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The Effect of Predeformation Level on the

Variability of Forming Properties of Low Carbon


Steel
S.E. Oraby, Member, IAENG and A.M. Alaskari

of metals can be enhanced by various ways such as by alloying


Abstract—In forming processes, metal is usually subjected to [1]-[5], heat treatment [6]-[11], or mechanical deformation
multi-stages deformation. In order to process one stage [12]-[16]. Practically, the mechanical properties of low
effectively, actual information in term of mechanical and forming carbon steel can be probably improved during forming in term
properties of the preceding stage should be available to start with.
of increased strength and hardness. This is usually achieved on
It has long been assumed by those interested in forming processes
that the forming properties (behaviors) remain constant the account of lowering its ductility within the feasible usage
regardless the number of involved deformation stages. The domain. However, to reach efficient and accurate practical
validation of such an assumption is investigated in the current conditions under which material performs, a qualitative
study for low carbon steel. It has shown that the claim of forming judgment should be available. This is an essential requirement
parameters constancy is valid only within a limited domain of when common multi-stages forming process is involved since
strain rate between 0.05 and 0.1. Outside this region, different
at the beginning of any stage, relevant information regarding
behavior of forming parameter is noticed and, a compensatory
action should be considered. Mathematical formulation of the the current properties status is usually utilized in the
experimental data has led to the establishment of many functional preparation and the design of any subsequent deformation
empirical relations by which a correction factor is determined. stage. Although the mechanical properties of the deformed
Better understanding of the problem is shown via the qualitative material can be retrained by further heat treatment, this is not
response surface approach including the 3-D representation and usually the best approach since it adds to the cost and the time
quantitative contouring plots. Also, interrelationships are
of the manufacturing process.
empirically developed between the mechanical properties (yield
strength, ultimate tensile strength; and area reduction) and the Depending on the type of forming process, formability maybe
forming properties (strain hardening exponent and strength defined as the ability of the material to deform under specific
coefficient). load, from its original configuration to a defined final shape
without reaching failure. Buckling, necking, fracturing or their
Index Terms-Predeformation, Forming properties, Mechanical combination usually limits forming or deformation process
properties, Low carbon steel, Mathematical modeling. [17]. Buckling is a result of compressive loading; while
necking is a result of tensile loading under uniform flow that
transforms to local flow. In many sheet forming and tube
I. INTRODUCTION
forming processes, the deformation is usually characterized by
Carbon steels, by far, are the most common material to be used biaxial stretching. Failure in stretching operations normally
in industrial and manufacturing plants especially when forming occurs by a sharp localized necking on the surface.
processes are intended. The higher formability of low carbon The current study is an approach to investigate the possible
steel is due to its high ductility that is usually accompanied with variation involved in the forming properties of low carbon steel
moderate strength and hardness. This usually justifies the as it is affected by subsequent predeformation process.
increasing demands to conduct an elaborated investigation to Statistical and formulation procedures are applied to the
shed more light on the possible in-process variability that may experimental data in order to accurately quantify and assess the
exist in the normal mechanical properties of the material during emerged interrelationship.
multi stages deformation process. The mechanical properties

Manuscript received December 11, 2006. This research was supported by a II. THEORETICAL ANALYSIS
contract grant (TS-05-001) from the Public Authority of Applied Education and
Training (PAAET), Kuwait.
S. E. Oraby is with the College of technological Studies, PAAET, P.O. Box Deformation may be classified as elastic, elastic-plastic, and
42325 Shuwaikh 70654 Kuwait (phone: +965 9549019; fax: +965 4832761; plastic. Figure 1 shows a typical stress-strain curve for tensile
e-mail: soraby@paaet.edu.kw).
A. M. Alaskari is with the College of technological Studies, PAAET, P.O. test. Additionally, there are also superplastic forming used in
Box 42325 Shuwaikh 70654 Kuwait (phone: +965 2314856; fax: +965 advance industries, such as aerospace and automotive
4832761; e-mail: aalaskari@gmail.com). industries, for sheet metals [8], [18]. When increasing load is
applied gradually to a piece of ductile metal, it will deform length and radius at shoulder respectively.
elastically at first. As load is increased to a certain level, the
metal is then deformed permanently and uniformly until
ultimate tensile strength, then non- uniformly until fracture.
Elastic deformation is recoverable and it vanishes as the
applied load is removed usually causing spring back in cold
forming. The elastic-plastic and plastic are permanent
deformations and irreversible forming process. A perfectly
plastic material is one that does not work-harden or
strain-harden, yet ductile materials show some work hardening
by cold working.
In metal forming, elastic-plastic zone should be considered
since the ductile metal is often uniformly deformed at that
region retaining a high portion of its strain under the applied
load. When metals are plastically deformed beyond the yield
point, and at temperatures below the recrystallization, they are
said to be cold worked. In addition to the accompanied shape
change due to deformation, strength and hardness usually
increase. Work hardening and strain hardening terms are Fig. 1 Typical stress-strain curve for tensile test
referring to such increase by cold working. Consequently, this
strengthening mechanism reduces the ductility of the metals.
Most materials show strain hardening behavior by cold work,
which can be expressed by the conventional equation as:

σcon= K(εo +εa )n, (1)

where ε0 is the effective strain prior to cold working, εa is the


effective strain due subsequent plastic deformation, σ is the
effective stress, n is the strain hardening exponent and K is the
strength coefficient. Both K and n are thought to be the material
constants that are free of predeformation (ε0 = 0). Yet in this
paper, K and n are investigated for variability of the
predeformation length of the specimen. This leads to the
currently proposed more precise equation of the true stress as
follows:
Fig. 2 Experimental setup and data acquisition system
n
σ exp = K .ε , (2)
A moderate capacity Hoytom Di-10-Cp/MH 1491
considering K and n are essentially predeformation dependent. universal tensile testing machine is used. As shown in Fig. 2,
Although there are many testing techniques to evaluate work specimen is held between upper and lower grippers while load
hardening behavior such as direct compression, torsion, is induced gradually. Data are digitally in-process transferred
balanced biaxial or bulged testing, and plain-strain to PC using compatible Hoytom software. Typical output is
compression, tensile test is considered the most common shown in Fig. 3-a.
destructive technique due to its simplicity and ability to
generate sufficient information regarding mechanical
properties of the tested piece. IV. DATA ANALYSIS AND FORMULATION

III. EXPERIMENTAL PROCEDURE AND SETUP Testing procedures are designed to include four levels of
predeformation: 8, 12, 16, and 20 mm in addition to the original
Due to its wide utilization in many engineering applications (no predeformation) case. For each level, the specimen is first
and due to its economical feasibility, low carbon steel is predeformed to the specified elongation level and then the load
selected for the current study. Common chemical composition is removed. The predeformed specimen is then tested in the
of the employed low carbon steel is 0.16 % C, 0.21 % Si, 0.54 conventional tensile testing procedures until fracture. For the
% Mn, 0.009 % P and 0.022 % S. Long flat specimens are same predeformation level, testing is repeated at least three
prepared according to BS 18. Specimen configuration is: 25, times using different specimen.
100, 300, 25 mm for width, gauge length, parallel length, total The onset of the predeformation level (8 mm.) is selected
based on preliminary tests so that to be well at the beginning of For the five specimen, the exponent n is found varies
the elastic-plastic (forming) zone. For a precise illustration of between 0.2170 and 0.2279 with an average value of 0.2218;
the underlined topics and, to cover the entire practical hence:
functional domain, predeformation levels are selected to be
equally spaced. The utmost predeformation level 20 mm. is σ = Kε 0.2218 . (4)
specified considering two factors: i) to be well within the
elastic-plastic zone and, ii) to be well before the ultimate tensile The strength coefficient (K) can be determined using any
stress. Between the onset and the utmost predeformation point within the elastic-plastic zone (between yield and
levels, two intermediate levels (12 and 16 mm.) are considered. ultimate tensile stress). Its range is found to be between 692
i) No Predeformation Characteristics and 723 Mpa with an average value of 707.3. Therefore, a
The original (no predeformation) specimen is tested until general equation of the material is:
fracture to obtain the nominal mechanical and forming
properties of low carbon steel. For consistency, these
σ = 707.3ε 0.2218 (5)
procedures are repeated individually and independently five
times using similar specimen. As shown in Fig. 3-a the onset of
This equation represents the main features and the
elastic plastic zone is determined just following the yield point.
mechanical properties of the tested low carbon steel.
The latter is specified as the vertical intersection of the curve at
According to conventional approach by many investigators,
strain ratio of 0.5 %. Even though an alternative approach of
e.g. [13], both K and n are considered constant throughout
strain ratio of 0.2 % is sometimes proposed in the literatures, a
forming process regardless the number of deformation stages.
more practical ratio 0.5% is preferred to avoid inaccuracy due
However, it is one of the main goal of the current research is to
to possible slipping between gripper and specimen at the
examine the validation of such an assumption.
beginning of the test.
ii) Predeformation Characterizes
As described earlier, four sets of predeformation levels are
prepared with at least three-repeated specimen for each level.
During testing procedures, the operating and testing conditions
are maintained with only predeformation level as a variable.
Typical data are graphically shown in Figs. 3(b-e). A common
trend can be observed that, as predeformation level increases,
yield strength gradually increases with a corresponding
(a) No predeform. (b) Level 1: 8 mm predeform. decrease in elongation (ductility). Also, the higher the
predeformation level, the closer yield and ultimate tensile
strengths in magnitudes. In other words, the curve beyond the
yield point becomes more and more flattened as
predeformation level becomes higher. This supports the
approach proposed here that forming parameters K and n are
not constant. For each test, K and n have been determined in
the same way as described in the previous section as the
(c) Level 2: 12 mm predeform. (d) Level 3: 16 mm predeform. average of at least three repeated experiments. This has
resulted in the following set of equations for predeformation
8,12, 16 and 20 mm respectively:

σ 8 _ exp = 665.89ε 0.1552 . (6)

σ 12 _ exp = 640.71ε 0.1212 . (7)


(e) Level 4: 20 mm predeform.
Fig.3 Typical output of specimen tensile testing with and
σ 16 _ exp = 611.49ε 0.0853 . (8)
without predeformation
Strain hardening exponent (n) is extracted from the curve at
the ultimate tensile stress point and, it is calculated from the σ 20 _ exp = 578.96 ε 0.0603 . (9)
equations follows:
These equations represent the general trend of the functional
n = ε ult . (3) interrelation between the mechanical properties of the tested
material, represented by the strength and ductility, and the
forming parameters represented by K and n.
Hcorr _8 Hcor r_12 Hcorr _16 Hcor r_20
As predeformation level becomes higher, the forming
70
properties (K & n) show a different trend that supports the
[A] [B] [C]
proposed approach that the mechanical properties of the 60

predeformed material are not constant. To verify such an 50


aspect, a set of corresponding equations has to be deduced
40
using the conventional approach (1). This has led to the
development of the following relation: 30

20

σ con = 707.293( ε o + ε a )0.2218 , (10) 10

0
where εo is the initial predeformation level of the true strain.
To determine the difference between the two approaches
T r ue st r a i n
at different predeformation level, a correction factor (Hcorr) is
proposed here as: Fig. 4 Correction factor (Hcorr) for predeformation levels.
However, at region B within a strain range (from 0.05 to
H corr_i = σ Con _ i − σ exp_ i , (11) 0.1), both conventional (σcon) and proposed (σexp) seem to lead
to almost similar output or, minimum difference. The
where i is the predeformation level: 8, 12, 16 or 20 mm. while underlined region comprises the minimum intersection points
σcon-i and σexp.-i are the conventional and the current approach for all levels. If predeformation level 16 mm is disregarded, the
respectively. region B is strictly limited to strain value of approximately
Graphical representation of the calculated correction 0.075. Therefore, it can be definitely suggested that there is a
factor Hcorr, as affected by the strain and predeformation level, limitation on the application of the conventional approach of
is shown in Fig. 4. For each predeformation level a consistent the properties constancy. In other words, the assumptions that
trend is observed where the difference (correction factor Hcorr) both K and n are constant regardless the predeformation level is
is significantly high at low strain and, as strain increases, Hcorr. valid only within a strain range of 0.05 to 0.1 with the most
decreases non-linearly until it reaches a critical point after credible value at 0.075.
which it tends to behave differently according to its Generally, it may be concluded that, according to the
predeformation level. Generally the more severe the current experiment verification and outcome, the claim of
predeformation level, the higher tendency to change its forming properties constancy is not unanimously valid except
decreasing trend as strain increases and vice versa. in a narrow strain domain of 0.05 to 0.1. Around this region, a
Considering all experimental data for the four levels of correction factor should be considered as indicated in (11).
predeformation, three regions on the curve may be clearly It is thought that a better understanding of the problem
distinguished. The first region A, with nonlinear rapid negative may be globally enhanced through the establishment of
slope, the intermediate region B, at which data tend to behave response surface representation of 3-D contouring plots. A
differently and the third, region C with almost linear low slope qualitative description for the whole set of experimental data
trend that also level of predeformation dependent. under study is explained by 3-D response surface graphics as
At region A, at given strain, smaller values of correction shown in Fig. 5. Values of correction factor Hcorr are plotted as
factor (Hcorr) are obtained at higher predeformation levels. This a surface where at given predeformation level and strain value,
means that the use of the conventional relation (σcon) seems to the corresponding Hcorr can be determined. Surface clearly
indicates the nature of the three regions named in Fig. 4.
over-estimate the stress (σ). However, this trend is clearly
Interpretation may be explained by observing the relation
reversed in region C at moderate to high strain values. An
between the poles of the surface and their interaction. Surface
interpretation may be proposed that relation (σcon) seems to
poles are: low strain-low predeformation (lower left corner);
over estimate the stress (σ) with higher difference magnitudes
low strain-high predeformation (upper left corner); high
at high predeformation level.
strain-low predeformation (lower right corner); and high
strain-high predeformation (upper right corner). However, a
better qualitative approach to get digitalized values of the
correction factor Hcorr is obtained using the response surface
contours as shown in Fig. 6. Each contour represents a unique
value of Hcorr r as it is affected by each of predeformation level
and initial strain and, accordingly, the correct stress σ exp can be
defined.
In Fig. 6, three different regions can be distinguished: A, B,
and C. Region A is for low strain with non-linear attitude and
the correction factor is always high for any level of
predeformation. This is described in the figure as tight contour V. MATHMATICAL MODELING OF THE FORMING PROPERTIES
plots with higher comparative difference. This region
represents the operating domain explained in Fig. 4 for the In the last section, a compensatory correction factor (Hcorr) is
strain range of 0.02 and 0.05. Also, this can be shown in the developed to determine the real experimental value of the stress
3-D graph, Fig. 5 around left poles. at any deformation stage. However, in the current section,
Region B, that is bound by the dotted thick line, Fig. 6, another approach is rather presented to estimate the forming
comprises the values of minimum correction factor where both properties (K and n) as well as the mechanical properties (yield
strength, ultimate tensile strength, and ductility). This is of
σcon and σ exp are usually close in magnitude. While this
vital interest for those involved in forming process evaluation
includes all practical strain for all deformation levels between
based on the actual response (σexp)
0.05 and 0.1, its further effects extends at higher strain range up
Mathematical modeling analysis has proved to be more
to 0.15 but only for low predeformation levels of 8 and 12 mm.
effective to evaluate many experimental problems and to detect
However, in region C, at the top-right corner of the contour, the
the functional relationships between involved variables and
two high levels of predeformation are represented (16 and 20
their interaction [19]. Nonlinear regression analysis, available
mm.). At this region, greater correction factor values are
with SPSS computer package, is used to investigate the whole
obtained as strain increases.
set of the obtained experimental data bearing in mind the
following functional interrelations:

[n & K] αφ ( ∆L ) , (12)

where ã L is the instantaneous predeformation level: 8, 12, 16


or 20 mm.
Trying many different structures of nonlinear estimation
process has led to the best models:

Strain Hardening Exponent (n) = 1.292[ ]


∆L . (13)

Strength Coefficient (K) = 103.43 ( ∆L) - 3.81 ( ∆L) 2 . (14)

Excellent statistical measures are obtained with nothing has


been emerged against models significance and adequacy.
Fig. 5. 3-D response surface representation of the whole set
While adjusted determination factor (R2) are 0.991 and 0.998
of experimental data
for models 13 and 14 respectively, the corresponding F-value
are 1244 and 412 which they are extremely satisfactory for the
0.18
size of the experimental data employed.
Region C
Additionally, it is thought that helpful way to enhance the
problem manipulation and understanding is by the estimation
0.16
of mechanical properties based on the forming properties. To
do this, experimental data are fitted into linear regression
Predeformation Strain

procedures and, this has led to the following significant and


0.14
adequate models:
Region B

0.12
Yield Strength ( σ y ) = [ −1588.13 / n ] + 0.94( K ) , (15)
with R2 = 0.999 and F_ exp value = 9312.
Region A
0.1
Ultimate Tensile strength ( σ ult ) = [ −1203.46 / n ] + 0.914( K ) ,
(16)
0.08
with R2 = 1.0 and F_value = 63758.
0.02 0.04 0.06 0.08 0.1 0.12 0.14
True Strain Area Reduction = 114.08 (n) + 1.206E - 02 (K) , (17)
2
Fig 6. Response surface contours of the whole set of with R = 0.997 and F_value = 1614.
experiment data
VI. Conclusion REFERENCES
In this study it is investigated the effect of forming [1] W. D. Callister Jr, “Material Science and Engineering: An Introduction,”
predeformation on the forming parameters of low carbon steel. 6th ed., John Wiley publication, 2003.
[2] F. Li, D. H. Bae, and A. K. Ghosh, “Grain elongation and anisotropic
Tensile testing is carried out for specimen with four levels of
grain growth during superplastic deformation in an Al-Mg-Mn-Cy
predeformation: 8,12,16 and 20 mm. Results are compared to Alloy,” Acta Materials, vol. 45, no. 9, 1997, pp. 3887-3895.
those from conventional specimen with no predeformation. [3] D. Sampath, S. Moldenhauer, H. R. Schipper, K. Mechsner, and A.
Many technical topics and experimental observations have Hazler, “Decomposition of solid solution of AA5083 alloy upon
exposure to elevated Temperatures,” Materials Science Forum., vol. 331-
been noticed. These can be summarizes as: 337, 2000, pp. 1089-1094.
It has shown that, in general, there is a negative difference in [4] K. Shabata and Y. Mishima, “Effects of Cu and other tramp elements on
the values of K and n for predeformed specimen. Moreover, steel properties,” ISIJ International, vol. 37, no. 3, 1997, p. 197.
[5] T. R. McNelley, M. E. McMahon, and S. J. Hales, “An EBSP
this difference becomes bigger at higher predeformation levels. investigation of alternate microstructures for superplasticity in
Between the zero predeformation and the highest level of 20 aluminum–magnesium alloys,” Script Materials, vol. 36, no. 4, 1997, pp.
mm, reduction in strength coefficient K is about 6% while it is 369-375.
[6] E. M. Taleff, P. J. Nevland, and P.E. Krajewski, “Tensile ductility of
about 72.8% for strain hardening exponent n. several commercial aluminum alloys at elevated temperatures,”
Based on the previous observations, a correction factor is Metallurgical and Materials Trans. A, vol. 32, no. 5, May 2001, pp.
proposed as the mathematical difference in true stress between 1119-1130.
[7] R. W. Davis, J. S. Vetrano, M. T. Smith, and S. G. Pitman, “Mechanical
the conventional stationary approach and the real experimental
properties of aluminum tailor welded blanks at superplastic
one. For a given predeformation level within the practical true temperatures,” Journal of Materials Processing Technology, vol. 128, no.
strain of 0.02 to 0.16, calculated correction factor starts with a 1, October 2002, pp. 38-47.
higher value that decreases as strain increases. However, at [8] H. C. Heikkenen and T. R. Mcnelley, “Superplasticity in Aerospace,”
Annual Meeting of the Metallurgical Society, Arizona, January 1988,
higher predeformation level of 16 and 20 mm, the correction USA.
factor usually tends to reverse its trends and increases at higher [9] M. T. Perez-Prado, G. Gonzalez-Doncel, O. A. Ruano, and T. R.
values of strain. Moderate predeformation level of 12 mm McNelly, “Texture analysis of the transition from slip to grain boundary
sliding in a discontinuously recrystallized superplasctic aluminum
seem to maintain a constant value after passing a transient zone alloy,” Acta. Materials, vol. 49, 2001, pp. 2259-2268.
of true strain between 0.05 and 0.1. Nevertheless, for the lowest [10] C. F. Martyin, J. J. Blandin, and L. Salvo 2001, “Variation in
predeformation level of 8 mm, the correction factor decreases microstructure and texture during high temperature deformation Of Al-
Mg alloy,” Materials Science and Engineering, vol. 297, 2001, pp. 212-
slowly and gradually within and after that transient zone. 222.
Generally for all predeformation level, it may be concluded [11] C. Hsiao and J. C. Huang, “Deformation mechanism during low and
that the least error values between the conventional and the high temperature superplasticity in 5083 Al-Mg Alloy,” Metallurgical
proposed approaches exists within strain range of 0.05 to 0.1. It and Materials Trans. A, vol. 33, 2002, pp. 1373-1384,
[12] W. F. Hostford and R. M. Caddell, “Metal Forming: Mechanics and
can be said, accordingly, that this is the boundary of the Metallurgy,” 2nd ed., Prentice Hall Inc., 1993.
validation of the conventional approach where forming [13] E. M. Mielnik, “Metal Working Science and Engineering,” McGraw
parameters are kept constant regardless the sequence of the Hill, 1991.
[14] E. G. Thomsen, C. T. Yang, and S. Kobayashi, “Mechanics of plastic
predeformation process. deformation in metal deformation,” The Macmillan Company, New
Response surface 3-D representation of entire set of York, 1965.
experimental data clearly shows a hidden trend as the different [15] T. G. Nieh, J. Wadsworth, and O. D. Sherby, “Superplasticity in Metals
and Ceramics,” Cambridge University Press, 1979.
strain and predeformation levels affect the correction factor. [16] M. L. Mecartney, “ Grain boundary engineering of highly deformable
However, a quantitative digitized approach is presented as ceramics,” Current Status and Future Potential. (Materials Research
contour plots in which the various deformation zones are Society Symposium Proceedings, Warrendale, PA, USA: Mater. Res.
Soc, vol. 601, 2000, pp. 81-91.
distinguished.
[17] A. M. Alaskari and S. Das, “Practical numerical analysis of a crack near
To build a database approach that might be helpful as a a weld subjected to primary loading and hydrogen embrittlement,”
work-floor information source, forming parameters K and n are Journal of Materials Processing Technology, vol. 173 no. 1, March
empirically related to mechanical properties. Excellent 2006, pp. 1-13.
[18] O. D. Sherby and J. Wadsworth, “Superplasticity- Recent Advances and
significant and adequate models are developed with high Future Directions,” Progress of Materials Science, vol. 33, 1989, pp.
confidence and statistical criteria. 169-221.
[19] S. E. Oraby, A. M. Alaskari and E. A. Almeshaiei, “Quantitative and
qualitative evaluation of surface roughness-tool wear correlation in
turning operations,” Kuwait Journal of Science & Engineering (KJSE),
ACKNOWLEDGMENT An International Journal of Kuwait University, vol. 31 no. 1, 2004, pp.
219-244.
The authors wish to thank the PAAET for supporting the
project under the grant contract no. (TS-05-001). Also, they
express their deep grateful to the departmental staff and
Technological Studies College and PAAET higher education &
researches administrations for whatever assistance produced.
Special thanks for Mr. A. Albannay for his technical assistance
in specimen preparation and setup procedures.

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