Professional Documents
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F l a me Sele c tio n
JQA-0376
URL http://www.shimadzu.com The contents of this brochure are subject to change without notice.
T h e n ew ly d ev e l o p e d , h i g h t h ro u g h p u t dy n a m i c b e a m m a n ag e r s y s t e m
a ch i ev e s m e a s u r e m e n t s w i t h t h e wo r l d ’s h i g h e s t l ev e l o f s e n s i t i v i t y ( D i r e c t
determination - Flame: Pb, 0.1ppm; Furnace: Pb, 0.3ppb)
• A n ex t g e n e ra t i o n d o u bl e b e a m s y s t e m w h i c h d ra s t i c a l l y r e d u c e s t h e n o i s e o f a
d o u bl e b e a m o p t i c a l s y s t e m t h r o u g h t h e a d o p t i o n o f a h i g h t h r o u g h p u t d y n a m i c
b e a m m a n a g e r s y s t e m a n d a h i g h s p e e d o p e ra t i o n d i g i t a l f i l t e r.
F DA 2 1 C F R Pa r t 1 1 C o m p l i a n c e
• F u r t h e r evo l ve d W i z A A r d a n d C L A S S - A g e n t s o f t wa r e c o m b i n e t o a c h i eve
F DA 2 1 C F R Pa r t 1 1 C o m p l i a n c e.
• W i z A A r d a l o n e o f t e r s c o m p r e h e n s i ve s y s t e m m a n a g e m e n t f u n c t i o n s, i n c l u d i n g
s y s t e m p o l i c y s e t t i n g s, u s e r m a n a g e m e n t , I o g b r ow s e r, a u d i t t ra i l , a n d e l e c t r o n i c
s i g n a t u r e s.
• C o m b i n a t i o n w i t h C L A S S - A g e n t s o f t wa r e a c h i eve s eve n m o r e e f t i c i e n t d a t a b a s e
management.
• C o m p r e h e n s i ve a c c u ra c y m a n a g e m e n t f u n c t i o n s. ( Q A / Q C, e t c . )
• H a r d wa r e va l i d a t i o n s o f t wa r e i s a l s o s t a n d a r d e q u i p m e n t .
S w i t ch s m o o t h ly b e t w e e n F l a m e a n d F u r n a c e
• A l l t h a t i s i nvo l ve d i n sw i t c h i n g f r o m f l a m e t o f u r n a c e i s t o r e m ove t h e bu r n e r h e a d
a n d p u t i n p l a c e t h e f u r n a c e s e c t i o n . T h e s e s t e p s r e q u i r e n o t o o l s, a n d c a n b e
d o n e e a s i l y a n d s p e e d i l y.
• F u r t h e r m o r e, t h e s i n g l e a u t o s a m p l e r c a n b e u s e d fo r b o t h f l a m e a n d f u r n a c e,
Atomic absorption that has evolved for the new century w h i c h n e g a t e s t h e n e e d t o p r e p a r e t h e a u t o s a m p l e r fo r e a c h a n a l y s i s m e t h o d .
AA-6300
A d o p t i o n o f Au t o m a t i c B u r n e r H e a d H e i g h t C o n t ro l M e ch a n i s m
• l n a d d i t i o n t o t h e a u t o m a t e d c o n t r o l o f t h e f l a m e g a s f l ow ra t e c o n d i t i o n s, t h e
bu r n e r h e a d h e i g h t c a n b e a u t o m a t i c a l l y c o n t r o l l e d a s we l l . T h e o p t i m a l
p a ra m e t e r s fo r e a c h e l e m e n t / s a m p l e c a n b e s e t a u t o m a t i c a l l y t o
e n a bl e c o n t i nu o u s m e a s u r e m e n t .
T h e n ew ly d ev e l o p e d , h i g h t h ro u g h p u t dy n a m i c b e a m m a n ag e r s y s t e m
a ch i ev e s m e a s u r e m e n t s w i t h t h e wo r l d ’s h i g h e s t l ev e l o f s e n s i t i v i t y ( D i r e c t
determination - Flame: Pb, 0.1ppm; Furnace: Pb, 0.3ppb)
• A n ex t g e n e ra t i o n d o u bl e b e a m s y s t e m w h i c h d ra s t i c a l l y r e d u c e s t h e n o i s e o f a
d o u bl e b e a m o p t i c a l s y s t e m t h r o u g h t h e a d o p t i o n o f a h i g h t h r o u g h p u t d y n a m i c
b e a m m a n a g e r s y s t e m a n d a h i g h s p e e d o p e ra t i o n d i g i t a l f i l t e r.
F DA 2 1 C F R Pa r t 1 1 C o m p l i a n c e
• F u r t h e r evo l ve d W i z A A r d a n d C L A S S - A g e n t s o f t wa r e c o m b i n e t o a c h i eve
F DA 2 1 C F R Pa r t 1 1 C o m p l i a n c e.
• W i z A A r d a l o n e o f t e r s c o m p r e h e n s i ve s y s t e m m a n a g e m e n t f u n c t i o n s, i n c l u d i n g
s y s t e m p o l i c y s e t t i n g s, u s e r m a n a g e m e n t , I o g b r ow s e r, a u d i t t ra i l , a n d e l e c t r o n i c
s i g n a t u r e s.
• C o m b i n a t i o n w i t h C L A S S - A g e n t s o f t wa r e a c h i eve s eve n m o r e e f t i c i e n t d a t a b a s e
management.
• C o m p r e h e n s i ve a c c u ra c y m a n a g e m e n t f u n c t i o n s. ( Q A / Q C, e t c . )
• H a r d wa r e va l i d a t i o n s o f t wa r e i s a l s o s t a n d a r d e q u i p m e n t .
S w i t ch s m o o t h ly b e t w e e n F l a m e a n d F u r n a c e
• A l l t h a t i s i nvo l ve d i n sw i t c h i n g f r o m f l a m e t o f u r n a c e i s t o r e m ove t h e bu r n e r h e a d
a n d p u t i n p l a c e t h e f u r n a c e s e c t i o n . T h e s e s t e p s r e q u i r e n o t o o l s, a n d c a n b e
d o n e e a s i l y a n d s p e e d i l y.
• F u r t h e r m o r e, t h e s i n g l e a u t o s a m p l e r c a n b e u s e d fo r b o t h f l a m e a n d f u r n a c e,
Atomic absorption that has evolved for the new century w h i c h n e g a t e s t h e n e e d t o p r e p a r e t h e a u t o s a m p l e r fo r e a c h a n a l y s i s m e t h o d .
AA-6300
A d o p t i o n o f Au t o m a t i c B u r n e r H e a d H e i g h t C o n t ro l M e ch a n i s m
• l n a d d i t i o n t o t h e a u t o m a t e d c o n t r o l o f t h e f l a m e g a s f l ow ra t e c o n d i t i o n s, t h e
bu r n e r h e a d h e i g h t c a n b e a u t o m a t i c a l l y c o n t r o l l e d a s we l l . T h e o p t i m a l
p a ra m e t e r s fo r e a c h e l e m e n t / s a m p l e c a n b e s e t a u t o m a t i c a l l y t o
e n a bl e c o n t i nu o u s m e a s u r e m e n t .
The High-Throughput Dynamic Beam Manager System developed uniquely for the AA-6300 automatically sets the photometric system to The Microsampling Method
optical double-beam for flame measurement, and to electrical double-beam for furnace measurement. Furthermore, the optical system has Flame measurements require at least 1 mL (1000µL) of solution since the sample is normally sucked in continuously. With the microsampling
been designed to produce its maximum performance in each of the measurement methods through the optimal adjustment of the light beam, method, about 50 to 100µL of the sample is injected into the flame in one go to quantitate the sample using the height and area of the peak-
high speed operation digital filter, and employment of optical components which suppress light loss. shaped signal obtained. As a result, this method has the following characteristics.
Long Term Stability Because High Sensitivity Despite Only a small amount of sample is required.
of the Double Beam the Double Beam Multiple elements can be measured even with a small amount of sample.
The data in the diagram below shows the flame long term stability of Direct measurement of Pb: 0.1ppm is achieved. The burner slot does not get blocked so easily, even with high salt content samples.
Cu. The results are of Cu: 2ppm, The diagram below is the calibration curve of Pb: 0.1ppm to 0.4ppm. Working in concert with the autosampler*, automatic dilution measurements are possible.
5 repeated measurements conducted for 1 hour. A %RSD of approx. *In order for it to work together with the autosampler, the microsampling kit (sold separately) is required,
Measurement time 1. Inject the sample into the microsampling port 2. Open the solenoid valve and introduce in one go into the flame.
Cu Flame 60 Minute Measurement
The following safety mechanisms have been incorporated. The burner head is made of titanium,
Safe ignition / extinction sequence The chamber is polypropylene,
Flashback prevention through the gas pressure monitor The disperser is ceramic -
Prevention of raw gas release when the flame dies out Durability has been taken into account as well.
Burner misuse prevention
Automatic search for optimal fuel gas flow rate and optimal
Automatic flame extinction in a power failure
burner height
Each condition is automatically changed within a fixed range, The flow rate and height Example of running * Furthermore, a higher level of safety is ensured through the safety inspection
at which the ditference in absorbance between a standard sample and a blank sample an optimal burner support provided by software, and the self-diagnostics function which
is at its maximum is displayed on a graph. height search determines whether the system safety mechanisms are in working order.
4 5
Fe atur es
The High-Throughput Dynamic Beam Manager System developed uniquely for the AA-6300 automatically sets the photometric system to The Microsampling Method
optical double-beam for flame measurement, and to electrical double-beam for furnace measurement. Furthermore, the optical system has Flame measurements require at least 1 mL (1000µL) of solution since the sample is normally sucked in continuously. With the microsampling
been designed to produce its maximum performance in each of the measurement methods through the optimal adjustment of the light beam, method, about 50 to 100µL of the sample is injected into the flame in one go to quantitate the sample using the height and area of the peak-
high speed operation digital filter, and employment of optical components which suppress light loss. shaped signal obtained. As a result, this method has the following characteristics.
Long Term Stability Because High Sensitivity Despite Only a small amount of sample is required.
of the Double Beam the Double Beam Multiple elements can be measured even with a small amount of sample.
The data in the diagram below shows the flame long term stability of Direct measurement of Pb: 0.1ppm is achieved. The burner slot does not get blocked so easily, even with high salt content samples.
Cu. The results are of Cu: 2ppm, The diagram below is the calibration curve of Pb: 0.1ppm to 0.4ppm. Working in concert with the autosampler*, automatic dilution measurements are possible.
5 repeated measurements conducted for 1 hour. A %RSD of approx. *In order for it to work together with the autosampler, the microsampling kit (sold separately) is required,
Measurement time 1. Inject the sample into the microsampling port 2. Open the solenoid valve and introduce in one go into the flame.
Cu Flame 60 Minute Measurement
The following safety mechanisms have been incorporated. The burner head is made of titanium,
Safe ignition / extinction sequence The chamber is polypropylene,
Flashback prevention through the gas pressure monitor The disperser is ceramic -
Prevention of raw gas release when the flame dies out Durability has been taken into account as well.
Burner misuse prevention
Automatic search for optimal fuel gas flow rate and optimal
Automatic flame extinction in a power failure
burner height
Each condition is automatically changed within a fixed range, The flow rate and height Example of running * Furthermore, a higher level of safety is ensured through the safety inspection
at which the ditference in absorbance between a standard sample and a blank sample an optimal burner support provided by software, and the self-diagnostics function which
is at its maximum is displayed on a graph. height search determines whether the system safety mechanisms are in working order.
4 5
Fe atur es
By uniquely controlling the flow of the gas inside the graphite tube at atomization (Patent 2067563), high sensitivity measurement has been Sophisticated Autosampler
realized to a degree that is among the best in the world (sensitivity has been increased by a maximum of 1.4 times over Shimadzu's previous A maximum of 4 samples (such as the diluent, standard solution,
products). sample, matrix modifier) can at first be mixed and then injected
(without mixing is of course possible as well).
High Sensitivity Application Data (Se Measurement Example) Commercially available pipette tips or the Teflon tube can be
In the example of Se: selected for the injection nozzle.
0-5ppb measurement, it is The unit can be set to automatically dilute and repeat the
clearly evident that 1ppb of Se measurement if the calibration curve concentration is exceeded.
can be measured (20µL
injection, Pd modifier &
pyro-coated tube used)
F o r s t a ble fu rn ac e me a s u rement
• Improved stability through digital temperature control & digital gas control
By combining a high sensitivity optical sensor and a digital temperature control system, the temperature is controlled with a high degree of
precision over the entire temperature region from drying to atomization. By employing the electronic controller, the flow rate of the inner gas
can be controlled precisely in 0.01L/min units. The table above is an example of the measurement of Cd. The maximum concentration of the calibration curve has been set to 1ppb. At 1.8ppb, the sample of [003] has
exceeded the maximum concentration. As a result it has been automatically diluted by 4 times and re-measured.
Through these methods of control, not only the sensitivity but also the data stability is improved greatly.
6 7
Fe atur es
By uniquely controlling the flow of the gas inside the graphite tube at atomization (Patent 2067563), high sensitivity measurement has been Sophisticated Autosampler
realized to a degree that is among the best in the world (sensitivity has been increased by a maximum of 1.4 times over Shimadzu's previous A maximum of 4 samples (such as the diluent, standard solution,
products). sample, matrix modifier) can at first be mixed and then injected
(without mixing is of course possible as well).
High Sensitivity Application Data (Se Measurement Example) Commercially available pipette tips or the Teflon tube can be
In the example of Se: selected for the injection nozzle.
0-5ppb measurement, it is The unit can be set to automatically dilute and repeat the
clearly evident that 1ppb of Se measurement if the calibration curve concentration is exceeded.
can be measured (20µL
injection, Pd modifier &
pyro-coated tube used)
F o r s t a ble fu rn ac e me a s u rement
• Improved stability through digital temperature control & digital gas control
By combining a high sensitivity optical sensor and a digital temperature control system, the temperature is controlled with a high degree of
precision over the entire temperature region from drying to atomization. By employing the electronic controller, the flow rate of the inner gas
can be controlled precisely in 0.01L/min units. The table above is an example of the measurement of Cd. The maximum concentration of the calibration curve has been set to 1ppb. At 1.8ppb, the sample of [003] has
exceeded the maximum concentration. As a result it has been automatically diluted by 4 times and re-measured.
Through these methods of control, not only the sensitivity but also the data stability is improved greatly.
6 7
Sof tw ar e
For software that is easy to understand and use, with a high level of security
C h a ra c t eris tics o f th e “WizAArd” Sof t ware To r ealiz e elect ro n ic r eco rd s o f h ig h secu r it y
The “WizAArd” software used in the AA-6300 operates on Windows XP/2000. It has the following characteristics. Comprehensive System Management Functions
Provides a Wizard function that makes it easy to set the conditions, even for beginners.
• System Policy • CLASS-Agent
Equipped with a parameter editing function that enables conditions to be changed rapidly.
The System Policy settings allow detailed specifications of password and lockout settings. Connection to CLASS-Agent
The measurement screen is arranged so that the measurement status can be understood at a glance.
Security levels can also be set by selecting preset levels from “NO restriction” to permits effective database
Equipped with comprehensive data processing functions.
“Part11 Compatible”. management for large amounts of
Complies with the QA/QC of the EPA (U.S. Environmental Protection Agency).
longterm data.
Equipped with user level management, audit trail, and electronic signature functions.
Built-in hardware validation software.
Element Selection
8 9
Sof tw ar e
For software that is easy to understand and use, with a high level of security
C h a ra c t eris tics o f th e “WizAArd” Sof t ware To r ealiz e elect ro n ic r eco rd s o f h ig h secu r it y
The “WizAArd” software used in the AA-6300 operates on Windows XP/2000. It has the following characteristics. Comprehensive System Management Functions
Provides a Wizard function that makes it easy to set the conditions, even for beginners.
• System Policy • CLASS-Agent
Equipped with a parameter editing function that enables conditions to be changed rapidly.
The System Policy settings allow detailed specifications of password and lockout settings. Connection to CLASS-Agent
The measurement screen is arranged so that the measurement status can be understood at a glance.
Security levels can also be set by selecting preset levels from “NO restriction” to permits effective database
Equipped with comprehensive data processing functions.
“Part11 Compatible”. management for large amounts of
Complies with the QA/QC of the EPA (U.S. Environmental Protection Agency).
longterm data.
Equipped with user level management, audit trail, and electronic signature functions.
Built-in hardware validation software.
Element Selection
8 9
Sof tw ar e
2-way background correction function to enable usage of the optimal background correction method
Examples of elements / wavelengths where spectral interference caused by neighboring lines
Eq u i p p e d as s tan d a rd w ith t he deut erium lamp met hod ( D2 met ho d ) becomes a problem
a n d t h e h ig h s p ee d S elf-R eversal met hod ( SR met hod)
Element Analytical Coexisting Absorption Choosing
measured line (nm) element line (nm) a background correction method
The AA-6300 is equipped as standard with 2 background correction methods: the deuterium lamp method (D2 method) and the high speed Al 309.28 Mg 309.30
Self-Reversal method (SR method). These can be selected at the time of measurement. Both methods are certified in accordance with the JIS As 193.76 Fe 193.73 Samples suited to the SR method:
standards (General rules for atomic absorption spectrochemical analysis: K0121) and the EPA (U.S. Environmental Protection Agency). Each Ca 422.67 Fe 422.64 Samples with complex matrices (where large amounts of a
background correction method has its own characteristics, and the ability to select a method to suit the application and objectives of the Cd 228.80 Ni 228.84 specific element is included in the main constituent)
analysis is a significant benefit. Cu 324.75 Fe 324.73
Ga 294.36 Ni 294.39 Samples suited to the D2 method:
For high precision and wide range background correction : Self-Reversal Method (SR Method) Mg 285.21 Fe 285.18 Samples with relatively simple matrices such as purified
Principle Features water, drinking water, and environmental water
Ni 232.00 Fe 232.04
A small current IL (about 10mA) and a large current IH (about 1. The accuracy of background correction is generally better than the Pb 217.00 Fe 216.95
500mA) are applied alternately to the hollow-cathode lamp. When the deuterium lamp method. Since the atomic absorption and
current is large, there is a dip (Self Reverse) in the center of the Sb 217.58 Fe 217.55 Note:
background absorption can be measured with 1 Iamp, the
emission spectrum of the lamp - as shown in the diagram below - Se 196.03 Fe 196.05 When using the SR method, the L-2433 type hollow-cathode
correction error due to a mismatch of the optical axis is exceedingly
because of the self-absorption of the large amounts of atomic cloud Si 251.61 Fe 251.69 lamp is necessary. Note that the L-2433 type can be used
sputtered. Atomic absorption is largely unseen, and most of it is small. This method is suited to the quantitation of trace constituents
background absorption. On the other hand, the emission spectrum in matrices exhibiting complex background absorption, such as
Zn 213.856 Fe 213.8589 with the D2 Iamp method as well.
during the small current takes on the form of a single peak, and is biological samples and metallic materials.
affected by both atomic and background absorption. By determining 2. The background can be corrected over the entire 185nm to 900nm When a disparity arises between the D2 method and the SR method (E.g.: measurement of trace zinc in iron)
the difference in absorbance between the two, an accurate correction
wavelength range.
for the background absorption can be made, and the true atomic
absorption can be measured. 3. The spectral interfence caused by neighboring lines arising out of 1 Zn 0.25ppm
the resonance lines of other elements in the vicinity of the Atomic absorption signal Atomic absorption signal 2 Zn 0.50ppm
Background Background signal
Absorption analyiical line of the target element can also be corrected (refer to Background signal 3 Fe 0.1%
IH Spectrum
Background
the table on the right hand page) . 4 Fe 0.5%
Atomic Absorption
5 Fe 0.5%+Zn 0.25ppm
Lamp Current
IH Atomic 4. The measurements feature no light loss and a high S/N ratio since
Absorption
Atomic a polarizer is not used. 6 Fe 0.5%+Zn0.5ppm
Wavelength Wavelength Absorption Absorption
L
Layer 7 Fe 0.75%+Zn0.3ppm
IL Spectrum 5. The high speed illumination enables accurate measurements to be
Background
Time conducted without being aftected by the emission noise of the
Atomic Absorption
atomizer.
(Lamp Energy) (Sample Measurement) (Energy Component Ratio)
Measurement of Zn in Fe solution by the BGC-D2 method Measurement of Zn in Fe solution by the BGC-SR method
The absorbance of 6 is greater than 2 for the same 2 and 6 of the same Zn: 0.5ppm solution has been
For highly sensitive background correction : Deuterium Lamp(D2)Method Zn: 0.5ppm solution because of insufficient correction. corrected accurately and exhibit the same absorbance.
Principle Features
With the deuterium lamp method, the hollow-cathode lamp and 1. The detection sensitivity is better than the Self-Reversal method.
deuterium lamp are lit up alternately at high speeds. The light from For this reason, it is suited to measurements where the matrix is
the deuterium lamp maintains a width of 0.1 nm to 5nm even after it When there is no disparity between the D2 method and the SR method (E.g.: Molecular absorption, measurement of trace lead in 2% NaCl)
simple and a highly sensitive analysis is required, such as in
is split by the spectrophotometer. As a result, atomic absorption,
which is only about 1/1000nm wide, is hardly observed, while the environmental analysis, and the measurement of ultra-trace BGC-SR Method BGC-D2 Method
background absorption, such as those due to molecular absorption, impurities in ultrapure water.
which is wide, is observed. On the other hand, since the width of the 2. As the illumination frequency is high compared to the Self Reversal
light of the hollow-cathode lamp is about the same as the width of method, the noise due to the emission components of the flame
atomic absorption, the sum of the atomic absorption and background
and graphite tube can be removed, enabling the accurate
absorption is observed. The background is corrected by determining
the difference between the respective absorbances. measurement of atomic absorption. Background signal
3. The conventional hollow-cathode lamp can be used as it is.
D2 Lamp Spectrum Background Absorption
hollow-cathode lamp Spectrum Atomic Absorption + Background Absorption Analysis of Pb in 2% NaCl solution (The sensitivity is higher with the BGC-D2 method.)
10 11
Sof tw ar e
2-way background correction function to enable usage of the optimal background correction method
Examples of elements / wavelengths where spectral interference caused by neighboring lines
Eq u i p p e d as s tan d a rd w ith t he deut erium lamp met hod ( D2 met ho d ) becomes a problem
a n d t h e h ig h s p ee d S elf-R eversal met hod ( SR met hod)
Element Analytical Coexisting Absorption Choosing
measured line (nm) element line (nm) a background correction method
The AA-6300 is equipped as standard with 2 background correction methods: the deuterium lamp method (D2 method) and the high speed Al 309.28 Mg 309.30
Self-Reversal method (SR method). These can be selected at the time of measurement. Both methods are certified in accordance with the JIS As 193.76 Fe 193.73 Samples suited to the SR method:
standards (General rules for atomic absorption spectrochemical analysis: K0121) and the EPA (U.S. Environmental Protection Agency). Each Ca 422.67 Fe 422.64 Samples with complex matrices (where large amounts of a
background correction method has its own characteristics, and the ability to select a method to suit the application and objectives of the Cd 228.80 Ni 228.84 specific element is included in the main constituent)
analysis is a significant benefit. Cu 324.75 Fe 324.73
Ga 294.36 Ni 294.39 Samples suited to the D2 method:
For high precision and wide range background correction : Self-Reversal Method (SR Method) Mg 285.21 Fe 285.18 Samples with relatively simple matrices such as purified
Principle Features water, drinking water, and environmental water
Ni 232.00 Fe 232.04
A small current IL (about 10mA) and a large current IH (about 1. The accuracy of background correction is generally better than the Pb 217.00 Fe 216.95
500mA) are applied alternately to the hollow-cathode lamp. When the deuterium lamp method. Since the atomic absorption and
current is large, there is a dip (Self Reverse) in the center of the Sb 217.58 Fe 217.55 Note:
background absorption can be measured with 1 Iamp, the
emission spectrum of the lamp - as shown in the diagram below - Se 196.03 Fe 196.05 When using the SR method, the L-2433 type hollow-cathode
correction error due to a mismatch of the optical axis is exceedingly
because of the self-absorption of the large amounts of atomic cloud Si 251.61 Fe 251.69 lamp is necessary. Note that the L-2433 type can be used
sputtered. Atomic absorption is largely unseen, and most of it is small. This method is suited to the quantitation of trace constituents
background absorption. On the other hand, the emission spectrum in matrices exhibiting complex background absorption, such as
Zn 213.856 Fe 213.8589 with the D2 Iamp method as well.
during the small current takes on the form of a single peak, and is biological samples and metallic materials.
affected by both atomic and background absorption. By determining 2. The background can be corrected over the entire 185nm to 900nm When a disparity arises between the D2 method and the SR method (E.g.: measurement of trace zinc in iron)
the difference in absorbance between the two, an accurate correction
wavelength range.
for the background absorption can be made, and the true atomic
absorption can be measured. 3. The spectral interfence caused by neighboring lines arising out of 1 Zn 0.25ppm
the resonance lines of other elements in the vicinity of the Atomic absorption signal Atomic absorption signal 2 Zn 0.50ppm
Background Background signal
Absorption analyiical line of the target element can also be corrected (refer to Background signal 3 Fe 0.1%
IH Spectrum
Background
the table on the right hand page) . 4 Fe 0.5%
Atomic Absorption
5 Fe 0.5%+Zn 0.25ppm
Lamp Current
IH Atomic 4. The measurements feature no light loss and a high S/N ratio since
Absorption
Atomic a polarizer is not used. 6 Fe 0.5%+Zn0.5ppm
Wavelength Wavelength Absorption Absorption
L
Layer 7 Fe 0.75%+Zn0.3ppm
IL Spectrum 5. The high speed illumination enables accurate measurements to be
Background
Time conducted without being aftected by the emission noise of the
Atomic Absorption
atomizer.
(Lamp Energy) (Sample Measurement) (Energy Component Ratio)
Measurement of Zn in Fe solution by the BGC-D2 method Measurement of Zn in Fe solution by the BGC-SR method
The absorbance of 6 is greater than 2 for the same 2 and 6 of the same Zn: 0.5ppm solution has been
For highly sensitive background correction : Deuterium Lamp(D2)Method Zn: 0.5ppm solution because of insufficient correction. corrected accurately and exhibit the same absorbance.
Principle Features
With the deuterium lamp method, the hollow-cathode lamp and 1. The detection sensitivity is better than the Self-Reversal method.
deuterium lamp are lit up alternately at high speeds. The light from For this reason, it is suited to measurements where the matrix is
the deuterium lamp maintains a width of 0.1 nm to 5nm even after it When there is no disparity between the D2 method and the SR method (E.g.: Molecular absorption, measurement of trace lead in 2% NaCl)
simple and a highly sensitive analysis is required, such as in
is split by the spectrophotometer. As a result, atomic absorption,
which is only about 1/1000nm wide, is hardly observed, while the environmental analysis, and the measurement of ultra-trace BGC-SR Method BGC-D2 Method
background absorption, such as those due to molecular absorption, impurities in ultrapure water.
which is wide, is observed. On the other hand, since the width of the 2. As the illumination frequency is high compared to the Self Reversal
light of the hollow-cathode lamp is about the same as the width of method, the noise due to the emission components of the flame
atomic absorption, the sum of the atomic absorption and background
and graphite tube can be removed, enabling the accurate
absorption is observed. The background is corrected by determining
the difference between the respective absorbances. measurement of atomic absorption. Background signal
3. The conventional hollow-cathode lamp can be used as it is.
D2 Lamp Spectrum Background Absorption
hollow-cathode lamp Spectrum Atomic Absorption + Background Absorption Analysis of Pb in 2% NaCl solution (The sensitivity is higher with the BGC-D2 method.)
10 11
O pt i on
Employs the quick, tool-less switching mechanism, making it as easy and effortless as shown in the photo.
GFA-EX7i Various graphite tubes for the GFA-EX7i Compressors, Gas Pressure Resulators
Graphite Furnace Atomizer High-density graphite tube (P/N: 206-50587) Low Noise Air Compressor (P/N: 208-91750- **)
The graphite furnace design achieves Digital Temperature Control Although it can be used with Working pressure: 0.5 to 0.7MPa
Digital temperature control places all heating under computer control all elements, it is particularly Tank capacity: 15L
Greater effective for low boiling point Power requirements: AC100V 6.2A max. 50/60Hz
to achieve optimal heating with little temperature overshoot.
elements (such as Cd, Pb, Na, Size: Width 380 x Depth 380 x Height 480mm
Conventional GFA GFA-EX7(i)
Digital Gas Control K, Zn, Mg). Weight: 26kg
Pb 0.12 ppb 0.085 ppb Electronic flow controllers achieve precise inner gas flow
Improved control at every stage. Air Compressor (P/N : 208-91742-91)
Mn 0.02 ppb 0.015 ppb
Working pressure: 0.39 to 0.59MPa
(Detection lower limit values) Temperature Control
Pyro-coated graphite tube (P/N: 206-50588) Tank capacity: 12L
Over Entire Temperature Range Power requirements: AC100V 4.0A max. 50/60Hz
Accurate temperature repeatability over the entire temperature range Effective for elements which
Size: Width 210 x Depth 411 x Height 506mm
is achieved by the high-sensitivity optical temperature sensor and tend to produce carbides
E a s y a n a lysis even of high m a tr ix easily (such as Ni, Fe, Cu, Ca,
Weight: 16kg
buiit-in automatic temperature correction functions over the current
control range. Ti, Si, V, Mo). Mist Separator Kit (P/N: 206-52458-91)
Analysis of Pb in 2% NaCl solution
Completely removes oil and moisture mixed in the air
Unique High-sensitivity Mode
supplied from the air compressor, Required at the time of air
Selecting the high-sensitivity mode during sample atomization
compressor use other than the above.
achieves more sensitive and accurate microanalysis.
Size: Width 110 x Depth 201 x Height 252mm
Platform tube (P/N: 206-50887-02)
Dual Gas System Weight: Approx. 1kg
Automatic switching between two gases allows the use of air to Suppresses chemical
promote the ashing of organic samples. interference caused by Precision Gas Pressure Regulator
coexisting substances.
Cylinder attachment
Pressure regulator P/N
Variety of Graphite Tubes (Special Accessories) Effective for environmental screw spec.
Three types of graphite tube (high-density graphite tube, pyro-coated samples such as seawater YR-71 for C2H2 040-72020-01 AC2 fixing bracket
graphite tube, platform-type graphite tube) are available to suit the and industrial waste, as MAF85S for N20 040-72019-11 W22-14RH
0ppb 2ppb 4ppb
added properties of the analyzed elements and sample. well as biological samples. MAF106S for Ar 040-72019-21 W22-14RH
12 13
O pt i on
Employs the quick, tool-less switching mechanism, making it as easy and effortless as shown in the photo.
GFA-EX7i Various graphite tubes for the GFA-EX7i Compressors, Gas Pressure Resulators
Graphite Furnace Atomizer High-density graphite tube (P/N: 206-50587) Low Noise Air Compressor (P/N: 208-91750- **)
The graphite furnace design achieves Digital Temperature Control Although it can be used with Working pressure: 0.5 to 0.7MPa
Digital temperature control places all heating under computer control all elements, it is particularly Tank capacity: 15L
Greater effective for low boiling point Power requirements: AC100V 6.2A max. 50/60Hz
to achieve optimal heating with little temperature overshoot.
elements (such as Cd, Pb, Na, Size: Width 380 x Depth 380 x Height 480mm
Conventional GFA GFA-EX7(i)
Digital Gas Control K, Zn, Mg). Weight: 26kg
Pb 0.12 ppb 0.085 ppb Electronic flow controllers achieve precise inner gas flow
Improved control at every stage. Air Compressor (P/N : 208-91742-91)
Mn 0.02 ppb 0.015 ppb
Working pressure: 0.39 to 0.59MPa
(Detection lower limit values) Temperature Control
Pyro-coated graphite tube (P/N: 206-50588) Tank capacity: 12L
Over Entire Temperature Range Power requirements: AC100V 4.0A max. 50/60Hz
Accurate temperature repeatability over the entire temperature range Effective for elements which
Size: Width 210 x Depth 411 x Height 506mm
is achieved by the high-sensitivity optical temperature sensor and tend to produce carbides
E a s y a n a lysis even of high m a tr ix easily (such as Ni, Fe, Cu, Ca,
Weight: 16kg
buiit-in automatic temperature correction functions over the current
control range. Ti, Si, V, Mo). Mist Separator Kit (P/N: 206-52458-91)
Analysis of Pb in 2% NaCl solution
Completely removes oil and moisture mixed in the air
Unique High-sensitivity Mode
supplied from the air compressor, Required at the time of air
Selecting the high-sensitivity mode during sample atomization
compressor use other than the above.
achieves more sensitive and accurate microanalysis.
Size: Width 110 x Depth 201 x Height 252mm
Platform tube (P/N: 206-50887-02)
Dual Gas System Weight: Approx. 1kg
Automatic switching between two gases allows the use of air to Suppresses chemical
promote the ashing of organic samples. interference caused by Precision Gas Pressure Regulator
coexisting substances.
Cylinder attachment
Pressure regulator P/N
Variety of Graphite Tubes (Special Accessories) Effective for environmental screw spec.
Three types of graphite tube (high-density graphite tube, pyro-coated samples such as seawater YR-71 for C2H2 040-72020-01 AC2 fixing bracket
graphite tube, platform-type graphite tube) are available to suit the and industrial waste, as MAF85S for N20 040-72019-11 W22-14RH
0ppb 2ppb 4ppb
added properties of the analyzed elements and sample. well as biological samples. MAF106S for Ar 040-72019-21 W22-14RH
12 13
Accessor i es
Accessories
Sp ecial A ccesso r ies
S t a n d a rd A c c e s s o ries
( R efer t o t h e “ A A Ser ies A ccesso r ies” b ro ch u r e fo r de ta i l s . )
Software to connect AA-6300 WizAArd software to CLASS-Agent Pyro-coated graphite tube 206-50588
H o l l ow - C a t h o d e L a m p
Product Name Part No. Remarks
L-233 series 200-38422-**
L-2433 series 200-38456-** For the SR method
14 15
Accessor i es
Accessories
Sp ecial A ccesso r ies
S t a n d a rd A c c e s s o ries
( R efer t o t h e “ A A Ser ies A ccesso r ies” b ro ch u r e fo r de ta i l s . )
Software to connect AA-6300 WizAArd software to CLASS-Agent Pyro-coated graphite tube 206-50588
H o l l ow - C a t h o d e L a m p
Product Name Part No. Remarks
L-233 series 200-38422-**
L-2433 series 200-38456-** For the SR method
14 15
Spe ci fi cati on s
A A-6 30 0 Au t o s a m p l e r ASC-6100F
Photometric Wavelength range 185 to 900nm Furnace kit ASK-6100
system Mounting Aberration-corrected Czerny-Turner mounting, Number of grating grooves: 1800lines/mm, Forcal length: 298 mm ASK-6300
Bandwidth 0.2 0.7 0.7 (Low) 2,0(Low) nm (4 step automatic switching )
Detector Photomultiplier (short wavelengths), semiconductor (long wavelengths) Specifications common to flame and furnace
No. of lamps mounted 6 Iamps, 2 user-selected lamps can be illuminated at the same time Function • Zero point detection
(1 for measurement,1 warming up for next measurement) • Auto rinse
Photometric method Flame: Optical double beam. Furnace: Electrical double beam
• Auto diagnosis
Background correction High-speed self-reversal method (BGC-SR), high-speed deuterium lamp method (BGC-D2)
• Random access
Lamp mode EMISSION, NON-BGC, BGC-SR, BGC-D2,
Max. no. of samples/ • For reagents - 8 positions
Software requirments MS-Windows XP/2000 (both can be accessed randomly)
Data reagents 60 samples
processing Parameter settings Wizard method
Measurement mode Flame suction method, flame microsampling method, furnace method Sample Container • 16mL sample vial (test tube for flame suction), or
Concentration Calibration curve method (can be selected from 1st, 2nd, and 3rd orders) 2mL (sample cup for flame micro-sampling/furnace)
conversion mode Standard addition method (1st order), simple standard addition method (1st order) • 40mL sample vial (glass container for flame suction), or
Repeat analysis Max. 20 times, Display of mean values, deviation (SD), coefficient of variation (RSD) 20mL (sample cup for flame micro-sampling/furnace)
Automatic exclusion of deviant value by setting SD and %RSD Nozzle rinse • Solvent discharge method (during flame micro-sampling/ furnace measurement)
Baseline correction Automatic correction of the baseline drift through offset processing in peak height/ peak area mode • Solvent aspiration method (during flame measurement)
Signal processing interval settings Signal processing interval setting in peak height/peak area mode Rinse water bottle 2L
Sensitivity correction Automatic calibration curve correction with sensitivity monitoring
Power requirements AC100V, 100VA, both 50/60Hz
Tabular data processing Calculation of final concentration from sample volume, Iab bench dilutions, autosampler dilutions, and weight factors
ASC-6100F: 330 W x 285 H x 280 D mm, 7.5kg
Multi-tasking Software such as word processors can be used while the measurements are running
If the ASC/ASK is combined: 360 W x 360 H x 280 D mm, 15kg
Parameters recall Template function available
Procedure/ results display MRT worksheet (MRT : Measured Result Table)
Results printout Summary report F u r n ace / ( f lam e m icro - sam p lin g ) sp ecif icat io n s
QA/QC-related It is possible to choose between aborting or continuing the measurement in the event of the Sampling function • Automatic dilution
reference values for the correlation coefficient, LCS, SPK, DUP, %RSD etc. being exceeded. • Automatic reagent addition
Electronic records • Management using login IDs/ passwords • Access restrictions according to user level
Syringe 250 µL
• Recording of the log • Audit trail • Electronic signatures
Injection volume 2 to 100 µL
Power requirements AC100V, 120V, 230V ±10% (no sudden voltage fluctuations)
Operational Repeatablity 1%R.S.D. (20 µL)
environment 230VA, 50/60Hz
Dimensions & Weight Width 835 x Depth 545 x Height 460mm, 70kg (not including the flue, protruding parts) Carryover • Rinse port Below 0.00001
Ambient temp. 10°C to 35°C • Mixing port Below 0.00001
Ambient humidity 20% to 80% (however, below 70% at over 30°C) Mixing port cleaning Solvent discharge method
Type Air-cooled premix type Solvent discharge and rinse with next sample
Burner unit
Burner head Made of titanium, 10cm slot (the 5cm slot for high temperature flames is optional.) Mixing function Uses the mixing port
Nebulizer Pt-lr capillary with teflon orifice and ceramic impact bead (Hydrofluoric acids can be used.) Max, mixable volume 600 µL
Chamber Polypropylene No. of reagents added Max. 4 solutions The injection order of the sample and reagent can be set (when not mixing)
Positioning control Automatic search for the optimal burner height, automatic adjustment of vertical position, The number of solutions that can be mixed are:
manual adjustment of back and forth position
• Calibration curve method: Max. 5 solutions
Flow rate control Fuel gas, support gas, automatic flow rate setting (0.1 L/min step), automatic search for the optimal gas flow rate
Gas control • Standard addition method: Max. 6 solutions
unit Safety measures • Safe ignition/ extinction sequence • Automatic extinction in a power failure
Automatic dilution With the calibration curve created by the measurement results for an unknown sample.
• Flashback prevention through gas pressure monitoring
• Prevention of raw gas release when the flame dies out • Burner misuse prevention reanalysis • Diluted by the factor that is automatically calculated so that it falls within the calibration curve range.
• Support for safety inspections through software, system safety mechanisms self-diagnostics function • To be set to 10 times in all cases when the factor cannot be calculated.
Heating control system Drying: Current control system through automatic temperature calibration
Graphite Perso n al C o m p u t er Sp ecif icat io n s
Furnace Ashing, atomization; digital temperature control via optical sensor system
A PC, display, and printer which satisfy the following specifications are required separately.
Atomizer Heating temp, range • Room temperature to 3000°C
GFA-EX7i Heating conditions setting • Max. 20 stages • 2 Iine switching of the inner gas type • Compatible OS: Microsoft Windows XP/2000 • CPU: Pentium 2 200MHz or better
• Setting of the high sensitivity mode • Enrichment inside furnace Max. 20 time • RAM: More than 128MB • HDD: More than 20MB required to install the AA software
• Optimal temperature program search function
• FDD: at least one 3.5 inch floppy disk drive • CD-ROM drive (for installing the software)
Safety measures • Cooling water monitor • Gas pressure (2 Iine) monitor • Overcurrent protection
• Display: XGA(1024 x 768) or better • RS232C serial port: at least 1 port
• Furnace block cooling check
Cooling water, Ar gas Cooling water: 0.6 to 1.5L/min (supply pressure 0.08 to 0.15MPa), water temp. 10 to 30°C • Keyboard • Mouse or pointing device • Printer
Ar gas: Max. 3.5L/min, supply pressure 0.32 to 0.38MPa
Note
Power requirements AC200V ±5%, max. 6000VA, both 50/60Hz • The PC, display, and printer are not included in the standard configuration. Make arrangements to obtain these separately.
Dimensions & weight of • 255 W mm x 428 D mmx 460 H mm, 41 kg • The ASC-6100F. ASK-6100, ASK-6300, GFA-EX7i are special accessories.
• The separate micro-sampling kit is required for flame micro-sampling measurement.
power supply unit • Windows is a registered trademark of Microsoft Corporation, USA.
16 17
Spe ci fi cati on s
A A-6 30 0 Au t o s a m p l e r ASC-6100F
Photometric Wavelength range 185 to 900nm Furnace kit ASK-6100
system Mounting Aberration-corrected Czerny-Turner mounting, Number of grating grooves: 1800lines/mm, Forcal length: 298 mm ASK-6300
Bandwidth 0.2 0.7 0.7 (Low) 2,0(Low) nm (4 step automatic switching )
Detector Photomultiplier (short wavelengths), semiconductor (long wavelengths) Specifications common to flame and furnace
No. of lamps mounted 6 Iamps, 2 user-selected lamps can be illuminated at the same time Function • Zero point detection
(1 for measurement,1 warming up for next measurement) • Auto rinse
Photometric method Flame: Optical double beam. Furnace: Electrical double beam
• Auto diagnosis
Background correction High-speed self-reversal method (BGC-SR), high-speed deuterium lamp method (BGC-D2)
• Random access
Lamp mode EMISSION, NON-BGC, BGC-SR, BGC-D2,
Max. no. of samples/ • For reagents - 8 positions
Software requirments MS-Windows XP/2000 (both can be accessed randomly)
Data reagents 60 samples
processing Parameter settings Wizard method
Measurement mode Flame suction method, flame microsampling method, furnace method Sample Container • 16mL sample vial (test tube for flame suction), or
Concentration Calibration curve method (can be selected from 1st, 2nd, and 3rd orders) 2mL (sample cup for flame micro-sampling/furnace)
conversion mode Standard addition method (1st order), simple standard addition method (1st order) • 40mL sample vial (glass container for flame suction), or
Repeat analysis Max. 20 times, Display of mean values, deviation (SD), coefficient of variation (RSD) 20mL (sample cup for flame micro-sampling/furnace)
Automatic exclusion of deviant value by setting SD and %RSD Nozzle rinse • Solvent discharge method (during flame micro-sampling/ furnace measurement)
Baseline correction Automatic correction of the baseline drift through offset processing in peak height/ peak area mode • Solvent aspiration method (during flame measurement)
Signal processing interval settings Signal processing interval setting in peak height/peak area mode Rinse water bottle 2L
Sensitivity correction Automatic calibration curve correction with sensitivity monitoring
Power requirements AC100V, 100VA, both 50/60Hz
Tabular data processing Calculation of final concentration from sample volume, Iab bench dilutions, autosampler dilutions, and weight factors
ASC-6100F: 330 W x 285 H x 280 D mm, 7.5kg
Multi-tasking Software such as word processors can be used while the measurements are running
If the ASC/ASK is combined: 360 W x 360 H x 280 D mm, 15kg
Parameters recall Template function available
Procedure/ results display MRT worksheet (MRT : Measured Result Table)
Results printout Summary report F u r n ace / ( f lam e m icro - sam p lin g ) sp ecif icat io n s
QA/QC-related It is possible to choose between aborting or continuing the measurement in the event of the Sampling function • Automatic dilution
reference values for the correlation coefficient, LCS, SPK, DUP, %RSD etc. being exceeded. • Automatic reagent addition
Electronic records • Management using login IDs/ passwords • Access restrictions according to user level
Syringe 250 µL
• Recording of the log • Audit trail • Electronic signatures
Injection volume 2 to 100 µL
Power requirements AC100V, 120V, 230V ±10% (no sudden voltage fluctuations)
Operational Repeatablity 1%R.S.D. (20 µL)
environment 230VA, 50/60Hz
Dimensions & Weight Width 835 x Depth 545 x Height 460mm, 70kg (not including the flue, protruding parts) Carryover • Rinse port Below 0.00001
Ambient temp. 10°C to 35°C • Mixing port Below 0.00001
Ambient humidity 20% to 80% (however, below 70% at over 30°C) Mixing port cleaning Solvent discharge method
Type Air-cooled premix type Solvent discharge and rinse with next sample
Burner unit
Burner head Made of titanium, 10cm slot (the 5cm slot for high temperature flames is optional.) Mixing function Uses the mixing port
Nebulizer Pt-lr capillary with teflon orifice and ceramic impact bead (Hydrofluoric acids can be used.) Max, mixable volume 600 µL
Chamber Polypropylene No. of reagents added Max. 4 solutions The injection order of the sample and reagent can be set (when not mixing)
Positioning control Automatic search for the optimal burner height, automatic adjustment of vertical position, The number of solutions that can be mixed are:
manual adjustment of back and forth position
• Calibration curve method: Max. 5 solutions
Flow rate control Fuel gas, support gas, automatic flow rate setting (0.1 L/min step), automatic search for the optimal gas flow rate
Gas control • Standard addition method: Max. 6 solutions
unit Safety measures • Safe ignition/ extinction sequence • Automatic extinction in a power failure
Automatic dilution With the calibration curve created by the measurement results for an unknown sample.
• Flashback prevention through gas pressure monitoring
• Prevention of raw gas release when the flame dies out • Burner misuse prevention reanalysis • Diluted by the factor that is automatically calculated so that it falls within the calibration curve range.
• Support for safety inspections through software, system safety mechanisms self-diagnostics function • To be set to 10 times in all cases when the factor cannot be calculated.
Heating control system Drying: Current control system through automatic temperature calibration
Graphite Perso n al C o m p u t er Sp ecif icat io n s
Furnace Ashing, atomization; digital temperature control via optical sensor system
A PC, display, and printer which satisfy the following specifications are required separately.
Atomizer Heating temp, range • Room temperature to 3000°C
GFA-EX7i Heating conditions setting • Max. 20 stages • 2 Iine switching of the inner gas type • Compatible OS: Microsoft Windows XP/2000 • CPU: Pentium 2 200MHz or better
• Setting of the high sensitivity mode • Enrichment inside furnace Max. 20 time • RAM: More than 128MB • HDD: More than 20MB required to install the AA software
• Optimal temperature program search function
• FDD: at least one 3.5 inch floppy disk drive • CD-ROM drive (for installing the software)
Safety measures • Cooling water monitor • Gas pressure (2 Iine) monitor • Overcurrent protection
• Display: XGA(1024 x 768) or better • RS232C serial port: at least 1 port
• Furnace block cooling check
Cooling water, Ar gas Cooling water: 0.6 to 1.5L/min (supply pressure 0.08 to 0.15MPa), water temp. 10 to 30°C • Keyboard • Mouse or pointing device • Printer
Ar gas: Max. 3.5L/min, supply pressure 0.32 to 0.38MPa
Note
Power requirements AC200V ±5%, max. 6000VA, both 50/60Hz • The PC, display, and printer are not included in the standard configuration. Make arrangements to obtain these separately.
Dimensions & weight of • 255 W mm x 428 D mmx 460 H mm, 41 kg • The ASC-6100F. ASK-6100, ASK-6300, GFA-EX7i are special accessories.
• The separate micro-sampling kit is required for flame micro-sampling measurement.
power supply unit • Windows is a registered trademark of Microsoft Corporation, USA.
16 17
I ns tal l ati on R e q u i r e m e n t s
1 . T h e Ta bl e F o r a f u ll syst em
Example of ventilation implementation
Prepare a table that is 150cm long (170cm if installing the GFA-EX7i), more
than 70cm deep, and strong enough to bear a load of 200kg. Leave
a 15 to 20cm space to the rear when installing the system. (The ASC is
attached to the instrument. The table is not required for the entire area of the
ASC bottom surface.) Exhaust fan
Wall
2 . Ve n t i l a t i o n
150~200
Approx. 700
The room must be ventilated as the combustible gas used in the atomic
255 835
absorption spectrophotometer may ignite.
450~550
Damper
3 . F l a m m a bl e s
545
When measuring inflammable samples, take care with the handling of
343
flammables, In addition, a fire extinguisher must be placed just in case there Approx. 700
is an accident.
450~550
460
360
280
4 . T h e Wa s t e D u c t
A duct for discharging the combustion gas of the burner must be installed
GFA-EX7i ASC-6100F AA-6300 Units: mm
above the atomic absorption spectrophotometer. +ASK-6100
+ASK-6300
460
5. Condensation
Avoid using the system in an environment where condensation is likely to F o r a f lam e syst em
occur. The system may not operate normally.
Units: mm
150~200
Pressure regulator Approx. 700
leaks due to deterioration of the hose. Acetylene gas
835
450~550
7 . Fa c i l i t i e s fo r F u r n a c e M e a s u r e m e n t
Full scale 0.5MPa 330
A mains water facility which provides water at a flow rate of 0.6 to 1.5L/min,
545
0.35MPa Dinitrogen oxide gas
with a water pressure of 0.08 to 0.15MPa, and at a water temperature of 10
Full scale 0.5MPa
280
to 30°C is required within 7m of the system (if the water pressure of the 0.35MPa
facility is high, the pressure can be reduced with the special accessory
460
pressure reducing valve). If a facility such as the one described is not Argon gas
Full scale 0.5MPa
available, make separate arrangements to obtain the special accessory 0.35MPa Drain separator
cooling water circulator and cooler connection kit. The maximum
consumption of the argon gas for furnace measurement is 3.5L/min.
Lab
Outdoors ASC-6100F AA-6300 Units: mm
Air compressor
Note
• The personal computer and printer are not shown above.
18 19
I ns tal l ati on R e q u i r e m e n t s
1 . T h e Ta bl e F o r a f u ll syst em
Example of ventilation implementation
Prepare a table that is 150cm long (170cm if installing the GFA-EX7i), more
than 70cm deep, and strong enough to bear a load of 200kg. Leave
a 15 to 20cm space to the rear when installing the system. (The ASC is
attached to the instrument. The table is not required for the entire area of the
ASC bottom surface.) Exhaust fan
Wall
2 . Ve n t i l a t i o n
150~200
Approx. 700
The room must be ventilated as the combustible gas used in the atomic
255 835
absorption spectrophotometer may ignite.
450~550
Damper
3 . F l a m m a bl e s
545
When measuring inflammable samples, take care with the handling of
343
flammables, In addition, a fire extinguisher must be placed just in case there Approx. 700
is an accident.
450~550
460
360
280
4 . T h e Wa s t e D u c t
A duct for discharging the combustion gas of the burner must be installed
GFA-EX7i ASC-6100F AA-6300 Units: mm
above the atomic absorption spectrophotometer. +ASK-6100
+ASK-6300
460
5. Condensation
Avoid using the system in an environment where condensation is likely to F o r a f lam e syst em
occur. The system may not operate normally.
Units: mm
150~200
Pressure regulator Approx. 700
leaks due to deterioration of the hose. Acetylene gas
835
450~550
7 . Fa c i l i t i e s fo r F u r n a c e M e a s u r e m e n t
Full scale 0.5MPa 330
A mains water facility which provides water at a flow rate of 0.6 to 1.5L/min,
545
0.35MPa Dinitrogen oxide gas
with a water pressure of 0.08 to 0.15MPa, and at a water temperature of 10
Full scale 0.5MPa
280
to 30°C is required within 7m of the system (if the water pressure of the 0.35MPa
facility is high, the pressure can be reduced with the special accessory
460
pressure reducing valve). If a facility such as the one described is not Argon gas
Full scale 0.5MPa
available, make separate arrangements to obtain the special accessory 0.35MPa Drain separator
cooling water circulator and cooler connection kit. The maximum
consumption of the argon gas for furnace measurement is 3.5L/min.
Lab
Outdoors ASC-6100F AA-6300 Units: mm
Air compressor
Note
• The personal computer and printer are not shown above.
18 19
C122-E056F
F l a me Sele c tio n
JQA-0376
URL http://www.shimadzu.com The contents of this brochure are subject to change without notice.