Professional Documents
Culture Documents
PREVIEW
This PREVIEW contains mainly the software documentation for the usage of theTC1 & TD4.
TC1
Ring/Plate Tensiometer
LMT 870
TD4
Automatic Tensiometer
LMT 860
Version 00/00/00
LAUDA Scientific GmbH
Postfach 1251
97922 Lauda-Königshofen
Germany
Phone: (+49) 09343/ 503-0
Fax: (+49) 09343/ 503-222
e-mail info@lauda-scientific.de
Internet http://www.lauda-scientific.de
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Table of contents
Table of contents.............................................................................................................................3
List of figures...................................................................................................................................5
List of tables ....................................................................................................................................5
1 Safety information ....................................................................................................................6
1.1 General safety information .................................................................................................6
1.2 Other safety information.....................................................................................................6
1.3 Special symbols..................................................................................................................6
2 Brief instructions.......................................................................................................................7
2.1 Brief description and application ........................................................................................7
3 Controls and functional elements .............................................................................................9
4 Device description ..................................................................................................................10
4.1 Ambient conditions ..........................................................................................................10
4.2 Measurement methods .....................................................................................................10
4.3 Installation of TC1 / TD4 ..................................................................................................10
4.4 Tensio.Touch ...................................................................................................................11
4.4.1 Status bar.................................................................................................................11
4.4.2 Function bar .............................................................................................................12
4.4.3 Process control ........................................................................................................12
4.4.4 Interaction ................................................................................................................12
5 Login ......................................................................................................................................13
6 Home .....................................................................................................................................13
7 Measurement .........................................................................................................................13
7.1 Measurement with the Du Noüy ring .................................................................................14
7.1.1 Surface Tension (SFT) .............................................................................................14
7.1.2 Surface tension pull-through (SFT pull-through) .......................................................15
7.1.3 Surface tension time (SFT time) ...............................................................................15
7.1.4 Interfacial Tension (IFT) ...........................................................................................16
7.1.5 Interfacial tension pull-through (IFT pull-through) .....................................................17
7.2 Measurement with the Wilhelmy plate ..............................................................................18
7.2.1 Surface Tension (SFT) .............................................................................................18
7.3 Utilities ............................................................................................................................19
7.3.1 Weight......................................................................................................................19
7.3.2 Density .....................................................................................................................20
7.3.3 Check balance .........................................................................................................21
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7.3.4 Clean ring.................................................................................................................21
7.3.5 Clean plate...............................................................................................................21
7.3.6 Clean vessel ............................................................................................................21
8 Results ...................................................................................................................................22
9 Configuration..........................................................................................................................22
9.1 Method ........................................................................................................................22
9.1.1 Edit ring geometries .................................................................................................22
9.1.2 Edit plate geometries................................................................................................23
9.1.3 Norm methods..........................................................................................................23
9.1.4 User specific measurement methods .......................................................................23
9.1.5 Printer configuration .................................................................................................23
9.2 System ........................................................................................................................24
9.2.1 Measurement configuration ......................................................................................24
9.2.2 Language .................................................................................................................25
9.2.3 Time/Date ................................................................................................................25
9.2.4 User level .................................................................................................................25
9.2.5 About .......................................................................................................................25
9.3 Data.............................................................................................................................26
9.3.1 Log...........................................................................................................................26
9.3.2 Backup.....................................................................................................................26
10 Popup .................................................................................................................................27
10.1 Alerts ...........................................................................................................................27
10.2 Set temperature ...........................................................................................................27
10.3 Manual platform control ...............................................................................................27
10.4 Abort measurement .....................................................................................................28
10.5 Edit ring geometries.....................................................................................................28
10.6 Edit plate geometries........................................................................................................28
10.7 Adjusting of weighing system.......................................................................................28
10.8 Adjust density ..............................................................................................................29
10.9 Filter measurement methods .......................................................................................29
10.10 Save user specific measurement method.................................................................29
10.11 User management....................................................................................................29
10.11.1 Add user ...............................................................................................................29
10.11.2 Edit user ...............................................................................................................30
10.12 Keyboard..................................................................................................................30
10.12.1 Enter text ..............................................................................................................30
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10.12.2 Enter numbers ......................................................................................................31
10.13 Edit user specific methods parameter ......................................................................31
10.14 Import norm method .................................................................................................31
11 Update firmware .................................................................................................................32
12 Quick start ..........................................................................................................................33
13 Parameter description.........................................................................................................35
14 Appendix.............................................................................................................................36
14.1 Reference values for checking the TC1 / TD4.....................................................................36
14.2 Disposal of packaging .......................................................................................................36
14.3 Technical data..................................................................................................................37
14.4 Order numbers and accessories ........................................................................................38
14.5 References .......................................................................................................................39
List of figures
Figure 1: Tensio.Touch home screen ...............................................................................................11
Figure 2: Status bar ........................................................................................................................11
Figure 3: Function bar ....................................................................................................................12
Figure 4: Process control ................................................................................................................12
Figure 5: Keyboard text ..................................................................................................................30
Figure 6: Keyboard numbers...........................................................................................................31
Figure 7: Update firmware start ......................................................................................................32
Figure 8: Update firmware process..................................................................................................32
List of tables
Table 1: Functions of function bar buttons.......................................................................................12
Table 2: Alerts ................................................................................................................................27
Table 3: Parameter description of measurement parameters............................................................35
Table 4: Parameter description of configuration parameters ............................................................35
Table 5: Surface tension reference values, [mN/m] ..........................................................................36
Table 6: Interfacial tension referred to water reference values, [mN/m] ...........................................36
Table 7: Disposal of packaging ........................................................................................................36
Table 8: Technical data ...................................................................................................................37
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1 Safety information
1.1 General safety information
Surface and interfacial tension are determined with a tensiometer. It may be necessary to stabilise
the temperature of samples to be tested. Hazards arise from this due to high or low temperatures,
fire and the general hazards due to the application of electrical energy. The user is extensively
protected by the application of the relevant standards. Further hazard sources can arise from the
type of material for which the temperature is to be stabilised or from the sample to be measured,
e.g. on exceeding or undercutting certain temperature thresholds or with the fracture of the con-
tainer and reaction with the tempering liquid.
It is not feasible to include all possible situations. They remain essentially subject to the judgement
and responsibility of the operator.
The devices may only be used as intended, that is as described in this operating manual. This in-
cludes operation by instructed specialist personnel.
The devices are not designed for use under medical conditions according to DIN EN 60601-1 or
IEC601-1.
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2 Brief instructions
These brief instructions are intended to give you a quick introduction to the operation
of the device. However, for the safe operation of the tensiometer it is essential to read
the instructions completely and carefully and to follow the safety information.
It is possible to carry out a wide variety of measurement tasks by using the most varied test probes
in conjunction with precise weighing technology and high quality electronics.
In case of surface and interfacial tension the following test probes specified according to ASTM
D971 and DIN 53914 are used:
The Wilhelmy platinum plate.
The du Noüy platinum/iridium ring.
When using the Lauda PTT+ Peltier Thermostating Unit with internal stirrer, measurements over a
temperature range of 5-80°C can be carried out.
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Determination of surface and interfacial tension of liquids
The measurement of surface and interfacial tension is carried out using the Wilhelmy plate or du
Noüy ring method. The vertical force is measured which is exerted on the test probe by the surface
or interface of the liquid.
An especially sensitive, displacement-free measurement system is required to acquire this force. A
force measurement system of this type is the main constituent component of the TC1 / TD4 meas-
urement console. This is achieved through electromagnetic compensation in the force transferred
via the test probe onto a measuring beam. An optoelectronic detector supplies the position deter-
mination of the measuring beam needed for displacement-free measurement.
In the case of measurement with the du Noüy ring, the TC1 / TD4 facilitates the up and down
movement of the sample table, which is required for acquiring the maximum force, through a lim-
ited force range defined by the user.
When using the Wilhelmy plate, the table movement stops immediately once the measurement
system has registered contact between the plate and the liquid.
After entering the measuring parameters, such as measurement method, number of tests, stability
criteria (standard deviation), the measurement can be started by the press of a button. To raise or
lower the test liquid without vibration the TD4 has a motor-controlled sample table which enables
the necessary vibration-free table movement at a speed specified by the user.
Density measurement
The determination of the density occurs by dipping a suitable sample probe, previously tared in air,
into the liquid to be measured. The measured upthrust corresponds to the weight of the displaced
liquid. If the volume of the buoyancy probe is known, the density can be directly determined.
Weight measurement
The sample to be measured can be attached, either directly or indirectly using a suitable holder, to
the hook on the measurement system and its weight determined.
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3 Controls and functional elements
1 Measurement console
2 Sample
3 Platform
4 Tensio.Touch
5 Type plate
8 Power supply
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4 Device description
4.1 Ambient conditions
The use of the tensiometer is only admissible under the conditions specified in DIN EN 61010-
2010:2003 and DIN EN 61010-1:2001:
Plate measurement
Measurement of the surface and interfacial tensions by the Wilhelmy method using a Pt/Ir plate
specified according to DIN 53914, ASTM D971 and other standards.
Ring measurement
Measurement of the surface and interfacial tensions by the du Noüy method using a Pt/Ir ring
specified according to DIN 53914, ASTM D971 and other standards.
Weight measurement
Measurement of small weights (max. 5 g).
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4.4 Tensio.Touch
The Tensio.Touch is the central user interface of the TC1 / TD4.
Status bar
Process control
Interaction
Function bar
Figure 1: Tensio.Touch home screen
The basic screen consists of four main screen parts (see Figure 1). The following chapters explain
the four parts in detail.
The text on the left side contains the navigation information. In the middle of the status bar you can
see the username of the current logged in user. The temperatures show the actual and the set
temperature of the sample, when the optional PTT+ is connected. The right side contains the time
and the date.
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4.4.2 Function bar
1 2 3 4 5 6 7 8
Figure 3: Function bar
The function bar contains the most important buttons for the usage of the device. The picture
shows all possible function bar-buttons. They are shown or hidden in dependence of their necessi-
ty. The function of each button is explained in the following table:
5. Light-blue colored tabs are not selected at the moment, but you can se- 3
lect them
6. Dark-blue colored tabs are already selected and have no interaction pos-
sibilities 4
7. Grey tabs are inactive and therefore not selectable
Figure 4: Process
control
4.4.4 Interaction
This screen part is reserved for interactions. All inputs are done within this screen area.
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5 Login
Login
The login screen shows the selectable user names in a drop-down menu. Every saved user has
his own priority level (Technician, Supervisor or Admin) and password. You may use the „No
Login“-button to login as “Technician” with the lowest priority level or login with your name and
password by tapping the „Login“-button.
6 Home
Home
The home-screen contains no interaction functions. It is the starting point where you may return to
from nearly every other screen using the „Home“- button on the bottom right side of the screen.
You also get to the home-screen after the login-screen.
7 Measurement
Home Method
This screen allows you to select a measurement method. When you are logged in with the user
level “Supervisor” or “Admin”, you may choose from all available measurement methods.
Being logged in with the lowest priority level “Technician”, you are only able to choose from previ-
ously saved user specific measurement methods.
Assuming you are logged in with a higher priority level than “Technician”, the screen is mainly di-
vided into the tabs “Ring”, “Plate”, “Norm”, “User specific” and “Utilities” whereby each subtab con-
tains several measurement methods.
Ring
This subtab contains all measurement methods according to the Du Noüy ring (see 7.1).
Plate
This subtab “Plate” contains all measurement methods according to the Wilhelmy plate (see 7.2).
Norm
The subtab “Norm” contains measurement methods according to the most important norms, where
you have the possibility to choose between eight different methods. Furthermore you may
hide/show specific methods in the configuration menu (see Norm methods).
User specific
The subtab “User specific” contains measurement methods that were specified by a user before.
The user specific measurement methods are user defined methods that are derived from given
measurement methods. When the amount of the saved measurement methods exceeds the num-
ber of eight visible buttons, the „Left“- and „Right“-arrow buttons are activated. This allows you to
have an unlimited amount of saved measurement methods.
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Utilities
The subtab “Utilities” contains methods for measuring the density or weight. Furthermore you may
check the balance of the weight system or let you guide through the correct cleaning of the Du
Noüy ring or the glass vessel by tapping the button “Clean ring” or “Clean vessel”.
1. Set parameter: Predefined recommended parameters for measuring water. If you have any
other liquid, edit the parameters by tapping the related edit fields
2. Test preparation: A guideline to prepare a measurement correctly
3. Measurement: The measurement progress
Set parameters
The predefined parameters are loaded automatically after choosing the measurement method.
When the parameters are changed, they will be saved until the device will be switched off and on
again or another measurement method is chosen.
After selecting the surface tension method, the device shows the automatically loaded parameter
values. The red framed box is a mandatory field and has to be set whereas any other box may be
edited, if needed. The ring geometry can be chosen from three predefined geometries by using the
drop-down menu. The parameters of the chosen ring geometry are shown in the same box. The
function bar contains, among other buttons, the „Save“- button for saving the parameters to a user
specific measurement method and the “>” button to go over to the test preparation. These buttons
are greyed out, as long as the mandatory field “Sample ID” is empty.
Test preparation
The test preparation guides you to the start of the measurement. The first step of the preparation is
to insert the glass vessel with the sample fluid. After inserting the sample glass and confirming with
the „>“- button, the Du Noüy ring has to be mounted on the hook of the measurement system. The
guideline shows that in a separate screen.
Tap the „>“- button to confirm the mounting of the ring and to get to the taring screen, where the
device automatically begins to tare the weighing system. This is done every time before measure-
ment is started. As long as the environment is not stable enough for the set sensitivity of the weigh-
ing system, the device will wait. When the stability is reached, the label “Unstable” switches to
“Stable” and taring of the weighing system succeeds. A successful taring also activates the
„START“- button and the „<“- button. It is also possible to abort the taring procedure by tapping the
„Abort“- button and start the measurement without taring the measurement system, but it is not
recommended. After aborting the taring procedure it is also possible to restart it.
The “Delay”-field shows the time, that will be waited after tapping the „START“- button to delay the
start of the measurement. The value may be edited in the system settings (see 9.2).
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Measurement
The measurement screen is divided into three main parts. The labels on the left side show the
measured live values of the force, the lamella height, the speed of the platform and the calculated
surface tension. Furthermore the expired measurement time can be seen. The diagram on the right
side shows the measured force over time. It is very important to see what is going on during a
measurement. By tapping the „Data“- button in the function bar, the diagram-view is switched to
the table view, where every force-maximum can be seen with a timestamp, the calculated surface
tension, the standard deviation and the temperature.
Measurement process
With the start of the measurement, the TD4 begins automatically to search the surface. After hav-
ing found the surface, the position is saved and the ring is immersed 2 mm into the liquid. When
this position is reached, the platform changes its movement direction and pulls out the ring of the
liquid while measuring the force. When the maximum of the force is reached, the movement direc-
tion of the platform changes again and pulls the ring back into the liquid. This movement is
stopped, when the maximum return value is reached. The measurement is stopped until the pause
time has expired and the system pulls the ring out of the liquid again measuring the force. This will
be repeated until the calculated standard deviation falls below the standard deviation that was giv-
en in the “Set parameters”-section. Thus, the measurement finishes and the system will wait for the
confirmation with the appearing „OK“- button to switch to the results view.
The measurement can be aborted by tapping the „Abort“- button and confirming the decision in the
appearing popup.
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7.1.4 Interfacial Tension (IFT)
Set parameters
The predefined parameters are loaded automatically after choosing the measurement method.
When the parameters are changed, they will be saved until the device will be switched off and on
again or when another measurement method is chosen.
After selecting the interfacial tension method, the device shows the automatically loaded parameter
values. The red framed box is a mandatory field and has to be set whereas any other box may be
edited, if needed. The ring geometry can be chosen from three predefined geometries by using the
drop-down menu. The parameters of the chosen ring geometry are shown in the same box. The
function bar contains, among other buttons, the „Save“- button for saving the parameters to a user
specific measurement method and the “>”- button to go over to the test preparation. These buttons
are greyed out, as long as the mandatory field for “Sample ID” is empty.
Test preparation
The test preparation guides you to the start of the measurement. The first step of the preparation is
to insert the glass vessel with the light solvent phase fluid.
After inserting the sample glass and confirming this with the „>“- button, the Du Noüy ring has to be
mounted on the hook of the measurement system.
Tap the „>“- button to confirm that and switch to the next step. Here the device automatically im-
merses the ring into the light solvent phase liquid detecting and saving the surface position.
You may abort the immersing by tapping the „Abort“- button, but it is necessary that the platform
will be moved down manually until the ring is outside of the liquid after an abort. This has to be
done, because the device searches for the surface while immersing the ring. When the ring is al-
ready immersed, the platform will move upwards until it reaches the highest point allowed.
When the ring is immersed successfully, you have to cover the light phase with the heavy phase
carefully and confirm it by tapping the „>“- button. This leads to the taring-step, which is the last
preparation step before the measurement can be started.
Taring of the weighing system must be done within both phases. It is done automatically after the
confirmation of the coverage of the light phase covering by the heavy phase.
As long as the environment is not stable enough for the set sensitivity of the weighing system, the
device waits. When the stability is reached, the label “Unstable” switches to “Stable” and taring of
the weighing system succeed. A successful taring activates the greyed-out „START“-button and
the „<“- button. It is also possible to abort the taring procedure by tapping the „Abort“- button and
start the measurement without taring the measurement system, but it is not recommended. After
aborting the taring procedure it is also possible to restart it.
Measurement
The measurement is divided into three main parts. The labels on the left side show the measured
live values of the force, the lamella height, the speed of the platform and the calculated surface
tension. Furthermore the expired measurement time can be seen. The diagram on the right side
shows the measured force over time. It is very important to see what is going on during a meas-
urement. The third important part is the table with the measured results. By tapping the „Data“-
button in the function bar, the diagram-view is switched to the table view, where every force-
maximum can be seen with a timestamp, the calculated surface tension, the standard deviation
and the temperature.
16
Measurement process
With the start of the measurement, the TD4 begins automatically to pull out the ring of the light
liquid while measuring the force. When the maximum of the force is reached, the movement direc-
tion of the platform changes and pulls the ring back into the light liquid. The lamella in an interfacial
tension measurement is very sensitive. Hence the speed of pulling back the ring into the light liquid
is highly increased to make sure that the lamella cannot break. This movement is stopped, when
the maximum return value, that was typed in in the “Set parameters”-section, is reached. Then the
system waits until the pause time expires and pulls the ring out of the liquid again while measuring
the force. This will be repeated until the set standard deviation is reached.
As soon as the calculated standard deviation falls below the standard deviation that was given in
the “Set parameters” section, the measurement finishes and the system will wait for the confirma-
tion with the appearing „OK“- button to switch to the results view.
The measurement can be aborted by tapping the „Abort“- button and confirming the decision in the
appearing popup.
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7.2 Measurement with the Wilhelmy plate
Home Method Plate
Set parameters
The predefined parameters are loaded automatically after choosing the measurement method.
When the parameters are changed, they will be saved until the device will be switched off and on
again or when another measurement method is chosen.
After selecting the surface tension method, the device shows the automatically loaded parameter
values. The red framed box is a mandatory field and has to be set whereas any other box may be
edited, if needed. The plate geometry can be chosen from three predefined geometries by using
the drop-down menu. The parameters of the chosen plate geometry are shown in the same box.
The function bar contains, among other buttons, the „Save“- button for saving the parameters to a
user specific measurement method and the „>“- button to go to the test preparation. These buttons
are greyed out, as long as the mandatory field for “Sample ID” is empty.
Test preparation
The test preparation guides you to the start of the measurement. The first step of the preparation is
to insert the glass vessel with the sample fluid.
After inserting the glass vessel and confirming it with the „>“- button, the Wilhelmy plate has to be
mounted on the hook of the measurement system. Tap the “>”- button to get to the taring screen,
where the system begins automatically to tare the weighing system. This is done every time before
a measurement is started.
As long as the environment is not stable enough for the set sensitivity of the weighing system, the
device waits. When the sensitivity is reached, the label “Unstable” switches to “Stable” and the
taring procedure of the weighing system succeeds. It is also possible to abort the taring procedure
by tapping the „Abort“- button and start the measurement without taring the measurement system,
but it is not recommended. After aborting the taring procedure it is also possible to restart it.
A successful taring or the abort of the taring procedure activates the „START“- button and the „<“-
button.
The “Delay”-field shows the time, that will be waited after tapping the „START“- button to delay the
start of the measurement. The value may be edited in the system settings (see 9.2).
Measurement
The measurement is divided into three main parts. The labels on the left side show the measured
live values of the force, the lamella height, the speed of the platform and the calculated surface
tension. Furthermore the expired measurement time can be seen. The diagram on the right side
shows the measured force over time. The diagram is very important to see what is going on during
a measurement. The third important part is the table with the measured results. By tapping the
„Data“- button in the function bar, the diagram-view is switched to the table view, where every
force-maximum can be seen with a timestamp, the calculated surface tension, the standard devia-
tion and the temperature.
Measurement process
With the start of the measurement, the TD4 begins automatically to search the surface of the liquid.
When the plate touches the liquid, the point is detected by the weighing system and saved as the
18
surface position. The plate is immersed 2 mm into the liquid to ensure that the whole area of the
plate is moistened, what increases the precision of the measurement. When the plate is mois-
tened, the platform changes its movement direction and pulls out the plate exactly to the previously
stored surface position. This can be seen by comparing the force before and after the immersion. It
has to be nearly the same.
As soon as the calculated standard deviation falls below the standard deviation that was given in
the “Set parameters” section, the measurement finishes and the system will wait for the confirma-
tion with the appearing „OK“- button to switch to the results view.
The measurement can be aborted by tapping the „Abort“- button and confirming the decision in the
appearing popup.
7.3 Utilities
Home Method Utilities
7.3.1 Weight
Measuring the weight can be done by mounting a weight sample on the hook.
Set parameters
The predefined parameters are loaded automatically after choosing the measurement method.
When the parameters are changed, they will be saved until the device will be switched off and on
again or another measurement method is chosen. After selecting the weight method, the device
shows the automatically loaded parameter values. The red framed box is a mandatory field and
has to be set whereas any other box may be edited, if needed. The function bar contains, among
other buttons, the „Save“- button for saving the parameters to a user specific measurement method
and the “>” button to go over to the test preparation. These buttons are greyed out, as long as the
mandatory field for “Sample ID” is empty.
Test preparation
The test preparation guides you to the start of the measurement. The first step asks you to remove
any weight tool from the hook. By tapping the „>“- button you get to the taring step, where the de-
vice begins automatically to tare the weighing system. This is done every time before a measure-
ment is started. As long as the environment is not stable enough for the set sensitivity of the weigh-
ing system, the device will wait. When the sensitivity is reached, the label “Unstable” switches to
“Stable” and the taring procedure of the weighing system succeeds. It is also possible to abort the
taring procedure by tapping the „Abort“- button and to start the measurement without taring the
measurement system, but it is not recommended. After aborting the taring procedure it is also pos-
sible to restart it.
A successful taring or the abort of the taring procedure activates the “START”- button and the „<“-
button. Furthermore the button in the middle of the function bar switches from “Abort” to “Tare”
allowing repeating the taring procedure of the measurement system. Tapping the „START“- button
starts the measurement procedure.
Measurement
The measurement screen shows you the elapsed time of the measurement with the measured
value of the weight and the calculated standard deviation. As soon as the calculated standard de-
viation falls below the standard deviation given in the “Set parameters”- section, the measurement
finishes and the system waits for the confirmation of the appearing „OK“- button to switch to the
results view. During this time, the result of the measurement is shown on the screen.
19
The measurement can be aborted by tapping the “Abort”- button and confirming the decision in the
appearing popup.
7.3.2 Density
Measuring the density can be done by mounting the displacement body on the hook.
Set parameters
The predefined parameters are loaded automatically after choosing the measurement method.
When the parameters are changed, they will be saved until the device will be switched off and on
again or another measurement method is chosen. After selecting the density method, the device
shows the automatically loaded parameter values. The red framed box is a mandatory field and
has to be set whereas any other box may be edited, if needed. The function bar contains, among
other buttons, the „Save“- button for saving the parameters to a user specific measurement method
and the “>” button to go over to the test preparation. These buttons are greyed out, as long as the
mandatory field for “Sample ID” is empty.
After confirming the sample ID, the “Save”- button and the “>“- button get activated.
Test preparation
The test preparation guides you to the start of the measurement. The first step is to mount the dis-
placement body on the hook.
By tapping the „>“- button you get to the taring screen, where the system begins to tare the weigh-
ing system. This is done automatically every time before a measurement is started. As long as the
environment is not stable enough for the set sensitivity of the weighing system, the device waits.
When the sensitivity is reached, the label “Unstable” switches to “Stable” and the taring procedure
of the weighing system succeeds. It is also possible to abort the taring procedure by tapping the
„Abort“- button and to start the measurement without taring the measurement system, but it is not
recommended. After aborting the taring procedure it is also possible to restart it.
A successful taring or the abort of the taring procedure activates the „START“- button and the „<“-
button. Furthermore the button in the middle of the function bar switches from “Abort” to “Tare”
allowing to repeat the taring procedure of the measurement system. Tapping the „START“- button
starts the measurement procedure.
Measurement procedure
Before the measurement of the density can be started, the displacement body has to be immersed
completely into the sample liquid. This is done automatically when the measurement procedure
starts.
The device automatically recognizes the surface position of the liquid and immerses the displace-
ment body completely into the liquid. Directly after the immersion, the density measurement starts.
You may abort the immersing by tapping the “Abort”- button, but it is necessary that the platform
will be moved down manually until the displacement body is outside of the liquid after an abort.
This has to be done, because the device searches for the surface while immersing the displace-
ment body. When it is already immersed, the platform will move upwards until it reaches the high-
est point allowed.
The measurement screen view shows the elapsed time of the measurement with the measured
value of the density and the calculated standard deviation. As soon as the calculated standard de-
viation falls below the standard deviation that was given in the “Set parameters”- section, the
20
measurement finishes and the system will wait for the confirmation with the appearing „OK“- button
to switch to the results view.
The measurement can be aborted by tapping the „Abort“- button and confirming the decision in the
appearing popup.
1. Remove the ring carefully from the hook with the usage of tweezers. The usage of tweezers
is important to keep the ring clean and be safe when heating it in the next steps.
2. Rinse the ring with methyl alcohol in a prepared glass vessel. Please try to rinse the entire
surface area that will get in touch with the sample fluid in a measurement.
3. Heat the ring in the oxidizing portion of the gas flame of the Bunsen burner. This ensures
that no combustion residues will stick to the ring. When the ring glows, remove it from the
flame, turn the Bunsen burner off and mount the ring on the hook.
1. Remove the plate carefully from the hook with the usage of tweezers. The usage of twee-
zers is important to keep the plate clean and be safe when heating it in the next steps.
2. Rinse the plate with methyl alcohol in a prepared glass vessel. Please try to rinse the entire
surface area that will get in touch with the sample fluid in a measurement.
3. Heat the plate in the oxidizing portion of the gas flame of the Bunsen burner. This ensures
that no combustion residues will stick to the plate. When it glows, remove it from the flame,
turn the Bunsen burner off and mount the plate on the hook.
1. Remove the glass vessel from its position in the device and dispose the content correctly.
2. Rinse the glass vessel at least three times with methyl alcohol. Make sure that the entire
surface area is touched by the methyl alcohol.
3. Dispose the methyl alcohol correctly and rinse the glass vessel with distilled water.
21
8 Results
Home Results
The result screen is divided into two parts. The list on the left side shows the last five measure-
ments with the related sample id, the date and the time of the measurement. The latest measure-
ment is selected automatically when you open the result-section. To see former measurements,
use the up/down arrow buttons.
The right side of the screen shows the general view with the most important values of a measure-
ment.
Tapping the “Filter”-button in the function bar opens a popup that allows you to filter the results by
measurement methods (see 10.9). If a filter is active, the “Filter”-button is colored orange.
Choosing the results of a surface or interfacial tension measurement opens the following functions:
The central button in the function bar is now visible and allows you to switch the screen view. Tap-
ping The “Data”-button opens the table view with the measurement data showing the timestamp of
each single measurement with the measured force and temperature as well as the calculated sur-
face or interfacial tension and the standard deviations.
The name of the central button in the function bar changes now to “Chart”. Tapping that button,
switches the screen view to a chart, were you can see the calculated values of the surface or inter-
facial tension measurement over time.
The name of the central button in the function bar changes again to “Parameter”. This view shows
you the input parameter of the measurement on three pages. This allows you to see the values of
the parameters that were entered for a particular measurement. The following pictures show the
three pages and the values that can be seen.
9 Configuration
Home Configuration
The configuration menu offers many settings as well as the possibilities to edit the user specific
measurement methods or the geometries of the rings and plates. Furthermore it is possible to ex-
port result data to an USB-device or update the firmware with the usage of a specific USB-device.
The configuration is divided into three main tabs called “Method”, “System” and “Data”.
9.1 Method
This tab contains five subtabs that will be described in this section.
The subtab contains three LAUDA Scientific- standardized ring geometries. The geometries, their
ID and the related correction may be edited by selecting the ring number in the table on the left
22
side of the screen and tapping the “Edit”- button in the function bar. This opens the popup for edit-
ing the ring geometry (see 10.5).
The only limitation is that no geometry can be added or deleted.
The printer configuration allows you to customize the company name on the top of every printout.
Furthermore you may choose if you want to have a long or a short printout of the measurement
and you have the possibility to print the results automatically after every measurement or manually
by selecting the respective result in the “Results” tab and tapping the “Print”- button.
23
9.2 System
The tab „System“ contains the most important configuration options for measurements, language,
time and date and user management.
Brightness
You can set up the brightness of the backlight in 4 steps between 25 % and 100 % by choosing the
corresponding field in the drop-down menu.
Sensitivity
By choosing the sensitivity from the corresponding drop-down menu, you set up the device for the
environmental conditions.
“Stable” means, the device is placed on a stable location with no flow of air or vibrations.
When you only have a location, where vibrations or airflow can occur, please choose “Rough”. This
will let the device accept less accurate values, but you will be able to measure. Note that this set-
ting leads to more inexact results!
Otherwise choose “Normal” when you have more or less stable conditions.
Temperature scale:
The temperature scale can be chosen to be displayed as “°C” or “F”.
Measure delay
This is the time that will be waited before the start of a measurement. This includes all measure-
ments except the “Norm methods”, because their delay times are given by the concerning stand-
ard.
Gravity
The gravity value is important for the calculation of the surface tension and the interfacial tension. It
is important to set this value as precise as possible to get the most accurate results.
Adjust density
Tapping this button opens a user guide for adjusting the weighing system for density measure-
ments. Please prepare a reference liquid, the displacement body and a tweezer and follow the user
guide.
The user guide is also described in section XX
24
Auto login supervisor
By tapping this field you de-/activate the automatic login. When this field is activated, the device
will automatically login with the current user without asking for a password when the device is
switched on.
Audio on/off
The device gives acoustic feedback during a measurement or after a measurement. This allows
you to switch it off or on.
9.2.2 Language
The language of the device can be chosen by tapping the language in the “Language”- subtab.
After the choice of a language, you will have to confirm your decision.
Note that the device will restart automatically after confirming your choice!
9.2.3 Time/Date
This subtab contains all necessary configurations to setup time and date.
You can change the time and the date by tapping the concerning field and editing the value.
The time format can be chosen between “12h” and “24h”.
The buttons for deleting and editing a user are deactivated as long as no user is selected.
Selecting the current logged in user activates only the button for editing a user.
The number of created users is limited to five. As soon as this number is reached, the button for
adding a new user will be deactivated.
9.2.5 About
This subtab contains all necessary information about the manufacturer LAUDA Scientific GmbH as
well as the software-versions and serial numbers of the connected devices.
25
9.3 Data
The „Data“-tab contains the two subtabs “Log” and “Backup”.
9.3.1 Log
The logging function of the TC1 / TD4 logs all important actions in a separate file on the device.
This simplifies the servicing of the device and helps finding errors. Furthermore a supervisor can
control, which measurements were done and if they were done regularly or at specific times.
9.3.2 Backup
Factory settings
This function allows you to reset the device to factory settings. Tapping that button and confirming
the upcoming popup window will delete the database with the measurement results and causes a
reset of all changed configurations.
Update firmware
This button is normally disabled. When an USB storage device is plugged-in and contains a newer
firmware version of the TC1 / TD4 firmware, the button is activated automatically (contact service
for more information). Tapping that button and confirming the upcoming popup will start the update
process (see 11).
Note: Please do not switch off the device or remove the USB-device during an update. This cor-
rupts the copied data and the device will have to be serviced!
Clear results
This function clears the complete result database.
Note: Causes loss of all measurement results. Restoring after clearing the database will not be
possible.
26
10 Popup
Popups are important for showing information during a running process or are used as quick ac-
cess for various configurations. This chapter shows all popups that may appear during the usage.
10.1 Alerts
An alert can be an error, a warning, information or a confirmation. Depending on the type of the
alert, the four main elements of the popup change.
The first element denotes the frame. It changes its color in dependence of the alert type. The sec-
ond element is the symbol showing the alert type (see Table 2). The third element is the short form
explanation of the occurring alert. Element 4 consists of the button for closing the popup. When the
popup is a confirmation-popup, a second button will appear additionally to the existing one to con-
firm the described question or decline it with the “Close” button.
The following table shows the opportunities of the alerts with the related looks:
Table 2: Alerts
Error Red
Information Green
Warning Orange
Confirmation Yellow
Tapping on the light blue box lets the keyboard popup in number mode so that you can type in the
desired temperature value. The red frame means that the box is a mandatory field and must be
filled out to confirm the new temperature with “OK”.
Tapping the „Save“-button saves the changes that were made, the “Cancel”-
button discards all changes. 2
1
2
Tapping the „Save“-button saves the changes that were made, the “Cancel”-
button discards all changes. 1
Tapping the “Adjust” button confirms the standard weight value and starts immediately the adjust-
ment process. After finishing the process, the screen view shows that and a “Close”- button ap-
28
pears instead of the “Abort”- button. Tapping the „Close“- button closes the popup and the adjust-
ment is done successfully.
Therefore you must have the “Admin”-level to get into the configuration menu and have the right to
add, edit or delete a user. This can be done in the subtab “User level”.
29
10.11.2 Edit user
A user can be edited by changing his password and/or priority level. The user name cannot be
changed.
10.12 Keyboard
The Tensio.Touch has a virtual keyboard to enter numbers or texts. This keyboard pops up auto-
matically and depending on the type of edit field (text or number), when it is tapped.
(see 10.12.2). To get back to text view, you only have to tap the “ABC”-button.
30
10.12.2 Enter numbers
When you tap edit fields where numbers have to be entered, like temperature or standard devia-
tion, the keyboard opens directly in numbers-view, but also with disabled special characters and a
disabled button to switch over to the character-view. Furthermore you can see a field with the per-
mitted range of the value that has to be typed in. The picture shows the described keyboard view
with an allowed temperature range of 5 to 80°C.
Cancelling the editing will discard all changes. By tapping the “OK”-button, the changes will be
saved.
31
11 Update firmware
In order to check if you have the latest version, go to “Configuration”, tap the tab “System” and
open the subtab “About”. Here you can see the current versions of your devices and the service
number.
To update the firmware you have to open the tab “Configuration”, tap the tab “Data” and open the
subtab “Backup”. After plugging in the USB-device with the new firmware version, the button
“Firmware update” activates automatically if the version on the USB-device is newer than the one
on your device. Tapping the button and confirming the appearing popup will switch to the update
screen view (see Figure 7).
The updating process begins automatically. You can see the progress through the coloring of the
LAUDA Scientific logo (see Figure 8).
When the update process is completed, a „Close“- button appears. Tapping this button will cause
the system to restart.
Note: It may take a few seconds, until the system initiates the reboot process.
32
12 Quick start
This chapter describes a quick start for measurements.
1. Switch on the device and login as the desired user after it has booted-up.
33
4. Enter a sample-id for your measurement and adjust the preset parameters, if needed
Ring 7.1.1
Plate 7.2.1
Weight 7.3.1
Density 7.3.2
5. To achieve an optimal result, clean the ring/plate according to the description in 7.3.4 or
7.3.5 and mount it on the hook of the device
7. Insert the glass vessel into the given position in the device
8. Fill the glass vessel with the sample fluid (about 30ml)
34
13 Parameter description
Measurement
Table 3: Parameter description of measurement parameters
Parameter Definition
Sample ID: Identification of sample liquid
Δρ: Surface tension: Density difference of the test liquid against air.
Interfacial tension: Density difference of the test liquid against
Adjustment range (0.01…2.5) g/cm³
Stdv. Specification of the admissible standard deviation for the last measured points.
When this value is undercut, the measurements are regarded as stable. The
measurement is terminated.
Adjustment range (0.01…1) % or (0.01…1) mN/m
Speed Speed at which the sample platform is raised (1...100)
Pause Pause time between two measurement points.
Adjustment range (1...999) s.
Meas. points Specification of the number of the last measured values for determining the
standard deviation.
Adjustment range (3…9)
Ring Preconfigured ring geometries with LAUDA Scientific-standard parameters (to
adjust see 9.1.1)
Temp. Ambient temperature when no PTT+ is connected. Otherwise the set tempera-
ture of the PTT+ will be taken.
Adjustment range (5…80) °C or (41…176) °F
Max. return Defines how far the ring is withdrawn after detecting the force maximum.
Adjustment range (0…100) %
Example:
Here, after detecting the first maximum the ring is moved back until 10% of the
maximum force is reached. The ring remains above the level of the interface until
the next extraction is started after the specified pause time. On entering 100%
the ring moves back completely to the interface.
Max. duration Specifies the maximum duration of the measurement. The measurement finishes
after the entered time expires.
Adjustment range (0…199) min
Plate Preconfigured plate geometries with LAUDA Scientific-standard parameters (to
adjust see 9.1.2)
Max. time Maximum duration of the measurement.
Adjustment range (1…999) s.
Configuration
Table 4: Parameter description of configuration parameters
Parameter Definition
Radius ring Radius of a Du Noüy measuring ring (see 10.5)
Radius wire Wire radius of a Du Noüy measuring ring (see 10.5)
Correction Correction factor for the calculation of the surface tension
Length plate Length of the Wilhelmy plate (see 10.6)
Thickness Thickness of the Wilhelmy plate (see 10.6)
plate
35
14 Appendix
14.1 Reference values for checking the TC1 / TD4
The measurement of pure liquids with known surface and interfacial tension is recommended for
checking the accuracy.
Note: The reference values quoted in the literature can often only be verified with highly pure
liquids and with a great deal of effort in the cleaning of sample containers and test
probes and only over a short period of time.
It is therefore quite possible that measurements obtained with the TD 3 in practice may
deviate significantly from the reference values, particularly in the case of interfacial
tension measurements.
System 15 °C 20 °C 25 °C
Water 73.5 72.8 72
Benzene 29.5 28.9 28.2
Etahnol 22.7 22.3 21.4
Diethyl ether - 17.0 -
System 20 °C
Benzene 35.0
Chloroform 10.7
Diethyl ether 32.8
If recycling is not possible, the packaging parts can also be disposed of in the normal refuse.
36
14.3 Technical data
The following tables shows the technical data of the TC1 / TD4.
37
14.4 Order numbers and accessories
Device type Order no.
Standard accessories TC1 (incl. Tensio.Touch and power supply unit) LMT 870
(included in price) TD4 (incl. Tensio.Touch and power supply unit) LMT 860
Du Noüy measuring ring (2-limb, Pt/Ir)
Calibrating weight 500 mg
Displacement body (glass, for density measurement)
Tweezers
Set of beakers (10 pcs.) 6 cm dia.
Plastic case
Optional accessories Du Noüy measuring ring (4-limb, Pt/Ir)
Wilhelmy plate (Pt/Ir)
Calibrating weight with DKD certificate 500 mg
Set of beakers (10 pcs., for density measurement)
Set of beakers (10 pcs.) 6 cm dia.
Burning-off burner (for cleaning ring / plate)
Data output Dot-matrix printer for recording the data
Ink ribbon for printer, replacement
Paper roll for printer (pack of 10), replacement
Software Data transfer software for PC / TD 2/3
RS 232 connecting lead
Integrable PTT Peltier PTT+ (Peltier thermostating unit with integrated magnetic
Thermostating Unit stirrer and temperature sensor for external control, for
beaker 6 cm dia.)
Standard accessories PTFE stirring rod
for PTT+ Transparent plastic cover with opening
(included in price) Pt 100 temperature sensor for PTT
38
14.5 References
39