KIIT UNIVERSITY

Time: 2Hrs Mid semester Full Marks: 25

Subject: Analytical Instrumentation [EI-701]
Branch: Electronics and Instrumentation Engg.

All the questions are compulsory.

1. (a) What is the basic working principle lying within the concentration measurement by flame [5X1=5
photometer? ]

(b) Why double beam filter photometer is preferred than single beam?
(c) Why infrared spectrophotometer is preferred than filter photometers?
(d) What are the basic parts of emission system in context with flame photometry? What is
the advantage of atomize a fluid before injection in the flame chamber?
(e) What is the basic difference between optical filter, prism and optical grater?
2. (a) Describe the basic working principle of Deflection type O 2 analyzer with a suitable [2.5]
diagram.
(b) How the concentration of a sample solution can be measured Double beam flame [2.5]
photometer instruments? Describe with suitable diagram.
3. (a) What are the basic components of Infrared spectrophotometers? Describe in brief. [5]
4. (a) What are the two processes involved for measurement in Direct Reading [2.5]
Spectrophotometer? Describe with suitable diagram.
(b) What are the sources of error in Spectrophotometric measurements? [2.5]
5. (a) How the concentration in a sample can be measured using Optical Null Method infrared [2.5]
spectrophotometer?
(b) Describe the basic working principle of Double beam Filter Photometer with a suitable [2.5]
diagram.