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International Journal of Rock Mechanics & Mining Sciences 46 (2009) 514–520

Contents lists available at ScienceDirect

International Journal of
Rock Mechanics & Mining Sciences
journal homepage: www.elsevier.com/locate/ijrmms

Dynamic behavior of a Mediterranean natural stone under tensile loading


Domenico Asprone a,, Ezio Cadoni b, Andrea Prota a, Gaetano Manfredi a
a
Department of Structural Engineering, University of Naples ‘‘Federico II’’, Naples, Italy
b
University of Applied Sciences of Southern Switzerland, Lugano, Switzerland

a r t i c l e in f o a b s t r a c t

Article history: Historical buildings are important structures commonly occurring in Mediterranean cities. The behavior
Received 4 April 2008 of their constituent materials under high dynamic loads is fundamental to investigate the vulnerability
Received in revised form of such structures under extreme dynamic events. The main aim of our investigation was to study the
5 August 2008
effect of high dynamic loading conditions on a classical porous natural stone from the Naples area,
Accepted 21 September 2008
namely yellow tuff, used in hundreds of historical buildings and monuments in Naples and other
Available online 12 November 2008
Mediterranean cities. Hence, dynamic characterization was performed through high strain-rate failure
Keywords: tensile tests. A wide range of strain-rates was investigated, from 105 s1 to 50 s1. The obtained data
Porous natural stone were processed to obtain stress–strain relationships at different strain-rate levels. The results reveal
Yellow tuff
that Neapolitan yellow tuff presents a significantly strain-rate sensitive behavior, exhibiting dynamic
Strain-rate
tensile strength increasing with strain-rate, up to about three times that from quasi-static conditions in
Dynamic behavior
Dynamic increase factor the case of very high strain-rates. Dynamic increase factors (DIFs) vs. strain-rate curves for tensile
Tensile strength failure stress were also evaluated and discussed.
& 2008 Elsevier Ltd. All rights reserved.

1. Introduction different loading conditions, such as uniaxial compression [8,9],


uniaxial tension [10] and triaxial compression [11]. Regarding
Investigating the dynamic properties of construction materials tensile loading conditions, it is recognized that natural stones
is a crucial matter for structural engineering. It is widely exhibit higher strength values as the strain-rate increases; this
recognized that structural design and/or assessment of critical behavior is mainly due to microscopic inhomogeneity, affecting
infrastructures or buildings need to allow for particularly severe principally sensitiveness to medium strain-rates, and microcrack
dynamic scenarios which could occur on structures during their formations, interfering failure surface development, which pri-
lifetime (i.e. strong earthquakes and man-made blast events). marily influence the high strain-rate regime [12].
Since the dynamic mechanical properties of materials can differ The present paper discusses the results of an experimental
greatly from those exhibited in quasi-static conditions, specific campaign conducted to investigate the dynamic properties at
investigations in such dynamic ranges appear necessary in order different strain-rates of a classic Mediterranean natural stone,
to fully understand the behavior of structures subjected to high namely Neapolitan yellow tuff (NYT). NYT is a zeolitized tuff, the
dynamic loading conditions. product of a huge eruption dated about 15,000 years ago in the
To date, research has focused on experimental investigation of Campi Flegrei volcanic area west of Naples, which generated
the dynamic mechanical properties of common construction about 50 km3 of material [13]. The mechanical behavior of NYT is
materials, especially concrete and steel which are widely used in similar to that exhibited by several natural stones of the
civil infrastructures [1–7]. However, especially in assessing Mediterranean area that, generated by volcanic eruptions, present
existing structures, such as historical buildings or monuments, common characteristics and composition properties. Such stones
specific knowledge of the dynamic properties of materials used were once widely used in Mediterranean cities as construction
less recently, like masonry, becomes necessary. material, and are thus found in numerous buildings forming part
On the other hand, within rock mechanics literature, a number of the architectural heritage of historical cities, but also in
of studies are available investigating the influence of strain-rate strategic structures. Focusing on one of such stones is unavoid-
on the mechanical properties of different types of rocks. able, due to their wide variability, but the results from the present
Dependence on the strain-rate of natural stones was tested in study can provide interesting data about their dynamic behavior.
Due to its extensive use, the quasi-static mechanical properties
of NYT are well known [14], but no data are available on its
 Corresponding author. Tel.: +39 0817683672; fax: +39 0817683491. behavior under controlled dynamic conditions. Hence, the
E-mail address: d.asprone@unina.it (D. Asprone). objective of our research was to assess the dynamic behavior of

1365-1609/$ - see front matter & 2008 Elsevier Ltd. All rights reserved.
doi:10.1016/j.ijrmms.2008.09.010
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D. Asprone et al. / International Journal of Rock Mechanics & Mining Sciences 46 (2009) 514–520 515

NYT, at different strain-rates, in order to verify its behavior under measurements of Young’s modulus E were conducted on 3
dynamic loading conditions, such as those induced by seismic or specimens 60 mm in diameter and 110 mm high. In the case of
blast actions. NYT is a brittle material with good mechanical 60 mm diameter specimens an average compression failure stress
properties and sufficient workability that make it highly-prized of 3.57 MPa and a standard deviation of 1.15 MPa were obtained
construction material. As might be expected from a natural stone, revealing, according to characterization defined in [15], a medium
NYT is affected by the great variability in its mechanical compression strength tuff. Moreover, results from smaller specimen
characteristics, which may depend on the extraction location or tests (20 mm in diameter) revealed a higher average compression
depth of extraction. NYT is composed by volcanic glass particles failure stress, equal to 5.15 MPa, with a standard deviation of
and lava fragments, giving rise to irregularly shaped grains, whose 0.83 MPa. This was probably caused by a size effect influencing the
size is that of a sandy silt. In this matrix pumix and silica behavior of NYT, which is due to its inhomogeneity at a
fragments are present, whose diameter can vary from less than microscopic scale. Indeed, it is widely accepted that a reduction
3–50 mm [14]. Compression strength of NYT is characterized by in specimen size, in the case of non-homogeneous materials, can
high variability within its different varieties, ranging between 1.62 lead to an increase in strength values experienced [17]. The elastic
and 10.60 MPa, as reported in [15]; however, most commonly used modulus was also measured, following the Swiss standard SIA
NYT presents an average compression strength of 3–4 MPa [15]. It 162/1, obtaining an average value of 2407 MPa, with a standard
can be observed that a medium strength stone is characterized by deviation of 271 MPa.
a compression failure stress fc of about 4 MPa. By contrast, tensile Tensile failure tests were also performed on cylindrical speci-
failure stress ft is characterized by values of one order smaller mens 20 mm in diameter and 20 mm high by means of a universal
than fc [16]. Porosity and saturation represent two important servo-controlled machine with a constant strain-rate of 105. Six
parameters that can influence the mechanical properties of tests were conducted, obtaining an average tensile strength of
natural stones, as widely investigated in the available literature 0.68 MPa, with a standard deviation of 0.15 MPa. Fig. 1 shows a
[17–20]. As both increase mechanical properties generally specimen before and after the test. An average tensile failure
degrade; in particular in the case of NYT, compression strength stress of 0.68 MPa was obtained, corresponding to 13% of the
can be affected by reductions of as high as 36% [15]. Young’s average compression failure stress, obtained for the same-size
modulus E of NYT can vary between 800 and 3000 MPa, with 80% specimens. This value is actually close to values indicated in the
of values over 1000 MPa [15]. Furthermore, the specific weight g is literature which, as reported above, suggests a ratio of about 9%.
also affected by high variability, ranging between 14.6 and Tests were conducted on specimens under ordinary conditions of
17.5 kN/m3 [14]. temperature and humidity. However, to control such aspects, total
Here, a dynamic tensile characterization conducted on an NYT porosity and saturation degree were also determined, obtaining
variety is described. In particular, failure tensile tests at different values of 0.607 and 2%, respectively. A brief consideration about
strain-rates were carried out, ranging between 105 s1, con- the choice of specimen sizes is here provided. As described in the
ducted in quasi-static loading conditions and 50 s1. Static tensile sections below, dynamic tests were conducted on 20 mm diameter
and compression tests were first performed to assess the specimens. Hence, in order to compare dynamic and quasi-static
mechanical properties of the investigated NYT variety. The results regime directly, purging the results of any size effect influence,
obtained are given below. tensile static tests were also conducted on 20 mm diameter
specimens. Furthermore, in order to appreciate the influence of
size effect, compression static tests were conducted on both 60
2. Static characterization of NYT and 20 mm diameter specimens.

A preliminary static characterization was conducted on the


investigated NYT. Five compression failure tests were performed 3. Dynamic tests on NYT
on 60 mm-high cylindrical specimens with a diameter of 60 mm
and the same number of tests were conducted on cylindrical Tensile failure tests were conducted, in the DynaMat labora-
specimens 20 mm in diameter and height. Moreover, three tory of the University of Applied Sciences of Southern Switzerland,

Fig. 1. Specimen before (a) and after (b) a static tensile failure test.
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Fig. 2. HPM functioning scheme.

on NYT specimens, investigating medium strain-rate and high Table 1


strain-rate. The former, commonly considered as ranging between Results of medium strain-rate tensile failure tests
101 and 10 s1, can be induced by severe seismic actions, while
Strain-rate Specimen ft (MPa) ft average ft standard
the latter, varying between 10 and 102 s1, can be due to impact or (s1) value (MPa) deviation (MPa)
blast loading. Two different experimental setups were used. For
medium strain-rate tests a hydro-pneumatic machine (HPM) was 101 1 0.97 0.86 0.22
employed, whereas a modified Hopkinson bar (MHB) [21,22] 2 1.10
3 1.04
apparatus was used to conduct high strain-rate tests. In both cases 4 0.53
the specimens were cylindrical, with a diameter of 20 mm and a 5 0.71
height of 20 mm. 6 0.82

5 7 0.79 1.19 0.32


8 1.09
3.1. Medium strain-rate tests 9 1.42
10 1.34
11 0.75
In the medium strain-rate range, six tests were conducted at a
12 1.34
strain-rate level of 101 s1 and seven at a strain-rate level of 5 s1. 13 1.60
The HPM functioning scheme is presented in Fig. 2. At the
beginning of the test, a sealed piston divides a cylindrical tank
into two chambers, one being filled with gas at high pressure transducers, sensing the displacement of the plate target fixed
(e.g. 150 bars), the other with water. At first, equal pressure is to both specimen ends. Such acquisitions allow the stress vs.
established in the water and gas chambers so that forces acting on strain relationship to be obtained at the strain-rate level reached
the two piston faces are in equilibrium. The test starts when the during the test. Results of the conducted tests are presented in
second chamber discharges the water through a calibrated orifice, Table 1. It can be observed that average tensile failure stresses of
activated by a fast electro-valve. Then the piston starts moving, 0.86 and 1.19 MPa were obtained for strain-rates of 101 and 5 s1,
expelling the gas through a sealed opening; the end of the piston respectively. These values are slightly higher than quasi-static
shaft is connected to the steel specimen. The specimen is linked to tensile failure stress, revealing the strain-rate sensitivity of NYT,
the piston shaft and to one end of an elastic bar, whose other end even at medium strain-rate conditions.
is rigidly fixed to a supporting structure. When the piston shaft
moves, the specimen is pulled at a fixed strain-rate level,
depending on the velocity of the gas expelled from the chamber. 3.2. High strain-rate tests
The elastic bar is instrumented with a strain-gauge that provides,
through the elastic properties of the bar, the force acting on the In the high strain-rate range three tests were conducted at
specimen during the test. Two targets are attached on both ends both the 20 s1 and 50 s1 strain-rate level. To conduct these tests
of the specimen and their movements are measured by two the MHB apparatus in Fig. 3 was employed. The machine consists
contact-less displacement transducers. of two longitudinally aligned aluminum bars 20 mm in diameter,
It can be shown that movement of the piston at a constant the namely input bar (3 m long) and output bar (6 m long). The
speed guarantees the constancy of the strain-rate during the test; specimen with the same diameter as the input and output bar is
this depends mainly on the constancy of the force exerted by the located between them, glued using a high-strength epoxy resin. A
gas pressure on the piston face. A good result in this sense was high-strength steel pretension bar 6 m long and 12 mm in
obtained with a small change in gas volume during the test in diameter is directly connected to the input bar and used to store
order to have a small gas pressure decrease and hence a small elastic energy, which is provided by a hydraulic actuator at one
piston force decrease. Furthermore, load P resisted by the end of the bar and is resisted by a blocking device at the other. The
specimen is measured by the dynamometric elastic bar, whereas diameter of the pretension bar was chosen to have the same
specimen elongation DL is measured by the displacement acoustical impedance of the aluminum input bar so that
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D. Asprone et al. / International Journal of Rock Mechanics & Mining Sciences 46 (2009) 514–520 517

Fig. 3. Modified Hopkinson bar apparatus.

undesired wave reflections were avoided [5]. Then the stored Table 2
energy is instantaneously released to the input bar, causing a Results of high strain-rate tensile failure tests
tensile wave to travel in it; this wave hits the specimen and is then
Strain-rate Specimen ft (MPa) ft average ft standard
divided into a reflected part, coming back in the input bar, and a (s1) value (MPa) deviation (MPa)
transmitted part, passing into the output bar. This phenomenon
leads the specimen to failure. The strain-gauge station, located on 20 14 1.77 1.71 0.44
the input bar and on the output bar (symmetrically placed at 15 1.25
16 2.12
900 mm from the specimen) allows the strain histories to be
acquired with which, according to one-dimensional elastic wave 50 17 2.03 1.97 0.32
propagation theory [5], the stress vs. strain curves may be 18 1.63
19 2.26
obtained for the strain-rate level reached. The stress, strain and
strain-rate are obtained by the following equations:

A0
sðtÞ ¼ E0 T ðtÞ (1)
A 3
Z t
2C 0 50 s-1
ðtÞ ¼  R ðtÞ dt (2)
L 0
2.5 20 s-1

2C 0
0 ðtÞ ¼  R ðtÞ (3)
L
2
where E0 is the elastic modulus of the bars, equal to 69 GPa; A0 is
stress [MPa]

their cross-section area, equal to 314 mm2; A is the specimen


cross-section area, equal to 314 mm2; eT is the transmitted strain
measured in the output bar; L is the specimen, 20 mm long; C0 is 1.5
the sound velocity of the bar material, 5064 m/s; and eR is the
reflected strain measured in the input bar.
Further details about the test setup and data processing are 1
available in [23]. Results of the conducted tests are reported in
Table 2, revealing an average tensile failure stress of 1.71 and
1.97 MPa for a strain-rate level of 20 and 50 s1, respectively. In 0.5
Fig. 4, two stress vs. time curves at 20 and 50 s1 are depicted. It
can be observed that, as the strain-rate increased, the specimens
were able to withstand higher forces before reaching failure, 0
but time to fracture reduced at higher strain-rates. Accordingly, 0 1 10-5 2 10-5 3 10-5 4 10-5 5 10-5
Table 3 reports time to fracture both for medium and high strain-
time [s]
rates, revealing a marked reduction varying from lower strain
rates to higher ones. Fig. 4. Stress vs. time curve for the two high strain-rates.
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Table 3
Time to fracture, DIF for tensile failure stresses and energy characteristics

Strain-rate (s1) Time of fracture (s) Experimental DIF,ft CEB formulation DIF,ft Fracture energy GF (J/m2) Characteristic length lc (mm)

105 – – – 18.30 151.0


101 7  103 1.26 2.4 – –
5 9  104 1.75 3.3 – –
20 28  106 2.51 3.7 21.88 24.5
50 20  106 2.90 4.6 29.66 18.0

4. Assessment of experimental results 2.5

Experimental data were processed to obtain stress vs. crack 50 s-1


opening displacement curves at different strain-rates. Fig. 5 shows 20 s-1
2 5 s-1
some of the curves obtained for each of the investigated strain- 10-1 s-1
rates, compared with those obtained from quasi-static loading 10-5 s-1
conditions, indicated with a strain-rate of 105 s1. It can be
observed that as the strain-rate increases, so does ultimate failure
stress. By contrast, the corresponding crack opening displacement 1.5

stress [MPa]
does not change its value significantly, except for 50 s1, where
fracture occurs at a lower strain value. In particular, crack opening
displacements were obtained by direct measurement of the
displacement transducers in the case of medium strain-rate tests, 1
conducted via HPM, and from Eq. (2) multiplying strain by the
specimen length, in the case of high strain-rates, conducted via
MHB. The increase in the ultimate stress and the decrease in the
strain at failure indicate that as the strain-rate increases, the 0.5
material assumes a more brittle behavior. Moreover, Fig. 6 depicts
the strain histories measured by the input strain-gauge during high
strain-rate tests, distinguished into two curves (20 s1 and at 50 s1
of strain-rate). The figure shows how different pre-loads, used to 0
obtain different strain-rates, generate different velocities of the 0 0.05 0.1 0.15 0.2
tests; this is observable in the slopes of the initial and final parts, COD [mm]
representing the transmission and the reflection of the strain wave,
Fig. 5. Stress vs. COD curves at different strain-rates.
respectively, which are higher as the strain-rate increases.
In order to appreciate the improved strength under dynamic
loading conditions the results of the average tensile failure stresses
were processed in terms of dynamic increase factor, DIF,ft, defined 0.0006
as the ratio of the dynamic values of the tensile failure stress to the input strain (20 s-1) NYT
static one. The results in Table 3 were thus obtained, revealing a input strain (50 s-1)
maximum DIF,ft equal to 2.90, in the case of a strain-rate of 50 s1. 0.0005
These data were then processed depending on the strain-rate in
logarithmic scale, obtaining the curve depicted in Fig. 7. As
expected, this figure reveals a behavior similar to that experienced 0.0004
in the case of brittle ceramic materials, like concrete. In the case of ε (50 s-1)
input strain

R
concrete, in fact, DIF,ft dependence on the strain-rate level in
ε (50 s-1)

logarithmic scale presents two different slopes for medium strain- 0.0003
rate and high strain-rate and the variation of the gradient is located
I

at about 1 s1 [2,3]. In the first case, the increase in strength is due
to moisture content, involving viscosity mechanisms, whereas for 0.0002
high strain-rates inertia effects in cracking propagation become ε (20 s-1)
R
ε (20 s-1)

sizeable, providing further resistance [2,3,24]. In the present case, a


two-segment trend-line was also drawn, revealing a knee located at 0.0001
about 2.2 s1 of strain-rate.
I

Unfortunately, no specific formulations were found in the


literature on natural stones. However, given the similarities 0
described above with the behavior of concrete and given that 0 0.0001 0.0002 0.0003 0.0004 0.0005
both concrete and NYT are brittle ceramic materials presenting a time [s]
certain level of porosity and water content, formulation provided
in [2] was employed. This relationship, namely CEB formulation, Fig. 6. Input strain history at different strain-rates.

actually elaborated for concrete, allows the dynamic tensile


 1=3
strength to be evaluated at a given strain-rate level, starting from _
static mechanical properties. It allows prediction of DIFft as:
DIF; f t ¼ Z for _ 430 s1 (5)
_ 0
 1:016d
_ where _ is the strain-rate; _ 0 is a constant equal to 3  106 s1
DIF; f t ¼ for _ p30 s1 (4)
_ 0 and has the meaning of the static strain-rate; and
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5.00 lead to higher spread of results in medium and high strain-rate


Average values tests compared to quasi-static tests.
4.50
Experimental data Finally, in order to compare the results usefully with those of
4.00 Trend line other experimental campaigns considering loading-rate instead of
CEB formulation strain-rate, conversion values from strain-rates to loading-rates
3.50 need to be provided. In particular, strain-rates of 101, 5, 20 and 50
3.00 correspond to loading-rates of 0.1, 1.2, 80 and 180 GPa/s,
DIF, ft

respectively.
2.50

2.00
5. Conclusions
1.50
In this work, a dynamic characterization of NYT under tensile
1.00
loading was presented. NYT is a natural stone, widely used in the
0.50 2.2 Naples area as construction material and found in many
important historical buildings and monuments in the city.
0.00 Preliminary analyses were conducted, revealing static mechanical
0.00001 0.0001 0.001 0.01 0.1 1 10 100
properties and porosity and saturation degrees of the investigated
-1
Strain rate [s ] material. Then dynamic tensile failure tests were conducted on
NYT samples, at given strain-rate levels, ranging between 101
Fig. 7. DIF,ft vs. strain-rate experimental data.
and 50 s1. The tests were conducted using a Hydro-pneumatic
machine for medium strain-rates and a modified Hopkinson bar
log Z ¼ 7:11d  2:33, where d ¼ 1=½10 þ 6ðf c =f 0 Þ, fc is the static apparatus for high strain-rates. Experimental analyses revealed
compression strength; and f0 is a constant equal to 10 MPa that the investigated NYT, under high strain-rate conditions, is
(1450 psi). able to withstand tensile forces about three times those resisted in
This relationship was then used in an attempt to predict the static conditions. Such results indicate that NYT under tensile
experimental values of DIF,ft via numerical elaboration. To do so, loading conditions is strain-rate sensitive. We then sought to
the static compression strength was assumed equal to 3.57 MPa, reproduce our results in terms of DIF,ft, via the CEB relationship for
as obtained from the preliminary static tests. Results in Table 3 tensile strain-rate sensitivity of concrete, given the similarities
were found, whereas Fig. 7 depicts the obtained curve on the that NYT presents with concrete. However, the CEB formulation
experimental data. It can be observed that CEB formulation applied to the investigated NYT strongly overestimates the
overestimates the experimental results, providing higher values of experimental data.
DIF,ft. This was actually expected since CEB formulation was Hence, it appears necessary that further mechanical dynamic
calibrated for concrete, presenting higher static compression characterization under tensile loading conditions needs to be
strength. conducted, also accounting for size effect, in order to obtain
Furthermore, in order to quantify energy dissipation involved further data and calibrate a specific relationship for NYT.
in the failure mechanisms of the investigated material under Furthermore, the influence of water content on the dynamic
uniaxial tensile loading, fracture energy GF dissipated during both behavior of NYT requires investigation, given its importance in
static and dynamic tests was computed; Table 3 reports the determining static mechanical properties of NYT. Hence, further
average values for high strain-rate and quasi-static regimes. tests are being carried out to replicate the conducted experi-
Fracture energy is represented by the area under the stress-crack mental campaign on completely dry and completely wet NYT
opening displacement curve and, as it might be expected, it samples.
revealed an increasing trend with strain-rate. However, this
increase in fracture energy cannot be attributed to a correspond-
Acknowledgments
ing increase in ductility, since fracture energy does not distinguish
ductility from brittleness. In order to appreciate ductility and
brittleness contributions, data were elaborated to obtain the The authors are grateful to Matteo Dotta, Daniele Forni and
characteristic length lc [25], defined as Samuel Antonietti of the University of Applied Sciences of
Southern Switzerland for their collaboration in carrying out
EGF laboratory tests.
lc ¼ 2
(6)
ft
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