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International Journal of Mining Science and Technology xxx (2018) xxx–xxx

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International Journal of Mining Science and Technology


journal homepage: www.elsevier.com/locate/ijmst

Hydraulic drill hole reaming technology with large flow and draining of
coal mine gas
Li Dingqi
School of Energy Science and Engineering, Henan Polytechnic University, Jiaozuo 454001, China

a r t i c l e i n f o a b s t r a c t

Article history: This paper takes Zhaozhuang mine in Shanxi province as an example to study the technology of hydraulic
Received 4 June 2017 reaming drill hole for improving the gas extraction. The influence of the physical properties of coal seam
Received in revised form 2 April 2018 on the hydraulic reaming drill holes and the draining of coal mine gas were analyzed and discussed for
Accepted 5 June 2018
different coal structure areas, and the following conclusions were made. Hydraulic drill hole reaming has
Available online xxxx
had a positive impact in Zhaozhuang Mine, and can improve the efficiency of gas extraction to different
degrees. The water jet pressure used in hydraulic drill hole reaming mainly depends on the structure of
Keywords:
the coal. When the coal seam basically becomes integrated, the critical water jet pressure increases, the
Coal seam with low permeability
Gas extraction
discharge becomes relatively easy to achieve, the blocking effect on the gas extraction decreases, and the
Coal physical parameters gas extraction significantly increases after the reaming process. When the coal seam is broken, the critical
Water jet water jet pressure decreases, the discharge becomes difficult to achieve, the blocking effect on the gas
Permeability improvement extraction becomes obvious, and the gas extraction changes slightly after reaming.
Ó 2018 Published by Elsevier B.V. on behalf of China University of Mining & Technology. This is an open
access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).

1. Introduction ing, hydraulic flushing, hydraulic reaming, and hydraulic slotting


[7–14]. Hydraulic flushing, hydraulic reaming and hydraulic slot-
The permeability of coal seam is low in most areas in China, and ting can improve the permeability of coal seam using a water
coalbed methane exploration on the ground and through under- jet. For a coal seam under the danger of a coal and gas outburst,
ground mine gas extraction becomes difficult [1,2]. China is one a water jet is normally used in a floor rock roadway and cross layer
of the biggest coal-producing countries in the world, but the effi- drill hole, whereas for a coal seam without the danger of a coal
ciency of its coal gas extraction process is low, causing much and gas outburst, a water jet can also be used in a coal seam road-
higher gas emissions than in other countries. In China, coal mine way or in a drill hole along the coal seam [15–17]. The coal mines
gas emissions accounted for 41% of the world’s total gas emission in many areas of China face the danger of coal and gas outbursts,
in 2005 [3,4]. At the same time, China has also become one of and to avoid such outbursts, a water jet is used in the floor rock
the countries most affected by coal mine gas disasters [5]. With roadway and cross layer drill hole. Hydraulic flushing is usually
an increase in mining depth, the in-situ stress and content of the used for soft coal with the danger of a coal and gas outburst.
coal bed gas are increasing, but the permeability of coal seam decli- Hydraulic flushing reduces the in-situ stress and improves the per-
nes, and the extraction of coal mine gas and the control of gas dis- meability of the coal seam by causing a small-scale coal and gas
asters are more difficult to achieve. Coalmine gas is a type of outburst with a water jet in the cross layer drill hole. During
greenhouse gas, and is dangerous in underground. However, hydraulic fracturing, hydraulic reaming and slotting are more suit-
through improvements in coal seam permeability, and the effi- able for some relatively hard coal seam. At present, the water flow
ciency of gas extraction and utilization, this type of harmful green- used in hydraulic reaming and slotting is slight, and thus a slag
house can be turned into a clean energy source [6]. discharge is difficult to achieve when using these methods in oily
A significant amount of research by scholars at home and and broken coal seam. In this case, a large flow and medium pres-
abroad has been conducted to increase the permeability of coal sure are more suitable for hydraulic reaming and slag discharge,
seam, including mining protective layer, deep hole blasting, thin thereby improving the working efficiency of a water jet. Therefore,
sub-layer mining, high-pressure gas fracturing, hydraulic fractur- using the coal mining area of Zhaozhuang as an example, the influ-
ence of the physical properties of the coal seam on a hydraulic
reaming drill hole and the draining of coal mine gas is studied
E-mail address: lidingqi@hpu.edu.cn and discussed in this paper.

https://doi.org/10.1016/j.ijmst.2018.06.003
2095-2686/Ó 2018 Published by Elsevier B.V. on behalf of China University of Mining & Technology.
This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).

Please cite this article in press as: Li D. Hydraulic drill hole reaming technology with large flow and draining of coal mine gas. Int J Min Sci Technol (2018),
https://doi.org/10.1016/j.ijmst.2018.06.003
2 D. Li / International Journal of Mining Science and Technology xxx (2018) xxx–xxx

2. Test on hydraulic reaming

2.1. Test sites

The Zhaozhuang Coal Mine is an extremely large, and it belongs


to Jincheng Anthracite Mining Group Co., Ltd., China. The design
production capacity of the Zhaozhuang Coal Mine is 8 Mt/a. The
mine is located in the southeastern part of the Qinshui coalfield,
53 km south from Jincheng city. #3 coal seam is the main mining
coal seam, the thickness of which ranges from 0 to 6.35 m, or
4.69 m on average. As a whole, the permeability of the coal seam
in the Zhaozhuang Coal Mine is poor, the attenuation of the gas Fig. 1. Coal sample from test site No. 1.
flow is fast, and gas extraction is difficult to achieve. The regional
differences in the gas bearing are obvious. The gas content of the
first panel of #3 coal seam is 6.99 to 12.73 m3/t, the permeability
coefficient is 0.21 to 0.46 m3/MPa2 d, the original gas pressure is
0.06–0.71 MPa, the gas flow per 100 m drill hole is 0.0005–
0.0039 m3/minhm, and the gas flow attenuation coefficient of a
drill hole is 0.14–0.39 d 1. Two sites were used to test the hydrau-
lic reaming. Test site No. 1 is in the return air roadway in the north
wing of seam #3, and test site No. 2 is in the floor rock roadway of
13091. Coal samples were obtained from three different sub-layers
of #3 coal seam, and the physical parameters were measured. The
average values of the measured physical parameters are shown in
Table 1. The coal seam on test site No. 1 is relatively integrated, and
the coal seam on test site No. 2 is broken. The structures of the coal Fig. 2. Coal sample from test site No. 2.
samples from test site No. 1 and test site No. 2 are shown in Figs. 1
and 2.
connected with a sealed rotary joint is 25 mm. A quick connector
and U-shape oblique key are used to connect the water pipe, pres-
2.2. Test equipment sure pump, and rotary joint.

The technology used in hydraulic drill hole reaming can (3) Sealed drill pipe
improve the diameter and gas drainage of a drill hole when using
a high-pressure water jet. The hydraulic reaming system greatly The structure of the sealed drill pipe was optimized to improve
influences the effect of hydraulic drill hole reaming. The hydraulic the strength and sealability of the sealed drill pipe. For the seal, a
reaming system includes a rig, sealed drill pipes, drill bit, high- parallel section used was added in a conical joint, and a rubber ring
pressure pump, tank, sealed rotary joint, high-pressure control was embedded in the joint’s inner wall. In Fig. 3, conical joint with
valve, high-pressure nozzle, prevention device, and a gas and water a screw thread is used to connect the drill pipe, the parallel section
separation device. is used for the seal, and the rubber ring is used for the seal. Com-
pared with an ordinary sealed drill pipe, this type of sealed drill
(1) Rig used for testing pipe has a greater connection strength, better sealability, and
longer service life.
The type of rig used for testing is a ZDY—4200LPS, which is a
common rig used in coal mines with a wide speed range and a (4) Jet device
large torque, meeting the demands of drilling and hydraulic ream-
ing. A drill pipe with a diameter of 73 mm and a drill bit with a The jet device is the key part of a hydraulic reaming system. It
diameter of 133 mm were used to match the rig. greatly influences the effect of the hydraulic striping and slagging
in a drill hole. During the tests, the jet device was improved
(2) High-pressure water pipe through the addition of two or three nozzles to the back of the
jet device to strengthen the discharge of the coal cinder. In Fig. 4,
A high-pressure water pipe is connected with a pressure pump, conical joint with a screw thread is used to connect the drill pipe
sealed rotary joint, and sealed drill pipes. And it is an important and bit, the parallel section is used for the seal, the rubber ring is
part of high-pressure water transport over long distances. A used for the seal, the nozzles are used for the slagging, and the noz-
high-pressure water pipe is made of rubber and steel wire and zles used to strip the coal from the drill hole wall. The number and
has a rated pressure of 40 MPa. The outer diameter of the high- diameter of the nozzles are designed for different flows used in a
pressure water pipe connected with the pressure pump is 38 slag discharge. When the structure of the coal seam is integrated
mm, and the outer diameter of the high-pressure water pipe and the coal has greater hardness, a higher water pressure and

Table 1
Physical parameters of coal seam at the test sites.

Test Bulk modulus Shear modulus Strength of extension Internal friction angle Cohesion Firmness Type of deformed
site (GPa) (GPa) (MPa) (°) (MPa) coefficient coal
No. 1 1.65 0.75 0.13 20.0 1.57 0.65 III
No. 2 1.52 0.56 0.11 18.8 0.52 0.50 Ⅱ

Please cite this article in press as: Li D. Hydraulic drill hole reaming technology with large flow and draining of coal mine gas. Int J Min Sci Technol (2018),
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Table 2
Test parameters for site No. 1.

Drill hole number Quality of discharge (t) Jet pressure Jet flow
(MPa) (L/min)
1 5.4 25 260
2 8.6 30 320
Fig. 3. Structure of sealed drill pipe.
3 0.2 10 108
4 0.2 15 162
5 13 30 320
6 16 30 320
7 10 30 320
8 16 30 320
9 0.8 20 216
10 12 30 320

Fig. 4. Structure of jet device. during the test was about 5.4 t. The other drill holes were hydrauli-
cally reamed with water pressure of 30 MPa, and the discharge of
the coal cinder during the test was no less than 8 t for each drill
lower water flow are needed. In this case, only the nozzles used to hole. According to the quantity of coal cinder discharge and the
strip coal from a drill hole wall are utilized. corresponding water pressure, the suitable water pressure for the
jet is 25–30 MPa. The test parameters are shown in Table 2. The
(5) High-pressure pump particle size of the coal cinder was relatively uniform, generally
less than 10 mm, and the slag discharge was relatively easy to
An emulsion pump, a BRW400/37, was used as the high- achieve during the test.
pressure pump for the testing. The rated flow is 400 L/min, and
the rated pressure is 37 MPa. A rectangle water tank was con- (3) Data of gas extraction
nected with an emulsion pump, and used to store water. The
length, width, and height of the tank are 2.45, 1.45, and 1.4 m, As the quality of the coal cinder discharge is relatively large, #1,
respectively, and the volume is 2.5 m3. #2, #5, #6, #7, #8, and #10 drill holes were used to analyze the
effect of gas extraction after hydraulic reaming. The data on the
2.3. Test at site No. 1 gas extraction after the hydraulic reaming of #1 drill hole are
shown in Fig. 4. Within 0–40 d, the gas extraction flow reached
(1) Location of site No. 1 10–100 m3/d after hydraulic reaming. Within 40–58 d, the gas
Site No. 1 was within the range of 100 m near connection road- extraction flow reached about 10 m3/d after hydraulic reaming.
way #8 in the return air roadway in the north wing of #3 coal Within 59–77 d, the gas extraction flow showed a significant
seam. The thickness of the coal seam is 5–6 m, and the dip angle improvement, reaching 50–125 m3/d after hydraulic reaming.
is 1°–3°. The width of the return air roadway is 5.5 m, the height Within 78–90 d, the gas extraction flow showed a significant
is 4.334 m, and the largest ventilation air flow is 192 m3/s. The dis- decrease, reaching 10 to 50 m3/d after hydraulic reaming. As
tance between the return air roadway and coal seam is 32–37 m. Figs. 6–12 show, the data on the gas extraction show a large vari-
The cross section area of the return air roadway is large, as is the ation after hydraulic reaming was applied.
ventilation air flow, and no obstructions are present in the neigh-
borhood, which provides favorable conditions for the test. (4) Correlation data
Because the water pressure used for the hydraulic reaming of
(2) Test parameters
#3, #4, and #9 drill holes was too low, the discharge of these drill
Drill holes were drilled in site No. 1, and as Fig. 5 shows, ten drill holes was very slight, and had almost no effect on the gas extrac-
holes were drilled, with a spacing between the adjacent drill holes tion. Thus, #3, #4, and #9 drill holes were used as the references
of 10 m, dip angle of 60°, azimuth angle of 0°, and drill hole diam- for a comparison and analysis of the effects on the gas extraction
eter of 133 mm. To obtain a suitable water pressure for the jet, #3, after the hydraulic reaming of #1, #2, #5, #6, #7, #8, and #10 drill
#4, #9, #1, and #2 drill holes were hydraulically reamed with dif- holes. The data on the gas extraction after the hydraulic reaming
ferent water pressures, and #3 and #4 drill holes were hydrauli- of#3, #4, and #9 drill holes are shown in Figs. 13–15, respectively.
cally reamed with a water pressure of 10 and 15 MPa, After the hydraulic reaming of these drill holes, the gas extraction
respectively. In addition, the discharge of coal cinder during the flow had less variation at 10–100 m3/d.
test was about 0.2 t. #9 drill hole was hydraulically reamed with
water pressure of 20 MPa, and the discharge of the coal cinder dur-
ing the test was about 0.8 t. #1 drill hole was hydraulically reamed
with water pressure of 25 MPa, and the discharge of the coal cinder

Fig. 5. Drill hole layout of test for site No. 1. Fig. 6. Data on gas extraction after hydraulic reaming of #11 drill hole.

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Fig. 11. Data on gas extraction after hydraulic reaming of #8 drill hole.
Fig. 7. Data on gas extraction after hydraulic reaming of #2 drill hole.

Fig. 8. Data on gas extraction after hydraulic reaming of #5 drill hole. Fig. 12. Data on gas extraction after hydraulic reaming of #10 drill hole.

Fig. 9. Data on gas extraction after hydraulic reaming of #6 drill hole. Fig. 13. Data on gas extraction after hydraulic reaming of #3 drill hole.

Fig. 10. Data on gas extraction after hydraulic reaming of #7 drill hole. Fig. 14. Data on gas extraction after hydraulic reaming of #4 drill hole.

are small, the average flow rate of the gas extraction within
(5) Effect analysis
zero to 70 d is 10–12 m3/d. When the water pressure of the jet
As shown in Figs. 6–15, the hydraulic reaming of a drill hole and the quality of the coal cinder discharge are large, the
has a significant impact on the gas extraction. When the water average flow rate of the gas extraction within zero to 70 d is
pressure of the jet and the quality of the coal cinder discharge 80–300 m3/d.

Please cite this article in press as: Li D. Hydraulic drill hole reaming technology with large flow and draining of coal mine gas. Int J Min Sci Technol (2018),
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(3) Data of gas extraction


#1309-1, #1309-2, #1309-3, #1309-4, and #1309-5 drill holes
were used to analyze the effects of gas extraction after hydraulic
reaming. The data on the gas extraction are shown in Figs. 17–
21. The average flow of the gas extraction after the hydraulic ream-
ing was about 10 m3/d.

(4) Correlation data


#1309-6 and #1309-7 drill holes without hydraulic reaming
were used as references for the comparison and analysis of the
Fig. 15. Data on gas extraction after hydraulic reaming of #9 drill hole.

2.4. Test at site No. 2

(1) Location of site No. 2


Site No. 2 is located 20 m away from water sump #17 in the
13091 floor rock roadway. The width and height of the 13091 floor
rock roadway are 4 and 2.8 m, respectively, and a local fan is used
to ventilate the test location. The distance between the 13091 floor
rock roadway and the coal seam is 7 m. The thickness of the coal
seam is 5–6 m, and the dip angle is 1–3°. The air flow of the venti-
Fig. 17. Data on gas extraction after hydraulic reaming of #1309-1 drill hole.
lation is small, which provides unfavorable conditions for the sec-
ond test.

(2) Test parameters

Drill holes were drilled at site No. 2. As shown in Fig. 14,


seven drill holes were drilled, with a spacing between adjacent
drill holes of 10 m, a dip angle of 60°, an azimuth angle of 0°,
and a drill hole diameter of 133 mm. Five of the drill holes were
used as the hydraulic reaming drill holes, and two of them were
used as the reference drill holes. The water pressure for the jet
was 8–27 MPa, the water flow rate of the jet was 86–292 L/min,
and the quality of the discharge was 3.5–11.5 t. The test param-
eters are shown in Table 3. The particle sizes of the coal cinder
Fig. 18. Data on gas extraction after hydraulic reaming of #1309-2 drill hole.
are relatively uneven, some reaching more than 50 mm, and
the slag discharge was relatively difficult to achieve during the
test (see Fig. 16).

Table 3
Test parameters for site No. 2.

Drill of hole number Quality of discharge (t) Jet pressure Jet flow
(MPa) (L/min)
#1309-1 3.5 8 86
#1309-2 4.2 27 292
#1309-3 7.8 27 292
#1309-4 13 25 270
#1309-5 11.5 17 184
Fig. 19. Data on gas extraction after hydraulic reaming of#1309-3 drill hole.

Fig. 16. Drill hole layout for site No. 2. Fig. 20. Data on gas extraction after hydraulic reaming of #1309-4 drill hole.

Please cite this article in press as: Li D. Hydraulic drill hole reaming technology with large flow and draining of coal mine gas. Int J Min Sci Technol (2018),
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(2) Impact on slag discharge

After hydraulic reaming at test site No. 1, the discharge is rela-


tively smooth, and the gas extraction effect is better, whereas after
hydraulic reaming at test site No. 2, the drill hole is frequently
blocked, the cinders are difficult to discharge during hydraulic
reaming, and the gas extraction effect is poor. The results were
analyzed by contrasting the pressure and flow rates used during
the tests. Using the same conditions for the test equipment, the
flow used for the discharge and jet pressure showed a positive cor-
relation. When a large pressure and flow were used at test site No.
1, owing to the intact coal structure, the drill wall was not easy to
Fig. 21. Data on gas extraction after hydraulic reaming of #1309-5 drill hole.
collapse, the slag discharge was cut into smaller cinders with an
even size by the jet, and slag discharge was easy to achieve. When
a large pressure and flow were used at test site No. 2, owing to the
broken coal structure, the drill wall was easily collapsed, many coal
cinders with a larger size block were generated in the drill hole,
and slag discharge was difficult to achieve. When a small pressure
and flow were used at test site No. 2, owing to the broken coal
structure, the size of the coal cinders was larger. Slag discharge
was also difficult to achieve for a small discharge flow and larger
sized coal cinders.

(3) Impact on gas extraction

To further explore the relationship between the jet flow and


Fig. 22. Data on gas extraction after hydraulic reaming of #1309-6 drill hole. slag discharge, we improved the jet by adding three nozzles to
the jet device, as shown in Fig. 2. The flow used for the discharge
was greatly improved under the same pump pressure. We con-
ducted a second test by adopting the improved jet device used at
test site No. 2. #1309-8 and #1309-9 drill holes was hydraulically
reamed during this test. The length of the hydraulic reaming was 6
and 8 m, the jet pressure was 6 and 8 MPa, the flow rate was 300
and 320 L/min, and the length of time for the hydraulic reaming
was 2 and 1.5 h, respectively. Slag discharge was easy to achieve,
and no blocking phenomena were observed during the test. The
gas extraction after the hydraulic reaming is shown in Figs. 24
and 25. Compared to the first test at test site No. 2, the flow of
gas extraction after hydraulic reaming shows an obvious increase.
From the data analysis above, we found that, under no-blocking
Fig. 23. Data on gas extraction after hydraulic reaming of #1309-7 drill hole. conditions, the flow of the gas drainage increased significantly
after hydraulic reaming at the same site. Under the condition of
a broken coal seam structure, when the drill hole was blocked dur-
effect on the gas extraction after the hydraulic reaming of #1309-1, ing hydraulic reaming, a large amount of water entered the broken
#1309-2, #1309-3, #1309-4, and #1309-5 drill holes. Data on the coal seam around the drill hole, which hindered the desorption and
gas extraction for #1309-6 and #1309-7 drill holes are shown in migration of the gas in the coal seam, thereby reducing the coal
Figs. 22 and 23. The average flow of the gas extraction was 8 m3/d. permeability and gas extraction.
To analyze the influence of water in the coal, the relationship
3. Discussion between the different moisture content and the permeability of
the coal sample was determined in a laboratory, as shown in Figs. 26
3.1. Impact of physical coal properties on the parameters of hydraulic and 27. The permeability of the coal sample greatly reduced with an
reaming increase in the moisture content of the coal sample.

(1) Impact on jet pressure


During the experiment, we found that the jet flow and pressure
have a close relationship with the structure of the coal. The jet
pressure required for test site No. 1 was 25–30 MPa, whereas the
jet pressure needed for test site No. 2 was 8–15 MPa. The main rea-
son for this is that the coal firmness coefficients for test sites No. 1
and No. 2 are similar, but the difference in the shear strengths at
the two sites is significant. The coal structure at test site No. 1 is
relatively intact and has a small degree of damage, and thus it is
more difficult to break the coal and strip the cinders from the coal
wall. The coal at test site No. 2 is broken, and the degree of damage
of the coal structure is higher, making it easy to break the coal and
strip the cinders from the coal wall. Fig. 24. Data on gas extraction after hydraulic reaming #1309-8 drill hole.

Please cite this article in press as: Li D. Hydraulic drill hole reaming technology with large flow and draining of coal mine gas. Int J Min Sci Technol (2018),
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The space between the two groups of drill holes was 10 m. The
spaces between the first group of drill holes were 2 and 3 m, and
the spaces between the second group of drill holes were 4 and 5
m. The drill holes used to test the influence the radius were sealed,
and connected with a flow meter and extraction system prior to
the hydraulic reaming. The influence of the hydraulic reaming
radius was estimated according to the variations in gas flow.
According to the test results, we found that the influence of
hydraulic reaming radius was 2–3 m at test site Nos. 1, and 3–4
m at test site No. 2. According to the test results, we found that
the influence of the hydraulic reaming radius was affected not only
Fig. 25. Data on gas extraction after hydraulic reaming #1309-9 drill hole.
by the final diameter of the drill hole after hydraulic reaming, but
also by the physical properties of the coal, particularly the coal
structure. When the coal structure was broken and the shear
strength was small, the influence of the hydraulic reaming radius
was larger.

4. Conclusions

(1) A hydraulically reamed drill hole was shown to have a good


effect in the Zhaozhuang Mine, and can improve the effi-
ciency of the gas extraction process to different degrees.
(2) The water jet pressure used for the hydraulic reaming of a
drill hole mainly depends on the structure of the coal. When
the coal seam is basically integrated, the critical pressure for
Fig. 26. Permeability of coal sample under moisture contents of 0% and 9.2%. the water jet is larger. When the coal seam is broken, the
critical pressure for the water jet is smaller.
(3) When the coal structure is relatively integrated, discharge is
relatively easy to achieve, the blocking effect on the gas
extraction is slight, and the gas extraction is significantly
increased after the reaming is applied.
(4) When the coal structure is broken, the discharge is difficult
to achieve, the blocking effect on the gas extraction is clear,
and the gas extraction changes slightly after reaming.
(5) When the coal structure is broken, lowering the jet pressure
and improving the jet flow can significantly improve the effi-
ciency of the reaming, thereby reducing the blocking of the
gas extraction.
(6) When the coal structure is broken, the shear strength is
slight, and the influence of the hydraulic reaming radius
Fig. 27. Permeability of coal sample under moisture contents of 0% and 4.9%. becomes greater.

3.2. Impact of the radius of hydraulic reaming


Acknowledgments
The influence of the hydraulic reaming radius was tested at test
sites Nos. 1 and 2. The primitive diameter of the drill hole before The author thanks the National Natural Science Foundation of
hydraulic reaming is 133 mm, and the final diameter of the drill China (No. 51404094), Postdoctoral Science Foundation of China
hole after hydraulic reaming is 1600 mm. The drill holes were per- (No. 2014M561988), and Doctor Funds of Henan Polytechnic
pendicular to the coal seam. University of China (No. B2012-026) for their support with this
The test method is as follows: project.
First, cross drill holes were drilled using conventional drill pipes
(U73) and drill bits (1 3 3), as shown in Fig. 28. Two groups of drill
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Please cite this article in press as: Li D. Hydraulic drill hole reaming technology with large flow and draining of coal mine gas. Int J Min Sci Technol (2018),
https://doi.org/10.1016/j.ijmst.2018.06.003

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