Dibromomethane U J4 0.00158 0.00500 0.00790 1 03/06/2019 19:43 WG1245869

03/13/19 15:42
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1
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cp
2
Tc
Dichlorodifluoromethane U 0.00129 0.00250 0.00395 1 03/06/2019 19:43 WG1245869 3
1,1-Dichloroethane U 0.000908 0.00250 0.00395 1 03/06/2019 19:43 WG1245869 Ss
4
Cn
trans-1,2-Dichloroethene U 0.00226 0.00500 0.00790 1 03/06/2019 19:43 WG1245869 5
1,2-Dichloropropane U 0.00201 0.00500 0.00790 1 03/06/2019 19:43 WG1245869 Tr
6
Sr
trans-1,3-Dichloropropene U 0.00242 0.00500 0.00790 1 03/06/2019 19:43 WG1245869 7
2,2-Dichloropropane U 0.00125 0.00250 0.00395 1 03/06/2019 19:43 WG1245869 Qc
8
Ethylbenzene 0.148 0.000837 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Gl
Isopropylbenzene 0.00499 0.00136 0.00250 0.00395 1 03/06/2019 19:43 WG1245869 9
p-Isopropyltoluene U 0.00368 0.00500 0.00790 1 03/06/2019 19:43 WG1245869 Al
2-Butanone (MEK) U 0.0197 0.0250 0.0395 1 03/06/2019 19:43 WG1245869
10
Sc
Naphthalene 0.0524 0.00493 0.0125 0.0197 1 03/06/2019 19:43 WG1245869
Styrene U 0.00431 0.0125 0.0197 1 03/06/2019 19:43 WG1245869
1,1,2,2-Tetrachloroethane U J4 0.000616 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Toluene 0.294 0.00197 0.00500 0.00790 1 03/06/2019 19:43 WG1245869
Trichloroethene U 0.000632 0.00100 0.00158 1 03/06/2019 19:43 WG1245869
Trichlorofluoromethane U 0.000790 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Vinyl chloride U 0.00108 0.00250 0.00395 1 03/06/2019 19:43 WG1245869
Xylenes, Total 1.05 0.00755 0.00650 0.0103 1 03/06/2019 19:43 WG1245869
(S) Toluene-d8 112 75.0-131 03/06/2019 19:43 WG1245869
(S) 1,2-Dichloroethane-d4 77.1 70.0-130 03/06/2019 19:43 WG1245869

TPH C6 - C12 U 23.7 50.0 79.0 1 03/10/2019 16:33 WG1246136
TPH C12 - C28 349 23.7 50.0 79.0 1 03/10/2019 16:33 WG1246136
TPH C28 - C35 59.7 J 23.7 50.0 79.0 1 03/10/2019 16:33 WG1246136
TPH C6 - C35 409 23.7 50.0 79.0 1 03/10/2019 16:33 WG1246136
(S) o-Terphenyl 111 70.0-130 03/10/2019 16:33 WG1246136

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Semi Volatile Organic Compounds (GC/MS) by Method 8270C

1
2
Tc
Anthracene U 0.0200 0.0333 0.105 2 03/05/2019 05:28 WG1244658 3
Benzidine U J4 0.201 0.333 1.05 2 03/05/2019 05:28 WG1244658 Ss
Benzo(a)anthracene 0.0336 J 0.0135 0.0333 0.105 2 03/05/2019 05:28 WG1244658
4
Benzo(b)fluoranthene 0.132 0.0220 0.0333 0.105 2 03/05/2019 05:28 WG1244658
Cn
Benzo(g,h,i)perylene 0.0613 J 0.0228 0.0333 0.105 2 03/05/2019 05:28 WG1244658 5
Benzo(a)pyrene U 0.0173 0.0333 0.105 2 03/05/2019 05:28 WG1244658 Tr
6
Sr
4-Bromophenyl-phenylether U 0.0360 0.333 1.05 2 03/05/2019 05:28 WG1244658 7
2-Chloronaphthalene U 0.0202 0.0333 0.105 2 03/05/2019 05:28 WG1244658 Qc
8
Chrysene 0.0461 J 0.0175 0.0333 0.105 2 03/05/2019 05:28 WG1244658
Gl
3,3-Dichlorobenzidine U 0.251 0.333 1.05 2 03/05/2019 05:28 WG1244658 9
2,4-Dinitrotoluene U 0.0192 0.333 1.05 2 03/05/2019 05:28 WG1244658 Al
10
Fluoranthene 0.362 0.0157 0.0333 0.105 2 03/05/2019 05:28 WG1244658
Sc
Fluorene 0.154 0.0215 0.0333 0.105 2 03/05/2019 05:28 WG1244658
Indeno(1,2,3-cd)pyrene 0.0499 J 0.0244 0.0333 0.105 2 03/05/2019 05:28 WG1244658
Isophorone U 0.0165 0.333 1.05 2 03/05/2019 05:28 WG1244658
Naphthalene 0.136 0.0281 0.0333 0.105 2 03/05/2019 05:28 WG1244658
n-Nitrosodiphenylamine U 0.284 0.333 1.05 2 03/05/2019 05:28 WG1244658
n-Nitrosodi-n-propylamine U 0.0286 0.333 1.05 2 03/05/2019 05:28 WG1244658
Phenanthrene 0.245 0.0167 0.0333 0.105 2 03/05/2019 05:28 WG1244658
Bis(2-ethylhexyl)phthalate 0.193 J 0.0379 0.333 1.05 2 03/05/2019 05:28 WG1244658
Di-n-butyl phthalate U 0.0344 0.333 1.05 2 03/05/2019 05:28 WG1244658
Diethyl phthalate U 0.0218 0.333 1.05 2 03/05/2019 05:28 WG1244658
Pyrene 0.449 0.0388 0.0333 0.105 2 03/05/2019 05:28 WG1244658
4-Chloro-3-methylphenol U 0.0151 0.333 1.05 2 03/05/2019 05:28 WG1244658
4,6-Dinitro-2-methylphenol U 0.392 0.333 1.05 2 03/05/2019 05:28 WG1244658
2,4-Dinitrophenol U 0.310 0.333 1.05 2 03/05/2019 05:28 WG1244658
2-Nitrophenol U 0.0411 0.333 1.05 2 03/05/2019 05:28 WG1244658
4-Nitrophenol U 0.166 0.333 1.05 2 03/05/2019 05:28 WG1244658
Phenol 0.0428 J 0.0220 0.333 1.05 2 03/05/2019 05:28 WG1244658
(S) Phenol-d5 71.6 10.0-120 03/05/2019 05:28 WG1244658

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1
2
Tc
(S) p-Terphenyl-d14 72.5 10.0-120 03/05/2019 05:28 WG1244658 3
Ss
Sample Narrative:
4
L1075168-20 WG1244658: Dilution due to matrix impact during extract concentration procedure
Cn
5
Tr
6
Sr
7
Qc
8
Gl
9
Al
10
Sc

03/13/19 15:42
16:10 76 of 161

Cp
2
3
Cn
5
6
Chloride 444 1.38 10.0 17.3 1 03/06/2019 19:17 WG1245719
7
Qc

Gl
Mercury 1.74 0.00484 0.0200 0.0346 1 03/05/2019 09:04 WG1245047 9
Al
10
Arsenic 20.8 0.796 2.00 3.46 1 03/07/2019 20:44 WG1245191
Barium 24400 1.47 0.500 4.32 5 03/08/2019 10:06 WG1245191
Cadmium U 0.605 0.500 4.32 5 03/08/2019 10:06 WG1245191
Chromium 28.5 0.242 1.00 1.73 1 03/07/2019 20:44 WG1245191
Lead 68.2 0.329 0.500 0.865 1 03/07/2019 20:44 WG1245191
Selenium 1.25 J 1.07 2.00 3.46 1 03/07/2019 20:44 WG1245191
Silver U 0.208 1.00 1.73 1 03/07/2019 20:44 WG1245191

Acetone U 0.0237 0.0250 0.0432 1 03/06/2019 12:03 WG1245896
Benzene 0.00225 0.000692 0.00100 0.00173 1 03/06/2019 12:03 WG1245896
Bromoform U 0.0103 0.0250 0.0432 1 03/06/2019 12:03 WG1245896
Chloroform U 0.000718 0.00250 0.00432 1 03/06/2019 12:03 WG1245896

03/13/19 15:42
16:10 77 of 161

1
2
Tc
4
Cn
6
Sr
8
Ethylbenzene 0.0612 0.000917 0.00250 0.00432 1 03/06/2019 12:03 WG1245896
Gl
Isopropylbenzene 0.00210 J 0.00149 0.00250 0.00432 1 03/06/2019 12:03 WG1245896 9
2-Butanone (MEK) 0.0242 J 0.0216 0.0250 0.0432 1 03/06/2019 12:03 WG1245896
10
Sc
Naphthalene 0.0587 B 0.00540 0.0125 0.0216 1 03/06/2019 12:03 WG1245896
Styrene U 0.00472 0.0125 0.0216 1 03/06/2019 12:03 WG1245896
Toluene 0.116 0.00216 0.00500 0.00865 1 03/06/2019 12:03 WG1245896
Xylenes, Total 0.477 0.00827 0.00650 0.0112 1 03/06/2019 12:03 WG1245896
(S) Toluene-d8 94.0 75.0-131 03/06/2019 12:03 WG1245896
(S) 1,2-Dichloroethane-d4 118 70.0-130 03/06/2019 12:03 WG1245896

TPH C6 - C12 332 J 259 50.0 865 10 03/09/2019 03:57 WG1246136
TPH C12 - C28 12800 259 50.0 865 10 03/09/2019 03:57 WG1246136
TPH C28 - C35 6420 259 50.0 865 10 03/09/2019 03:57 WG1246136
TPH C6 - C35 19500 259 50.0 865 10 03/09/2019 03:57 WG1246136
(S) o-Terphenyl 133 J1 70.0-130 03/09/2019 03:57 WG1246136

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16:10 78 of 161

1
2
Sample Narrative:
Tc
L1075168-21 WG1246136: Surrogate failure due to matrix interference
3
Semi Volatile Organic Compounds (GC/MS) by Method 8270C Ss
Analyte mg/kg mg/kg mg/kg mg/kg date / time Cn
5
Tr
Anthracene 0.391 J 0.219 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Benzidine U J4 2.20 0.333 11.5 20 03/05/2019 06:27 WG1244658 6
Benzo(a)anthracene 0.531 J 0.148 0.0333 1.15 20 03/05/2019 06:27 WG1244658 Sr
Benzo(b)fluoranthene 1.85 0.240 0.0333 1.15 20 03/05/2019 06:27 WG1244658
7
Qc
Benzo(g,h,i)perylene 0.893 J 0.249 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Benzo(a)pyrene U 0.190 0.0333 1.15 20 03/05/2019 06:27 WG1244658 8
Bis(2-chlorethoxy)methane U 0.266 0.333 11.5 20 03/05/2019 06:27 WG1244658 Gl
9
Al
2-Chloronaphthalene U 0.221 0.0333 1.15 20 03/05/2019 06:27 WG1244658 10
4-Chlorophenyl-phenylether U 0.217 0.333 11.5 20 03/05/2019 06:27 WG1244658 Sc
Chrysene 0.699 J 0.192 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Fluoranthene 6.75 0.172 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Fluorene 1.85 0.236 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Indeno(1,2,3-cd)pyrene 0.777 J 0.267 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Isophorone U 0.181 0.333 11.5 20 03/05/2019 06:27 WG1244658
Naphthalene U 0.308 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Phenanthrene 3.27 0.183 0.0333 1.15 20 03/05/2019 06:27 WG1244658
Pyrene 3.55 0.426 0.0333 1.15 20 03/05/2019 06:27 WG1244658
2-Nitrophenol U 0.450 0.333 11.5 20 03/05/2019 06:27 WG1244658
4-Nitrophenol U 1.82 0.333 11.5 20 03/05/2019 06:27 WG1244658

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16:10 79 of 161

1
2
Tc
Phenol U 0.240 0.333 11.5 20 03/05/2019 06:27 WG1244658
2,4,6-Trichlorophenol U 0.269 0.333 11.5 20 03/05/2019 06:27 WG1244658 3
(S) 2-Fluorophenol 69.0 J7 12.0-120 03/05/2019 06:27 WG1244658 Ss
(S) Phenol-d5 68.4 J7 10.0-120 03/05/2019 06:27 WG1244658
4
(S) Nitrobenzene-d5 92.0 J7 10.0-122 03/05/2019 06:27 WG1244658
Cn
(S) 2-Fluorobiphenyl 55.2 J7 15.0-120 03/05/2019 06:27 WG1244658
(S) 2,4,6-Tribromophenol 51.0 J7 10.0-127 03/05/2019 06:27 WG1244658 5
(S) p-Terphenyl-d14 83.4 J7 10.0-120 03/05/2019 06:27 WG1244658 Tr
6
Sample Narrative:
Sr
L1075168-21 WG1244658: Dilution due to matrix.
7
Qc
8
Gl
9
Al
10
Sc

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Cp
2
3
Cn
5
6
Chloride 664 1.32 10.0 16.6 1 03/06/2019 19:25 WG1245719
7
Qc

Gl
Mercury 0.641 0.00466 0.0200 0.0333 1 03/05/2019 09:07 WG1245047 9
Al
10
Arsenic 18.9 0.766 2.00 3.33 1 03/07/2019 20:47 WG1245191
Barium 26300 1.41 0.500 4.16 5 03/08/2019 10:09 WG1245191
Cadmium U 0.583 0.500 4.16 5 03/08/2019 10:09 WG1245191
Chromium 30.1 0.233 1.00 1.66 1 03/07/2019 20:47 WG1245191
Lead 68.9 0.316 0.500 0.832 1 03/07/2019 20:47 WG1245191
Selenium 1.88 J 1.03 2.00 3.33 1 03/07/2019 20:47 WG1245191
Silver U 0.200 1.00 1.66 1 03/07/2019 20:47 WG1245191

Acetone 0.135 0.0228 0.0250 0.0416 1 03/06/2019 12:22 WG1245896
Benzene 0.0156 0.000666 0.00100 0.00166 1 03/06/2019 12:22 WG1245896
Bromoform U 0.00995 0.0250 0.0416 1 03/06/2019 12:22 WG1245896
Chloroform U 0.000691 0.00250 0.00416 1 03/06/2019 12:22 WG1245896

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1
2
Tc
4
Cn
6
Sr
8
Ethylbenzene 0.107 0.000882 0.00250 0.00416 1 03/06/2019 12:22 WG1245896
Gl
Isopropylbenzene 0.00217 J 0.00144 0.00250 0.00416 1 03/06/2019 12:22 WG1245896 9
2-Butanone (MEK) 0.0400 J 0.0208 0.0250 0.0416 1 03/06/2019 12:22 WG1245896
10
Sc
Naphthalene 0.0458 B 0.00519 0.0125 0.0208 1 03/06/2019 12:22 WG1245896
Styrene U 0.00454 0.0125 0.0208 1 03/06/2019 12:22 WG1245896
Toluene 0.619 0.00208 0.00500 0.00832 1 03/06/2019 12:22 WG1245896
Xylenes, Total 0.726 0.00796 0.00650 0.0108 1 03/06/2019 12:22 WG1245896
(S) Toluene-d8 96.5 75.0-131 03/06/2019 12:22 WG1245896

TPH C6 - C12 U 25.0 50.0 83.2 1 03/09/2019 23:30 WG1246136
TPH C12 - C28 225 25.0 50.0 83.2 1 03/09/2019 23:30 WG1246136
TPH C28 - C35 39.6 J 25.0 50.0 83.2 1 03/09/2019 23:30 WG1246136
TPH C6 - C35 265 25.0 50.0 83.2 1 03/09/2019 23:30 WG1246136
(S) o-Terphenyl 119 70.0-130 03/09/2019 23:30 WG1246136

03/13/19 15:42
16:10 82 of 161

1
2
Tc
Anthracene U 0.0210 0.0333 0.111 2 03/05/2019 05:48 WG1244658 3
Benzidine U J4 0.212 0.333 1.11 2 03/05/2019 05:48 WG1244658 Ss
4
Cn
Benzo(g,h,i)perylene U 0.0240 0.0333 0.111 2 03/05/2019 05:48 WG1244658 5
Benzo(a)pyrene U 0.0182 0.0333 0.111 2 03/05/2019 05:48 WG1244658 Tr
6
Sr
2-Chloronaphthalene U 0.0213 0.0333 0.111 2 03/05/2019 05:48 WG1244658 Qc
8
Chrysene U 0.0185 0.0333 0.111 2 03/05/2019 05:48 WG1244658
Gl
3,3-Dichlorobenzidine U 0.264 0.333 1.11 2 03/05/2019 05:48 WG1244658 9
2,4-Dinitrotoluene U 0.0202 0.333 1.11 2 03/05/2019 05:48 WG1244658 Al
10
Sc
Fluorene U 0.0227 0.0333 0.111 2 03/05/2019 05:48 WG1244658
Isophorone U 0.0174 0.333 1.11 2 03/05/2019 05:48 WG1244658
Naphthalene 0.0296 J 0.0296 0.0333 0.111 2 03/05/2019 05:48 WG1244658
Pyrene 0.143 0.0409 0.0333 0.111 2 03/05/2019 05:48 WG1244658
2-Nitrophenol U 0.0433 0.333 1.11 2 03/05/2019 05:48 WG1244658
4-Nitrophenol U 0.175 0.333 1.11 2 03/05/2019 05:48 WG1244658
Phenol 0.0355 J 0.0231 0.333 1.11 2 03/05/2019 05:48 WG1244658
(S) Phenol-d5 62.1 10.0-120 03/05/2019 05:48 WG1244658

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1
2
Tc
(S) p-Terphenyl-d14 62.4 10.0-120 03/05/2019 05:48 WG1244658 3
Ss
Sample Narrative:
4
Cn
5
Tr
6
Sr
7
Qc
8
Gl
9
Al
10
Sc

03/13/19 15:42
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Cp
2
3
Cn
5
6
Chloride 909 1.26 10.0 15.9 1 03/06/2019 19:34 WG1245719
7
Qc

Gl
Mercury 0.872 0.00445 0.0200 0.0318 1 03/05/2019 09:14 WG1245047 9
Al
10
Arsenic 21.0 0.731 2.00 3.18 1 03/07/2019 20:50 WG1245191
Barium 23300 1.35 0.500 3.97 5 03/08/2019 10:12 WG1245191
Cadmium U 0.556 0.500 3.97 5 03/08/2019 10:12 WG1245191
Chromium 36.9 0.223 1.00 1.59 1 03/07/2019 20:50 WG1245191
Lead 77.9 0.302 0.500 0.795 1 03/07/2019 20:50 WG1245191
Selenium U 0.985 2.00 3.18 1 03/07/2019 20:50 WG1245191
Silver U 0.191 1.00 1.59 1 03/07/2019 20:50 WG1245191

Acetone U 0.0218 0.0250 0.0397 1 03/06/2019 14:30 WG1245896
Benzene 0.00214 0.000636 0.00100 0.00159 1 03/06/2019 14:30 WG1245896
Bromoform U 0.00951 0.0250 0.0397 1 03/06/2019 14:30 WG1245896
n-Butylbenzene 0.0198 J 0.00610 0.0125 0.0199 1 03/06/2019 14:30 WG1245896
Chloroform U 0.000660 0.00250 0.00397 1 03/06/2019 14:30 WG1245896

03/13/19 15:42
16:10 85 of 161

1
2
Tc
4
Cn
6
Sr
8
Ethylbenzene 0.527 0.000842 0.00250 0.00397 1 03/06/2019 14:30 WG1245896
Gl
Isopropylbenzene 0.0242 0.00137 0.00250 0.00397 1 03/06/2019 14:30 WG1245896 9
p-Isopropyltoluene 0.0127 0.00370 0.00500 0.00795 1 03/06/2019 14:30 WG1245896 Al
2-Butanone (MEK) U 0.0199 0.0250 0.0397 1 03/06/2019 14:30 WG1245896
10
Sc
Naphthalene 0.324 0.00496 0.0125 0.0199 1 03/06/2019 14:30 WG1245896
Styrene U 0.00434 0.0125 0.0199 1 03/06/2019 14:30 WG1245896
Toluene 1.24 0.00199 0.00500 0.00795 1 03/06/2019 14:30 WG1245896
Xylenes, Total 3.51 0.00760 0.00650 0.0103 1 03/06/2019 14:30 WG1245896
(S) Toluene-d8 95.6 75.0-131 03/06/2019 14:30 WG1245896
Sample Narrative:
L1075168-23 WG1245896: Lowest possible dilution due to sample foaming.

03/13/19 15:42
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1
2
TPH C6 - C12 99.5 23.8 50.0 79.5 1 03/09/2019 01:11 WG1246136
Tc
TPH C12 - C28 1720 23.8 50.0 79.5 1 03/09/2019 01:11 WG1246136
TPH C28 - C35 197 23.8 50.0 79.5 1 03/09/2019 01:11 WG1246136 3
TPH C6 - C35 2020 23.8 50.0 79.5 1 03/09/2019 01:11 WG1246136 Ss
(S) o-Terphenyl 129 70.0-130 03/09/2019 01:11 WG1246136
4
Cn
Tr
Acenaphthene U 0.102 0.0333 0.529 10 03/05/2019 06:46 WG1244658 6
Acenaphthylene U 0.107 0.0333 0.529 10 03/05/2019 06:46 WG1244658 Sr
Anthracene 0.315 J 0.100 0.0333 0.529 10 03/05/2019 06:46 WG1244658
7
Benzidine U J4 1.01 0.333 5.29 10 03/05/2019 06:46 WG1244658
Qc
Benzo(a)anthracene 0.696 0.0680 0.0333 0.529 10 03/05/2019 06:46 WG1244658
Benzo(b)fluoranthene 2.03 0.110 0.0333 0.529 10 03/05/2019 06:46 WG1244658 8
Benzo(k)fluoranthene 0.184 J 0.0925 0.0333 0.529 10 03/05/2019 06:46 WG1244658 Gl
Benzo(g,h,i)perylene 0.855 0.115 0.0333 0.529 10 03/05/2019 06:46 WG1244658
9
Benzo(a)pyrene 0.474 J 0.0871 0.0333 0.529 10 03/05/2019 06:46 WG1244658
Al
Bis(2-chloroethyl)ether U 0.142 0.333 5.29 10 03/05/2019 06:46 WG1244658 10
Bis(2-chloroisopropyl)ether U 0.121 0.333 5.29 10 03/05/2019 06:46 WG1244658 Sc
Chrysene 0.647 0.0882 0.0333 0.529 10 03/05/2019 06:46 WG1244658
Fluoranthene 7.09 0.0788 0.0333 0.529 10 03/05/2019 06:46 WG1244658
Fluorene 2.02 0.108 0.0333 0.529 10 03/05/2019 06:46 WG1244658
Indeno(1,2,3-cd)pyrene 0.612 0.123 0.0333 0.529 10 03/05/2019 06:46 WG1244658
Isophorone U 0.0830 0.333 5.29 10 03/05/2019 06:46 WG1244658
Naphthalene 1.30 0.141 0.0333 0.529 10 03/05/2019 06:46 WG1244658
n-Nitrosodiphenylamine 2.56 J 1.43 0.333 5.29 10 03/05/2019 06:46 WG1244658
Phenanthrene 2.99 0.0839 0.0333 0.529 10 03/05/2019 06:46 WG1244658
Pyrene 4.67 0.196 0.0333 0.529 10 03/05/2019 06:46 WG1244658

03/13/19 15:42
16:10 87 of 161

1
2
Tc
2-Nitrophenol U 0.207 0.333 5.29 10 03/05/2019 06:46 WG1244658
4-Nitrophenol U 0.834 0.333 5.29 10 03/05/2019 06:46 WG1244658 3
Pentachlorophenol U 0.763 0.333 5.29 10 03/05/2019 06:46 WG1244658 Ss
Phenol U 0.110 0.333 5.29 10 03/05/2019 06:46 WG1244658
4
Cn
(S) Phenol-d5 56.0 10.0-120 03/05/2019 06:46 WG1244658 5
(S) Nitrobenzene-d5 142 J1 10.0-122 03/05/2019 06:46 WG1244658 Tr
6
Sr
(S) p-Terphenyl-d14 79.8 10.0-120 03/05/2019 06:46 WG1244658
7
Sample Narrative: Qc
L1075168-23 WG1244658: Dilution due to matrix.
8
Gl
9
Al
10
Sc

03/13/19 15:42
16:10 88 of 161

Cp
2
3
Cn
5
6
Chloride 498 1.42 10.0 17.9 1 03/06/2019 19:59 WG1245719
7
Qc

Gl
Mercury 0.758 0.00500 0.0200 0.0357 1 03/05/2019 09:17 WG1245047 9
Al
10
Arsenic 20.2 0.822 2.00 3.57 1 03/07/2019 20:53 WG1245191
Barium 25200 1.52 0.500 4.47 5 03/08/2019 10:14 WG1245191
Cadmium U 0.625 0.500 4.47 5 03/08/2019 10:14 WG1245191
Chromium 47.0 0.250 1.00 1.79 1 03/07/2019 20:53 WG1245191
Lead 78.9 0.339 0.500 0.893 1 03/07/2019 20:53 WG1245191
Selenium U 1.11 2.00 3.57 1 03/07/2019 20:53 WG1245191
Silver U 0.214 1.00 1.79 1 03/07/2019 20:53 WG1245191

Acetone U 0.0245 0.0250 0.0447 1 03/06/2019 14:49 WG1245896
Benzene 0.0152 0.000715 0.00100 0.00179 1 03/06/2019 14:49 WG1245896
Bromoform U 0.0107 0.0250 0.0447 1 03/06/2019 14:49 WG1245896
n-Butylbenzene 0.00715 J 0.00686 0.0125 0.0223 1 03/06/2019 14:49 WG1245896
Carbon tetrachloride 0.00544 J 0.00193 0.00500 0.00893 1 03/06/2019 14:49 WG1245896
Chloroform U 0.000741 0.00250 0.00447 1 03/06/2019 14:49 WG1245896

03/13/19 15:42
16:10 89 of 161

1
2
Tc
4
Cn
6
Sr
8
Ethylbenzene 0.0888 0.000947 0.00250 0.00447 1 03/06/2019 14:49 WG1245896
Gl
Isopropylbenzene U 0.00154 0.00250 0.00447 1 03/06/2019 14:49 WG1245896 9
p-Isopropyltoluene 0.00783 J 0.00416 0.00500 0.00893 1 03/06/2019 14:49 WG1245896 Al
2-Butanone (MEK) U 0.0223 0.0250 0.0447 1 03/06/2019 14:49 WG1245896
10
Sc
Naphthalene 0.0641 B 0.00557 0.0125 0.0223 1 03/06/2019 14:49 WG1245896
Styrene U 0.00488 0.0125 0.0223 1 03/06/2019 14:49 WG1245896
Toluene 0.526 0.00223 0.00500 0.00893 1 03/06/2019 14:49 WG1245896
Xylenes, Total 0.654 0.00854 0.00650 0.0116 1 03/06/2019 14:49 WG1245896
(S) Toluene-d8 99.0 75.0-131 03/06/2019 14:49 WG1245896

TPH C6 - C12 142 26.8 50.0 89.3 1 03/09/2019 02:20 WG1246136
TPH C12 - C28 4650 134 50.0 447 5 03/09/2019 23:58 WG1246136
TPH C28 - C35 153 26.8 50.0 89.3 1 03/09/2019 02:20 WG1246136
TPH C6 - C35 4950 134 50.0 447 5 03/09/2019 23:58 WG1246136
(S) o-Terphenyl 139 J1 70.0-130 03/09/2019 02:20 WG1246136
(S) o-Terphenyl 157 J1 70.0-130 03/09/2019 23:58 WG1246136

03/13/19 15:42
16:10 90 of 161

1
2
Tc
Sample Narrative:
L1075168-24 WG1246136: Surrogate failure due to matrix interference 3
Ss
4
Result (dry) Qualifier SDL (dry) Unadj. MQL MQL (dry) Dilution Analysis Batch Cn
5
Tr
Anthracene U 1.13 0.0333 5.95 100 03/05/2019 12:37 WG1244658 6
Benzidine U J4 0.228 0.333 1.19 2 03/05/2019 06:07 WG1244658 Sr
Benzo(a)anthracene 0.168 0.0153 0.0333 0.119 2 03/05/2019 06:07 WG1244658
7
Qc
Benzo(g,h,i)perylene 0.0806 J 0.0258 0.0333 0.119 2 03/05/2019 06:07 WG1244658 8
Benzo(a)pyrene 0.0893 J 0.0196 0.0333 0.119 2 03/05/2019 06:07 WG1244658 Gl
9
Al
2-Chloronaphthalene U 1.14 0.0333 5.95 100 03/05/2019 12:37 WG1244658 Sc
Chrysene 0.243 0.0198 0.0333 0.119 2 03/05/2019 06:07 WG1244658
Fluorene U 1.22 0.0333 5.95 100 03/05/2019 12:37 WG1244658
Isophorone U 0.0187 0.333 1.19 2 03/05/2019 06:07 WG1244658
Naphthalene U 0.0318 0.0333 0.119 2 03/05/2019 06:07 WG1244658
Phenanthrene 2.20 J 0.943 0.0333 5.95 100 03/05/2019 12:37 WG1244658
Pyrene 1.61 0.0440 0.0333 0.119 2 03/05/2019 06:07 WG1244658
2-Nitrophenol U 0.0465 0.333 1.19 2 03/05/2019 06:07 WG1244658

03/13/19 15:42
16:10 91 of 161

1
2
4-Nitrophenol U 9.38 0.333 59.5 100 03/05/2019 12:37 WG1244658
Tc
Phenol U 0.0248 0.333 1.19 2 03/05/2019 06:07 WG1244658 3
2,4,6-Trichlorophenol U 1.39 0.333 59.5 100 03/05/2019 12:37 WG1244658 Ss
4
(S) 2-Fluorophenol 74.5 J7 12.0-120 03/05/2019 12:37 WG1244658
Cn
(S) Phenol-d5 60.2 J7 10.0-120 03/05/2019 12:37 WG1244658
(S) Phenol-d5 67.1 10.0-120 03/05/2019 06:07 WG1244658 5
(S) Nitrobenzene-d5 169 J1 10.0-122 03/05/2019 06:07 WG1244658 Tr
(S) Nitrobenzene-d5 111 J7 10.0-122 03/05/2019 12:37 WG1244658
6
Sr
(S) 2-Fluorobiphenyl 79.9 J7 15.0-120 03/05/2019 12:37 WG1244658
(S) 2,4,6-Tribromophenol 70.7 10.0-127 03/05/2019 06:07 WG1244658 7
(S) 2,4,6-Tribromophenol 74.8 J7 10.0-127 03/05/2019 12:37 WG1244658 Qc
(S) p-Terphenyl-d14 87.8 10.0-120 03/05/2019 06:07 WG1244658
8
(S) p-Terphenyl-d14 84.1 J7 10.0-120 03/05/2019 12:37 WG1244658
Gl
Sample Narrative: 9
L1075168-24 WG1244658: IS/SURR failed on lower dilution. Al
10
Sc

03/13/19 15:42
16:10 92 of 161
WG1246056 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Gravimetric Analysis by Method 2540 C-2011 L1075168-01,02,03,04
Method Blank (MB) 1

Cp
(MB) R3390172-1 03/07/19 23:39
MB Result MB Qualifier MB MDL MB RDL 2
Analyte mg/l mg/l mg/l Tc
Dissolved Solids U 2.82 10.0
3
Ss
L1075168-04 Original Sample (OS) • Duplicate (DUP) 4
(OS) L1075168-04 03/07/19 23:39 • (DUP) R3390172-3 03/07/19 23:39

Cn
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier 5
Limits
Tr
Analyte mg/l mg/l % %
Dissolved Solids 1700 1720 1 0.878 5 6
Sr
Laboratory Control Sample (LCS) 7

Qc
(LCS) R3390172-2 03/07/19 23:39
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier 8

Gl
Dissolved Solids 8800 8720 99.1 85.0-115
9
Al
10
Sc

03/13/19 15:42
16:10 93 of 161
Gravimetric Analysis by Method 2540 C-2011 L1075168-05,06,07,08,09,10,11,12,13,14
Method Blank (MB) 1

Cp
(MB) R3390170-1 03/07/19 23:09
3
Ss
(OS) L1075168-06 03/07/19 23:09 • (DUP) R3390170-3 03/07/19 23:09

Cn
DUP RPD
Limits
Tr
Dissolved Solids 1120 1020 1 8.79 J3 5 6
Sr

Qc
(LCS) R3390170-2 03/07/19 23:09

Gl
9
Al
10
Sc

03/13/19 15:42
16:10 94 of 161
Gravimetric Analysis by Method 2540 C-2011 L1075168-15,16,17,18,19
Method Blank (MB) 1

Cp
(MB) R3390171-1 03/08/19 01:53
3
Ss
(OS) L1075168-18 03/08/19 01:53 • (DUP) R3390171-3 03/08/19 01:53

Cn
DUP RPD
Limits
Tr
Dissolved Solids 116 127 1 9.05 J3 5 6
Sr

Qc
(LCS) R3390171-2 03/08/19 01:53

Gl
9
Al
10
Sc

03/13/19 15:42
16:10 95 of 161
Total Solids by Method 2540 G-2011 L1075168-20,21
Method Blank (MB) 1

Cp
(MB) R3389442-1 03/06/19 14:08
Analyte % % % Tc
Total Solids 0.00100
3
Ss
(OS) L1075104-02 03/06/19 14:08 • (DUP) R3389442-3 03/06/19 14:08

Cn
DUP RPD
Limits
Tr
Analyte % % % %
Total Solids 87.5 91.8 1 4.82 10 6
Sr

Qc
(LCS) R3389442-2 03/06/19 14:08
Analyte % % % %
Gl
Total Solids 50.0 50.0 100 85.0-115
9
Al
10
Sc

03/13/19 15:42
16:10 96 of 161
Total Solids by Method 2540 G-2011 L1075168-22,23,24
Method Blank (MB) 1

Cp
(MB) R3389479-1 03/06/19 10:56
Analyte % % % Tc
Total Solids 0.00100
3
Ss
(OS) L1075101-12 03/06/19 10:56 • (DUP) R3389479-3 03/06/19 10:56

Cn
DUP RPD
Limits
Tr
Analyte % % % %
Total Solids 81.0 80.6 1 0.407 10 6
Sr

Qc
(LCS) R3389479-2 03/06/19 10:56
Analyte % % % %
Gl
Total Solids 50.0 50.0 100 85.0-115
9
Al
10
Sc

03/13/19 15:42
16:10 97 of 161
Wet Chemistry by Method 2320 B-2011 L1075168-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19
Method Blank (MB) 1

Cp
(MB) R3389725-1 03/07/19 14:26
Alkalinity U 2.71 20.0
3
Ss
Sample Narrative:
BLANK: Endpoint pH 4.5 4
Cn

Tr
(OS) L1075168-01 03/07/19 14:32 • (DUP) R3389725-2 03/07/19 14:38
DUP RPD 6
Original Result DUP Result Dilution DUP RPD DUP Qualifier Sr
Limits
7
Alkalinity 157 157 1 0.0644 20
Qc
Sample Narrative: 8
OS: Endpoint pH 4.5 headspace Gl
DUP: Endpoint pH 4.5
9
Al
(OS) L1075168-19 03/07/19 17:04 • (DUP) R3389725-4 03/07/19 17:11

Sc
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier Limits
Alkalinity 339 335 1 1.26 20
Sample Narrative:
OS: Endpoint pH 4.5 headspace
DUP: Endpoint pH 4.5
Laboratory Control Sample (LCS)

(LCS) R3389725-3 03/07/19 15:33
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Alkalinity 100 93.4 93.4 85.0-115
Sample Narrative:
LCS: Endpoint pH 4.5

03/13/19 15:42
16:10 98 of 161
Wet Chemistry by Method 300.0 L1075168-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19
Method Blank (MB) 1

Cp
(MB) R3389142-1 03/06/19 00:32
Chloride U 0.0519 1.00
3
Sulfate U 0.0774 5.00
Ss
4
L1075175-01 Original Sample (OS) • Duplicate (DUP) Cn
(OS) L1075175-01 03/06/19 01:29 • (DUP) R3389142-3 03/06/19 01:44
5
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Tr
Limits
Analyte mg/l mg/l % % 6
Chloride 21.8 21.7 1 0.349 20 Sr
Sulfate 51.2 51.1 1 0.281 20
7
Qc
(OS) L1075168-08 03/06/19 04:49 • (DUP) R3389142-6 03/06/19 05:04

Gl
DUP RPD
Limits
Al
Chloride 13.3 13.2 1 0.777 20 10
Sulfate 10.7 10.6 1 0.786 20 Sc

(LCS) R3389142-2 03/06/19 00:47
Chloride 40.0 40.3 101 90.0-110
Sulfate 40.0 41.0 103 90.0-110
L1075175-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1075175-01 03/06/19 01:29 • (MS) R3389142-4 03/06/19 01:59 • (MSD) R3389142-5 03/06/19 02:15
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l % % % % %
Chloride 50.0 21.8 71.2 71.5 98.7 99.3 1 80.0-120 0.414 20
Sulfate 50.0 51.2 98.4 99.0 94.4 95.5 1 80.0-120 0.537 20

03/13/19 15:42
16:10 99 of 161
Wet Chemistry by Method 300.0 L1075168-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19
L1075168-08 Original Sample (OS) • Matrix Spike (MS) 1

Cp
(OS) L1075168-08 03/06/19 04:49 • (MS) R3389142-7 03/06/19 05:19
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier 2
Analyte mg/l mg/l mg/l % % Tc
Chloride 50.0 13.3 62.5 98.5 1 80.0-120
3
Sulfate 50.0 10.7 60.2 99.0 1 80.0-120
Ss
4
Cn
5
Tr
6
Sr
7
Qc
8
Gl
9
Al
10
Sc

03/13/19 15:42
16:10 100 of 161
Wet Chemistry by Method 9040C L1075168-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16

Cp
(OS) L1075088-06 03/05/19 11:55 • (DUP) R3388776-2 03/05/19 11:55
DUP RPD
Limits Tc
Analyte su su % %
pH 8.28 8.30 1 0.241 1 3
Ss
Sample Narrative:
4
OS: 8.28 at 16.3C Cn
DUP: 8.3 at 16.3C
5
Tr
L1075168-16 Original Sample (OS) • Duplicate (DUP)
6
(OS) L1075168-16 03/05/19 11:55 • (DUP) R3388776-3 03/05/19 11:55 Sr
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier Limits 7
Analyte su su % % Qc
pH 7.91 7.90 1 0.127 1
8
Gl
Sample Narrative:
OS: 7.91 at 13.3C 9
DUP: 7.9 at 13.3C Al
10
Sc
(LCS) R3388776-1 03/05/19 11:55
Analyte su su % %
pH 10.0 10.0 100 99.0-101
Sample Narrative:
LCS: 10.01 at 16.9C

03/13/19 15:42
16:10 101 of 161
Wet Chemistry by Method 9040C L1075168-17,18,19

Cp
(OS) L1075431-04 03/06/19 09:50 • (DUP) R3389133-2 03/06/19 09:50
DUP RPD
Limits Tc
Analyte su su % %
pH 12.7 12.7 1 0.0786 1 3
Ss
Sample Narrative:
4
OS: 12.71 at 18.1C Cn
DUP: 12.72 at 18.1C
5
Tr
L1075510-10 Original Sample (OS) • Duplicate (DUP)
6
(OS) L1075510-10 03/06/19 09:50 • (DUP) R3389133-3 03/06/19 09:50 Sr
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier Limits 7
Analyte su su % % Qc
pH 11.7 11.7 1 0.000 1
8
Gl
Sample Narrative:
OS: 11.71 at 15.5C 9
DUP: 11.71 at 15.5C Al
10
Sc
(LCS) R3389133-1 03/06/19 09:50
Analyte su su % %
pH 10.0 10.0 100 99.0-101
Sample Narrative:
LCS: 10 at 15.7C

03/13/19 15:42
16:10 102 of 161
Wet Chemistry by Method 9050A L1075168-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19
Method Blank (MB) 1

Cp
(MB) R3389563-1 03/07/19 13:22
Analyte umhos/cm umhos/cm umhos/cm Tc
Specific Conductance U 10.0 10.0
3
Ss
(OS) L1075168-01 03/07/19 13:22 • (DUP) R3389563-3 03/07/19 13:22

Cn
DUP RPD
Limits
Tr
Analyte umhos/cm umhos/cm % %
Specific Conductance 4510 4500 1 0.222 20 6
Sr

Qc
(OS) L1075285-01 03/07/19 13:22 • (DUP) R3389563-4 03/07/19 13:22
DUP RPD 8
Original Result DUP Result Dilution DUP RPD DUP Qualifier Gl
Limits
9
Specific Conductance 239 239 1 0.0838 20
Al
10
Laboratory Control Sample (LCS) Sc
(LCS) R3389563-2 03/07/19 13:22
Specific Conductance 877 861 98.2 90.0-110

03/13/19 15:42
16:10 103 of 161
Wet Chemistry by Method 9050AMod L1075168-20,21,22,23,24
Method Blank (MB) 1

Cp
(MB) R3389320-1 03/06/19 21:03
Analyte umhos/cm umhos/cm umhos/cm Tc
Specific Conductance U 10.0 10.0
3
Ss
(OS) L1075168-20 03/06/19 21:03 • (DUP) R3389320-3 03/06/19 21:03

Cn
DUP RPD
Limits
Tr
Specific Conductance 933 936 1 0.321 20 6
Sr

Qc
(OS) L1075732-04 03/06/19 21:03 • (DUP) R3389320-4 03/06/19 21:03
DUP RPD 8
Original Result DUP Result Dilution DUP RPD DUP Qualifier Gl
Limits
9
Specific Conductance 122 122 1 0.164 20
Al
10
Laboratory Control Sample (LCS) Sc
(LCS) R3389320-2 03/06/19 21:03
Specific Conductance 877 876 99.9 90.0-110

03/13/19 15:42
16:10 104 of 161
Wet Chemistry by Method 9056A L1075168-20,21,22,23,24
Method Blank (MB) 1

Cp
(MB) R3389346-1 03/06/19 18:26
Analyte mg/kg mg/kg mg/kg Tc
Chloride 3.71 J 0.795 10.0
3
Ss
(OS) L1075394-07 03/06/19 20:08 • (DUP) R3389346-5 03/06/19 20:17

Cn
DUP RPD
Limits
Tr
Analyte mg/kg mg/kg % %
Chloride 103 145 1 34.2 J3 15 6
Sr

Qc
(LCS) R3389346-2 03/06/19 18:34

Gl
Chloride 200 208 104 80.0-120
9
Al
L1075168-20 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) 10
Sc
(OS) L1075168-20 03/06/19 18:51 • (MS) R3389346-3 03/06/19 19:00 • (MSD) R3389346-4 03/06/19 19:08
Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry) (dry)
Analyte mg/kg mg/kg mg/kg mg/kg % % % % %
Chloride 790 265 1150 1170 113 115 1 80.0-120 1.33 15

03/13/19 15:42
16:10 105 of 161
Mercury by Method 7470A L1075168-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19
Method Blank (MB) 1

Cp
(MB) R3388767-1 03/05/19 09:34
Mercury U 0.0000490 0.000200
3
Ss
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) 4
(LCS) R3388767-2 03/05/19 09:36 • (LCSD) R3388767-3 03/05/19 09:38

Cn
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
5
Analyte mg/l mg/l mg/l % % % % % Tr
Mercury 0.00300 0.00275 0.00283 91.5 94.2 80.0-120 2.90 20
6
Sr
(OS) L1075168-01 03/05/19 09:41 • (MS) R3388767-4 03/05/19 09:43 • (MSD) R3388767-5 03/05/19 09:46 Qc
8
Analyte mg/l mg/l mg/l mg/l % % % % % Gl
Mercury 0.00300 U 0.00232 0.00221 77.4 73.8 1 75.0-125 J6 4.74 20
9
Al
10
Sc

03/13/19 15:42
16:10 106 of 161
Mercury by Method 7471A L1075168-20,21,22,23,24
Method Blank (MB) 1

Cp
(MB) R3388747-1 03/05/19 08:13
Mercury U 0.00280 0.0200
3
Ss
(LCS) R3388747-2 03/05/19 08:16 • (LCSD) R3388747-3 03/05/19 08:18

Cn
5
Analyte mg/kg mg/kg mg/kg % % % % % Tr
Mercury 0.500 0.472 0.457 94.4 91.3 80.0-120 3.32 20
6
Sr
(OS) L1074765-04 03/05/19 08:21 • (MS) R3388747-4 03/05/19 08:24 • (MSD) R3388747-5 03/05/19 08:26 Qc
8
Analyte mg/kg mg/kg mg/kg mg/kg % % % % % Gl
Mercury 0.500 0.0334 0.537 0.508 101 94.8 1 75.0-125 5.58 20
9
Al
10
Sc

03/13/19 15:42
16:10 107 of 161
Metals (ICP) by Method 6010B L1075168-20,21,22,23,24
Method Blank (MB) 1

Cp
(MB) R3389806-1 03/07/19 19:39
Arsenic U 0.460 2.00
3
Barium U 0.170 0.500
Ss
Cadmium U 0.0700 0.500
Chromium U 0.140 1.00 4
Lead U 0.190 0.500 Cn
Selenium U 0.620 2.00
5
Silver U 0.120 1.00
Tr
6
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) Sr
(LCS) R3389806-2 03/07/19 19:41 • (LCSD) R3389806-3 03/07/19 19:44
7
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Qc
Analyte mg/kg mg/kg mg/kg % % % % %
Arsenic 100 100 101 100 101 80.0-120 0.278 20 8
Barium 100 108 107 108 107 80.0-120 0.120 20

Gl
Cadmium 100 103 102 103 102 80.0-120 0.647 20
9
Chromium 100 106 105 106 105 80.0-120 0.569 20 Al
Lead 100 104 103 104 103 80.0-120 0.724 20
Selenium 100 105 102 105 102 80.0-120 2.72 20 10
Silver 20.0 19.9 19.6 99.3 98.0 80.0-120 1.31 20

Sc
(OS) L1074966-06 03/07/19 19:46 • (MS) R3389806-6 03/07/19 19:54 • (MSD) R3389806-7 03/07/19 19:57
Arsenic 100 4.69 102 104 97.5 99.5 1 75.0-125 1.87 20
Barium 100 82.6 189 191 106 108 1 75.0-125 0.949 20
Cadmium 100 ND 101 101 101 101 1 75.0-125 0.0713 20
Chromium 100 26.8 116 130 89.5 103 1 75.0-125 11.4 20
Lead 100 21.3 130 126 108 105 1 75.0-125 2.95 20
Selenium 100 ND 100 101 100 101 1 75.0-125 0.220 20
Silver 20.0 ND 19.8 19.6 98.8 97.8 1 75.0-125 0.988 20

03/13/19 15:42
16:10 108 of 161
Metals (ICPMS) by Method 6020 L1075168-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19
Method Blank (MB) 1

Cp
(MB) R3389340-1 03/06/19 20:06
Arsenic U 0.000250 0.00200
3
Barium U 0.000360 0.00500
Ss
Cadmium U 0.000160 0.00100
Calcium U 0.0460 1.00 4
Chromium 0.000593 J 0.000540 0.00200 Cn
Lead U 0.000240 0.00200
5
Magnesium U 0.100 1.00
Tr
Potassium U 0.0370 1.00
Selenium U 0.000380 0.00200 6
Silver U 0.000310 0.00200 Sr
Sodium U 0.110 1.00
7
Qc
(LCS) R3389340-2 03/06/19 20:11 • (LCSD) R3389340-3 03/06/19 20:15

Gl
9
Analyte mg/l mg/l mg/l % % % % % Al
Arsenic 0.0500 0.0503 0.0500 101 99.9 80.0-120 0.633 20
Barium 0.0500 0.0481 0.0470 96.2 94.0 80.0-120 2.28 20 10
Cadmium 0.0500 0.0489 0.0471 97.7 94.3 80.0-120 3.59 20

Sc
Calcium 5.00 4.93 4.90 98.5 98.0 80.0-120 0.496 20
Chromium 0.0500 0.0512 0.0510 102 102 80.0-120 0.387 20
Lead 0.0500 0.0458 0.0465 91.6 92.9 80.0-120 1.48 20
Magnesium 5.00 4.94 4.91 98.7 98.3 80.0-120 0.476 20
Potassium 5.00 4.76 4.75 95.2 95.0 80.0-120 0.196 20
Selenium 0.0500 0.0485 0.0541 97.0 108 80.0-120 11.0 20
Silver 0.0500 0.0463 0.0465 92.6 92.9 80.0-120 0.386 20
Sodium 5.00 4.78 4.77 95.6 95.3 80.0-120 0.298 20
(OS) L1075168-04 03/06/19 20:20 • (MS) R3389340-5 03/06/19 20:29 • (MSD) R3389340-6 03/06/19 20:34
Arsenic 0.0500 0.00198 0.0506 0.0496 97.3 95.2 1 75.0-125 2.10 20
Barium 0.0500 2.43 2.51 2.48 165 106 1 75.0-125 V 1.18 20
Cadmium 0.0500 U 0.0473 0.0475 94.7 95.0 1 75.0-125 0.331 20
Calcium 5.00 211 213 215 44.7 79.4 1 75.0-125 V 0.808 20
Chromium 0.0500 U 0.0475 0.0464 95.1 92.8 1 75.0-125 2.44 20

03/13/19 15:42
16:10 109 of 161
Metals (ICPMS) by Method 6020 L1075168-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19
Cp
(OS) L1075168-04 03/06/19 20:20 • (MS) R3389340-5 03/06/19 20:29 • (MSD) R3389340-6 03/06/19 20:34
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 2
Analyte mg/l mg/l mg/l mg/l % % % % % Tc
Potassium 5.00 1.78 6.54 6.44 95.2 93.1 1 75.0-125 1.58 20
3
Lead 0.0500 U 0.0468 0.0475 93.6 95.0 1 75.0-125 1.49 20
Ss
Magnesium 5.00 22.8 27.4 27.3 93.0 89.5 1 75.0-125 0.631 20
Selenium 0.0500 U 0.0501 0.0531 100 106 1 75.0-125 5.79 20 4
Silver 0.0500 U 0.0467 0.0465 93.5 93.0 1 75.0-125 0.489 20 Cn
Sodium 5.00 279 282 279 56.0 0.000 1 75.0-125 V V 1.26 20
5
Tr
6
Sr
7
Qc
8
Gl
9
Al
10
Sc

03/13/19 15:42
16:10 110 of 161
Volatile Organic Compounds (GC) by Method 8021B L1075168-01,02,04
Method Blank (MB) 1

Cp
(MB) R3388962-2 03/05/19 11:56
Benzene 0.000320 J 0.000190 0.000500
3
Toluene U 0.000412 0.00100
Ss
Ethylbenzene U 0.000160 0.000500
Total Xylene U 0.000510 0.00150 4
(S) 98.2 79.0-125
Cn
a,a,a-Trifluorotoluene(PID)
5
Tr
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
6
(LCS) R3388962-1 03/05/19 10:52 • (LCSD) R3388962-5 03/05/19 21:04 Sr
Analyte mg/l mg/l mg/l % % % % % 7
Qc
Benzene 0.0500 0.0425 0.0418 84.9 83.7 77.0-122 1.51 20
Toluene 0.0500 0.0410 0.0406 82.1 81.2 80.0-121 1.06 20 8
Ethylbenzene 0.0500 0.0432 0.0430 86.4 85.9 80.0-123 0.522 20 Gl
Total Xylene 0.150 0.127 0.124 84.7 82.5 47.0-154 2.63 20
9
(S)
a,a,a-Trifluorotoluene(PID) 97.6 97.0 79.0-125 Al
10
Sc
(OS) L1075077-01 03/05/19 13:21 • (MS) R3388962-3 03/05/19 19:50 • (MSD) R3388962-4 03/05/19 20:11
Benzene 0.0500 ND 0.0505 0.0368 100 73.1 1 10.0-160 J3 31.2 21
Toluene 0.0500 ND 0.0493 0.0361 98.6 72.2 1 12.0-148 J3 31.0 21
Ethylbenzene 0.0500 ND 0.0513 0.0385 103 76.9 1 22.0-149 J3 28.6 21
Total Xylene 0.150 ND 0.155 0.114 103 76.0 1 13.0-155 J3 30.2 21
(S) 96.3 97.4 79.0-125

03/13/19 15:42
16:10 111 of 161
Volatile Organic Compounds (GC) by Method 8021B L1075168-05,06,07,09,10,11
Method Blank (MB) 1

Cp
(MB) R3390274-3 03/05/19 23:44
Benzene U 0.000190 0.000500
3
Toluene U 0.000412 0.00100
Ss
Total Xylene U 0.000510 0.00150 4
(S) 100 79.0-125
Cn
5
Tr
6
(LCS) R3390274-1 03/05/19 22:41 • (LCSD) R3390274-2 03/05/19 23:02 Sr
Analyte mg/l mg/l mg/l % % % % % 7
Qc
Benzene 0.0500 0.0505 0.0421 101 84.3 77.0-122 18.1 20
Toluene 0.0500 0.0498 0.0408 99.6 81.6 80.0-121 19.9 20 8
Ethylbenzene 0.0500 0.0525 0.0422 105 84.4 80.0-123 J3 21.7 20 Gl
Total Xylene 0.150 0.152 0.119 101 79.5 47.0-154 J3 24.1 20
9
(S)
a,a,a-Trifluorotoluene(PID) 95.6 97.2 79.0-125 Al
10
Sc
(OS) L1075168-11 03/06/19 06:20 • (MS) R3390274-4 03/06/19 06:42 • (MSD) R3390274-5 03/06/19 07:03
Benzene 0.0500 U 0.0253 0.0246 50.7 49.2 1 10.0-160 2.88 21
Toluene 0.0500 U 0.0269 0.0260 53.8 52.0 1 12.0-148 3.36 21
Ethylbenzene 0.0500 U 0.0338 0.0319 67.6 63.9 1 22.0-149 5.68 21
Total Xylene 0.150 0.000570 0.102 0.0954 67.6 63.2 1 13.0-155 J6 J6 6.69 21
(S) 98.8 99.0 79.0-125

03/13/19 15:42
16:10 112 of 161
Volatile Organic Compounds (GC) by Method 8021B L1075168-08
Method Blank (MB) 1

Cp
(MB) R3390562-2 03/11/19 12:37
Benzene U 0.000190 0.000500
3
Toluene U 0.000412 0.00100
Ss
Total Xylene U 0.000510 0.00150 4
(S) 96.2 79.0-125
Cn
5
Tr
6
(LCS) R3390562-1 03/11/19 11:49 Sr
Analyte mg/l mg/l % % 7
Qc
Benzene 0.0500 0.0520 104 77.0-122
Toluene 0.0500 0.0475 95.0 80.0-121 8
Ethylbenzene 0.0500 0.0480 96.0 80.0-123 Gl
Total Xylene 0.150 0.146 97.5 47.0-154
9
(S)
a,a,a-Trifluorotoluene(PID) 96.9 79.0-125 Al
10
Sc

03/13/19 15:42
16:10 113 of 161
Volatile Organic Compounds (GC/MS) by Method 8260B L1075168-20
Method Blank (MB) 1

Cp
(MB) R3389241-2 03/06/19 10:04
Acetone U 0.0137 0.0250
3
Acrylonitrile U 0.00190 0.0125
Ss
Benzene U 0.000400 0.00100
Bromobenzene U 0.00105 0.0125 4
Bromodichloromethane U 0.000788 0.00250 Cn
Bromoform U 0.00598 0.0250
5
Bromomethane U 0.00370 0.0125
Tr
n-Butylbenzene U 0.00384 0.0125
sec-Butylbenzene U 0.00253 0.0125 6
tert-Butylbenzene U 0.00155 0.00500 Sr
Carbon tetrachloride U 0.00108 0.00500
7
Chlorobenzene U 0.000573 0.00250
Qc
Chlorodibromomethane U 0.000450 0.00250
Chloroethane U 0.00108 0.00500 8
Chloroform U 0.000415 0.00250 Gl
Chloromethane U 0.00139 0.0125
9
2-Chlorotoluene U 0.000920 0.00250
Al
1,2-Dibromo-3-Chloropropane U 0.00510 0.0250 10
1,2-Dibromoethane U 0.000525 0.00250 Sc
Dibromomethane U 0.00100 0.00500
1,2-Dichlorobenzene U 0.00145 0.00500
Dichlorodifluoromethane U 0.000818 0.00250
1,1-Dichloroethane U 0.000575 0.00250
1,1-Dichloroethene U 0.000500 0.00250
cis-1,2-Dichloroethene U 0.000690 0.00250
trans-1,2-Dichloroethene U 0.00143 0.00500
1,2-Dichloropropane U 0.00127 0.00500
1,1-Dichloropropene U 0.000700 0.00250
cis-1,3-Dichloropropene U 0.000678 0.00250
trans-1,3-Dichloropropene U 0.00153 0.00500
Di-isopropyl ether U 0.000350 0.00100
Hexachloro-1,3-butadiene U 0.0127 0.0250
Isopropylbenzene U 0.000863 0.00250

03/13/19 15:42
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Method Blank (MB) 1

Cp
(MB) R3389241-2 03/06/19 10:04
p-Isopropyltoluene U 0.00233 0.00500
3
2-Butanone (MEK) U 0.0125 0.0250
Ss
Methylene Chloride 0.00764 J 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.0100 0.0250 4
Methyl tert-butyl ether U 0.000295 0.00100 Cn
Naphthalene U 0.00312 0.0125
5
n-Propylbenzene U 0.00118 0.00500
Tr
Styrene U 0.00273 0.0125
1,1,1,2-Tetrachloroethane U 0.000500 0.00250 6
1,1,2,2-Tetrachloroethane U 0.000390 0.00250 Sr
Tetrachloroethene U 0.000700 0.00250
7
Toluene U 0.00125 0.00500
Qc
1,1,2-Trichlorotrifluoroethane U 0.000675 0.00250
1,2,3-Trichlorobenzene 0.000847 J 0.000625 0.00250 8
1,2,4-Trichlorobenzene U 0.00482 0.0125 Gl
1,1,1-Trichloroethane U 0.000275 0.00250
9
Al
Trichloroethene U 0.000400 0.00100
Trichlorofluoromethane U 0.000500 0.00250 10
1,2,3-Trichloropropane U 0.00510 0.0125 Sc
1,2,3-Trimethylbenzene U 0.00115 0.00500
Vinyl chloride U 0.000683 0.00250
Xylenes, Total U 0.00478 0.00650
(S) Toluene-d8 105 75.0-131
(S) 4-Bromofluorobenzene 100 67.0-138
(S) 1,2-Dichloroethane-d4 92.1 70.0-130

(LCS) R3389241-1 03/06/19 09:07
Acetone 0.625 0.783 125 10.0-160
Acrylonitrile 0.625 0.738 118 45.0-153
Benzene 0.125 0.123 98.6 70.0-123
Bromobenzene 0.125 0.106 84.6 73.0-121
Bromodichloromethane 0.125 0.107 85.6 73.0-121

03/13/19 15:42
16:10 115 of 161

Cp
(LCS) R3389241-1 03/06/19 09:07
Analyte mg/kg mg/kg % % Tc
Bromoform 0.125 0.144 115 64.0-132
3
Bromomethane 0.125 0.104 83.5 56.0-147
Ss
n-Butylbenzene 0.125 0.121 96.4 68.0-135
sec-Butylbenzene 0.125 0.114 91.5 74.0-130 4
tert-Butylbenzene 0.125 0.119 95.0 75.0-127 Cn
Carbon tetrachloride 0.125 0.131 105 66.0-128
5
Chlorobenzene 0.125 0.112 89.3 76.0-128
Tr
Chlorodibromomethane 0.125 0.129 103 74.0-127
Chloroethane 0.125 0.122 97.8 61.0-134 6
Chloroform 0.125 0.112 89.8 72.0-123 Sr
Chloromethane 0.125 0.111 88.4 51.0-138
7
2-Chlorotoluene 0.125 0.137 110 75.0-124
Qc
4-Chlorotoluene 0.125 0.137 109 75.0-124
1,2-Dibromo-3-Chloropropane 0.125 0.124 99.2 59.0-130 8
1,2-Dibromoethane 0.125 0.111 88.6 74.0-128 Gl
Dibromomethane 0.125 0.155 124 75.0-122 J4
9
1,2-Dichlorobenzene 0.125 0.108 86.6 76.0-124
Al
1,4-Dichlorobenzene 0.125 0.106 84.5 77.0-121 10
Dichlorodifluoromethane 0.125 0.162 129 43.0-156 Sc
1,1-Dichloroethane 0.125 0.123 98.7 70.0-127
1,2-Dichloroethane 0.125 0.133 106 65.0-131
1,1-Dichloroethene 0.125 0.0970 77.6 65.0-131
cis-1,2-Dichloroethene 0.125 0.150 120 73.0-125
trans-1,2-Dichloroethene 0.125 0.111 88.6 71.0-125
1,2-Dichloropropane 0.125 0.127 102 74.0-125
1,1-Dichloropropene 0.125 0.118 94.8 73.0-125
cis-1,3-Dichloropropene 0.125 0.126 101 76.0-127
trans-1,3-Dichloropropene 0.125 0.142 114 73.0-127
Di-isopropyl ether 0.125 0.126 101 60.0-136
Ethylbenzene 0.125 0.122 97.8 74.0-126
Hexachloro-1,3-butadiene 0.125 0.107 85.4 57.0-150
Isopropylbenzene 0.125 0.117 93.2 72.0-127
p-Isopropyltoluene 0.125 0.128 102 72.0-133
2-Butanone (MEK) 0.625 0.835 134 30.0-160
Methylene Chloride 0.125 0.104 83.1 68.0-123
4-Methyl-2-pentanone (MIBK) 0.625 0.804 129 56.0-143
Methyl tert-butyl ether 0.125 0.128 103 66.0-132

03/13/19 15:42
16:10 116 of 161

Cp
(LCS) R3389241-1 03/06/19 09:07
Analyte mg/kg mg/kg % % Tc
Naphthalene 0.125 0.123 98.5 59.0-130
3
n-Propylbenzene 0.125 0.118 94.6 74.0-126
Ss
Styrene 0.125 0.122 97.5 72.0-127
1,1,1,2-Tetrachloroethane 0.125 0.128 103 74.0-129 4
1,1,2,2-Tetrachloroethane 0.125 0.170 136 68.0-128 J4 Cn
Tetrachloroethene 0.125 0.0969 77.5 70.0-136
5
Toluene 0.125 0.103 82.1 75.0-121
Tr
1,1,2-Trichlorotrifluoroethane 0.125 0.0906 72.5 61.0-139
1,2,3-Trichlorobenzene 0.125 0.155 124 59.0-139 6
1,2,4-Trichlorobenzene 0.125 0.118 94.5 62.0-137 Sr
1,1,1-Trichloroethane 0.125 0.101 80.7 69.0-126
7
Qc
Trichloroethene 0.125 0.0957 76.5 76.0-126
Trichlorofluoromethane 0.125 0.126 101 61.0-142 8
1,2,3-Trichloropropane 0.125 0.135 108 67.0-129 Gl
1,2,3-Trimethylbenzene 0.125 0.114 91.4 74.0-124
9
Al
Vinyl chloride 0.125 0.139 112 63.0-134 10
Xylenes, Total 0.375 0.316 84.3 72.0-127 Sc
(S) Toluene-d8 103 75.0-131
(S) 4-Bromofluorobenzene 98.9 67.0-138
(S) 1,2-Dichloroethane-d4 103 70.0-130
(OS) L1075744-01 03/06/19 13:19 • (MS) R3389241-3 03/06/19 14:36 • (MSD) R3389241-4 03/06/19 15:15
Acetone 0.625 0.422 0.827 1.15 54.9 98.7 1.18 10.0-160 32.7 40
Acrylonitrile 0.625 0.0241 0.699 0.773 91.5 102 1.18 10.0-160 10.1 40
Benzene 0.125 0.0427 0.204 0.202 109 108 1.18 10.0-149 0.777 37
Bromobenzene 0.125 U 0.132 0.129 89.4 87.4 1.18 10.0-156 2.33 38
Bromodichloromethane 0.125 0.00279 0.121 0.121 80.1 79.9 1.18 10.0-143 0.316 37
Bromoform 0.125 U 0.166 0.175 112 119 1.18 10.0-146 5.36 36
Bromomethane 0.125 U 0.0691 0.0679 46.9 46.0 1.18 10.0-149 1.81 38
n-Butylbenzene 0.125 0.155 0.364 0.334 142 121 1.18 10.0-160 8.55 40
sec-Butylbenzene 0.125 0.0283 0.217 0.202 128 118 1.18 10.0-159 7.04 39
tert-Butylbenzene 0.125 0.118 0.145 0.134 17.9 10.6 1.18 10.0-156 7.68 39

03/13/19 15:42
16:10 117 of 161
Cp
(OS) L1075744-01 03/06/19 13:19 • (MS) R3389241-3 03/06/19 14:36 • (MSD) R3389241-4 03/06/19 15:15
Analyte mg/kg mg/kg mg/kg mg/kg % % % % % Tc
Carbon tetrachloride 0.125 0.00184 0.161 0.150 108 101 1.18 10.0-145 6.50 37
3
Chlorobenzene 0.125 0.00142 0.138 0.131 92.5 88.1 1.18 10.0-152 4.85 39
Ss
Chlorodibromomethane 0.125 U 0.157 0.157 106 106 1.18 10.0-146 0.0586 37
Chloroethane 0.125 0.00310 0.0672 0.0681 43.5 44.1 1.18 10.0-146 1.28 40 4
Chloroform 0.125 0.00108 0.141 0.149 94.9 100 1.18 10.0-146 5.29 37 Cn
Chloromethane 0.125 U 0.107 0.0956 72.4 64.8 1.18 10.0-159 11.1 37
5
2-Chlorotoluene 0.125 0.00356 0.168 0.164 112 109 1.18 10.0-159 2.45 38
Tr
4-Chlorotoluene 0.125 0.0320 0.117 0.111 57.6 53.3 1.18 10.0-155 5.64 39
1,2-Dibromo-3-Chloropropane 0.125 U 0.111 0.124 75.4 84.4 1.18 10.0-151 11.2 39 6
1,2-Dibromoethane 0.125 U 0.129 0.132 87.6 89.2 1.18 10.0-148 1.84 34 Sr
Dibromomethane 0.125 U 0.187 0.162 127 110 1.18 10.0-147 14.2 35
7
1,2-Dichlorobenzene 0.125 U 0.126 0.125 85.4 84.7 1.18 10.0-155 0.879 37
Qc
1,3-Dichlorobenzene 0.125 U 0.132 0.130 89.8 88.2 1.18 10.0-153 1.73 38
1,4-Dichlorobenzene 0.125 U 0.128 0.124 86.5 84.2 1.18 10.0-151 2.70 38 8
Dichlorodifluoromethane 0.125 U 0.212 0.193 144 131 1.18 10.0-160 9.33 35 Gl
1,1-Dichloroethane 0.125 0.00175 0.155 0.162 104 109 1.18 10.0-147 4.28 37
9
1,2-Dichloroethane 0.125 0.00126 0.146 0.150 98.4 101 1.18 10.0-148 2.41 35
Al
1,1-Dichloroethene 0.125 U 0.0760 0.0703 51.5 47.7 1.18 10.0-155 7.74 37
cis-1,2-Dichloroethene 0.125 U 0.176 0.196 119 133 1.18 10.0-149 10.7 37 10
trans-1,2-Dichloroethene 0.125 U 0.117 0.120 79.3 81.4 1.18 10.0-150 2.58 37 Sc
1,2-Dichloropropane 0.125 0.0258 0.153 0.153 86.2 86.5 1.18 10.0-148 0.273 37
1,1-Dichloropropene 0.125 U 0.129 0.130 87.2 88.0 1.18 10.0-153 0.943 35
1,3-Dichloropropane 0.125 U 0.157 0.157 106 106 1.18 10.0-154 0.263 35
cis-1,3-Dichloropropene 0.125 U 0.152 0.144 103 97.4 1.18 10.0-151 5.94 37
trans-1,3-Dichloropropene 0.125 U 0.172 0.171 117 116 1.18 10.0-148 0.537 37
2,2-Dichloropropane 0.125 0.00207 0.157 0.151 105 101 1.18 10.0-138 3.90 36
Di-isopropyl ether 0.125 0.00106 0.153 0.156 103 105 1.18 10.0-147 1.90 36
Ethylbenzene 0.125 0.191 0.473 0.452 191 177 1.18 10.0-160 J5 J5 4.45 38
Hexachloro-1,3-butadiene 0.125 U 0.155 0.151 105 102 1.18 10.0-160 2.82 40
Isopropylbenzene 0.125 0.0247 0.189 0.179 112 104 1.18 10.0-155 5.86 38
p-Isopropyltoluene 0.125 0.0410 0.524 0.486 327 301 1.18 10.0-160 J5 J5 7.54 40
2-Butanone (MEK) 0.625 0.0721 1.09 1.12 139 142 1.18 10.0-160 2.31 40
Methylene Chloride 0.125 U 0.116 0.122 79.0 82.8 1.18 10.0-141 4.74 37
4-Methyl-2-pentanone (MIBK) 0.625 U 0.842 0.950 114 129 1.18 10.0-160 12.0 35
Methyl tert-butyl ether 0.125 0.00133 0.131 0.127 87.8 84.9 1.18 11.0-147 3.28 35
Naphthalene 0.125 0.326 0.576 0.612 170 194 1.18 10.0-160 J5 J5 5.98 36
n-Propylbenzene 0.125 0.115 0.335 0.307 149 130 1.18 10.0-158 8.72 38
Styrene 0.125 0.0139 0.175 0.173 109 108 1.18 10.0-160 0.868 40
1,1,1,2-Tetrachloroethane 0.125 U 0.156 0.154 106 104 1.18 10.0-149 1.56 39
1,1,2,2-Tetrachloroethane 0.125 0.00817 0.189 0.199 123 129 1.18 10.0-160 5.00 35

03/13/19 15:42
16:10 118 of 161
Cp
(OS) L1075744-01 03/06/19 13:19 • (MS) R3389241-3 03/06/19 14:36 • (MSD) R3389241-4 03/06/19 15:15
Tetrachloroethene 0.125 0.0566 0.177 0.165 81.6 73.7 1.18 10.0-156 6.76 39
3
Toluene 0.125 0.486 0.910 0.884 288 270 1.18 10.0-156 J5 J5 2.86 38
Ss
1,1,2-Trichlorotrifluoroethane 0.125 U 0.0872 0.0772 59.1 52.3 1.18 10.0-160 12.2 36
1,2,3-Trichlorobenzene 0.125 0.00258 0.184 0.187 123 125 1.18 10.0-160 1.67 40 4
1,2,4-Trichlorobenzene 0.125 U 0.141 0.146 95.7 98.7 1.18 10.0-160 3.17 40 Cn
1,1,1-Trichloroethane 0.125 0.00950 0.126 0.122 78.9 76.3 1.18 10.0-144 3.10 35
5
1,1,2-Trichloroethane 0.125 0.00827 0.173 0.172 112 111 1.18 10.0-160 0.697 35
Tr
Trichloroethene 0.125 U 0.120 0.115 81.2 77.9 1.18 10.0-156 4.10 38
Trichlorofluoromethane 0.125 0.00115 0.0967 0.0963 64.8 64.5 1.18 10.0-160 0.413 40 6
1,2,3-Trichloropropane 0.125 U 0.129 0.143 87.5 97.1 1.18 10.0-156 10.4 35 Sr
1,2,3-Trimethylbenzene 0.125 0.274 0.576 0.523 205 169 1.18 10.0-160 J5 J5 9.55 36
7
1,2,4-Trimethylbenzene 0.125 0.788 1.42 1.33 432 369 1.18 10.0-160 V V 6.71 36
Qc
1,3,5-Trimethylbenzene 0.125 0.187 0.432 0.400 166 144 1.18 10.0-160 J5 7.72 38
Vinyl chloride 0.125 U 0.140 0.129 95.1 87.8 1.18 10.0-160 8.01 37 8
Xylenes, Total 0.375 0.943 1.94 1.89 225 215 1.18 10.0-160 J5 J5 2.30 38 Gl
(S) Toluene-d8 103 105 75.0-131
9
(S) 4-Bromofluorobenzene 102 104 67.0-138
Al
(S) 1,2-Dichloroethane-d4 91.5 101 70.0-130
10
Sc

03/13/19 15:42
16:10 119 of 161
Volatile Organic Compounds (GC/MS) by Method 8260B L1075168-21,22,23,24
Method Blank (MB) 1

Cp
(MB) R3389403-3 03/06/19 11:08
Acetone U 0.0137 0.0250
3
Ss
Benzene U 0.000400 0.00100
Bromobenzene U 0.00105 0.0125 4
Bromodichloromethane U 0.000788 0.00250 Cn
Bromoform U 0.00598 0.0250
5
Tr
n-Butylbenzene U 0.00384 0.0125
sec-Butylbenzene U 0.00253 0.0125 6
tert-Butylbenzene U 0.00155 0.00500 Sr
7
Qc
Chlorodibromomethane U 0.000450 0.00250
Chloroethane U 0.00108 0.00500 8
Chloroform U 0.000415 0.00250 Gl
9
Al
1,2-Dibromo-3-Chloropropane U 0.00510 0.0250 10
1,2-Dibromoethane U 0.000525 0.00250 Sc

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Method Blank (MB) 1

Cp
(MB) R3389403-3 03/06/19 11:08
3
2-Butanone (MEK) U 0.0125 0.0250
Ss
Methylene Chloride 0.00775 J 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.0100 0.0250 4
Methyl tert-butyl ether U 0.000295 0.00100 Cn
Naphthalene 0.00675 J 0.00312 0.0125
5
Tr
Styrene U 0.00273 0.0125
7
Toluene U 0.00125 0.00500
Qc
1,2,3-Trichlorobenzene U 0.000625 0.00250 8
1,2,4-Trichlorobenzene 0.0103 J 0.00482 0.0125 Gl
9
Al
Trichloroethene U 0.000400 0.00100
Trichlorofluoromethane U 0.000500 0.00250 10
1,2,3-Trichloropropane U 0.00510 0.0125 Sc
(S) Toluene-d8 96.5 75.0-131
(S) 4-Bromofluorobenzene 88.9 67.0-138

(LCS) R3389403-1 03/06/19 09:53 • (LCSD) R3389403-2 03/06/19 10:12
Acetone 0.625 0.676 0.722 108 116 10.0-160 6.52 31
Acrylonitrile 0.625 0.789 0.783 126 125 45.0-153 0.734 22
Benzene 0.125 0.113 0.109 90.2 87.5 70.0-123 3.06 20
Bromobenzene 0.125 0.150 0.148 120 119 73.0-121 1.28 20
Bromodichloromethane 0.125 0.150 0.150 120 120 73.0-121 0.0806 20

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Cp
(LCS) R3389403-1 03/06/19 09:53 • (LCSD) R3389403-2 03/06/19 10:12
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 2
Analyte mg/kg mg/kg mg/kg % % % % % Tc
Bromoform 0.125 0.118 0.122 94.1 97.2 64.0-132 3.26 20
3
Bromomethane 0.125 0.0918 0.0918 73.4 73.5 56.0-147 0.0370 20
Ss
n-Butylbenzene 0.125 0.101 0.0995 80.6 79.6 68.0-135 1.21 20
sec-Butylbenzene 0.125 0.120 0.119 95.9 94.9 74.0-130 1.08 20 4
tert-Butylbenzene 0.125 0.115 0.117 92.2 93.6 75.0-127 1.51 20 Cn
Carbon tetrachloride 0.125 0.148 0.149 118 119 66.0-128 0.819 20
5
Chlorobenzene 0.125 0.101 0.102 80.5 81.9 76.0-128 1.66 20
Tr
Chlorodibromomethane 0.125 0.128 0.128 103 103 74.0-127 0.0857 20
Chloroethane 0.125 0.102 0.102 81.9 81.9 61.0-134 0.0127 20 6
Chloroform 0.125 0.109 0.106 87.5 84.8 72.0-123 3.06 20 Sr
Chloromethane 0.125 0.126 0.121 100 96.9 51.0-138 3.54 20
7
2-Chlorotoluene 0.125 0.151 0.145 121 116 75.0-124 3.62 20
Qc
4-Chlorotoluene 0.125 0.115 0.118 91.8 94.2 75.0-124 2.61 20
1,2-Dibromo-3-Chloropropane 0.125 0.155 0.158 124 126 59.0-130 2.07 20 8
1,2-Dibromoethane 0.125 0.142 0.141 113 113 74.0-128 0.683 20 Gl
Dibromomethane 0.125 0.134 0.126 107 101 75.0-122 6.28 20
9
1,2-Dichlorobenzene 0.125 0.101 0.103 81.1 82.3 76.0-124 1.48 20
Al
1,4-Dichlorobenzene 0.125 0.114 0.117 90.9 93.8 77.0-121 3.09 20 10
Dichlorodifluoromethane 0.125 0.129 0.135 104 108 43.0-156 3.88 20 Sc
1,1-Dichloroethane 0.125 0.127 0.125 101 100 70.0-127 1.31 20
1,2-Dichloroethane 0.125 0.146 0.143 117 114 65.0-131 2.10 20
1,1-Dichloroethene 0.125 0.116 0.116 93.0 92.7 65.0-131 0.308 20
cis-1,2-Dichloroethene 0.125 0.106 0.103 84.5 82.4 73.0-125 2.50 20
trans-1,2-Dichloroethene 0.125 0.113 0.111 90.1 88.5 71.0-125 1.79 20
1,2-Dichloropropane 0.125 0.142 0.141 113 113 74.0-125 0.432 20
1,1-Dichloropropene 0.125 0.109 0.105 87.2 83.6 73.0-125 4.13 20
1,3-Dichloropropane 0.125 0.124 0.124 99.3 99.4 80.0-125 0.0684 20
cis-1,3-Dichloropropene 0.125 0.111 0.112 89.2 89.3 76.0-127 0.157 20
trans-1,3-Dichloropropene 0.125 0.117 0.116 93.4 93.0 73.0-127 0.355 20
Di-isopropyl ether 0.125 0.107 0.107 85.5 85.4 60.0-136 0.174 20
Ethylbenzene 0.125 0.104 0.106 83.5 84.5 74.0-126 1.17 20
Hexachloro-1,3-butadiene 0.125 0.115 0.106 91.6 85.2 57.0-150 7.33 20
Isopropylbenzene 0.125 0.0966 0.0997 77.3 79.8 72.0-127 3.15 20
p-Isopropyltoluene 0.125 0.115 0.115 92.1 92.0 72.0-133 0.167 20
2-Butanone (MEK) 0.625 0.833 0.782 133 125 30.0-160 6.28 24
Methylene Chloride 0.125 0.113 0.111 90.5 88.9 68.0-123 1.82 20
4-Methyl-2-pentanone (MIBK) 0.625 0.540 0.562 86.4 89.9 56.0-143 3.96 20
Methyl tert-butyl ether 0.125 0.104 0.103 83.5 82.1 66.0-132 1.68 20

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Cp
(LCS) R3389403-1 03/06/19 09:53 • (LCSD) R3389403-2 03/06/19 10:12
Naphthalene 0.125 0.152 0.147 121 117 59.0-130 3.22 20
3
n-Propylbenzene 0.125 0.112 0.111 89.4 88.6 74.0-126 0.885 20
Ss
Styrene 0.125 0.121 0.122 96.9 97.9 72.0-127 0.979 20
1,1,1,2-Tetrachloroethane 0.125 0.0980 0.101 78.4 81.1 74.0-129 3.31 20 4
1,1,2,2-Tetrachloroethane 0.125 0.112 0.114 90.0 91.4 68.0-128 1.54 20 Cn
Tetrachloroethene 0.125 0.102 0.107 81.4 85.6 70.0-136 5.10 20
5
Toluene 0.125 0.0973 0.0979 77.8 78.4 75.0-121 0.688 20
Tr
1,1,2-Trichlorotrifluoroethane 0.125 0.114 0.115 91.4 92.2 61.0-139 0.899 20
1,2,3-Trichlorobenzene 0.125 0.103 0.0994 82.6 79.5 59.0-139 3.73 20 6
1,2,4-Trichlorobenzene 0.125 0.157 0.150 125 120 62.0-137 4.12 20 Sr
1,1,1-Trichloroethane 0.125 0.125 0.123 100 98.8 69.0-126 1.32 20
7
1,1,2-Trichloroethane 0.125 0.135 0.138 108 110 78.0-123 1.77 20
Qc
Trichloroethene 0.125 0.145 0.142 116 114 76.0-126 2.18 20
Trichlorofluoromethane 0.125 0.114 0.117 90.8 93.5 61.0-142 2.95 20 8
1,2,3-Trichloropropane 0.125 0.136 0.132 109 105 67.0-129 3.49 20 Gl
1,2,3-Trimethylbenzene 0.125 0.111 0.113 89.0 90.5 74.0-124 1.70 20
9
Al
Vinyl chloride 0.125 0.103 0.103 82.4 82.6 63.0-134 0.259 20 10
Xylenes, Total 0.375 0.302 0.300 80.5 80.0 72.0-127 0.664 20 Sc
(S) Toluene-d8 90.3 92.1 75.0-131
(S) 4-Bromofluorobenzene 92.4 94.4 67.0-138
(S) 1,2-Dichloroethane-d4 119 120 70.0-130
(OS) L1075219-04 03/06/19 17:56 • (MS) R3389403-4 03/06/19 20:08 • (MSD) R3389403-5 03/06/19 20:27
Acetone 0.625 ND 0.450 0.324 72.0 51.9 1 10.0-160 32.5 40
Acrylonitrile 0.625 ND 0.653 0.530 105 84.8 1 10.0-160 20.9 40
Benzene 0.125 ND 0.0392 0.0521 31.4 41.7 1 10.0-149 28.2 37
Bromobenzene 0.125 ND 0.0776 0.101 62.1 81.0 1 10.0-156 26.4 38
Bromodichloromethane 0.125 ND 0.0766 0.0938 61.3 75.0 1 10.0-143 20.2 37
Bromoform 0.125 ND 0.0823 0.0902 65.9 72.2 1 10.0-146 9.13 36
Bromomethane 0.125 ND 0.0155 0.0245 12.4 19.6 1 10.0-149 J3 44.8 38
n-Butylbenzene 0.125 ND 0.0395 0.0547 31.6 43.7 1 10.0-160 32.3 40
sec-Butylbenzene 0.125 ND 0.0431 0.0654 34.5 52.4 1 10.0-159 J3 41.1 39
tert-Butylbenzene 0.125 ND 0.0441 0.0671 35.2 53.7 1 10.0-156 J3 41.5 39

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Cp
(OS) L1075219-04 03/06/19 17:56 • (MS) R3389403-4 03/06/19 20:08 • (MSD) R3389403-5 03/06/19 20:27
Carbon tetrachloride 0.125 ND 0.0362 0.0510 29.0 40.8 1 10.0-145 33.9 37
3
Chlorobenzene 0.125 ND 0.0452 0.0590 36.1 47.2 1 10.0-152 26.6 39
Ss
Chlorodibromomethane 0.125 ND 0.0832 0.0962 66.6 77.0 1 10.0-146 14.5 37
Chloroethane 0.125 ND 0.0118 0.0277 9.45 22.2 1 10.0-146 J6 J3 80.4 40 4
Chloroform 0.125 ND 0.0429 0.0553 34.3 44.2 1 10.0-146 25.2 37 Cn
Chloromethane 0.125 ND 0.0227 0.0308 18.2 24.7 1 10.0-159 30.2 37
5
2-Chlorotoluene 0.125 ND 0.0641 0.0876 51.3 70.1 1 10.0-159 31.0 38
Tr
4-Chlorotoluene 0.125 ND 0.0543 0.0710 43.4 56.8 1 10.0-155 26.8 39
1,2-Dibromo-3-Chloropropane 0.125 ND 0.0986 0.119 78.9 95.2 1 10.0-151 18.8 39 6
1,2-Dibromoethane 0.125 ND 0.0969 0.107 77.5 86.0 1 10.0-148 10.3 34 Sr
Dibromomethane 0.125 ND 0.0793 0.0870 63.4 69.6 1 10.0-147 9.31 35
7
1,2-Dichlorobenzene 0.125 ND 0.0596 0.0744 47.7 59.5 1 10.0-155 22.0 37
Qc
1,3-Dichlorobenzene 0.125 ND 0.0579 0.0736 46.3 58.8 1 10.0-153 23.8 38
1,4-Dichlorobenzene 0.125 ND 0.0627 0.0795 50.2 63.6 1 10.0-151 23.6 38 8
Dichlorodifluoromethane 0.125 ND 0.0306 0.0413 24.5 33.1 1 10.0-160 29.8 35 Gl
1,1-Dichloroethane 0.125 ND 0.0432 0.0578 34.6 46.3 1 10.0-147 28.9 37
9
1,2-Dichloroethane 0.125 ND 0.0829 0.0933 66.3 74.7 1 10.0-148 11.8 35
Al
1,1-Dichloroethene 0.125 ND 0.0272 0.0388 21.8 31.0 1 10.0-155 35.0 37
cis-1,2-Dichloroethene 0.125 ND 0.0377 0.0481 30.2 38.5 1 10.0-149 24.3 37 10
trans-1,2-Dichloroethene 0.125 ND 0.0263 0.0366 21.1 29.3 1 10.0-150 32.5 37 Sc
1,2-Dichloropropane 0.125 ND 0.0656 0.0847 52.5 67.8 1 10.0-148 25.5 37
1,1-Dichloropropene 0.125 ND 0.0290 0.0406 23.2 32.5 1 10.0-153 33.3 35
cis-1,3-Dichloropropene 0.125 ND 0.0566 0.0701 45.3 56.1 1 10.0-151 21.2 37
trans-1,3-Dichloropropene 0.125 ND 0.0744 0.0905 59.5 72.4 1 10.0-148 19.5 37
Di-isopropyl ether 0.125 ND 0.0556 0.0671 44.5 53.7 1 10.0-147 18.7 36
Ethylbenzene 0.125 ND 0.0363 0.0531 29.1 42.5 1 10.0-160 37.6 38
Hexachloro-1,3-butadiene 0.125 ND 0.0457 0.0604 36.6 48.3 1 10.0-160 27.6 40
Isopropylbenzene 0.125 ND 0.0345 0.0465 27.6 37.2 1 10.0-155 29.7 38
p-Isopropyltoluene 0.125 ND 0.0417 0.0629 33.4 50.3 1 10.0-160 J3 40.5 40
2-Butanone (MEK) 0.625 ND 0.788 0.674 126 108 1 10.0-160 15.7 40
Methylene Chloride 0.125 ND 0.0484 0.0597 38.7 47.7 1 10.0-141 20.9 37
4-Methyl-2-pentanone (MIBK) 0.625 ND 0.460 0.492 73.5 78.7 1 10.0-160 6.83 35
Methyl tert-butyl ether 0.125 ND 0.0655 0.0661 52.4 52.8 1 11.0-147 0.806 35
Naphthalene 0.125 ND 0.0923 0.110 70.8 85.3 1 10.0-160 17.9 36
n-Propylbenzene 0.125 ND 0.0408 0.0615 32.6 49.2 1 10.0-158 J3 40.6 38
Styrene 0.125 ND 0.0571 0.0717 45.7 57.3 1 10.0-160 22.6 40
1,1,1,2-Tetrachloroethane 0.125 ND 0.0521 0.0599 41.7 47.9 1 10.0-149 13.9 39
1,1,2,2-Tetrachloroethane 0.125 ND 0.0896 0.103 71.7 82.2 1 10.0-160 13.6 35

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Cp
(OS) L1075219-04 03/06/19 17:56 • (MS) R3389403-4 03/06/19 20:08 • (MSD) R3389403-5 03/06/19 20:27
Tetrachloroethene 0.125 0.283 0.0586 0.0721 0.000 0.000 1 10.0-156 J6 J6 20.6 39
3
Toluene 0.125 ND 0.0375 0.0524 27.6 39.4 1 10.0-156 32.9 38
Ss
1,1,2-Trichlorotrifluoroethane 0.125 ND 0.0280 0.0437 22.4 34.9 1 10.0-160 J3 43.9 36
1,2,3-Trichlorobenzene 0.125 ND 0.0689 0.0817 55.1 65.4 1 10.0-160 17.1 40 4
1,2,4-Trichlorobenzene 0.125 ND 0.0901 0.104 72.1 82.9 1 10.0-160 13.9 40 Cn
1,1,1-Trichloroethane 0.125 0.0249 0.0344 0.0477 7.60 18.3 1 10.0-144 J6 32.6 35
5
1,1,2-Trichloroethane 0.125 ND 0.0976 0.113 78.1 90.0 1 10.0-160 14.2 35
Tr
Trichloroethene 0.125 0.00202 0.0465 0.0628 35.6 48.6 1 10.0-156 29.9 38
Trichlorofluoromethane 0.125 ND 0.0222 0.0351 17.8 28.1 1 10.0-160 J3 44.8 40 6
1,2,3-Trichloropropane 0.125 ND 0.108 0.122 86.2 97.6 1 10.0-156 12.4 35 Sr
1,2,3-Trimethylbenzene 0.125 ND 0.0545 0.0730 41.4 56.2 1 10.0-160 29.0 36
7
1,2,4-Trimethylbenzene 0.125 0.00509 0.0509 0.0680 36.7 50.3 1 10.0-160 28.7 36
Qc
1,3,5-Trimethylbenzene 0.125 ND 0.0422 0.0610 31.3 46.4 1 10.0-160 36.5 38
Vinyl chloride 0.125 ND 0.0166 0.0280 13.3 22.4 1 10.0-160 J3 51.2 37 8
Xylenes, Total 0.375 ND 0.116 0.151 31.0 40.3 1 10.0-160 26.0 38 Gl
(S) Toluene-d8 94.3 97.0 75.0-131
9
(S) 4-Bromofluorobenzene 91.9 87.4 67.0-138
Al
10
Sc

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Volatile Organic Compounds (GC/MS) by Method 8260C L1075168-03,12,13,14
Method Blank (MB) 1

Cp
(MB) R3389083-2 03/05/19 13:02
Acetone U 0.0100 0.0500
3
Acrolein U 0.00887 0.0500
Ss
Benzene U 0.000331 0.00100 4
Bromobenzene U 0.000352 0.00100 Cn
Bromodichloromethane U 0.000380 0.00100
5
Bromoform U 0.000469 0.00100
Tr
n-Butylbenzene U 0.000361 0.00100 6
sec-Butylbenzene U 0.000365 0.00100 Sr
tert-Butylbenzene U 0.000399 0.00100
7
Qc
Chlorodibromomethane U 0.000327 0.00100 8
Chloroethane U 0.000453 0.00500 Gl
Chloroform U 0.000324 0.00500
9
Al
4-Chlorotoluene U 0.000351 0.00100 10
1,2-Dibromo-3-Chloropropane U 0.00133 0.00500 Sc
1,2-Dibromoethane U 0.000381 0.00100

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Method Blank (MB) 1

Cp
(MB) R3389083-2 03/05/19 13:02
3
Ss
2-Butanone (MEK) U 0.00393 0.0100
Methylene Chloride U 0.00100 0.00500 4
4-Methyl-2-pentanone (MIBK) U 0.00214 0.0100 Cn
Methyl tert-butyl ether U 0.000367 0.00100
5
Tr
Styrene U 0.000307 0.00100 6
1,1,2,2-Tetrachloroethane U 0.000130 0.00100
7
Qc
Toluene U 0.000412 0.00100
1,1,2-Trichlorotrifluoroethane U 0.000303 0.00100 8
1,2,4-Trichlorobenzene U 0.000355 0.00100
9
Al
Trichloroethene U 0.000398 0.00100 10
Trichlorofluoromethane U 0.00120 0.00500 Sc
1,2,3-Trichloropropane U 0.000807 0.00250
(S) Toluene-d8 106 80.0-120

(LCS) R3389083-1 03/05/19 12:22
Acetone 0.125 0.102 82.0 19.0-160
Acrolein 0.125 0.124 99.1 10.0-160
Acrylonitrile 0.125 0.122 97.8 55.0-149
Benzene 0.0250 0.0237 94.6 70.0-123

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Cp
(LCS) R3389083-1 03/05/19 12:22
Analyte mg/l mg/l % % Tc
Bromobenzene 0.0250 0.0232 92.8 73.0-121
3
Bromodichloromethane 0.0250 0.0232 92.8 75.0-120
Ss
Bromoform 0.0250 0.0280 112 68.0-132
Bromomethane 0.0250 0.0234 93.6 10.0-160 4
n-Butylbenzene 0.0250 0.0234 93.6 73.0-125 Cn
sec-Butylbenzene 0.0250 0.0238 95.2 75.0-125
5
tert-Butylbenzene 0.0250 0.0244 97.7 76.0-124
Tr
Carbon tetrachloride 0.0250 0.0257 103 68.0-126
Chlorobenzene 0.0250 0.0237 94.8 80.0-121 6
Chlorodibromomethane 0.0250 0.0256 102 77.0-125 Sr
Chloroethane 0.0250 0.0217 86.7 47.0-150
7
Chloroform 0.0250 0.0228 91.0 73.0-120
Qc
Chloromethane 0.0250 0.0239 95.4 41.0-142
2-Chlorotoluene 0.0250 0.0233 93.2 76.0-123 8
4-Chlorotoluene 0.0250 0.0232 92.9 75.0-122 Gl
1,2-Dibromo-3-Chloropropane 0.0250 0.0259 104 58.0-134
9
1,2-Dibromoethane 0.0250 0.0242 96.7 80.0-122
Al
Dibromomethane 0.0250 0.0240 95.9 80.0-120
1,2-Dichlorobenzene 0.0250 0.0241 96.3 79.0-121 10
1,3-Dichlorobenzene 0.0250 0.0235 94.0 79.0-120 Sc
Dichlorodifluoromethane 0.0250 0.0236 94.3 51.0-149
1,1-Dichloroethane 0.0250 0.0234 93.6 70.0-126
1,2-Dichloroethane 0.0250 0.0229 91.5 70.0-128
1,1-Dichloroethene 0.0250 0.0289 116 71.0-124
cis-1,2-Dichloroethene 0.0250 0.0234 93.5 73.0-120
trans-1,2-Dichloroethene 0.0250 0.0241 96.6 73.0-120
1,2-Dichloropropane 0.0250 0.0237 94.6 77.0-125
1,1-Dichloropropene 0.0250 0.0235 94.1 74.0-126
1,3-Dichloropropane 0.0250 0.0241 96.3 80.0-120
cis-1,3-Dichloropropene 0.0250 0.0229 91.6 80.0-123
trans-1,3-Dichloropropene 0.0250 0.0244 97.4 78.0-124
Di-isopropyl ether 0.0250 0.0253 101 58.0-138
Ethylbenzene 0.0250 0.0241 96.2 79.0-123
Hexachloro-1,3-butadiene 0.0250 0.0279 112 54.0-138
Isopropylbenzene 0.0250 0.0252 101 76.0-127
p-Isopropyltoluene 0.0250 0.0243 97.2 76.0-125
2-Butanone (MEK) 0.125 0.122 97.5 44.0-160
Methylene Chloride 0.0250 0.0247 98.8 67.0-120

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Cp
(LCS) R3389083-1 03/05/19 12:22
Analyte mg/l mg/l % % Tc
4-Methyl-2-pentanone (MIBK) 0.125 0.124 99.3 68.0-142
3
Methyl tert-butyl ether 0.0250 0.0255 102 68.0-125
Ss
Naphthalene 0.0250 0.0256 102 54.0-135
n-Propylbenzene 0.0250 0.0230 92.0 77.0-124 4
Styrene 0.0250 0.0259 104 73.0-130 Cn
1,1,1,2-Tetrachloroethane 0.0250 0.0246 98.5 75.0-125
5
1,1,2,2-Tetrachloroethane 0.0250 0.0225 90.1 65.0-130
Tr
Tetrachloroethene 0.0250 0.0240 96.1 72.0-132
Toluene 0.0250 0.0244 97.7 79.0-120 6
1,1,2-Trichlorotrifluoroethane 0.0250 0.0271 109 69.0-132 Sr
1,2,3-Trichlorobenzene 0.0250 0.0259 103 50.0-138
7
1,2,4-Trichlorobenzene 0.0250 0.0265 106 57.0-137
Qc
1,1,2-Trichloroethane 0.0250 0.0232 92.9 80.0-120 8
Trichloroethene 0.0250 0.0243 97.2 78.0-124 Gl
Trichlorofluoromethane 0.0250 0.0249 99.5 59.0-147
9
1,2,3-Trichloropropane 0.0250 0.0219 87.6 73.0-130
Al
1,2,4-Trimethylbenzene 0.0250 0.0229 91.8 76.0-121 10
1,3,5-Trimethylbenzene 0.0250 0.0237 95.0 76.0-122 Sc
Vinyl chloride 0.0250 0.0227 90.6 67.0-131
Xylenes, Total 0.0750 0.0727 96.9 79.0-123
(S) Toluene-d8 104 80.0-120

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Volatile Organic Compounds (GC/MS) by Method 8260C L1075168-15,16,17,18,19
Method Blank (MB) 1

Cp
(MB) R3389504-3 03/06/19 13:17
Acetone U 0.0100 0.0500
3
Acrolein U 0.00887 0.0500
Ss
Benzene U 0.000331 0.00100 4
Bromobenzene U 0.000352 0.00100 Cn
Bromodichloromethane U 0.000380 0.00100
5
Bromoform U 0.000469 0.00100
Tr
n-Butylbenzene U 0.000361 0.00100 6
sec-Butylbenzene U 0.000365 0.00100 Sr
tert-Butylbenzene U 0.000399 0.00100
7
Qc
Chlorodibromomethane U 0.000327 0.00100 8
Chloroethane U 0.000453 0.00500 Gl
Chloroform U 0.000324 0.00500
9
Al
4-Chlorotoluene U 0.000351 0.00100 10
1,2-Dibromo-3-Chloropropane U 0.00133 0.00500 Sc
1,2-Dibromoethane U 0.000381 0.00100

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Method Blank (MB) 1

Cp
(MB) R3389504-3 03/06/19 13:17
3
2-Butanone (MEK) U 0.00393 0.0100
Ss
Methylene Chloride U 0.00100 0.00500 4
4-Methyl-2-pentanone (MIBK) U 0.00214 0.0100 Cn
Methyl tert-butyl ether U 0.000367 0.00100
5
Tr
Styrene U 0.000307 0.00100
Naphthalene U 0.00100 0.00500 Sr
1,1,2,2-Tetrachloroethane U 0.000130 0.00100
7
Qc
1,2,3-Trichlorobenzene U 0.000230 0.00100 8
9
Al
Toluene U 0.000412 0.00100
Trichloroethene U 0.000398 0.00100 10
Trichlorofluoromethane U 0.00120 0.00500 Sc
1,2,3-Trichloropropane U 0.000807 0.00250
(S) Toluene-d8 107 80.0-120

(LCS) R3389504-1 03/06/19 12:17 • (LCSD) R3389504-2 03/06/19 12:37
Analyte mg/l mg/l mg/l % % % % %
Acetone 0.125 0.152 0.152 122 122 19.0-160 0.114 27
Acrolein 0.125 0.0967 0.101 77.4 80.6 10.0-160 4.09 26
Acrylonitrile 0.125 0.126 0.127 100 102 55.0-149 1.32 20
Bromobenzene 0.0250 0.0223 0.0231 89.2 92.5 73.0-121 3.60 20

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Cp
(LCS) R3389504-1 03/06/19 12:17 • (LCSD) R3389504-2 03/06/19 12:37
Analyte mg/l mg/l mg/l % % % % % Tc
Bromodichloromethane 0.0250 0.0220 0.0219 87.9 87.7 75.0-120 0.182 20
3
Bromoform 0.0250 0.0266 0.0265 107 106 68.0-132 0.478 20
Ss
Bromomethane 0.0250 0.0227 0.0225 91.0 89.8 10.0-160 1.28 25
n-Butylbenzene 0.0250 0.0226 0.0230 90.2 92.2 73.0-125 2.16 20 4
sec-Butylbenzene 0.0250 0.0230 0.0238 92.1 95.3 75.0-125 3.35 20 Cn
tert-Butylbenzene 0.0250 0.0236 0.0237 94.3 94.9 76.0-124 0.679 20
5
Carbon tetrachloride 0.0250 0.0246 0.0243 98.2 97.4 68.0-126 0.873 20
Tr
Chlorobenzene 0.0250 0.0233 0.0233 93.2 93.0 80.0-121 0.147 20
Chlorodibromomethane 0.0250 0.0247 0.0244 98.6 97.7 77.0-125 0.936 20 6
Chloroethane 0.0250 0.0221 0.0220 88.3 87.8 47.0-150 0.473 20 Sr
Chloroform 0.0250 0.0218 0.0215 87.2 86.1 73.0-120 1.22 20
7
Chloromethane 0.0250 0.0227 0.0229 91.0 91.7 41.0-142 0.812 20
Qc
2-Chlorotoluene 0.0250 0.0225 0.0231 90.0 92.3 76.0-123 2.50 20
Benzene 0.0250 0.0230 0.0227 91.8 91.0 70.0-123 0.976 20 8
4-Chlorotoluene 0.0250 0.0222 0.0227 88.7 90.8 75.0-122 2.27 20 Gl
1,2-Dibromo-3-Chloropropane 0.0250 0.0256 0.0266 102 106 58.0-134 3.65 20
9
1,2-Dibromoethane 0.0250 0.0235 0.0234 93.9 93.7 80.0-122 0.219 20
Al
Dibromomethane 0.0250 0.0230 0.0229 91.9 91.8 80.0-120 0.152 20
1,2-Dichlorobenzene 0.0250 0.0230 0.0238 92.0 95.2 79.0-121 3.40 20 10
1,3-Dichlorobenzene 0.0250 0.0225 0.0234 89.9 93.6 79.0-120 4.08 20 Sc
Dichlorodifluoromethane 0.0250 0.0229 0.0228 91.4 91.4 51.0-149 0.0730 20
1,1-Dichloroethane 0.0250 0.0226 0.0224 90.3 89.8 70.0-126 0.526 20
1,2-Dichloroethane 0.0250 0.0219 0.0221 87.7 88.6 70.0-128 1.00 20
1,1-Dichloroethene 0.0250 0.0277 0.0242 111 97.0 71.0-124 13.4 20
cis-1,2-Dichloroethene 0.0250 0.0226 0.0224 90.2 89.8 73.0-120 0.507 20
trans-1,2-Dichloroethene 0.0250 0.0232 0.0231 93.0 92.5 73.0-120 0.484 20
1,1-Dichloropropene 0.0250 0.0225 0.0224 90.0 89.7 74.0-126 0.274 20
cis-1,3-Dichloropropene 0.0250 0.0219 0.0219 87.6 87.7 80.0-123 0.141 20
trans-1,3-Dichloropropene 0.0250 0.0231 0.0233 92.6 93.1 78.0-124 0.558 20
2,2-Dichloropropane 0.0250 0.0262 0.0265 105 106 58.0-130 1.08 20
Di-isopropyl ether 0.0250 0.0240 0.0241 96.1 96.5 58.0-138 0.403 20
Hexachloro-1,3-butadiene 0.0250 0.0249 0.0262 99.7 105 54.0-138 4.98 20
p-Isopropyltoluene 0.0250 0.0235 0.0240 94.0 96.1 76.0-125 2.28 20
2-Butanone (MEK) 0.125 0.128 0.128 102 103 44.0-160 0.338 20
Methylene Chloride 0.0250 0.0236 0.0233 94.3 93.1 67.0-120 1.22 20
4-Methyl-2-pentanone (MIBK) 0.125 0.123 0.124 98.8 99.5 68.0-142 0.727 20
Ethylbenzene 0.0250 0.0238 0.0235 95.1 94.1 79.0-123 1.01 20

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Cp
(LCS) R3389504-1 03/06/19 12:17 • (LCSD) R3389504-2 03/06/19 12:37
n-Propylbenzene 0.0250 0.0222 0.0231 88.8 92.2 77.0-124 3.71 20
3
Styrene 0.0250 0.0251 0.0251 100 100 73.0-130 0.248 20
Ss
1,1,1,2-Tetrachloroethane 0.0250 0.0234 0.0235 93.7 93.8 75.0-125 0.160 20
1,1,2,2-Tetrachloroethane 0.0250 0.0215 0.0223 85.8 89.1 65.0-130 3.77 20 4
Tetrachloroethene 0.0250 0.0240 0.0238 96.1 95.1 72.0-132 0.987 20 Cn
1,1,2-Trichlorotrifluoroethane 0.0250 0.0263 0.0217 105 86.6 69.0-132 19.4 20
5
Isopropylbenzene 0.0250 0.0244 0.0242 97.8 96.7 76.0-127 1.08 20
Tr
1,2,3-Trichlorobenzene 0.0250 0.0241 0.0254 96.6 101 50.0-138 4.88 20
1,2,4-Trichlorobenzene 0.0250 0.0247 0.0257 98.7 103 57.0-137 3.93 20 6
1,1,1-Trichloroethane 0.0250 0.0238 0.0235 95.2 94.1 73.0-124 1.21 20 Sr
1,1,2-Trichloroethane 0.0250 0.0224 0.0223 89.4 89.1 80.0-120 0.417 20
7
Trichloroethene 0.0250 0.0232 0.0230 93.0 91.8 78.0-124 1.26 20
Qc
Trichlorofluoromethane 0.0250 0.0250 0.0247 100 98.9 59.0-147 1.30 20
1,2,3-Trichloropropane 0.0250 0.0210 0.0213 84.0 85.4 73.0-130 1.65 20 8
Methyl tert-butyl ether 0.0250 0.0239 0.0242 95.4 96.7 68.0-125 1.31 20 Gl
9
Naphthalene 0.0250 0.0256 0.0258 103 103 54.0-135 0.580 20
Al
Vinyl chloride 0.0250 0.0213 0.0213 85.2 85.3 67.0-131 0.0456 20
Toluene 0.0250 0.0241 0.0239 96.4 95.6 79.0-120 0.789 20 10
1,2,4-Trimethylbenzene 0.0250 0.0223 0.0228 89.4 91.0 76.0-121 1.85 20 Sc
Xylenes, Total 0.0750 0.0712 0.0710 94.9 94.7 79.0-123 0.281 20
(S) Toluene-d8 106 104 80.0-120
(S) 4-Bromofluorobenzene 103 101 77.0-126

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Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 L1075168-02,03,04,06,07,08,09
Method Blank (MB) 1

Cp
(MB) R3389132-3 03/06/19 09:44
TPH C6 - C12 U 0.600 0.900
3
TPH C12 - C28 1.67 0.600 0.900
Ss
TPH C28 - C35 U 0.600 0.900
TPH C6 - C35 1.67 0.600 0.900 4
(S) o-Terphenyl 82.7 70.0-130 Cn
5
Tr
(LCS) R3389132-1 03/06/19 02:49 • (LCSD) R3389132-2 03/06/19 03:05 6
Sr
7
TPH C6 - C12 41.7 45.4 45.2 109 108 75.0-125 0.442 20 Qc
TPH C12 - C28 41.7 45.5 46.4 109 111 75.0-125 1.96 20
TPH C6 - C35 83.4 90.9 91.6 109 110 75.0-125 0.767 20 8
(S) o-Terphenyl 92.9 94.2 70.0-130

Gl
9
Al
10
Sc

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Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 L1075168-10,11,12,13,14,15,16,17,18,19
Method Blank (MB) 1

Cp
(MB) R3389426-1 03/06/19 14:53
TPH C6 - C12 U 0.600 0.900
3
TPH C12 - C28 U 0.600 0.900
Ss
TPH C28 - C35 U 0.600 0.900
TPH C6 - C35 U 0.600 0.900 4
5
Tr
(LCS) R3389426-2 03/06/19 15:09 • (LCSD) R3389426-3 03/06/19 15:26 6
Sr
7
TPH C6 - C12 41.7 45.1 43.8 108 105 75.0-125 2.92 20 Qc
TPH C12 - C28 41.7 45.1 43.2 108 104 75.0-125 4.30 20
TPH C6 - C35 83.4 90.2 87.0 108 104 75.0-125 3.61 20 8
(S) o-Terphenyl 91.7 90.4 70.0-130

Gl
9
Al
10
Sc

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Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 L1075168-01,05
Method Blank (MB) 1

Cp
(MB) R3389770-1 03/07/19 13:33
TPH C6 - C12 U 0.600 0.900
3
TPH C12 - C28 U 0.600 0.900
Ss
TPH C28 - C35 U 0.600 0.900
TPH C6 - C35 U 0.600 0.900 4
5
Tr
(LCS) R3389770-2 03/07/19 13:50 • (LCSD) R3389770-3 03/07/19 14:07 6
Sr
7
TPH C6 - C12 41.7 46.1 41.0 111 98.3 75.0-125 11.7 20 Qc
TPH C12 - C28 41.7 47.6 41.4 114 99.3 75.0-125 13.9 20
TPH C6 - C35 83.4 93.7 82.4 112 98.8 75.0-125 12.8 20 8
(S) o-Terphenyl 95.6 84.0 70.0-130

Gl
9
Al
10
Sc

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Semi-Volatile Organic Compounds (GC) by TCEQ Method 1005 L1075168-20,21,22,23,24
Method Blank (MB) 1

Cp
(MB) R3389780-1 03/07/19 20:53
TPH C6 - C12 U 15.0 50.0
3
TPH C12 - C28 U 15.0 50.0
Ss
TPH C28 - C35 U 15.0 50.0
TPH C6 - C35 U 15.0 50.0 4
5
Tr
(LCS) R3389780-2 03/07/19 21:07 • (LCSD) R3389780-3 03/07/19 21:20 6
Sr
7
TPH C6 - C12 250 252 266 101 106 75.0-125 5.41 20 Qc
TPH C12 - C28 250 246 257 98.4 103 75.0-125 4.37 20
TPH C6 - C35 500 498 523 99.6 105 75.0-125 4.90 20 8
(S) o-Terphenyl 100 102 70.0-130

Gl
9
Al
10
(OS) L1074953-17 03/08/19 23:33 • (MS) R3390154-1 03/08/19 23:47 • (MSD) R3390154-2 03/09/19 00:01 Sc
Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry) (dry)
TPH C6 - C12 271 U 314 338 116 125 1 75.0-125 7.31 20
TPH C12 - C28 271 77.4 377 467 111 144 1 75.0-125 J3 J5 21.3 20
TPH C6 - C35 542 299 691 805 72.4 93.4 1 75.0-125 J6 15.2 20
(S) o-Terphenyl 114 117 70.0-130

03/13/19 15:42
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Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1075168-20,21,22,23,24
Method Blank (MB) 1

Cp
(MB) R3388714-3 03/05/19 01:53
Acenaphthene U 0.00642 0.0333
3
Acenaphthylene U 0.00671 0.0333
Ss
Anthracene U 0.00632 0.0333
Benzidine U 0.0637 0.333 4
Benzo(a)anthracene U 0.00428 0.0333 Cn
Benzo(b)fluoranthene U 0.00695 0.0333
5
Benzo(k)fluoranthene U 0.00582 0.0333
Tr
Benzo(g,h,i)perylene U 0.00721 0.0333
Benzo(a)pyrene U 0.00548 0.0333 6
Bis(2-chlorethoxy)methane U 0.00770 0.333 Sr
Bis(2-chloroethyl)ether U 0.00896 0.333
7
Bis(2-chloroisopropyl)ether U 0.00760 0.333
Qc
4-Bromophenyl-phenylether U 0.0114 0.333
2-Chloronaphthalene U 0.00639 0.0333 8
4-Chlorophenyl-phenylether U 0.00627 0.333 Gl
Chrysene U 0.00555 0.0333
9
Dibenz(a,h)anthracene U 0.00821 0.0333
Al
3,3-Dichlorobenzidine U 0.0794 0.333
2,4-Dinitrotoluene U 0.00607 0.333 10
2,6-Dinitrotoluene U 0.00737 0.333 Sc
Fluoranthene U 0.00496 0.0333
Fluorene U 0.00682 0.0333
Hexachlorobenzene U 0.00856 0.333
Hexachlorocyclopentadiene U 0.0587 0.333
Hexachloroethane U 0.0134 0.333
Indeno(1,2,3-cd)pyrene U 0.00772 0.0333
Isophorone U 0.00522 0.333
Nitrobenzene U 0.00695 0.333
n-Nitrosodimethylamine U 0.0647 0.333
n-Nitrosodiphenylamine U 0.0900 0.333
n-Nitrosodi-n-propylamine U 0.00906 0.333
Phenanthrene U 0.00528 0.0333
Benzylbutyl phthalate U 0.0103 0.333
Bis(2-ethylhexyl)phthalate U 0.0120 0.333
Di-n-butyl phthalate U 0.0109 0.333
Diethyl phthalate U 0.00691 0.333
Dimethyl phthalate U 0.00540 0.333
Di-n-octyl phthalate U 0.00907 0.333

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Method Blank (MB) 1

Cp
(MB) R3388714-3 03/05/19 01:53
Pyrene U 0.0123 0.0333
3
Ss
4-Chloro-3-methylphenol U 0.00477 0.333
2-Chlorophenol U 0.00831 0.333 4
2,4-Dichlorophenol U 0.00746 0.333 Cn
2,4-Dimethylphenol U 0.0471 0.333
5
4,6-Dinitro-2-methylphenol U 0.124 0.333
Tr
2,4-Dinitrophenol U 0.0980 0.333
2-Nitrophenol U 0.0130 0.333 6
4-Nitrophenol U 0.0525 0.333 Sr
Pentachlorophenol U 0.0480 0.333
7
Phenol U 0.00695 0.333
Qc
2,4,6-Trichlorophenol U 0.00779 0.333
(S) Nitrobenzene-d5 68.2 10.0-122 8
(S) 2-Fluorobiphenyl 68.8 15.0-120 Gl
(S) p-Terphenyl-d14 78.1 10.0-120
9
(S) Phenol-d5 73.1 10.0-120
Al
(S) 2-Fluorophenol 86.6 12.0-120
(S) 2,4,6-Tribromophenol 72.7 10.0-127 10
Sc
Method Blank (MB)

(MB) R3390471-1 03/10/19 17:38
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Anthracene U 0.00632 0.0333
Benzidine U 0.0637 0.333
Benzo(a)anthracene U 0.00428 0.0333
Benzo(a)pyrene U 0.00548 0.0333
Bis(2-chlorethoxy)methane U 0.00770 0.333
2-Chloronaphthalene U 0.00639 0.0333

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Method Blank (MB) 1

Cp
(MB) R3390471-1 03/10/19 17:38
4-Chlorophenyl-phenylether U 0.00627 0.333
3
Chrysene U 0.00555 0.0333
Ss
3,3-Dichlorobenzidine U 0.0794 0.333 4
2,4-Dinitrotoluene U 0.00607 0.333 Cn
2,6-Dinitrotoluene U 0.00737 0.333
5
Tr
Fluorene U 0.00682 0.0333
Hexachlorobenzene U 0.00856 0.333 6
Hexachloro-1,3-butadiene U 0.0100 0.333 Sr
7
Qc
Isophorone U 0.00522 0.333 8
Naphthalene U 0.00889 0.0333 Gl
9
Al
n-Nitrosodi-n-propylamine U 0.00906 0.333 10
Phenanthrene U 0.00528 0.0333 Sc
Pyrene U 0.0123 0.0333
2-Chlorophenol U 0.00831 0.333
2,4-Dichlorophenol U 0.00746 0.333
2-Nitrophenol U 0.0130 0.333
Phenol U 0.00695 0.333
(S) Nitrobenzene-d5 79.9 10.0-122

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Method Blank (MB) 1

Cp
(MB) R3390471-1 03/10/19 17:38
(S) 2-Fluorobiphenyl 73.0 15.0-120
3
(S) p-Terphenyl-d14 80.8 10.0-120
Ss
(S) Phenol-d5 75.7 10.0-120
(S) 2-Fluorophenol 82.0 12.0-120 4
(S) 2,4,6-Tribromophenol 57.2 10.0-127 Cn
5
Tr
(LCS) R3388714-1 03/05/19 01:14 • (LCSD) R3388714-2 03/05/19 01:34 6
Sr
7
Acenaphthene 0.666 0.485 0.412 72.8 61.9 38.0-120 16.3 22 Qc
Acenaphthylene 0.666 0.497 0.444 74.6 66.7 40.0-120 11.3 22
Anthracene 0.666 0.495 0.444 74.3 66.7 42.0-120 10.9 20 8
Benzidine 1.33 ND ND 0.000 0.000 1.00-120 J4 J4 0.000 40

Gl
Benzo(a)anthracene 0.666 0.542 0.504 81.4 75.7 44.0-120 7.27 20
9
Benzo(b)fluoranthene 0.666 0.521 0.473 78.2 71.0 43.0-120 9.66 22 Al
Benzo(k)fluoranthene 0.666 0.534 0.486 80.2 73.0 44.0-120 9.41 21
Benzo(g,h,i)perylene 0.666 0.487 0.458 73.1 68.8 43.0-120 6.14 22 10
Benzo(a)pyrene 0.666 0.514 0.479 77.2 71.9 45.0-120 7.05 20

Sc
Bis(2-chlorethoxy)methane 0.666 0.407 0.378 61.1 56.8 20.0-120 7.39 23
Bis(2-chloroethyl)ether 0.666 0.517 0.453 77.6 68.0 16.0-120 13.2 31
Bis(2-chloroisopropyl)ether 0.666 0.418 0.421 62.8 63.2 23.0-120 0.715 30
4-Bromophenyl-phenylether 0.666 0.560 0.491 84.1 73.7 40.0-120 13.1 21
2-Chloronaphthalene 0.666 0.466 0.417 70.0 62.6 35.0-120 11.1 24
4-Chlorophenyl-phenylether 0.666 0.538 0.474 80.8 71.2 40.0-120 12.6 22
Chrysene 0.666 0.491 0.461 73.7 69.2 43.0-120 6.30 20
Dibenz(a,h)anthracene 0.666 0.467 0.444 70.1 66.7 44.0-120 5.05 22
3,3-Dichlorobenzidine 1.33 0.764 0.735 57.4 55.3 28.0-120 3.87 23
2,4-Dinitrotoluene 0.666 0.518 0.461 77.8 69.2 45.0-120 11.6 21
2,6-Dinitrotoluene 0.666 0.500 0.433 75.1 65.0 42.0-120 14.4 21
Fluoranthene 0.666 0.514 0.475 77.2 71.3 44.0-120 7.89 21
Fluorene 0.666 0.507 0.447 76.1 67.1 41.0-120 12.6 22
Hexachlorobenzene 0.666 0.558 0.493 83.8 74.0 39.0-120 12.4 21
Hexachloro-1,3-butadiene 0.666 0.469 0.426 70.4 64.0 15.0-120 9.61 28
Hexachlorocyclopentadiene 0.666 0.497 0.423 74.6 63.5 15.0-120 16.1 31
Hexachloroethane 0.666 0.454 0.407 68.2 61.1 17.0-120 10.9 31
Indeno(1,2,3-cd)pyrene 0.666 0.487 0.456 73.1 68.5 45.0-120 6.57 21
Isophorone 0.666 0.414 0.381 62.2 57.2 23.0-120 8.30 23

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Cp
(LCS) R3388714-1 03/05/19 01:14 • (LCSD) R3388714-2 03/05/19 01:34
Naphthalene 0.666 0.388 0.352 58.3 52.9 18.0-120 9.73 24
3
Nitrobenzene 0.666 0.403 0.385 60.5 57.8 17.0-120 4.57 26
Ss
n-Nitrosodimethylamine 0.666 0.509 0.473 76.4 71.0 10.0-125 7.33 33
n-Nitrosodiphenylamine 0.666 0.489 0.418 73.4 62.8 40.0-120 15.7 21 4
n-Nitrosodi-n-propylamine 0.666 0.484 0.464 72.7 69.7 26.0-120 4.22 27 Cn
Phenanthrene 0.666 0.494 0.447 74.2 67.1 42.0-120 9.99 20
5
Benzylbutyl phthalate 0.666 0.462 0.428 69.4 64.3 40.0-120 7.64 21
Tr
Bis(2-ethylhexyl)phthalate 0.666 0.450 0.421 67.6 63.2 41.0-120 6.66 21
Di-n-butyl phthalate 0.666 0.481 0.440 72.2 66.1 43.0-120 8.90 20 6
Diethyl phthalate 0.666 0.475 0.431 71.3 64.7 43.0-120 9.71 21 Sr
Dimethyl phthalate 0.666 0.487 0.432 73.1 64.9 43.0-120 12.0 22
7
Di-n-octyl phthalate 0.666 0.460 0.426 69.1 64.0 40.0-120 7.67 21
Qc
Pyrene 0.666 0.536 0.478 80.5 71.8 41.0-120 11.4 21
1,2,4-Trichlorobenzene 0.666 0.421 0.402 63.2 60.4 17.0-120 4.62 26 8
4-Chloro-3-methylphenol 0.666 0.443 0.409 66.5 61.4 28.0-120 7.98 20 Gl
2-Chlorophenol 0.666 0.498 0.435 74.8 65.3 28.0-120 13.5 28
9
2,4-Dichlorophenol 0.666 0.464 0.416 69.7 62.5 25.0-120 10.9 21
Al
2,4-Dimethylphenol 0.666 0.418 0.398 62.8 59.8 15.0-120 4.90 26
4,6-Dinitro-2-methylphenol 0.666 0.542 0.526 81.4 79.0 16.0-120 3.00 33 10
2,4-Dinitrophenol 0.666 0.293 0.286 44.0 42.9 10.0-120 2.42 40 Sc
2-Nitrophenol 0.666 0.424 0.402 63.7 60.4 20.0-120 5.33 25
4-Nitrophenol 0.666 0.464 0.445 69.7 66.8 27.0-120 4.18 24
Pentachlorophenol 0.666 0.448 0.386 67.3 58.0 29.0-120 14.9 25
Phenol 0.666 0.525 0.479 78.8 71.9 28.0-120 9.16 27
2,4,6-Trichlorophenol 0.666 0.552 0.478 82.9 71.8 37.0-120 14.4 24
(S) Nitrobenzene-d5 67.9 61.9 10.0-122
(S) 2-Fluorobiphenyl 74.5 64.9 15.0-120
(S) p-Terphenyl-d14 79.0 68.8 10.0-120
(S) Phenol-d5 74.5 64.7 10.0-120
(S) 2-Fluorophenol 85.0 75.2 12.0-120
(S) 2,4,6-Tribromophenol 79.0 66.2 10.0-127
(OS) L1075036-08 03/05/19 07:45 • (MS) R3388714-4 03/05/19 08:05 • (MSD) R3388714-5 03/05/19 08:25
Acenaphthene 0.660 ND 0.554 0.444 83.9 69.6 10 18.0-120 22.0 32
Acenaphthylene 0.660 ND 0.556 0.441 84.2 69.1 10 25.0-120 23.1 32

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Cp
(OS) L1075036-08 03/05/19 07:45 • (MS) R3388714-4 03/05/19 08:05 • (MSD) R3388714-5 03/05/19 08:25
Anthracene 0.660 ND 0.538 0.425 81.5 66.6 10 22.0-120 23.5 29
3
Benzidine 1.32 ND ND ND 0.000 0.000 10 1.00-120 J6 J6 0.000 40
Ss
Benzo(a)anthracene 0.660 ND 0.642 0.568 97.3 89.0 10 25.0-120 12.2 29
Benzo(b)fluoranthene 0.660 ND 0.647 0.540 98.0 84.6 10 19.0-122 18.0 31 4
Benzo(k)fluoranthene 0.660 ND 0.594 0.479 90.0 75.1 10 23.0-120 21.4 30 Cn
Benzo(g,h,i)perylene 0.660 ND 0.570 0.450 86.4 70.5 10 10.0-120 23.5 33
5
Benzo(a)pyrene 0.660 ND 0.615 0.494 93.2 77.4 10 24.0-120 21.8 30
Tr
Bis(2-chlorethoxy)methane 0.660 ND 0.573 0.467 86.8 73.2 10 10.0-120 20.4 34
Bis(2-chloroethyl)ether 0.660 ND 0.645 0.530 97.7 83.1 10 10.0-120 19.6 40 6
Bis(2-chloroisopropyl)ether 0.660 ND 0.641 0.468 97.1 73.4 10 10.0-120 31.2 40 Sr
4-Bromophenyl-phenylether 0.660 ND 0.630 0.504 95.5 79.0 10 27.0-120 22.2 30
7
2-Chloronaphthalene 0.660 ND 0.554 0.410 83.9 64.3 10 20.0-120 29.9 32
Qc
4-Chlorophenyl-phenylether 0.660 ND 0.563 0.453 85.3 71.0 10 24.0-120 21.7 29
Chrysene 0.660 ND 0.562 0.528 85.2 82.8 10 21.0-120 6.24 29 8
Dibenz(a,h)anthracene 0.660 ND 0.520 0.395 78.8 61.9 10 10.0-120 27.3 32 Gl
3,3-Dichlorobenzidine 1.32 ND ND ND 0.000 0.000 10 10.0-120 J6 J6 0.000 34
9
2,4-Dinitrotoluene 0.660 ND 0.590 0.426 89.4 66.8 10 30.0-120 J3 32.3 31
Al
2,6-Dinitrotoluene 0.660 ND 0.551 0.348 83.5 54.5 10 25.0-120 J3 45.2 31
Fluoranthene 0.660 ND 0.626 0.635 94.8 99.5 10 18.0-126 1.43 32 10
Fluorene 0.660 ND 0.604 0.471 91.5 73.8 10 25.0-120 24.7 30 Sc
Hexachlorobenzene 0.660 ND 0.604 0.449 91.5 70.4 10 27.0-120 J3 29.4 28
Hexachloro-1,3-butadiene 0.660 ND 0.758 0.488 115 76.5 10 10.0-120 J3 43.3 38
Hexachlorocyclopentadiene 0.660 ND ND ND 0.000 0.000 10 10.0-120 J6 J6 0.000 40
Hexachloroethane 0.660 ND 0.426 0.256 64.5 40.1 10 10.0-120 J3 49.9 40
Indeno(1,2,3-cd)pyrene 0.660 ND 0.552 0.467 83.6 73.2 10 10.0-120 16.7 32
Isophorone 0.660 ND 0.576 0.491 87.3 77.0 10 13.0-120 15.9 34
Naphthalene 0.660 ND 0.547 0.422 82.9 66.1 10 10.0-120 25.8 35
Nitrobenzene 0.660 ND 0.596 0.493 90.3 77.3 10 10.0-120 18.9 36
n-Nitrosodimethylamine 0.660 ND 0.935 0.662 142 104 10 10.0-127 J5 34.2 40
n-Nitrosodiphenylamine 0.660 ND ND ND 0.000 0.000 10 17.0-120 J6 J6 0.000 29
n-Nitrosodi-n-propylamine 0.660 ND 0.657 0.469 99.5 73.5 10 10.0-120 33.4 37
Phenanthrene 0.660 ND 0.563 0.468 85.3 73.4 10 17.0-120 18.4 31
Benzylbutyl phthalate 0.660 ND 0.534 0.428 80.9 67.1 10 23.0-120 22.0 30
Bis(2-ethylhexyl)phthalate 0.660 ND 0.588 0.492 89.1 77.1 10 17.0-126 17.8 30
Di-n-butyl phthalate 0.660 ND 0.635 0.533 96.2 83.5 10 30.0-120 17.5 29
Diethyl phthalate 0.660 ND 0.713 0.875 108 137 10 26.0-120 J5 20.4 28
Dimethyl phthalate 0.660 ND 0.553 0.439 83.8 68.8 10 25.0-120 23.0 29
Di-n-octyl phthalate 0.660 ND 0.570 0.455 86.4 71.3 10 21.0-123 22.4 29
Pyrene 0.660 ND 0.567 0.562 85.9 88.1 10 16.0-121 0.886 32
1,2,4-Trichlorobenzene 0.660 ND 0.627 0.474 95.0 74.3 10 12.0-120 27.8 37

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Cp
(OS) L1075036-08 03/05/19 07:45 • (MS) R3388714-4 03/05/19 08:05 • (MSD) R3388714-5 03/05/19 08:25
4-Chloro-3-methylphenol 0.660 ND 0.632 0.508 95.8 79.6 10 15.0-120 21.8 30
3
2-Chlorophenol 0.660 ND 0.621 0.461 94.1 72.3 10 15.0-120 29.6 37
Ss
2,4-Dichlorophenol 0.660 ND 0.642 0.509 97.3 79.8 10 20.0-120 23.1 31
2,4-Dimethylphenol 0.660 ND 0.673 0.503 102 78.8 10 10.0-120 28.9 33 4
4,6-Dinitro-2-methylphenol 0.660 ND ND ND 0.000 0.000 10 10.0-120 J6 J6 0.000 39 Cn
2,4-Dinitrophenol 0.660 ND ND ND 0.000 0.000 10 10.0-121 J6 J6 0.000 40
5
2-Nitrophenol 0.660 ND 0.535 0.313 81.1 49.1 10 12.0-120 J3 52.4 39
Tr
4-Nitrophenol 0.660 ND 0.537 0.527 81.4 82.6 10 10.0-137 1.88 32
Pentachlorophenol 0.660 ND 0.562 ND 85.2 0.000 10 10.0-160 J3 J6 200 31 6
Phenol 0.660 ND 0.636 0.539 96.4 84.5 10 12.0-120 16.5 38 Sr
2,4,6-Trichlorophenol 0.660 ND 0.637 0.518 96.5 81.2 10 19.0-120 20.6 32
7
(S) Nitrobenzene-d5 108 82.4 10.0-122
Qc
(S) p-Terphenyl-d14 87.3 77.7 10.0-120 8
(S) Phenol-d5 95.5 75.2 10.0-120 Gl
(S) 2-Fluorophenol 102 79.6 12.0-120
9
Al
Sample Narrative: 10
OS: Dilution due to matrix impact during extract concentration procedure Sc

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Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1075168-14,15,16,17,18,19
Method Blank (MB) 1

Cp
(MB) R3389408-3 03/07/19 01:39
3
Ss
Anthracene U 0.000291 0.00100
Benzidine U 0.00432 0.0100 4
5
Tr
Benzo(a)pyrene U 0.000340 0.00100 6
7
Qc
Chrysene U 0.000332 0.00100
9
Al
Fluorene U 0.000323 0.00100
Isophorone U 0.000272 0.0100

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Method Blank (MB) 1

Cp
(MB) R3389408-3 03/07/19 01:39
Pyrene U 0.000330 0.00100
3
Ss
2-Chlorophenol U 0.000283 0.0100 4
2,4-Dichlorophenol U 0.000284 0.0100 Cn
5
Tr
2-Nitrophenol U 0.000320 0.0100 6
4-Nitrophenol U 0.00201 0.0100 Sr
7
Phenol U 0.000334 0.0100
Qc
(S) p-Terphenyl-d14 67.3 10.0-128
9
(S) Phenol-d5 25.8 10.0-120
Al
Sc

(LCS) R3389408-1 03/07/19 00:52 • (LCSD) R3389408-2 03/07/19 01:16
Acenaphthene 0.0500 0.0353 0.0368 70.6 73.6 41.0-120 4.16 22
Acenaphthylene 0.0500 0.0365 0.0373 73.0 74.6 43.0-120 2.17 22
Anthracene 0.0500 0.0356 0.0360 71.2 72.0 45.0-120 1.12 20
Benzidine 0.100 0.0680 0.0336 68.0 33.6 1.00-120 J3 67.7 36
Benzo(b)fluoranthene 0.0500 0.0353 0.0383 70.6 76.6 46.0-120 8.15 20
Benzo(g,h,i)perylene 0.0500 0.0376 0.0407 75.2 81.4 48.0-121 7.92 20
Benzo(a)pyrene 0.0500 0.0356 0.0379 71.2 75.8 47.0-120 6.26 20

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Cp
(LCS) R3389408-1 03/07/19 00:52 • (LCSD) R3389408-2 03/07/19 01:16
3
Chrysene 0.0500 0.0349 0.0368 69.8 73.6 48.0-120 5.30 20
Ss
3,3-Dichlorobenzidine 0.100 0.0748 0.0791 74.8 79.1 44.0-120 5.59 20 4
2,4-Dinitrotoluene 0.0500 0.0401 0.0418 80.2 83.6 49.0-124 4.15 20 Cn
2,6-Dinitrotoluene 0.0500 0.0370 0.0389 74.0 77.8 46.0-120 5.01 21
5
Fluoranthene 0.0500 0.0378 0.0394 75.6 78.8 51.0-120 4.15 20
Tr
Fluorene 0.0500 0.0376 0.0384 75.2 76.8 47.0-120 2.11 20
Hexachlorobenzene 0.0500 0.0374 0.0385 74.8 77.0 44.0-120 2.90 20 6
Hexachloro-1,3-butadiene 0.0500 0.0304 0.0286 60.8 57.2 19.0-120 6.10 32 Sr
7
Qc
Indeno(1,2,3-cd)pyrene 0.0500 0.0382 0.0409 76.4 81.8 49.0-122 6.83 20
Isophorone 0.0500 0.0327 0.0335 65.4 67.0 36.0-120 2.42 23 8
Naphthalene 0.0500 0.0296 0.0293 59.2 58.6 27.0-120 1.02 27 Gl
Nitrobenzene 0.0500 0.0319 0.0329 63.8 65.8 27.0-120 3.09 29
9
Al
n-Nitrosodiphenylamine 0.0500 0.0350 0.0357 70.0 71.4 47.0-120 1.98 20
n-Nitrosodi-n-propylamine 0.0500 0.0369 0.0364 73.8 72.8 31.0-120 1.36 28 10
Phenanthrene 0.0500 0.0347 0.0361 69.4 72.2 46.0-120 3.95 20 Sc
Di-n-butyl phthalate 0.0500 0.0383 0.0403 76.6 80.6 49.0-121 5.09 20
Diethyl phthalate 0.0500 0.0401 0.0418 80.2 83.6 48.0-122 4.15 20
Pyrene 0.0500 0.0348 0.0363 69.6 72.6 47.0-120 4.22 20
1,2,4-Trichlorobenzene 0.0500 0.0285 0.0277 57.0 55.4 24.0-120 2.85 29
4-Chloro-3-methylphenol 0.0500 0.0340 0.0351 68.0 70.2 40.0-120 3.18 21
2-Chlorophenol 0.0500 0.0347 0.0341 69.4 68.2 25.0-120 1.74 35
2,4-Dichlorophenol 0.0500 0.0347 0.0353 69.4 70.6 36.0-120 1.71 26
2,4-Dimethylphenol 0.0500 0.0337 0.0339 67.4 67.8 33.0-120 0.592 26
4,6-Dinitro-2-methylphenol 0.0500 0.0330 0.0371 66.0 74.2 38.0-138 11.7 25
2,4-Dinitrophenol 0.0500 0.0177 0.0214 35.4 42.8 10.0-120 18.9 39
2-Nitrophenol 0.0500 0.0369 0.0377 73.8 75.4 31.0-120 2.14 29
4-Nitrophenol 0.0500 0.0149 0.0161 29.8 32.2 10.0-120 7.74 33
Pentachlorophenol 0.0500 0.0189 0.0229 37.8 45.8 23.0-120 19.1 25
Phenol 0.0500 0.0148 0.0145 29.6 29.0 10.0-120 2.05 36
(S) Nitrobenzene-d5 61.7 61.0 10.0-127

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16:10 147 of 161

Cp
(LCS) R3389408-1 03/07/19 00:52 • (LCSD) R3389408-2 03/07/19 01:16
3
(S) p-Terphenyl-d14 68.3 73.1 10.0-128
Ss
(S) Phenol-d5 27.0 26.2 10.0-120
(S) 2-Fluorophenol 46.6 44.8 10.0-120 4
(S) 2,4,6-Tribromophenol 74.0 76.5 10.0-155 Cn
5
Tr
(OS) L1074326-01 03/07/19 02:03 • (MS) R3389408-4 03/07/19 02:27 • (MSD) R3389408-5 03/07/19 02:51 6
Sr
7
Naphthalene 0.0500 U 0.0313 0.0314 62.6 62.8 1 10.0-120 0.319 31 Qc
Acenaphthene 0.0500 U 0.0357 0.0366 71.4 73.2 1 28.0-120 2.49 25
Acenaphthylene 0.0500 U 0.0370 0.0380 74.0 76.0 1 31.0-121 2.67 25 8
Anthracene 0.0500 U 0.0350 0.0354 70.0 70.8 1 36.0-120 1.14 23

Gl
Benzidine 0.100 U 0.0178 0.0124 17.8 12.4 1 1.00-120 35.8 37
9
Benzo(a)anthracene 0.0500 U 0.0393 0.0399 78.6 79.8 1 39.0-120 1.52 23 Al
Benzo(b)fluoranthene 0.0500 U 0.0359 0.0366 71.8 73.2 1 37.0-120 1.93 23
Benzo(k)fluoranthene 0.0500 U 0.0346 0.0349 69.2 69.8 1 37.0-120 0.863 26 10
Benzo(g,h,i)perylene 0.0500 U 0.0388 0.0391 77.6 78.2 1 37.0-123 0.770 25

Sc
Benzo(a)pyrene 0.0500 U 0.0352 0.0361 70.4 72.2 1 37.0-120 2.52 24
Bis(2-chlorethoxy)methane 0.0500 U 0.0311 0.0311 62.2 62.2 1 17.0-120 0.000 31
Bis(2-chloroethyl)ether 0.0500 U 0.0330 0.0334 66.0 66.8 1 14.0-120 1.20 33
Bis(2-chloroisopropyl)ether 0.0500 U 0.0329 0.0341 65.8 68.2 1 18.0-120 3.58 34
4-Bromophenyl-phenylether 0.0500 U 0.0367 0.0378 73.4 75.6 1 37.0-120 2.95 24
2-Chloronaphthalene 0.0500 U 0.0336 0.0344 67.2 68.8 1 29.0-120 2.35 28
4-Chlorophenyl-phenylether 0.0500 U 0.0373 0.0391 74.6 78.2 1 36.0-120 4.71 23
Chrysene 0.0500 U 0.0346 0.0349 69.2 69.8 1 38.0-120 0.863 23
Dibenz(a,h)anthracene 0.0500 U 0.0379 0.0388 75.8 77.6 1 36.0-121 2.35 24
3,3-Dichlorobenzidine 0.100 U 0.0531 0.0539 53.1 53.9 1 10.0-134 1.50 30
2,4-Dinitrotoluene 0.0500 U 0.0405 0.0411 81.0 82.2 1 39.0-125 1.47 25
Fluoranthene 0.0500 U 0.0372 0.0374 74.4 74.8 1 41.0-121 0.536 22
Fluorene 0.0500 U 0.0376 0.0388 75.2 77.6 1 37.0-120 3.14 24
Hexachlorobenzene 0.0500 U 0.0366 0.0388 73.2 77.6 1 35.0-122 5.84 24
Hexachloro-1,3-butadiene 0.0500 U 0.0357 0.0364 71.4 72.8 1 12.0-120 1.94 34
Hexachlorocyclopentadiene 0.0500 U 0.0332 0.0339 66.4 67.8 1 10.0-120 2.09 33
Hexachloroethane 0.0500 U 0.0328 0.0334 65.6 66.8 1 10.0-120 1.81 40
Indeno(1,2,3-cd)pyrene 0.0500 U 0.0385 0.0391 77.0 78.2 1 38.0-125 1.55 24

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Cp
(OS) L1074326-01 03/07/19 02:03 • (MS) R3389408-4 03/07/19 02:27 • (MSD) R3389408-5 03/07/19 02:51
Isophorone 0.0500 U 0.0336 0.0337 67.2 67.4 1 21.0-120 0.297 27
3
Nitrobenzene 0.0500 U 0.0325 0.0329 65.0 65.8 1 12.0-120 1.22 30
Ss
n-Nitrosodimethylamine 0.0500 U 0.0204 0.0203 40.8 40.6 1 10.0-120 0.491 40
n-Nitrosodiphenylamine 0.0500 U 0.0344 0.0356 68.8 71.2 1 37.0-120 3.43 24 4
n-Nitrosodi-n-propylamine 0.0500 U 0.0362 0.0368 72.4 73.6 1 16.0-120 1.64 30 Cn
Phenanthrene 0.0500 U 0.0348 0.0350 69.6 70.0 1 33.0-120 0.573 22
5
Benzylbutyl phthalate 0.0500 U 0.0368 0.0373 73.6 74.6 1 34.0-126 1.35 24
Tr
Bis(2-ethylhexyl)phthalate 0.0500 U 0.0376 0.0384 75.2 76.8 1 33.0-126 2.11 25
Di-n-butyl phthalate 0.0500 U 0.0384 0.0388 76.8 77.6 1 35.0-128 1.04 23 6
Diethyl phthalate 0.0500 U 0.0402 0.0413 80.4 82.6 1 39.0-125 2.70 24 Sr
Dimethyl phthalate 0.0500 U 0.0375 0.0384 75.0 76.8 1 37.0-120 2.37 24
7
Di-n-octyl phthalate 0.0500 U 0.0394 0.0398 78.8 79.6 1 25.0-135 1.01 26
Qc
Pyrene 0.0500 U 0.0347 0.0346 69.4 69.2 1 39.0-120 0.289 22
1,2,4-Trichlorobenzene 0.0500 U 0.0313 0.0320 62.6 64.0 1 15.0-120 2.21 31 8
4-Chloro-3-methylphenol 0.0500 U 0.0291 0.0295 58.2 59.0 1 26.0-120 1.37 27 Gl
2-Chlorophenol 0.0500 U 0.0256 0.0256 51.2 51.2 1 18.0-120 0.000 34
9
2,4-Dichlorophenol 0.0500 U 0.0301 0.0312 60.2 62.4 1 19.0-120 3.59 27
Al
2,4-Dimethylphenol 0.0500 U 0.0292 0.0295 58.4 59.0 1 15.0-120 1.02 28
4,6-Dinitro-2-methylphenol 0.0500 U 0.0358 0.0372 71.6 74.4 1 10.0-144 3.84 39 10
2,4-Dinitrophenol 0.0500 U 0.0304 0.0341 60.8 68.2 1 10.0-120 11.5 40 Sc
2-Nitrophenol 0.0500 U 0.0334 0.0347 66.8 69.4 1 20.0-120 3.82 30
4-Nitrophenol 0.0500 U 0.00911 0.00960 18.2 19.2 1 10.0-120 5.24 40
Pentachlorophenol 0.0500 0.00227 0.0322 0.0323 59.9 60.1 1 10.0-128 0.310 37
Phenol 0.0500 U 0.00818 0.00865 16.4 17.3 1 10.0-120 5.59 40
2,4,6-Trichlorophenol 0.0500 U 0.0354 0.0372 70.8 74.4 1 26.0-120 4.96 31
(S) Nitrobenzene-d5 64.8 65.1 10.0-127
(S) p-Terphenyl-d14 70.3 70.7 10.0-128
(S) Phenol-d5 25.1 25.7 10.0-120
(S) 2-Fluorophenol 43.8 42.6 10.0-120

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Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1075168-03,12,13
Method Blank (MB) 1

Cp
(MB) R3389682-3 03/07/19 15:27
3
Ss
Anthracene U 0.000291 0.00100
Benzidine U 0.00432 0.0100 4
5
Tr
Benzo(a)pyrene U 0.000340 0.00100 6
7
Qc
Chrysene U 0.000332 0.00100
9
Al
Fluorene U 0.000323 0.00100
Isophorone U 0.000272 0.0100

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Method Blank (MB) 1

Cp
(MB) R3389682-3 03/07/19 15:27
Pyrene U 0.000330 0.00100
3
Ss
2-Chlorophenol U 0.000283 0.0100 4
2-Nitrophenol U 0.000320 0.0100 Cn
5
Tr
Phenol U 0.000334 0.0100
2,4,6-Trichlorophenol U 0.000297 0.0100 6
2,4-Dichlorophenol U 0.000284 0.0100 Sr
7
Qc
(S) p-Terphenyl-d14 73.6 10.0-128
9
(S) Phenol-d5 28.1 10.0-120
Al
Sc

(LCS) R3389682-1 03/07/19 14:40 • (LCSD) R3389682-2 03/07/19 15:04
Acenaphthene 0.0500 0.0346 0.0324 69.2 64.8 41.0-120 6.57 22
Acenaphthylene 0.0500 0.0355 0.0332 71.0 66.4 43.0-120 6.70 22
Anthracene 0.0500 0.0373 0.0358 74.6 71.6 45.0-120 4.10 20
Benzidine 0.100 0.0229 0.0218 22.9 21.8 1.00-120 4.92 36
Benzo(b)fluoranthene 0.0500 0.0399 0.0374 79.8 74.8 46.0-120 6.47 20
Benzo(g,h,i)perylene 0.0500 0.0416 0.0393 83.2 78.6 48.0-121 5.69 20
Benzo(a)pyrene 0.0500 0.0389 0.0369 77.8 73.8 47.0-120 5.28 20

03/13/19 15:42
16:10 151 of 161

Cp
(LCS) R3389682-1 03/07/19 14:40 • (LCSD) R3389682-2 03/07/19 15:04
3
Chrysene 0.0500 0.0362 0.0352 72.4 70.4 48.0-120 2.80 20
Ss
3,3-Dichlorobenzidine 0.100 0.0747 0.0711 74.7 71.1 44.0-120 4.94 20 4
2,4-Dinitrotoluene 0.0500 0.0383 0.0361 76.6 72.2 49.0-124 5.91 20 Cn
2,6-Dinitrotoluene 0.0500 0.0371 0.0346 74.2 69.2 46.0-120 6.97 21
5
Fluoranthene 0.0500 0.0373 0.0352 74.6 70.4 51.0-120 5.79 20
Tr
Fluorene 0.0500 0.0364 0.0344 72.8 68.8 47.0-120 5.65 20
Hexachlorobenzene 0.0500 0.0399 0.0380 79.8 76.0 44.0-120 4.88 20 6
Hexachloro-1,3-butadiene 0.0500 0.0318 0.0304 63.6 60.8 19.0-120 4.50 32 Sr
7
Qc
Indeno(1,2,3-cd)pyrene 0.0500 0.0418 0.0387 83.6 77.4 49.0-122 7.70 20
Isophorone 0.0500 0.0305 0.0294 61.0 58.8 36.0-120 3.67 23 8
Naphthalene 0.0500 0.0304 0.0292 60.8 58.4 27.0-120 4.03 27 Gl
Nitrobenzene 0.0500 0.0294 0.0280 58.8 56.0 27.0-120 4.88 29
9
Al
n-Nitrosodiphenylamine 0.0500 0.0385 0.0368 77.0 73.6 47.0-120 4.52 20
n-Nitrosodi-n-propylamine 0.0500 0.0308 0.0295 61.6 59.0 31.0-120 4.31 28 10
Phenanthrene 0.0500 0.0379 0.0361 75.8 72.2 46.0-120 4.86 20 Sc
Di-n-butyl phthalate 0.0500 0.0376 0.0353 75.2 70.6 49.0-121 6.31 20
Diethyl phthalate 0.0500 0.0372 0.0349 74.4 69.8 48.0-122 6.38 20
Pyrene 0.0500 0.0383 0.0365 76.6 73.0 47.0-120 4.81 20
1,2,4-Trichlorobenzene 0.0500 0.0305 0.0294 61.0 58.8 24.0-120 3.67 29
4-Chloro-3-methylphenol 0.0500 0.0330 0.0320 66.0 64.0 40.0-120 3.08 21
2-Chlorophenol 0.0500 0.0333 0.0320 66.6 64.0 25.0-120 3.98 35
2,4-Dichlorophenol 0.0500 0.0345 0.0322 69.0 64.4 36.0-120 6.90 26
2,4-Dimethylphenol 0.0500 0.0320 0.0312 64.0 62.4 33.0-120 2.53 26
4,6-Dinitro-2-methylphenol 0.0500 0.0483 0.0399 96.6 79.8 38.0-138 19.0 25
2,4-Dinitrophenol 0.0500 0.0280 0.0207 56.0 41.4 10.0-120 30.0 39
2-Nitrophenol 0.0500 0.0361 0.0345 72.2 69.0 31.0-120 4.53 29
4-Nitrophenol 0.0500 0.0177 0.0167 35.4 33.4 10.0-120 5.81 33
Pentachlorophenol 0.0500 0.0333 0.0254 66.6 50.8 23.0-120 J3 26.9 25
Phenol 0.0500 0.0157 0.0153 31.4 30.6 10.0-120 2.58 36
(S) Nitrobenzene-d5 58.4 55.5 10.0-127

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Cp
(LCS) R3389682-1 03/07/19 14:40 • (LCSD) R3389682-2 03/07/19 15:04
3
(S) p-Terphenyl-d14 73.4 68.1 10.0-128
Ss
(S) Phenol-d5 28.5 27.8 10.0-120
(S) 2-Fluorophenol 45.5 43.4 10.0-120 4
(S) 2,4,6-Tribromophenol 77.0 72.5 10.0-155 Cn
5
Tr
(OS) L1075329-01 03/07/19 17:26 • (MS) R3389682-4 03/07/19 17:50 • (MSD) R3389682-5 03/07/19 18:14 6
Sr
7
Acenaphthene 0.0500 U 0.0314 0.0319 62.8 63.8 1 28.0-120 1.58 25 Qc
Acenaphthylene 0.0500 U 0.0320 0.0321 64.0 64.2 1 31.0-121 0.312 25
Anthracene 0.0500 U 0.0337 0.0334 67.4 66.8 1 36.0-120 0.894 23 8
Benzidine 0.100 U ND ND 0.000 0.000 1 1.00-120 J6 J6 0.000 37

Gl
Benzo(a)anthracene 0.0500 U 0.0380 0.0381 76.0 76.2 1 39.0-120 0.263 23
9
Benzo(b)fluoranthene 0.0500 U 0.0369 0.0373 73.8 74.6 1 37.0-120 1.08 23 Al
Benzo(k)fluoranthene 0.0500 U 0.0366 0.0365 73.2 73.0 1 37.0-120 0.274 26
Benzo(g,h,i)perylene 0.0500 U 0.0382 0.0382 76.4 76.4 1 37.0-123 0.000 25 10
Benzo(a)pyrene 0.0500 U 0.0360 0.0348 72.0 69.6 1 37.0-120 3.39 24

Sc
Bis(2-chlorethoxy)methane 0.0500 U 0.0280 0.0273 56.0 54.6 1 17.0-120 2.53 31
Bis(2-chloroethyl)ether 0.0500 U 0.0265 0.0252 53.0 50.4 1 14.0-120 5.03 33
Bis(2-chloroisopropyl)ether 0.0500 U 0.0271 0.0254 54.2 50.8 1 18.0-120 6.48 34
4-Bromophenyl-phenylether 0.0500 U 0.0361 0.0368 72.2 73.6 1 37.0-120 1.92 24
2-Chloronaphthalene 0.0500 U 0.0298 0.0303 59.6 60.6 1 29.0-120 1.66 28
4-Chlorophenyl-phenylether 0.0500 U 0.0339 0.0346 67.8 69.2 1 36.0-120 2.04 23
Chrysene 0.0500 U 0.0337 0.0344 67.4 68.8 1 38.0-120 2.06 23
Dibenz(a,h)anthracene 0.0500 U 0.0375 0.0377 75.0 75.4 1 36.0-121 0.532 24
3,3-Dichlorobenzidine 0.100 U 0.0432 0.0196 43.2 19.6 1 10.0-134 J3 75.2 30
Fluoranthene 0.0500 U 0.0352 0.0356 70.4 71.2 1 41.0-121 1.13 22
Fluorene 0.0500 U 0.0338 0.0349 67.6 69.8 1 37.0-120 3.20 24
Hexachlorobenzene 0.0500 U 0.0358 0.0372 71.6 74.4 1 35.0-122 3.84 24
Hexachloro-1,3-butadiene 0.0500 U 0.0247 0.0215 49.4 43.0 1 12.0-120 13.9 34
Hexachlorocyclopentadiene 0.0500 U 0.0268 0.0233 53.6 46.6 1 10.0-120 14.0 33
Hexachloroethane 0.0500 U 0.0218 0.0182 43.6 36.4 1 10.0-120 18.0 40
Indeno(1,2,3-cd)pyrene 0.0500 U 0.0379 0.0382 75.8 76.4 1 38.0-125 0.788 24
Isophorone 0.0500 U 0.0284 0.0284 56.8 56.8 1 21.0-120 0.000 27

03/13/19 15:42
16:10 153 of 161
Cp
(OS) L1075329-01 03/07/19 17:26 • (MS) R3389682-4 03/07/19 17:50 • (MSD) R3389682-5 03/07/19 18:14
Naphthalene 0.0500 U 0.0264 0.0241 52.8 48.2 1 10.0-120 9.11 31
3
Nitrobenzene 0.0500 U 0.0283 0.0266 56.6 53.2 1 12.0-120 6.19 30
Ss
n-Nitrosodimethylamine 0.0500 U 0.0200 0.0216 40.0 43.2 1 10.0-120 7.69 40
n-Nitrosodiphenylamine 0.0500 U 0.0342 0.0334 68.4 66.8 1 37.0-120 2.37 24 4
n-Nitrosodi-n-propylamine 0.0500 U 0.0277 0.0283 55.4 56.6 1 16.0-120 2.14 30 Cn
Phenanthrene 0.0500 U 0.0346 0.0354 69.2 70.8 1 33.0-120 2.29 22
5
Benzylbutyl phthalate 0.0500 U 0.0352 0.0365 70.4 73.0 1 34.0-126 3.63 24
Tr
Bis(2-ethylhexyl)phthalate 0.0500 U 0.0333 0.0338 66.6 67.6 1 33.0-126 1.49 25
Di-n-butyl phthalate 0.0500 U 0.0352 0.0364 70.4 72.8 1 35.0-128 3.35 23 6
Diethyl phthalate 0.0500 U 0.0347 0.0359 69.4 71.8 1 39.0-125 3.40 24 Sr
Dimethyl phthalate 0.0500 U 0.0346 0.0360 69.2 72.0 1 37.0-120 3.97 24
7
Di-n-octyl phthalate 0.0500 0.000294 0.0358 0.0362 71.0 71.8 1 25.0-135 1.11 26
Qc
Pyrene 0.0500 U 0.0350 0.0355 70.0 71.0 1 39.0-120 1.42 22
1,2,4-Trichlorobenzene 0.0500 U 0.0248 0.0224 49.6 44.8 1 15.0-120 10.2 31 8
4-Chloro-3-methylphenol 0.0500 U 0.0322 0.0315 64.4 63.0 1 26.0-120 2.20 27 Gl
2-Chlorophenol 0.0500 U 0.0277 0.0260 55.4 52.0 1 18.0-120 6.33 34
9
2,4-Dichlorophenol 0.0500 U 0.0316 0.0294 63.2 58.8 1 19.0-120 7.21 27
Al
2,4-Dimethylphenol 0.0500 U 0.0290 0.0184 58.0 36.8 1 15.0-120 J3 44.7 28
4,6-Dinitro-2-methylphenol 0.0500 U 0.0506 0.0554 101 111 1 10.0-144 9.06 39 10
2,4-Dinitrophenol 0.0500 U 0.0472 0.0523 94.4 105 1 10.0-120 10.3 40 Sc
2-Nitrophenol 0.0500 U 0.0341 0.0324 68.2 64.8 1 20.0-120 5.11 30
4-Nitrophenol 0.0500 U 0.0194 0.0219 38.8 43.8 1 10.0-120 12.1 40
Pentachlorophenol 0.0500 0.00691 0.0406 0.0445 67.4 75.2 1 10.0-128 9.17 37
Phenol 0.0500 U 0.0138 0.0141 27.6 28.2 1 10.0-120 2.15 40
2,4,6-Trichlorophenol 0.0500 U 0.0378 0.0388 75.6 77.6 1 26.0-120 2.61 31
(S) Nitrobenzene-d5 52.3 48.3 10.0-127
(S) p-Terphenyl-d14 67.2 67.9 10.0-128
(S) Phenol-d5 25.9 26.5 10.0-120
(S) 2-Fluorophenol 38.9 38.6 10.0-120

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GLOSSARY OF TERMS ONE LAB. NATIONWIDE.
Guide to Reading and Understanding Your Laboratory Report 1
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
Cp
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
2
Abbreviations and Definitions Tc
(dry) Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
3
MDL Method Detection Limit. Ss
MQL (dry) Method Quantitation Limit.
MQL Method Quantitation Limit. 4
ND Not detected at the Method Quantitation Limit. Cn
RDL Reported Detection Limit.
5
Rec. Recovery. Tr
RPD Relative Percent Difference.
SDG Sample Delivery Group. 6
SDL Sample Detection Limit. Sr
SDL (dry) Sample Detection Limit.
7
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Qc
(S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Sample Detection Limit. 8
Gl
Unadj. MQL Unadjusted Method Quantitation Limit.
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
Analyte 9
reported. Al
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
Dilution 10
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor. Sc
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
Original Sample sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty Confidence level of 2 sigma.
(Radiochemistry)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Quality Control analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
Summary (Qc) being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
Sample Summary (Ss) times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J1 Surrogate recovery limits have been exceeded; values are outside upper control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.

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GLOSSARY OF TERMS ONE LAB. NATIONWIDE.
Qualifier Description 1
T8 Sample(s) received past/too close to holding time expiration.

Cp
V The sample concentration is too high to evaluate accurate spike recoveries.
2
Tc
3
Ss
4
Cn
5
Tr
6
Sr
7
Qc
8
Gl
9
Al
10
Sc

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ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network 1
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing Cp
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. 2
Tc
State Accreditations
3
Alabama 40660 Nebraska NE-OS-15-05 Ss
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
4
Arkansas 88-0469 New Jersey–NELAP TN002 Cn
California 2932 New Mexico ¹ n/a
Colorado TN00003 New York 11742
5
Connecticut PH-0197 North Carolina Env375 Tr
Florida E87487 North Carolina ¹ DW21704
Georgia NELAP North Carolina ³ 41
6
Georgia ¹ 923 North Dakota R-140 Sr
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
7
Indiana C-TN-01 Oregon TN200002 Qc
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
8
Kentucky ¹ ⁶ 90010 South Carolina 84004 Gl
Kentucky ² 16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴ 2006
9
Louisiana ¹ LA180010 Texas T104704245-18-15 Al
Maine TN0002 Texas ⁵ LAB0152
Maryland 324 Utah TN00003
10
Massachusetts M-TN003 Vermont VT2006 Sc
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA
Third Party Federal Accreditations

A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵ 1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.

03/13/19 15:42
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ANALYTICAL REPORT

March 13, 2019

Report To: Brian Mann

Entire Report Reviewed By:

12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com

Cp: Cover Page 1 1

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

Wet Chemistry by Method 9050AMod 104 1

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Laboratory Name: Pace Analytical National LRC Date: 03/13/2019 16:10

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