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FLOPRO NT
Revision No. Revision 1.1
Originator Matt Offenbacher
Access M-I SWACO Internal
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W E L L B O R E
P R O D U C T I V I T Y
1 TABLE OF CONTENTS
1 Table Of Contents........................................................................................................................................................ 2
2 FLOPRO NT System Description ............................................................................................................................... 3
2.1 Applications ........................................................................................................................................................... 3
2.2 Limitations ............................................................................................................................................................. 3
3 Design and Planning .................................................................................................................................................... 4
4 System and Additives .................................................................................................................................................. 5
4.1 Base Fluid .............................................................................................................................................................. 6
4.2 Viscosifiers ............................................................................................................................................................ 6
4.3 Filtration Control Additives................................................................................................................................... 6
4.4 Bridging Materials ................................................................................................................................................. 7
4.5 Other Additives ..................................................................................................................................................... 8
5 System Preparation .................................................................................................................................................... 15
6 Properties and Maintenance....................................................................................................................................... 16
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6.1 Solids ................................................................................................................................................................... 17
6.2 Cement ................................................................................................................................................................. 17
6.3 Fluid Loss ............................................................................................................................................................ 18
6.4 Alkalinity ............................................................................................................................................................. 18
6.5 Density................................................................................................................................................................. 18
6.6 Losses .................................................................................................................................................................. 18
6.7 Rheology.............................................................................................................................................................. 19
6.8 Pipe Slugs ............................................................................................................................................................ 19
6.9 Stuck Pipe ............................................................................................................................................................ 20
6.10 Internal Oxidizer Additions ............................................................................................................................... 20
7 Displacements and Screen Running .......................................................................................................................... 21
8 MUDSOLV NG Filtercake Breaker Options ............................................................................................................ 21
9 Case Histories and Publications ................................................................................................................................ 22
10 Revision History ................................................................................................................................................. 23
2.1 APPLICATIONS
FLOPRO NT is suited to a wide variety of applications, from producers to injectors where a basic, minimally
damaging reservoir drill-in fluid is desired. FLOPRO NT has been used in over 1000 wells worldwide, primarily in
clean sands with limited reactive shale.
2.2 LIMITATIONS
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FLOPRO NT is not compatible with most divalent brines with the exception of low saturation calcium chloride.
DIPRO or DIPRO LD are recommended for divalent base brine applications. Where the filter cake is confined as
part of the completion, such as expandable screens or openhole gravel packs, a filter cake breaker is recommended
to maximize production.
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600 rev/min 68
300 rev/min 50
200 rev/min 42
100 rev/min 32
6 rev/min 13
3 rev/min 11
Yield Point, lb/100 ft2 18
Plastic Viscosity, cP 32
Low Shear Rate Viscosity, cP @ 0.0636 sec-1 30,893
4.2 VISCOSIFIERS
Clarified xanthan gum is the traditional viscosifier for FLOPRO NT. This biopolymer provides excellent hole
cleaning characteristics.
Specific
Product Concentration Thermal Stability Description
Gravity
FLO-VIS PLUS 0.25 1.5 lb/bbl > 250F (121C) 1.5 Clarified xanthan gum, dispersible
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FLO-VIS L 2-4 lb/bbl > 250F (121C) 0.96 Clarified xanthan gum, liquid (pre-dispersed)
Thermal extenders enable FLO-VIS products to remain stable up to 330F (166C).
Specific
Product Concentration Thermal Stability Description
Gravity
DUAL-FLO 8 12 lb/bbl 250F (166C) 1.5 Modified starch
FLO-TROL 8 12 lb/bbl 250F (166C) 1.5 Modified starch
DUAL-FLO HT 8 - 12 lb/bbl 325F (149C) 1.5 Modified high temperature starch
Other starch additives for FLOPRO NT require testing and approval before consideration. It is strongly
recommended that one of the products listed above, and only one of the products listed is used. These starch
additives provide optimal fluid loss control, supplemental rheology and respond to enzyme treatments.
The combination of FLO-VIS PLUS and FLOTROL is the preferred combination for low temperature applications.
Specific
Product Concentration Thermal Stability Description
Gravity
Sized calcium carbonate (minimum 98% acid
SAFE-CARB As required lb/bbl - 2.75
soluble)
Sized salt systems required a saturated base brine so that the bridging material does not enter into solution. Salt is
easily removed with water, making removal easier.
Specific
Product Concentration Thermal Stability Description
Gravity
FLO-WATE As required lb/bbl - 2.16 Sized sodium chloride for sized salt systems
Additional sized salt additives are available from third party suppliers with a varied particle size distributions.
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Common products have been analyzed for use in OPTIBRIDGE.
Specific
Product Concentration Thermal Stability Description
Gravity
Buffer for sodium base brine systems
Soda Ash As required lb/bbl - 2.51
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(non-formate)
Magnesium Oxide As required lb/bbl - 3.6 Buffer for divalent base brine systems.
Sodium Buffer for formate based brine systems
As required lb/bbl - 2.16
Bicarbonate only
Specific
Product Concentration Thermal Stability Description
Gravity
PTS-200 24 lb/bbl 330F (148C) 1.01 Polymer temperature stabilizer
Potassium
15+ lb/bbl - 1.91 Potassium formate salt
Formate
Sodium Formate 15+ lb/bbl - 1.92 Sodium formate salt
Magnesium Oxide 5 10 lb/bbl - 3.6 Magnesium oxide
MEG 1 10 %v/v - 1.11 Monoethylene glycol
Specific
Product Concentration Thermal Stability Description
Gravity
SAFE-SCAVITE II 0.05 0.25 %v/v - 1.355 Scale Inhibitor
No Scale Inhibitor
With Scale Inhibitor
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Formation water and calcium brine precipitate (left)
SAFE-SCAVITE II additive prevents scale formation (right)
Specific
Product Concentration Thermal Stability Description
Gravity
KLA-CURE 48 lb/bbl 300F (149C) 1.22 Amine shale inhibitor
Amine shale inhibitor, divalent brine
KLA-GARD 48 lb/bbl 400F (204C) 1.1
compatible
KLA-STOP 14 % v/v 250F (121C) 1.05 Premium polyamine shale inhibitor
4.5.5 Lubricant
Lubricants are a particular challenge in water-based RDF applications as they may be necessary but carry
serious risks if improperly applied. Cheesing (emulsion) and greasing may result in serious formation damage.
Lubricants tend to coat solids, inhibiting access by breaker systems to later remove filter cake. If a lubricant
may be required, thorough testing should be performed to establish compatibility. LUBE 776 and LOTORQ
frequently demonstrate cheesing and are not recommended for FLOPRO NT.
In general lubricant performance does not dramatically improve past 3% v/v concentration. Should a lubricant
be required, it is recommended that gradual additions are added to observe for an improvement in
performance, increasing up to 3% v/v.
Lubricant Additives for FLOPRO NT System
Specific
Product Concentration Thermal Stability Description
Gravity
STARGLIDE 13 % v/v > 200F (93C) 0.95 Lubricant
SAFE-LUBE 13 %v/v - 1.01 Soluble brine lubricant
SAFE-LUBE CW 13 %v/v - 1.05 Soluble brine lubricant for cold weather
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Cheese and grease are common terms used to describe serious incompatibilities observed with lubricants.
Greasing is a visible phase that adheres to surfaces and cheese is the solid phase that precipitates from a fluid.
Cheese and grease can be induced in the presence of calcium, solids, shear and other environments. Some
lubricants demonstrate high cheese/grease tendencies while others do not regardless, it is recommended that
any water-based RDF formulation using a lubricant be tested for such an issue before a lubricant is approved
for use in the field.
Excess Specific
Product Concentration (initial) Description
Sulfite Gravity
100 300
SAFE-SCAV NA 1 gal/100 bbl 1.285 Oxygen scavenger for monovalent brines
ppm
Specific
Product Concentration Thermal Stability Description
Gravity
Oxygen scavenger for divalent base
SAFE-SCAV CA 0.15 lb/bbl - 1.65
brines
4.5.7 Defoamer
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Foaming may be an issue during mixing. It is worthwhile to have a defoamer available to control any foaming.
While silicone based defoamers perform at very low concentration, alcohol-based defoamers are also an
option.
Specific
Product Concentration Thermal Stability Description
Gravity
DEFOAM EXTRA 0.03 0.05 %v/v - 1.0 High strength silicone defoamer
DEFOAM
0.03 0.05 %v/v - 1.01 High strength silicone defoamer
EXTREME
4.5.8 Biocide
Many water-based RDFs contain high salinity base brine and may not be subject to biodegradation; however,
most starch is extremely sensitive to bacteria. Precautionary considerations should always be taken with
regular treatments of biocide.
Biopolymers and starches are subject to bacterial degradation, particularly in low salinity fluids in warm
climates. Biocides have a short lifespan and must be added at regular intervals (depending on the chemical) to
remain effective.
Biocide selection is generally limited by the regulations of the region where they will be used. Triazine
products are proven effective with little impact on fluid properties. In the United States, glutaraldehyde is most
common due to regulatory requirements.
Glutaraldehyde products have the potential to induce cross linking when combined with xanthan and some
shale inhibitors.
Glutaraldehyde cross linking a FLOPRO NT system with KLA-STOP. This can be avoided by substituting an
alternate biocide (preferred) or mitigated by thoroughly blending the biocide prior to adding xanthan and
shale inhibitor.
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Triazine 3/ 0.5a gal/100 bbl 55 1.155 Triazine
Greencide 25G 2 / 0.5b gal/100 bbl 25 1.067 Glutaraldehyde
X-Cide 102 2 / 0.5b gal/100 bbl 25 1.056 Glutaraldehyde
a
Weekly maintenance bDaily maintenance
Specific
Product Concentration Thermal Stability Description
Gravity
Zinc Carbonate 1.5 3 lb/bbl - 3.5 Zinc-based H2S scavenger
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Zinc Oxide 12 lb/bbl - 5.5 Zinc-based H2S scavenger
SAFE-SCAV HS 0.1 lb/bbl - 1.08 Zinc free H2S scavenger
SAFE-SCAV HSW 0.1 lb/bbl - 1.08 Zinc free H2S scavenger
Specific
Product Concentration Thermal Stability Description
Gravity
Preferred product. Coated internal
D-STROYER 0.5 2 lb/bbl - ~2.5 oxidizer. Drop in pH destroys coating
and activates oxidizer within filter cake.
Internal oxidizer. pH must be maintained
SAFE-BREAK MP 12 lb/bbl - 3
above 9 to avoid premature activation.
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5 SYSTEM PREPARATION
FLOPRO NT system preparation is simple but requires patience and care to avoid the creation of fisheyes when adding
polymers to the system.
Mixing FLOPRO NT at the liquid mud plant
Addition of large particles will depend upon rig capabilities to handle big bags, transport equipment to agitate and the
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duration the system will remain in transport.
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Modified HPHT filter press cell
A viscometer sag shoe test (VSST) may be run where necessary to monitor for sag risk. Review high risk wells for sag
potential. Conventional FLOPRO NT systems present a low sag risk unless weight/bridging material is not
appropriately dispersed.
6.1 SOLIDS
As with all reservoir drill-in fluids, solids must be monitored and treated with system dilution to prevent
contamination of the filter cake. Depending upon the type of well, the acid insoluble solids limit ranges from 1 to
2% v/v unless otherwise directed.
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Reactive solids are generally inhibited by the base brine, but the MBT should stay below 5 lb/bbl. Solids control
should be limited to shaker screens. Do not use centrifuges.
6.2 CEMENT
As with many polymer water-based drilling fluids, FLOPRO NT is susceptible to cement contamination. To avoid
contamination of the system, any cement should be drilled with the mud used to drill the upper part of the hole (or
seawater, if possible). If the FLOPRO NT system must be used to drill cement, pre-treatment with sodium
bicarbonate, magnesium oxide and/or citric acid is required. The most significant contaminant would be green
cement left on top of the wiper plugs. This cement should definitely be drilled with another system. In re-entry
wells or wells where the cement has had sufficient time to cure, cement contamination in FLOPRO NT has not been
a problem.
6.4 ALKALINITY
The pH should be maintained using the buffer selected during testing. Buffers are preferred sources of alkalinity.
High alkalinity filtrate may react with crude organic acids as a source of formation damage. Some clays are highly
reactive at high pH. Managing the pH within the appropriate range is effective in preventing these reactions.
Caustic soda should not be used as it is not a true buffer. It will lead to pH spikes that will adversely impact other
RDF additives and diminish fluid performance.
6.5 DENSITY
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The preferred density mechanism is through additional salt to the point of saturation. If additional weight is
required, calcium carbonate may be used to about 2.0 lb/gal above saturation. Calcium carbonate is primarily for
bridging and appropriate ratios of sized carbonates should be maintained.
In some situations, such as well control, barite may be used. In non-damaging applications it should be avoided
because it cannot be acidized. The planning phase should focus on achieving required density through base brine
and calcium carbonate.
To continuously weight up the solids-laden system with additional calcium carbonate will cause a significant
increase in viscosity and may hamper the cleanup efficiency. To avoid the undesired viscosity increase, the best
way to weight up is to use stock brine and/or appropriate salt, not to exceed saturation of the base brine in
conventional FLOPRO NT systems. To maintain product concentration, additional FLO-VIS PLUS and
FLOTROL may be required.
6.6 LOSSES
Seepage losses can be controlled through the addition of fine SAFE-CARB and FLOTROL. Increased viscosity
will aid to reduce loss rates into the formation. Elevated loss rates should be managed through a lost circulation
plan that includes pills featuring coarse SAFE-CARB.
6.7 RHEOLOGY
Low shear rate viscosity should be measured at bottom hole temperature (up to 180F/82C) where possible. In
high angle wells (55-75), the low shear rate viscosity should be greater than15,000 cP and ideally 20,000 cP or
greater.
Sweeps should not be necessary due to the elevated LSRV of FLOPRO NT. Risk of washout should limit any
sweep consideration to viscous, weighted sweeps. Adjust low end rheology readings with FLO-VIS PLUS. If
rheology is maintained at correct parameters, sweeps should not be required. Penetration rates of up to 200 ft/hr in
8 horizontal holes have been attained without hole cleaning problems. Simulate the ECD impact of the sweep
using VIRTUAL HYDRAULICS RHECON.
If a sweep is desired, increase the LSRV with FLO-VIS PLUS or FLO-VIS L to 100,000 cP, pumping sufficient
volume to cover 300 feet of the maximum annulus. The density may be elevated 1-2 lb/gal above the system
density with salt or calcium carbonate, but returns may have to be isolated. Observe the shakers for any increase in
cuttings.
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drill string. This is even more difficult in increased hole angle and with restrictions through the bottom hole
assembly. Slugging the pipe is still possible, but it is not guaranteed. Brine water has successfully slugged 3 2
drill strings. Most success has been found in 8 hole using the steps below:
Step Operation
Preparing for the possibility that slugs do not work, a correctly sized mud bucket with new rubber seals should be
available if possible. These have been used with great success when in proper condition for wet trips.
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pipe is free. circulation is established. Interface will
be low pH.
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The MUDSOLV NG service is designed to function in concert with optimized reservoir drill-in fluids for best
performance while integrated filter cake treatment into the completion phase, minimizing cost.
Performance Reports
Clark, P. 2002. FLOPRO NT and WELLZYME AE Help to Maximize Production in the North Sea. Performance
Report.
Diaz, L. 2005. Venezuela: FLOPRO formate system improves performance in microfractured zones. Performance
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Report.
Dick, M. 2008. FLOPRO NT Fluid Plus KLA-STOP Additive Stabilized Shale in Producing Intervals Completed with
Standalone Screens. Performance Report.
Klein, L. 2004. FLOPRO NT System Significantly Improves Production from Declining Well. Performance Report.
Unknown author. 2010. FLOPRO NT System Combats Abnormally Low Formation Pressure, High Permeability
Conditions. Performance report.
10 REVISION HISTORY
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