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or distribution, of this document and its contents are strictly prohibited unless expressly authorized in
writing by Lurgi. Offenders are liable for damages. All rights, including but not limited to all proprietary
Rev. 0a
rights in relation to patents, utility models and/or other industrial property rights, are reserved.
Lurgi Process DS Cover Sheet.xls
00
Revision
Case-Name:
All
Sheet
Normal Case
Name
Project Name
PuWa
Date
Prepared, Revised
04/10/2015
DiS
Name
Checked
CS
Name
Project No.
Cover
Process
Date
Approved
04/10/2015
06-T-0103
H2S Flash Column
Process Data Sheet
Index of Revisions
IFI
Status
Document No.
Issued for Information
/
00
Sheet / of Q.L. Revision
CONFIDENTIAL
Process
Rectisol
Any exploitation and/or other utilization, including but not limited to reproduction, dissemination and/
02 Unit Name
rights in relation to patents, utility models and/or other industrial property rights, are reserved.
General Notes:
1) For Tray design use information provided in "General Notes for column ".
Lurgi Process DS Column-Reactor Sections.xls
2 / 12 00
Case-Name: Normal Case Printed by / date / time: / /
Process
Rectisol
Any exploitation and/or other utilization, including but not limited to reproduction, dissemination and/
02 Unit Name
rights in relation to patents, utility models and/or other industrial property rights, are reserved.
3 / 12 00
Case-Name: Normal Case Printed by / date / time: / /
Process
Rectisol
Any exploitation and/or other utilization, including but not limited to reproduction, dissemination and/
02 Unit Name
rights in relation to patents, utility models and/or other industrial property rights, are reserved.
13 M8
1)
14 N 12
15 1
19x16"=304"
16
2 ) R e f e r t o D e t a il 1
17
18
19 20
20
35"
21 M7
21
22
1078"
19x16"=304"
23
24
25
26 40
27
35"
M6
28
T.L.-T.L. 204'
41
29
20x16"=320"
30
1590"
31
32
33
61
34
35 P2 00 1
S e c t io n I I
80"
36
37 2)
38 N 11 M5
39 1 1 / 2 " P a ll R in g s
20"
40 3 c e n t e r p i p e s1 2 " e a c h
41 N o v a p o r flo w
512"
th ro u g h p a c k e d b e d
42
20"
N10
43 P2
L3 B
44 L4B
382"
45
46 M4
47 L3 A ID 9 8 "
10"
L4A
48
49 V o rte x B re a k e r
50
51
V1
52 N9
N8
53 D2
54
55
56
Lurgi Process DS Sketch.xls
57
4 / 12 00
Case-Name: Normal Case Printed by / date / time: / /
Process
Rectisol
Any exploitation and/or other utilization, including but not limited to reproduction, dissemination and/
02 Unit Name
rights in relation to patents, utility models and/or other industrial property rights, are reserved.
17 N8
18 D2
19
20
21 1) To be confirm ed by dem ister
22 m anufacturer/ contractor
23
59"
24 1) Section III
T.L.-T.L. 204'
25 M3
26 N7
27 62
251"
28
12x16"=192"
29
30
31
771"
32
33
34 74
35
N6
Section IV
80"
36
P1
37 N5 M2
01
38 N14 1 1/2" P all R ings
N3 N4
39 3 center pipes 12" each
20"
40 N o vapor flow
41 through packed bed
520"
42
20"
43 L5B N2
44 L6B
L1B P1
45 L2B
46
390"
01
47 L5A
L6A M1
48 L1A
49 L2A
10"
50 T.L.
51 V ortex B re aker
Min. required
52
53
for piping
54
55 N1
56 D1
Lurgi Process DS Sketch.xls
57
5 / 12 00
Case-Name: Normal Case Printed by / date / time: / /
Process
Rectisol
Any exploitation and/or other utilization, including but not limited to reproduction, dissemination and/
02 Unit Name
rights in relation to patents, utility models and/or other industrial property rights, are reserved.
15
16
X X
17
18
B
A
( C ol u m n i n n e r di a m et er)
19
C
20 N ozzle N 1 1
21
D2
D1
22
23
24
25
26
27
28
29
30
31 H 2 S Fla sh C o lum n
32 N o zzle N 11
33 In let stre am 19 4
34 A inch 26 .8
35 B inch 3 6.6
36 C inch B y C on tra ctor
37 D S elected inch 23.6
S ection X
- X:
38 G D1 inch 98.0
39 D2 inch 2 0.0
40 L D3 inch 6.0
41 d4 inch 0.4
42 G S ele cted inch 11.8
8.3
I
43 15 15 H S elected inch
H
15 15 V apour
44 I inch 4.3
45 L inch 4.0
D3
46
N u m b er of hole at A 12 5x4
47 Liquid at B 150x2
48 To tal 80 0
49
d4
50
A ll h oles should be arranged in a un iform distrib ution all
51 over the distribu tion pipe le.ngth
52
53 T he m axim um differe ntial pressure drop of the distrib uto r
t
6 / 12 00
Case-Name: Normal Case Printed by / date / time: / /
Process
Rectisol
Any exploitation and/or other utilization, including but not limited to reproduction, dissemination and/
02 Unit Name
rights in relation to patents, utility models and/or other industrial property rights, are reserved.
B
19
A
C
D2
D1
N ozzle N3
24
25
26
Nozzle N14
27
28
29
30
31
32
33
34 Section X- X :
G
35
L
The m axim um differential pressure drop of the distributor
36 should not be higher than 7 psi at m axim um flow rate
37
D iam eter of holes (d4 ): 0. 3 to 0. 6 inch
I
38 15 15
H
15 15
40
41
42
43
d4
44
45
t
46
47
48
49
50
All holes should be arranged uniformly all over the
51 distributor pipe length
52
53
54 .
55
56
Lurgi Process DS Sketch.xls
57
7 / 12 00
Case-Name: Normal Case Printed by / date / time: / /
Process
Rectisol
Any exploitation and/or other utilization, including but not limited to reproduction, dissemination and/
02 Unit Name
rights in relation to patents, utility models and/or other industrial property rights, are reserved.
20 Operating temperature
21 Normal load lb/h 109515 110047 451935
22 Required load min. max. % 40.00 110.00 40.00 110.00 33.00 110.00
23 Density @ t op lb/ft 61.94 61.45 56.79
24 Dynamic viscosity @ t op
cP 0.99 0.93 0.72
25 Surface tension dyn/cm 23.56 23.35 22.53
26 Allowable pressure drop per tray psi 0.11 0.11 0.11
27 Allowable level in the downcomer in
28 Allowable hold-up time in the downcomer h
29 Allowable leakage rate per tray lb/h
30 Allowable flooding factor % 80 80 80
31 Foaming factor (system factor) 1 1 1
32 Column inside calculated in 68 68 98
33 diameter selected in
34 Type of tray Valve Valve Valve
35 Tray spacing in 16 16 16
36 Number of passes 1 1 2
37 Tray CS CS CS
Material
38 Valve SS SS SS
39 Bubble or tunnel caps
40
41 Remarks: row 8, 9) Count from top
row 32, 35) To be stated by tray manufacturer
Internals to be installed into the column/vessel through a manhole.
Maximum recommended downcomer inlet velocity: 0.39 ft/s
Maximum recommended downcomer clear liquid backup: 40%, I.e. 0.4 (TS + h_weir)
TS: Tray Spacing
h_weir: Outlet Weir Height
General Notes:
Row 34) Vendor to select appropriate Valves for column tray to accomodate high turdown ratios. Both Heavy valves and Light valves
to be used to optimize the tray design
Lurgi Process DS Tray.xls
8 / 12 00
Case-Name: Normal Case Printed by / date / time: / /
Process
Rectisol
Any exploitation and/or other utilization, including but not limited to reproduction, dissemination and/
02 Unit Name
rights in relation to patents, utility models and/or other industrial property rights, are reserved.
20 Operating temperature
21 Normal load lb/h 480760
22 Required load min. max. % 33.00 110.00
23 Density @ t op lb/ft 57.25
24 Dynamic viscosity @ t op
cP 0.59
25 Surface tension dyn/cm 21.17
26 Allowable pressure drop per tray psi 0.11
27 Allowable level in the downcomer in
28 Allowable hold-up time in the downcomer h
29 Allowable leakage rate per tray lb/h
30 Allowable flooding factor % 80
31 Foaming factor (system factor) 1
32 Column inside calculated in 98
33 diameter selected in
34 Type of tray Valve
35 Tray spacing in 16
36 Number of passes 2
37 Tray CS
Material
38 Valve SS
39 Bubble or tunnel caps
40
41 Remarks: row 8, 9) Count from top
row 32, 35) To be stated by tray manufacturer
Internals to be installed into the column/vessel through a manhole.
Maximum recommended downcomer inlet velocity: 0.39 ft/s
Maximum recommended downcomer clear liquid backup: 40%, I.e. 0.4 (TS + h_weir)
TS: Tray Spacing
h_weir: Outlet Weir Height
General Notes:
Row 34) Vendor to select appropriate Valves for column tray to accomodate high turdown ratios. Both Heavy valves and Light valves
to be used to optimize the tray design
Lurgi Process DS Tray.xls
9 / 12 00
Case-Name: Normal Case Printed by / date / time: / /
Process
Rectisol
Any exploitation and/or other utilization, including but not limited to reproduction, dissemination and/
02 Unit Name
rights in relation to patents, utility models and/or other industrial property rights, are reserved.
10 / 12 00
Case-Name: Normal Case Printed by / date / time: / /
Process
04
05 Case Normal Case
06 Nozzle-ID N1 N3 N6 N7
07 Nozzle designation H2S Laden Methanol H2S Laden Methanol Inlet Recycle Gas inlet from H2S Laden Methanol Inlet
08 Outlet to Section II to Sec-IV from 06-T-0102 06-T-0104 to Sec-IV to Sec-III from 06-P-0105 >
09 Stream no.
10 Internal stream no. 192 191 280 212
11 Stream designation MP Flashed H2S Methanol H2S Laden Methanol Recycle Gas H2S Laden Methanol
12 from 06-T-0103 to 06-T-0102 & 06-T-0113 from 06-T-0104 to 06-T-0103
13 Phase Liquid Mixed Vapour Liquid
14 Total flow lbmol/h 47041.0 34614 1957.8 12200.0
15 Total flow lb/h 1668902 1249190 68958 402005
16 Liquid Vapour Liquid Vapour Liquid Vapour Liquid Vapour
17 Vol. flow ft/h 27842.74 - 19622 - - 7153.16 -
18 Norm. vol. flow lbmol/h - - 607.46 - 1957.8 -
19 Mass flow lb/h 1668902 1198230 50955.45 68958 402005
20 Mole flow lbmol/h 47041.0 33280.72 1338.57 1957.8 12200.0
21 Molweight lb/lbmol 35.48 36 38.07 35.22 32.95
22 Eff. density lb/ft 59.94 61.06 2.42 2.06 56.20
23 Spec. heat cap. Btu/(lb F) 0.59 0.59 0.25 0.25 0.57
24 Viscosity cP 0.55 0.52 0.14 0.01 1.19
25 Ther. conductivity (Btu/h)/(ft F) 0.10 0.02 0.12
26 Mole fraction fraction 1.00 1.00 1.00
27 Mass fraction fraction 1.00 0.96 0.04 1.00 1.00
28 Temperature F 3 0.28 -7 -27
29 Pressure psi[g] 242.0 260.87 242.0 251.2
30
31 Nozzle-ID N8 N9 N11 N12
32 Nozzle designation Recycle Gas Outlet from H2S Laden Methanol H2S Laden Methanol from CO2 Laden Methanol to
33 Sec-III to 06-V-0130-1 Outlet from Sec-II to 06-T-> Sec-IV to Sec-II Sec-I from 06-E-0110
34 Stream no. 270 195 194
35 Internal stream no. 270 195 194 181
36 Stream designation Recycle Gas H2S Laden MeOH from Flashed H2S Laden MeOH CO2 Laden Methanol
37 from 06-T-0103 06-T-0103 to 06-T-0107 to 06-T-0103 Sec II to 06-T-0103
38 Phase Vapour Liquid Mixed Liquid
39 Total flow lbmol/h 1748.1 47655.0 47041.0 3150.0
40 Total flow lb/h 51777 1670071 1668902 111559
41 Liquid Vapour Liquid Vapour Liquid Vapour Liquid Vapour
42 Vol. flow ft/h - 27355.28 - 27114.33 - 1799.14 -
43 Norm. vol. flow lbmol/h - 1748.1 - - 236.1 -
44 Mass flow lb/h 51777 1670071 1659216 9686 111559
45 Mole flow lbmol/h 1748.1 47655.0 46804.5 236.5 3150.0
46 Molweight lb/lbmol 29.62 35.05 35.45 40.96 35.42
47 Eff. density lb/ft 1.61 61.05 61.19 1.43 62.01
48 Spec. heat cap. Btu/(lb F) 0.28 0.62 0.61 0.22 0.63
49 Viscosity cP 0.01 0.93 0.73 0.012 0.92
50 Ther. conductivity (Btu/h)/(ft F) 0.02 0.11 0.10 0.01 0.11
51 Mole fraction fraction 1.00 1.00 0.995 0.005 1.00
52 Mass fraction fraction 1.00 1.00 0.99 0.01 1.00
53 Temperature F 4 -38 -23 -40
Lurgi Process DS Nozzle Stream Table.xls
11 / 12 00
Case-Name: Normal Case Printed by / date / time: / /
Process
04
05 Case Normal Case
06 Nozzle-ID N13 N14
07 Nozzle designation LP1 CO2 Product Out H2S Laden Methanol Inlet
08 from Sec-I to 06-E-0116 to Sec-IV from 06-T-0113
09 Stream no.
10 Internal stream no. 230 691
11 Stream designation LP1-CO2 Product CO2 Laden Methanol
12 from 06-T-0103 (top) to 06-T-0103
13 Phase Vapour Mixed
14 Total flow lbmol/h 2535.9 13023.4
15 Total flow lb/h 110390 471384
16 Liquid Vapour Liquid Vapour Liquid Vapour Liquid Vapour
17 Vol. flow ft/h - 7338.05 - - -
18 Norm. vol. flow kmol/h - 1150.3 - 295.4 - -
19 Mass flow lb/h 110390 445614 25771
20 Mole flow lbmol/h 2535.9 12372.1 651.4
21 Molweight lb/lbmol 43.53 36.02 39.56
22 Eff. density lb/ft 0.89 60.73 2.51
23 Spec. heat cap. Btu/(lb F) 0.20 0.58 0.25
24 Viscosity cP 0.01 0.49 0.01
25 Ther. conductivity (Btu/h)/(ft F) 0.01 0.09 0.01
26 Mole fraction fraction 1.00 0.95 0.05
27 Mass fraction fraction 1.00 0.95 0.05
28 Temperature F -44 7
29 Pressure psi[g] 70.3 260.9
30
31 Nozzle-ID
32 Nozzle designation
33
34 Stream no.
35 Internal stream no.
36 Stream designation
37
38 Phase
39 Total flow lbmol/h
40 Total flow lb/h
41 Liquid Vapour Liquid Vapour Liquid Vapour Liquid Vapour
42 Vol. flow ft/h - - - -
43 Norm. vol. flow lbmol/h - - - -
44 Mass flow lb/h
45 Mole flow lbmol/h
46 Molweight lb/lbmol
47 Eff. density lb/ft
48 Spec. heat cap. Btu/(lb F)
49 Viscosity cP
50 Ther. conductivity (Btu/h)/(ft F)
51 Mole fraction fraction
52 Mass fraction fraction
53 Temperature F
Lurgi Process DS Nozzle Stream Table.xls
54 Pressure psi[g]
55 Remarks:
12 / 12 00
Case-Name: Normal Case Printed by / date / time: / /