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Abstract
In this study, stress relaxation phenomenon has been examined generally. Experiments were carried out on carbon steel wires with diameter
8 mm which are particularly used in prestressed concrete composites. Thermomechanically heat treatment was also carried out on this wire in
order to relieve the residual stresses accumulated after the cold work. The heat treatment temperature and the stretch ratio, which are the
parameters of thermomechanical heat treatment, were changed. Thermomechanical heat treatment experiments have been performed under
two separate groups. In one of the groups, stretch ratios were changed at a constant temperature of 350 8C. In the other group, the heat
treatment temperature was changed while the strain ratio was constant at 40%. The optimum thermomechanical heat treatment conditions
have been determined by changing the heat treatment temperature and stretch ratio and by observing the effect of these changes of tensile
stress and stress relaxation behaviour of the cold drawn steel wires.
It is not always feasible to perform stress relaxation experiments in long periods of time as 1000 h. The general conditions of the
laboratories are not suitable to permit this period of time. In this study, the results of the relaxation experiments are emphasised with empirical
formulas.
# 2003 Elsevier Science B.V. All rights reserved.
0924-0136/$ see front matter # 2003 Elsevier Science B.V. All rights reserved.
doi:10.1016/S0924-0136(03)00131-6
A. Zeren, M. Zeren / Journal of Materials Processing Technology 141 (2003) 8692 87
Table 2
Parameters of thermomechanical heat treatmenta
Non-treated Non-treated
20% stretch 250 8C
30% stretch 300 8C
40% stretch 350 8C
50% stretch 400 8C
a
Test material: steel specimen with 8 mm diameter.
2. Experimental study
Table 1
Chemical composition range of the steels tested
Fig. 4. The relationship between the relaxation and time for a constant stretch ratio of 40% and varying temperatures.
been placed in to a 30 t capacity machine chamber with the cementite lamella lying unfavourable to the deformation
20 8C temperature control precision and experiments are direction are broken. The tensile behaviour of this sorbitic
done with Metro-Com relaxation test equipment for 100 microstructure can be seen from Figs. 2 and 3, where the
200 h. As an initial strength 80% of tensile strength of first specimens had their highest Rp 0.1, Rp 0.2 and Rm values in
pieces from each group are taken. Results are plotted in log the temperature range of 350400 8C. A possible explana-
time vs. relaxation 100P0 P1 =P0 in the diagrams, tion of this behaviour is that in the cold drawn wire the
where P0 is the initial load and P1 the ultimate load. Stress diffusion is faster at elevated temperatures. Generally, small
relaxation test results are shown in Fig. 4. Here the specimens carbon and nitrogen atoms move fast at low temperatures
are prepared with constant stretch ratio and various tempera- and they are locked in the dislocations. This is the reason of
tures. In Fig. 5 also the result is shown where the specimen increased strength. Studies done at higher temperatures
are prepared at a constant temperature T 350 C and compared to this work show that there is a decrease of
various stretch ratios. strength in the higher temperatures due to the decrease of
A typical cold drawn wire microstructure is shown in cold work effect [13]. In Fig. 3, it is shown that the results
Fig. 6. As it can be seen from the light microscope micro- from the thermomechanical heat treatments in constant
graph the whole microstructure consists of fine pearlite. temperature and various stretch ratios are shown that Rp
The structure shows a heavy deformation where the pearlite 0.1, Rp 0.2, and Rm values are maximum at 4050% stretch
grains are elongated in the deformation direction. Some of ratio.
Fig. 5. The relationship between the relaxation and time for a constant temperature of 350 8C and varying stretch ratios.
A. Zeren, M. Zeren / Journal of Materials Processing Technology 141 (2003) 8692 89
Fig. 6. The cold drawn wire microstructure, fine pearlite, light microscopical image. The structure is etched with nital.
Fig. 7. The comparison of the experimental results with the s0/sstretch ratio values derived from the equations of Stussi, Maura, Sozen, Sies [1517] and
our modified equation.
Fig. 8. The comparison of the experimental results with the s0/stemperature values derived from the equations of Stussi, Maura, Sozen, and our modified
equation.
covers all types of steel, and is unchanged for normal and 3. Conclusions
lower relaxation in the steel, a new constant is determined by
the equation formed from the program which is given in This study is an attempt to show the effects of thermo-
Appendix A [15]. mechanical heat treatment on cold drawn carbon steels. The
Equations for normal (4) and lower relaxation (5) samples conclusions of this study are shown below:
are given below:
During the thermomechanical heat treatments which have
s log t s0 been carried out at various temperatures ranges and at
1 0:67 (4) constant stretching, it is observed from Fig. 2 that the
s0 10 sA
specimens had their highest Rp 0.1, Rp 0.2, Rm values in
s log t s0 the temperature range of 350400 8C.
1 0:73 (5) Results from the thermomechanical heat treatments at con-
s0 10 sA
stant temperature and various stretch ratios show that Rp
Values derived from these equations are compared with the 0.1, Rp 0.2, Rm values were maximum at 50% stretch ratio.
experimental results. In Figs. 7 and 8, comparison of the For constant stretch ratio and various temperature ranges,
experimental results with the values derived from the equa- the lowest stress relaxation value are observed in speci-
tions of Stussi et al., and our modified equations are shown. mens, which were heat treated at 400 8C.
The experimental results are similar to those derived from For specimens treated at a constant temperature and
the equations of Stussi, as it is seen from the figures. different stretch ratios, it was seen that the specimens
A. Zeren, M. Zeren / Journal of Materials Processing Technology 141 (2003) 8692 91
with 4050%-applied stretch have the lowest stress the requirement of 1000 h test or the whole period of
relaxation values. servicing. These equations shall prevent time consump-
It is evident that the relaxation rate can be determined by tion by providing a preliminary idea during production
the extrapolation of the figures using Eqs. (1)(5), without and planning.
Appendix A
92 A. Zeren, M. Zeren / Journal of Materials Processing Technology 141 (2003) 8692
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