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CEB 30403
Air Pollution Control Technology
Experiment 2 Part I
MONITORING OF PARTICULATE MATTER BY HIGH VOLUME SAMPLER
PREPARED BY:
Thermo Anderson with High Volume Sampler (PM10) is an equipment to monitor the air
quality. PM10 is the abbreviation to particulate matter with a diameter equal to or less than
10micrometer. It is originates primarily from stationary and fugitive resources.
High Volume Sampler typically operated during a 24-hour sampling period. Total
suspended particulates can be collected as well as 10-micron or 2.5-micron particles. It
also can be used with cascade impactors.
Location
Experiment
Procedure;
Procedure : 1. Filter Identification: The qualitative filter paper was cut with
20.5cm x 25.5cm and put in the sealed plastic for protection from any
other particles. The initial weight of the filter paper was taken using
analytical balance. The location and date also were taking into
account.
2. Filter weighing: Gloves was used during handling all the filter papers.
The weight of the filter paper was taken and the filter paper was
place in the sealed plastic bag when weighing is complete. The filter
paper was put into storage.
3. Filter Sampling: The facelift wing nuts were loosening and the
faceplate was removed. The filter paper was removed from the sealed
plastic bag and was put at the center of the support screen with the
rough side of the filter facing upward. The wing nuts were tightening
to secure the filter paper. After sampling was completed for 24 hours,
the filter paper was put backed in the sealed plastic bag.
4. PM10 measurement: The filter paper was weighing for final reading
after run for 24 hours using analytical balance and the reading was
recorded. The concentration of PM10 was calculated. The filter paper
was put into the proper storage for the analysis.
Start
Filter Identification
Filter Weighing
Filter Sampling
PM10 Measurement
End
20.5cm
Figure 12: Cut Off Filter Paper
Dickson Chart is used to estimate and indicate the air flow during 24 hours sampling. The
red pen is used to indicate the air flow and make a circulation on the Dickson chart. The
sample will be rejected when the air flow is not consistent or unstable flow and also if the
sampling exceeds 24 hours.
HIGH VOLUME / PM10 DATA RECORD
Site / Station :
Sample Date :
Collection Date :
Time :
Initial Filter Weight :
Gross Filter Weight :
Net Particulate Weight (A) :
Flow Rate (Using air flow : 40 ft3/min
meter)
Running Time Meter (Initial) :
(Final) :
Total Sample Time : 1720 – 280 = 1440min = 24 hours
Total Air Volume : (40 X 1440) X 0.028 = 1612.8 m3
Experiment 2
ANALYSIS OF METALLIC AIR POLLUTANTS
Scope : This method describes a collection procedure for air contaminants and
an analytical procedure for determination of lead (Pb).
Sample : The air contaminants on 20.5cm x 25.5cm qualitative fiber glass was
Preparation collected, passing air through the filter for 24 hours. The filters were cut
into small pieces 6.6cm in diameter, and digest for 30minutes in 100mL
of HCl over low heat. The solution was removed and extracted the
solids three times for 15 minutes each time, with water. The extracts and
the HCl was combined and evaporated nearly to dryness. Redissolve in
10mL HCl and 10 drop of HNO3 was added. The solution was
transferred to a 50 mL volumetric flask and make up to volume with
Deionized water.
25.5 cm
20.5 cm
6.6 cm
6.6 cm
Figure 15: Pattern of sub-sampling. Positions of discs cut from each qualitative filter
paper.