Professional Documents
Culture Documents
This NORSOK standard is developed with broad petroleum industry participation by interested parties in the
Norwegian petroleum industry and is owned by the Norwegian petroleum industry represented by The Norwegian
Oil Industry Association (OLF) and The Federation of Norwegian Industry. Please note that whilst every effort has
been made to ensure the accuracy of this NORSOK standard, neither OLF nor The Federation of Norwegian
Industry or any of their members will assume liability for any use thereof. Standards Norway is responsible for the
administration and publication of this NORSOK standard.
Standards Norway Telephone: + 47 67 83 86 00
Strandveien 18, P.O. Box 242 Fax: + 47 67 83 86 01
N-1326 Lysaker Email: petroleum@standard.no
NORWAY Website: www.standard.no/petroleum
Copyrights reserved
Provided by Standard Online AS for Ignatios+Staboulis 2014-06-23
NORSOK standard M-650 Edition 4, September 2011
Foreword 4
Introduction 4
1 Scope 5
2 Normative and informative references 5
2.1 Normative references 5
2.2 Informative references 5
3 Terms, definitions and abbreviations 5
3.1 Terms and definitions 5
3.2 Abbreviations 7
4 Responsibilities 8
4.1 Purchasers responsibility 8
4.2 Manufacturers responsibility 8
4.3 Responsibilities of Qualifying Company 8
5 Qualification of manufacturers 8
5.1 Basis for qualification of manufacturers 8
5.2 Evaluation for acceptance 8
5.3 Acceptance of qualification 8
5.4 Proof of acceptance 8
6 Validity of qualification 9
6.1 Term of validity 9
6.2 Renewal of qualification 9
6.3 Transitional arrangements 9
Foreword
The NORSOK standards are developed by the Norwegian petroleum industry to ensure adequate safety,
value adding and cost effectiveness for petroleum industry developments and operations. Furthermore,
NORSOK standards are, as far as possible, intended to replace oil company specifications and serve as
references in the authorities’ regulations.
The NORSOK standards are normally based on recognised international standards, adding the provisions
deemed necessary to fill the broad needs of the Norwegian petroleum industry. Where relevant, NORSOK
standards will be used to provide the Norwegian industry input to the international standardisation process.
Subject to development and publication of international standards, the relevant NORSOK standard will be
withdrawn.
The NORSOK standards are developed according to the consensus principle generally applicable for most
standards work and according to established procedures defined in NORSOK A-001.
The NORSOK standards are prepared and published with support by The Norwegian Oil Industry Association
(OLF), The Federation of Norwegian Industry, Norwegian Shipowners’ Association and The Petroleum Safety
Authority Norway.
Introduction
x clarification of scope;
x definitions included or changed for Company, equalization time, heat sink, holding time, main contractor,
manufacturer, Qualifying Company, soak time and test directions;
x clarification of responsibilities;
x clarification of transitional arrangements between Revision 3 and Edition 4 of this NORSOK standard;
x more stringent requirements to manufacturers knowledge;
x requirements to test laboratories and manufacturers of welded products included;
x type of etchants to be used and preparation of samples for micro examination, as applicable, shall be
stated in the Manufacturing Summary;
x new clause about heat treatment with requirements to equipment, heat treatment procedure and
verification of heat treatment procedure;
x changes in essential variables of the qualification tests especially regarding manufacturing equipment,
heat treatment, hipped products and start material;
x changes in test requirements for flanges, other type of forgings, plates, rolled bars and valves machined
from forgings;
x changes in extent and requirements to additional testing at mid-thickness for bars, forgings and hipped
(HIP) products;
x otherwise editorial changes for clarification.
1 Scope
This NORSOK standard establishes a set of qualification requirements to verify that the manufacturer has
sufficient competence and experience of the relevant material grades, and necessary facilities and equipment
to manufacture these in the required shapes and sizes with acceptable properties.
This standard is applicable to the following material grades and product forms:
This NORSOK standard is also applicable to critical components or product forms in other materials and for
special manufacturing/fabrication processes, e.g. titanium and nickel alloys in other product forms than
casting, carbon steel and low alloy steel products and induction/cold bending.
3.1.2
company
owner or organization that is responsible for development of and/or operation of an installation/facility
NOTE For the purpose of this standard this is normally an oil company.
3.1.3
equalization time
the time used to ensure a uniform pre-set temperature throughout a heat treatment load and/or throughout all
section thicknesses of a component (see also figure in Annex C)
3.1.4
heat sink
separate block of material made from the same generic type of material as the parts being heat treated to
monitor temperature during heat treatment
3.1.5
high alloyed austenitic SS
austenitic SS with PREN ≥ 40 or Ni + 2 x Mo > 30 (Mo > 2)
EXAMPLES SS type 6Mo, UNS S31266, UNS S32654, UNS S34565, UNS J95370.
3.1.6
holding time
time from the controlling thermocouple (normally furnace thermocouple) has reached set temperature until
the specified soaking time is completed.
NOTE Holding time consist of equalization time + soaking time. (see also figure in Annex C).
3.1.7
main contractor
3.1.8
manufacturer
party, including sub-contractors, which carry out operations affecting the material properties of the finished
product
3.1.9
may
verbal form used to indicate a course of action permissible within the limits of this NORSOK standard
3.1.10
pitting resistance equivalent PREN
PREN = %Cr + 3.3 x %Mo + 16 x %N
3.1.11
purchaser
party that purchase a product from a manufacturer
3.1.12
Qualifying Company
party which monitor the qualification exercise and in the end accept the resulting qualification test record
(QTR) by signing and stamping the QTR front page
The Qualifying Company can be the Company, the main contractor, the purchaser or a party authorised to act
on their behalf. Qualifying Company shall be independent of the manufacturer.
3.1.13
shall
verbal form used to indicate requirements strictly to be followed in order to conform to this NORSOK standard
and from which no deviation is permitted, unless accepted by all involved parties
3.1.14
should
verbal form used to indicate that among several possibilities one is recommended as particularly suitable,
without mentioning or excluding others, or that a certain course of action is preferred but not necessarily
required
3.1.15
soaking time
time that the entire part being heat treated (throughout its cross sections) remains at the specified set
temperature
3.1.16
type 22Cr duplex
ferritic/austenitic stainless steel alloys with 22 % Cr
3.1.17
type 25Cr duplex
ferritic/austenitic stainless steel alloys with 25 % Cr and PREN ≥ 40
EXAMPLES UNS S S32505, UNS S32550, UNS S32750, UNS S32760 and UNS S39274.
3.1.18
type 6Mo
3.1.19
test directions
test directions are defined relative to the geometry of the component to be tested
For the purpose of this NORSOK standard the definitions in ASTM A370-11, sect. 4, apply with axial defined
as the longitudinal axis of test specimen located parallel to the main axis of the component.
3.2 Abbreviations
API American Petroleum Institute
ASTM American Society for Testing and Materials
CD compact disc
EN European Standard
HIP hot isostatic pressed
IEC International Electrotechnical Commission
ISO International Organization for Standardization
MDS material data sheet
MOM minutes of meeting
NDE non-destructive examination
PREN pitting resistance equivalent
PWHT post weld heat treatment
QTR qualification test record
SS stainless steel
UNS unified numbering system
WPQR welding procedure qualification record
WPS welding procedure specification
4 Responsibilities
A manufacturer acquiring a "NORSOK M-650 qualification" assumes an obligation to carry out manufacturing
in accordance with the qualified Manufacturing Summary including its referred procedures. If an order
requiring "NORSOK M-650 qualification" is outside the qualified range, as defined in 10.2, the purchaser shall
be informed.
The Qualifying Company shall monitor the qualification exercise, review and in the end accept the resulting
qualification test record (QTR) and as proof of the acceptance sign and stamp the QTR front page.
It is important for acceptance of the QTR by other customers that the verification exercise is carried out by a
recognized Qualifying Company.
a) knowledge and relevant manufacturing experience with the type of material to be qualified (see Clause 7);
b) acceptable manufacturing facilities and equipment (see Clause 7 and Clause 9);
c) established Manufacturing Summary (procedure) covering all manufacturing steps from melting or semi
product to finished products (see Clause 8);
d) an established heat treatment procedure (see Clause 9);
e) manufacturers quality system, which shall fulfil the requirements of ISO 9001;
f) results of testing in compliance with this NORSOK standard (see Clause 10).
The review shall be carried out by technical competent personnel, with knowledge of metallurgical aspects of
the applicable alloys, including precipitation diagrams, effect of hot forming, welding, heat treatment, etc., and
who has experience relevant for the manufacturing process to be evaluated.
NOTE There is no official listing in the name of NORSOK of accepted manufacturers according to this NORSOK standard.
6 Validity of qualification
a) a manufacturer with regular production of the originally qualified products and alloys is considered re-
qualified and additional testing is normally not required. It is a pre-requisite that all test requirements in the
current revision of this NORSOK standard are complied with;
b) evaluation and review at the manufacturers and sub-suppliers premises according to 5.2 shall be carried
out by the Qualifying Company;
c) the Manufacturing Summary and referred procedures shall be reviewed, updated and a decision made
whether retesting is required;
d) the heat treatment procedure and its corresponding verification, see 9.3, shall be reviewed, and a
decision made whether a new verification is required;
e) a minutes of meeting (MOM) listing actual parts of the QTR which shall be updated and with conclusions
for renewal of the qualification shall be included in the re-qualified QTR;
f) a new QTR front page shall be established and properly signed.
In such case a statement shall be included in the box “Other information” on the original Revision 3 QTR front
page and signed off by the Qualifying Company. The original Revision 3 validity date shall be maintained.
7 General requirements
7.1.1 Knowledge
The manufacturer shall have in-house knowledge of relevant metallurgical aspects of the applicable alloys
including precipitation diagrams, effects of hot forming, welding, and heat treatment parameters, etc. as
applicable for his manufacturing process.
Relevant experience should be supported by statistical data presented in the form of a histogram for key
parameters, e.g. tensile strength, impact thoughness, corrosion resistance, etc. In addition a relevant
reference list from the last 2 years production for the products, materials and the range of sizes to be
qualified shall be included.
New manufacturers with less than 2 years of documented production for actual product and material may be
qualified to this NORSOK standard, but with a validity period limited to 2 years, after which a new evaluation
shall be carried out. A note to this effect shall be included on the QTR front page.
Requirements for heat treatment facilities and equipment are further described in 9.1.
7.3 Sub-contractors
If parts of the production are carried out by a sub-contractor, the manufacturer is responsible for ensuring that
the sub-contractor meets the requirements of this NORSOK standard for the manufacturing steps that the
sub-contractor is performing.
7.4 Quality requirements for test laboratories and manufacturers of welded products
8 Manufacturing Summary
NOTE Sometimes it can be convenient to combine several production routes, type of products and/or grade of materials into one
Manufacturing Summary, e.g. as shown in the flow chart in Annex A.
The Manufacturing Summary shall describe, step by step in a logical and correct sequence, all important
manufacturing activities with reference to detailed procedures. A short description and the main parameters
for each activity shall be included. Each production route shall be illustrated with a flow chart.
If the manufacturer has different plants or different production routes for a product, separate documentation
is required for each of these. If essential parts of the work (e.g. forming, heat treatment, pickling, etc.) are
subcontracted, this shall be identified in the documentation. The documentation shall then include the name
and address of each subcontractor and the relevant documentation from the subcontractor’s equipment and
procedures.
The Manufacturing Summary is the property of the manufacturer. Distribution is at the manufacturer's
discretion.
8.2.1 Scope
The scope of the Manufacturing Summary shall be clearly defined by stating
8.2.2 Content
8.2.2.1 General
The Manufacturing Summary shall include, but not be limited to, the requirements in 8.2.2.2 to 8.2.2.15.
8.2.2.2 The product type and the manufacturer’s requirements (purchasing specification) regarding start
material. Apply especially when semi finished products such as ingot, bar, pipe, plate, strip, etc., are used as
a basis for the manufacture. In such cases the manufacturer of the start material shall also be given.
8.2.2.9 Pickling.
8.2.2.10 Welding (including weld repair). The WPS and PQR applicable for the qualification shall be listed.
For duplex steels in particular more than one etchants may be required for detecting intermetallic phases,
carbides and nitrides.
9 Heat treatment
9.1.1 General
Heat treatment facilities and equipment shall fulfil the requirements in 9.1.2 to 9.1.8. In addition, API 6HT
should be used as a guideline.
9.1.2 Foundries
Foundries shall have heat treatment facilities within their own premises or they shall be located in their close
vicinity.
Furnaces shall be equipped with automatic temperature indicating, controlling and recording devices, which
shall possess an accuracy of ± 1 % of their full scale range.
A temperature uniformity survey of the quality heat treatment furnaces shall be carried out annually in
accordance with API Spec 6A:2010/ISO:2009, Annex M, ASTM A 991 or equivalent and additional
requirements given in Annex B. The initially temperature uniformity survey shall be carried out with maximum
load in the furnace.
Subsequent temperature uniformity surveys may be carried out with empty furnace.
9.1.4 Thermocouples
Thermocouples shall be calibrated and fulfil the requirements of API 6A (Twentieth Edition)/ISO 10423:2009,
Annex M.
Quenching facilities should include provisions for internal cooling for the quenching of products with
penetrating bores such as pipes.
The quenching bath shall be equipped with continuous temperature monitoring/recording devices.
For large components it is recognised that a transfer time of 60 s may be difficult to achieve. In such cases a
longer transfer time may be specifically qualified. Qualification tests shall comprise both thin and heavy
sections of such components as agreed with the Qualifying Company. Details of the extended transfer time
including for, which products it is applicable for, shall be highlighted on the QTR front page.
The transfer time is measured from the time the furnace door is fully open or the furnace roof is fully removed
and until the component(s) is completely submerged into the quenching bath.
9.2.1 General
A specific heat treatment procedure shall be established. Content of the procedure shall as a minimum be as
given in 9.2.2 to 9.2.6.
9.2.3 Loading and unloading of components and transfer between furnace and quenching bath
The following information shall be included:
a) loading temperature, heating rate, set temperature with tolerances and holding- and soaking time;
NOTE For definition of holding- and soaking time see figure in Annex C, 3.1.6 and 3.1.15.
b) cooling details, e.g. cooling medium (water, air, gas or a combination thereof, etc.), type of cooling
(quenching, spraying, etc.), relevant parameters (temperatures of quenching bath, for spraying medium
velocity, type and size of nozzles, etc.);
c) for continuous and semi continuous furnaces: travel speed and minimum soaking time as function of size
(e.g. thickness, diameter, cross section, etc.) of products to be heat-treated and other relevant
parameters.
a) principles for selection of components to be used for production testing within each heat treatment load.
(sketch to be prepared) taking into account that selection should be from the center close to the bottom of
a heat treatment load;
b) description of
1) how traceability of heat and heat treatment lot is ensured throughout the whole heat treatment process,
2) how components within each heat treatment load are identified,
3) how components used for production testing in each heat treatment load are identified.
9.3.1 General
Verification is required of procedures for heat treatment except for stress relieving heat treatment in
accordance with this NORSOK standard.
9.3.2 Objective
The objective of the verification is to ensure that the specified parameters in the established heat treatment
procedure are correct by comparing the readings of the furnace controlling thermocouple and the contact
thermocouples fixed onto the load/components.
After a major re-furbishment of a furnace or after a furnace modification changing the heating parameters, a
new verification shall be carried out.
a) contact thermocouples shall be fixed onto the surface of at least three components which are respectively
located in the middle of the heat treatment load and in two corners of the load diametrically opposite to
each other;
b) for heavier components holes shall be drilled into the components down to mid-thickness and the
thermocouples placed into the holes. The holes should be at least 100 mm from the second surface of the
component. To avoid damaging the components heat sinks may be used, which shall be made from the
same general type of material as the parts being heat treated. The cross section of the heat sink shall be
equal to that of the heaviest cross section of the parts being heat treated and the dimensions such as to
allow for location of the drilled hole as specified above. The number and location of the heat sinks shall be
as specified in a) above;
The definition of “heavier” component varies with the type of component (e.g. plate, pipe, fitting, forging,
casting, etc.) of the component and shall be agreed in each case also taking into consideration the proposed
soaking time in the heat treatment procedure for the component.
c) readings from the contact thermocouples shall be compared with the readings from the controlling
thermocouple of the furnace by superimposing the time temperature curves from the contact
thermocouples onto the curve from the controlling thermocouple of the furnace.
9.3.5 Reporting
A report shall be established identifying the furnace verified, describing the heat treatment load used and
location of thermocouples within the load (photograph). The superimposed time temperature curves from the
contact thermocouples and the controlling thermocouple(s) of the furnace shall be included in the report.
9.3.6 Witnessing
The verification of the heat treatment procedure shall be witnessed by the Qualifying Company, who also
shall sign the final report onto completion of the verification exercise.
a) demonstrate that the proposed manufacturing route and production parameters result in products meeting
the specified requirements,
b) verify that the proposed production test sampling gives results, which are representative of the properties
of the actual components they represent.
10.2.1 General
A change in one or more of the manufacturing parameters stated in 10.2.2 to 10.2.13 requires re-qualification
of the manufacturing process.
a) the manufacturer of start material holds a valid NORSOK M-650 qualification for the specific start material,
b) it can be documented that the specific start material from a manufacturer already has been used in other
qualifications for the same grade of material.
10.2.8 Castings
Change of moulding method typically between
10.2.9 Forgings
Change of the following:
a) change of heat treatment temperature outside the allowable range. The allowable range of heat treatment
temperature shall be within –10 qC to +30 qC from the temperature used for the qualification testing of the
component;
b) change of heat treatment cycle, e.g. from a one step to a two step cycle or vice versa;
c) reduction of holding and/or soak time to a time shorter than that established during the verification of the
heat treatment procedure;
d) change from furnace heat treatment to induction heat treatment or vice versa;
e) change from batch furnace heat treatment to continuous furnace heat treatment or vice versa;
f) for hot finished seamless pipes only: change from furnace heat treatment to direct quench from hot finish
operation or vice versa;
g) change in quench medium from water to polymer, oil, nitrogen, air and similar or vice versa;
h) change in quenching method from quenching in bath to spray quenching or vice versa.
Change or re-furbishment of the heat treatment furnace within the same premises does not require re-
qualification provided the requirements in Clause 9 are fulfilled.
Components for testing should have a section thickness in the upper thickness range specified by the
Manufacturing Summary. Except for castings and open die forgings the components shall be representative
in geometry of what actually shall be manufactured. Castings and open die forgings selected for testing shall
be actual products, i.e. not test blocks. For castings qualification should be carried out on a cored
component, e.g. valve body.
For forged flanges, contour forged valves and similar products where production testing is planned to be
carried out on an integral prolongation such a prolongation shall be integrated in the qualification test forging.
Components for testing shall be from regular production or from test production manufactured according to
the normal manufacturing route and with regular production equipment.
10.3.2 Testing
a) production testing with test sampling as specified in NORSOK M-630: MDSs, other applicable standard
and/or the Manufacturing Summary,
b) additional testing for qualification according to Table 2,
c) for forged flanges, contour forged valves and similar products with integral prolongations testing shall be
carried out on both the prolongation and the product itself.
d) non-destructive testing as specified in NORSOK M-630 and relevant MDSs and/or other relevant material
specifications.
The type of tests to be performed and minimum requirements shall be as specified in NORSOK M-630 and
relevant MDS (or material standard/specification if materials are not covered by a MDS).
NOTE For qualification of dimensions outside the range specified by the respective MDSs special acceptance requirements may be
agreed, e.g. exception to the requirement for the impact test results to be 20 J higher during qualification than the production test
requirements. In such cases this shall be clearly stated onto the QTR front page.
10.3.2.4 Acceptance of production testing from integral prolongations from forged products
To accept production testing to be taken from the prolongation the test results from the prolongation shall be
representative of the properties obtained from the same position of the sacrificial product, e.g. position 1
(TH /2) for flanges.
It is at the discretion of the Qualifying Company to decide what is “representative”, i.e. an acceptable
difference between results from tests located in the prolongation and in the product itself.
Dished heads From over-length of the Tests shall be carried out from the over-length and from the
component. deformed area of the component. For dished heads made of
HIP components Integral test blocks. Testing shall be made from thin and thick sections of a sacrificial
except flanges product. Except for the additional testing test results shall fulfil the
requirements in the respective MDSs . Additional testing
For all materials having section thickness/diameter exceeding 50 mm and requiring impact- or corrosion
testing according to MDS/applicable specifications, additional testing shall be carried out as follows using
specimens located in the mid thickness position (T/2) and at a distance from any second surface of T or at
least 100 mm:
a) impact testing in axial and tangential direction. The minimum absorbed energy shall be minimum
27 J/20 J (average/single values) tested at -46 ºC;
b) corrosion and micro-examination in accordance with the requirements specified by the applicable MDS.
NOTE It is recognized that for certain applications corrosion properties and microstructure in mid-thickness are not important for the
functionality of the component as agreed with purchaser and Qualifying Company. In such cases it may be agreed that the
tests shall be carried out for information only and a note about this shall be included on the QTR front page.
The QTR shall be prepared with a front page with format and content as shown in Annex D.
It is essential that all documentation be accurate, specific and in accordance with this NORSOK standard.
The documentation will otherwise be rejected and thereby also the qualification.
Annex A
(Informative)
Manufacturing Summary front page and example
Plant(s) and location(s): Actual plants, locations and equipment facilities where
this procedure is relevant.
SEAMLESS PIPE
CUTTING
MARKING
EXPANDING
OVALIZATION OVALIZATION
(ELBOWS ONLY)
CALIBRATION RE-HEATING
RE-HEATING
FORMING
(ELBOWS ONLY) QUENCH
EXTRUSION
QUENCHING
CUTTING OF ENDS
HEAT TREATMENT
SAMPLING
MECHANICAL TEST
PICKLING
MACHINING
NDE EXAMINATION
MARKING
FINAL CLEANING
FINAL DOSSIER
PACKING
Annex B
(Normative)
Additional requirements to
API Spec 6A:2010/ISO 10423:2009 , Annex M, and ASTM A 991
B.1 General
Temperature uniformity survey of quality heat treatment furnaces shall be performed according to API Spec
6A:2010/ISO 10423:2009, Annex M, or ASTM A 991 with the following additional requirements:
a) the alternatives of attaching thermocouples to the extremities of each load, see ASTM A 991, Para 1.4, or
the alternative surveying techniques described in ASTM A 991, Para 7.7, are not acceptable as an
alternative to the specified temperature uniformity survey;
b) the temperature uniformity survey shall be carried out at the maximum set point temperature for the actual
materials to be processed in the furnace. The maximum limit of 1 100 ºC stated in ASTM A 991, Para
6.1.1.2, shall not apply;
c) the calibration shall be carried out with maximum load in the furnace. This is to demonstrate that the
required temperature uniformity and the maximum temperature specified can be reached. Subsequent
calibrations, which shall be carried out annually, may be carried out with empty furnace;
d) the documentation of the temperature uniformity survey shall include sketch of the furnace with working
zone of furnace and number and location of thermocouples used for the survey, see API Spec
6A:2010/ISO 10423:2009, Annex M, subclause M 3.3, or ASTM A 991, Paras 8.2.7 and 8.2.8;
a) for furnaces with set point temperature in the working zone above 800 ºC the temperature at any point
shall not vary by more than ± 14 ºC from the furnace set point temperature after the furnace working zone
has been brought up to temperature;
b) for furnaces with set point temperature in the working zone below 800 ºC shall not vary by more than
± 8 ºC from the furnace set point temperature after the furnace working zone has been brought up to
temperature;
c) once the furnace temperature has reached the set point temperature, the temperature of all test locations
shall be recorded at maximum 2 min intervals for at least 10 min. Then readings shall be taken at
maximum 5 min intervals for sufficient time to determine the recurrent temperature pattern of the furnace
working zone for at least 30 min.
B.3 Continuous conveyance and semi continuous conveyance furnaces
The temperature uniformity check may be carried out as verification of the heat treatment procedure, see 9.3.
Annex C
(Informative
Verification of heat treatment procedure – Example
Comparison of time temperature curves of the contact thermocouples (3 off) fixed to the load itself with the
furnace thermocouple. Note the time difference to reach set temperature between the furnace thermocouple
and the contact thermocouples fixed onto the load.
Annex D
(Normative)
Form for Qualification Test Record (QTR) Front Page
This form is available as a word file at the NORSOK home page http://www.standard.no/.
NORSOK M-650
Rev. No.:
Manufacturer
name/address/
Web page:
Reference standard NORSOK M-650, Edition 4
Qualification expires:
The manufacturer and this QTR are evaluated and found to be in compliance with the requirements of
NORSOK M-650 for supply of the above listed products and materials.
This acceptance does not exempt any purchaser from his responsibility to ensure that this qualification is valid
for his products within the essential variables of NORSOK M-650.
Qualified/Accepted by (company name /address): Signature/Date: