Professional Documents
Culture Documents
Laboratory Activities
2010-2011
Theodore Roosevelt High School
Mr. Carman & Mr. Knopick
Lab Activities Syllabus
The order and content of this syllabus may change depending on school events, snow days, materials
availability, and other schedule disruptions.
1. I will wear safety goggles at all times while working in the lab. If I wear contact lenses, I
will consult with my eye care professional about wearing contact lenses in the lab.
6. I will follow closely all written and verbal instructions. I will read the lab procedures before
the lab, and I will not skip steps.
10. I will use the wafting method when noting odors. I will use the fume hood when working
with chemicals that have noxious or toxic fumes.
11. I will keep flames away from any substance or object not involved in the lab. I will keep
flames away from flammable liquids.
12. I will heat only PYREX glassware that is free of chips and cracks.
13. I will dispose of broken glass ONLY in the Broken Glassware box; I will NOT place any
other trash in the Broken Glassware box.
14. I will distribute heat evenly along test tubes while pointing the open mouth away from
anyone nearby.
16. I will NOT put solids in the sink under any condition.
17. I will clean my lab area and glassware, return materials to their proper places, dispose of
any chemicals in their proper location, place trash in the trash can, and wash my hands
before leaving the lab.
How to Write a Lab Report
"An experiment is only as good as the lab report that describes it."
Lab reports are an essential part of all college laboratory courses and usually a significant part of your
grade. A lab report is how you explain what you did in experiment, what you learned, and what the
results meant. In CP Chemistry, you will submit your lab reports via Moodle, available at
http://www.kentschools.net/moodle/, within two days of completing the lab activity in class. Lab
reports will account for 30% of your total quarter grade.
Questions (6 pts)
This is where you will perform any calculations and answer any questions based on your data and/or
observations. Calculations worth more than one point usually require more than one step; questions
worth more than one point usually require more than one answer.
Errors (4 pts)
This is where you discuss any mistakes (at least two) you might have made while conducting the
experiment and describe the ways you might avoid those errors in future experiments. Stating our
Conclusion (5 pts)
Your conclusion should consist of at least two paragraphs that sum up what happened in the
experiment, whether your hypothesis (prediction) was accepted or rejected, and what your data and
results mean. Your interpretation of the experiment and its results is the most important part of your lab
report!
Modified from How to Write a Lab Report: Lab Reports Describe Your Experiment by Anne Marie Helmenstine, Ph.D.,
About.com (http://chemistry.about.com/od/chemistrylabexperiments/a/labreports.htm)
st
1 Quarter
Laboratory Activities
CP Chemistry Theodore Roosevelt High School Lab #1-0
By observing several scientific phenomena in this lab, you will discover that each logical method has its
own advantages and disadvantages. Because this is an exploratory stations lab, you will not be
required to turn in a write-up on Moodle for this activity.
Purpose
To practice explaining observations of scientific phenomena.
Safety Considerations
Stations 4 & 5 use acids and bases that require you to wear goggles for safety.
Stations 5 & 7 use dry ice, which can cause frostbite with prolonged exposure to the skin. Only
use tongs to manipulate the dry ice, NOT your hands.
Procedure
1. Complete the activities at each of the eight lab stations per the supplied directions.
2. Record your observations for each lab station.
CP Chemistry Theodore Roosevelt High School Lab #1-0
Station 1
Station 2
Station 3
Station 4
Station 5
Station 6
Station 7
Station 8
Errors
Think of two possible errors you may have committed in this lab that may have somehow affected your
results and record them below. Explain the specific steps you will take to avoid each of these errors in
the future.
1.
2.
Conclusion
Describe what you learned while doing this lab:
CP Chemistry Theodore Roosevelt High School Lab #1-1
Alchemy Lab
Introduction
Alchemy was a mixture of science, medicine, magic and religion. Many of the
processes and substances that we know today were discovered by
alchemists. They discovered alcohol, hydrogen, phosphorus and gun powder,
as well as the processes of distillation, evaporation and filtration. However,
one of the main goals of alchemy was to change a lesser metal such as
copper into gold. Producing gold was thought by the alchemists to be a major
step toward everlasting life.
Imagine that youre back in the Middle Ages when alchemists were at work trying to perfect their
methods of producing gold. The King has just asked for your advice in the case of a local alchemist,
who claims to have devised a way to make copper into silver and then into gold. Your instructions are
to reproduce the experiment, test the gold, and give the King your advice should he reward the
alchemist or hang him as a cheat? The King is very gracious in his rewards for good work and harsh in
his punishments for wrong answers.
Purpose
To use the Law of Conservation of Mass to test whether or not a copper penny can be turned into gold.
Prediction
Do you think you will actually be able to turn a penny into gold? Why or why not?
Equipment
balance ruler
beaker (100 mL) scoopula
beaker (250 mL) stirring rod
Bunsen burner striker
iron rings tongs
ring stand wire gauze
Materials
copper tokens (pennies) zinc powder
sodium hydroxide [3M NaOH (aq)]
Safety Considerations
Sodium hydroxide (NaOH) in this concentration is caustic and can be damaging to the eyes,
skin and respiratory system. Wash your skin with soap immediately if you come into contact
with NaOH. Avoid breathing the fumes from the boiling NaOH.
Zinc powder can spontaneously combust as it dries. Make sure you leave no clumps of zinc on
paper towels, and place all excess zinc in the waste beaker provided by your teacher.
Be sure you wear your goggles for the entire lab.
Always report spills and splashes to your teacher.
CP Chemistry Theodore Roosevelt High School Lab #1-1
Procedure
1. Set up a ring stand with wire gauze and two iron rings. Place the wire gauze on the bottom ring
and arrange the top ring so it will surround the 250mL beaker.
2. Pour approximately 100 mL of 3M sodium hydroxide (NaOH) solution into a 250mL beaker and
heat until it water vapor begins to come off.
3. Pour approximately 50mL of tap water in a 100mL beaker and set aside. This will be the wash
beaker.
4. Measure the mass of a clean copper token. Record this mass.
5. Measure the thickness and diameter of the clean copper token. Record these data.
6. Using tongs, immerse a clean copper token in the hot NaOH solution. Place a pinch of zinc
powder in the solution. Continue stirring the token until a color change has occurred. Move the
Bunsen burner away from the beaker, but do not turn it off.
7. Remove the token from the NaOH solution and place it in the wash beaker. Scrape off any
excess zinc on the tokens and dry it with a paper towel. Measure and record the mass of the
token.
8. Using tongs, gently hold the token by its edges and heat it in the Bunsen burner flame for a few
seconds until a complete color change occurs. Quickly place the token in the water to cool.
9. After the token cools, remove it from the wash beaker and dry it. Measure and record its mass.
10. If time allows, you may repeat the experiment with your own copper tokens.
Data you should create a data table in your lab write-up that looks something like this:
Token color Mass Thickness Diameter Volume* Density*
copper token
silver token
Questions
1. Was the change in the tokens a physical change or a chemical change? Give evidence for your
claim.
2. Based on your data, calculations and observations, is the gold token really gold? Give evidence
for your claim.
3. Pennies made before 1982 are solid copper; after 1982, they are made mostly of zinc with a thin
copper outer coating. Do you think your results would be affected by which kind of penny you
use? Why or why not?
CP Chemistry Theodore Roosevelt High School Lab #1-1
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining your calculations.
CP Chemistry Theodore Roosevelt High School Lab #1-1
It is important that the observations you make and record in the lab be as specific and
informative as possible. For example, you may observe a gas being given off as a result of a chemical
reaction. You should write your observation as gas formed rather than it fizzed. Whenever possible,
try to quantify the changes you observe using numbers or comparative terms like large or small. If
you think the mass has changed, use a balance to determine how much the mass has changed. If you
observe the material became hotter, use a thermometer to determine how much the temperature
changed.
Purpose
To observe chemical and physical changes; to explain observations of changes accurately and
completely; to recognize patterns of observations.
Prediction
Do you think we will perform more physical changes or chemical changes in this lab? Why do you think
so?
Equipment
scoopula test tube rack
small test tubes well plate
stirring rod
Materials
ammonium chloride [NH4Cl (s)] acetic acid [1M HC2H3O2 (aq)]
calcium carbonate [CaCO3 (s)] iodine solution (aq)
calcium chloride [CaCl2 (s)] phenolphthalein indicator (aq)
sodium bicarbonate [NaHCO3 (s)] potassium iodate [0.1M KI2O4 (aq)]
starch (s) sodium bisulfite [0.05M NaHSO3 (aq)]
sucrose [C12H22O11 (s)] sodium hydroxide [0.05M NaOH (aq)]
sodium sulfate [1M Na2SO4 (aq)]
strontium chloride [1M SrCl2 (aq)]
Safety Considerations
Iodine solution is corrosive to skin and eyes. Immediately wash spills and splashes off your skin
and clothing using plenty of water.
Acetic acid and sodium hydroxide in these concentrations can also be damaging to the eyes.
Be sure you wear your goggles and lab apron for the entire lab.
Always report spills and splashes to your teacher.
CP Chemistry Theodore Roosevelt High School Lab #1-2
Procedure
1. Using the small test tubes, mix the following chemicals; use a pea-sized sample of each solid and
a test tube for each liquid or solution. Hold the test tubes over the sink when adding liquids.
Stir each mixture with a stirring rod. Be sure to rinse the stirring rod after each use. Record your
observations, quantifying them when possible.
a. ammonium chloride + distilled water
b. calcium chloride + distilled water
c. sodium bicarbonate + acetic acid solution
d. calcium carbonate + acetic acid solution
e. sucrose + distilled water
2. Using a well plate, mix the following chemicals in the amounts listed. Stir each mixture with a
stirring rod. Be sure to rinse the stirring rod after each use. Record your observations,
quantifying them when possible.
a. 5 drops sodium hydroxide solution + 1 drop phenolphthalein solution
b. 5 drops acetic acid solution + 1 drop phenolphthalein solution
c. 5 drops sodium bisulfite solution + 5 drops potassium iodate solution
d. a pea-sized sample of starch + 10 drops distilled water + 1 drop iodine solution
e. 5 drops strontium chloride solution + 5 drops sodium sulfate solution
Data you should create a data table in your lab write-up that looks something like this:
Chemicals Observations
Questions
1. List each procedure step that represented a physical change and give evidence for why each was
a physical change.
2. List each procedure step that represented a chemical change and give evidence for why each
was a chemical change.
3. What was the most common evidence of a chemical change that you encountered in the lab?
What chemicals produced this evidence?
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining the difference between physical and chemical changes.
CP Chemistry Theodore Roosevelt High School Lab #1-2
In this lab, you will examine the reaction between magnesium metal (Mg) and
oxygen gas (O2). When heated strongly in an open crucible, magnesium reacts readily with oxygen in
the air. You will measure the mass of the magnesium that reacts as well as the mass of magnesium
oxide that is formed. This will allow you to calculate the mass of oxygen that reacted as well as the
mass ratio between magnesium and oxygen. Finally, you will compare your experimental mass ratio to
the accepted value to determine how successful your experiment was!
Purpose
To observe a chemical reaction between magnesium and oxygen; to calculate a mass ratio of
magnesium to oxygen; to practice measuring carefully in order to obtain accurate results.
Prediction
How close do you think your results will be to the accepted ratio of magnesium to oxygen (1.52 : 1)?
Why do you think so?
Equipment
balance ring stand
Bunsen burner scissors or tin snips
clay triangle sandpaper or steel wool
crucible w/lid striker
crucible tongs wash bottle
iron ring
Materials
distilled water magnesium [Mg (s)]
Safety Considerations
The crucible will get very hot during this experiment and may appear to be cool even when it is
not. Do not handle the crucible with your bare hands; only move it using the crucible tongs.
Safety goggles must be worn at all times.
Sometimes chemicals from previous labs still remain in glassware and on other lab equipment.
Wash all lab equipment before and after performing this lab.
Procedure
1. Obtain a piece of magnesium ribbon that is approximately 20 cm long. If the surface of the
magnesium is not shiny, use a piece of sandpaper or steel wool to shine the surface.
2. Measure the mass of your dry, clean crucible and its lid; record this value.
CP Chemistry Theodore Roosevelt High School Lab #1-3
3. Roll the magnesium ribbon into a loose coil and place it at the bottom of the crucible. Measure
the total mass of the crucible, lid and magnesium; record this value.
4. Set up the ring stand with an iron ring and clay triangle so that the crucible can sit in the triangle
approximately two inches above the Bunsen burner per the diagram above. Place the crucible in
the clay triangle and make sure its lid is completely on.
5. Using the Bunsen burner, heat the crucible gently by slowly moving the flame around underneath
it. If a large amount of smoke appears from the crucible, remove the heat temporarily until it stops
smoking.
6. After about four minutes of direct heating without any smoke produced, use the crucible tongs to
remove the lid slightly. Heat the crucible to redness for four minutes. Finally, remove the lid
completely and heat strongly for four more minutes.
7. Turn off the Bunsen burner and put the lid back on the crucible, allowing them to cool enough so
that they are safe to touch (be careful not to burn yourself!). Determine the total mass of the
crucible, lid and magnesium oxide product; record this value.
8. Add ten drops of distilled water to the crucible, replace the lid, and heat it for an additional four
minutes.
9. Repeat Procedure step #7. If there is a difference of more than 0.03 g between this measurement
and the last, you must repeat this step until there is an agreement between these values. Make
sure you record the mass each time!
Data you should create a data table in your lab write-up that looks something like this:
Object Mass
Questions
1. The accepted mass ratio of magnesium to oxygen in magnesium oxide is 1.52 g : 1.00 g. How
close was your final result to the accepted value? Why do you think this happened?
2. How would your results be affected if all the magnesium did not react?
3. Determine the correct formula for magnesium oxide. How does the mass ratio of magnesium and
oxygen compare to the ratio of elements in the chemical formula? Why do you think this is?
CP Chemistry Theodore Roosevelt High School Lab #1-3
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining your calculations.
CP Chemistry Theodore Roosevelt High School Lab #1-3
Purpose
To observe the colors emitted by various metal ions; to identify unknown salts by the color of their
flames.
Prediction
Do you think it will be easy or difficult to identify the unknown salts? Why?
Equipment
beakers (250-mL and 400-mL) Bunsen burner
Materials
barium nitrate [Ba(NO3)2 (s)] potassium nitrate [KNO3 (s)]
calcium nitrate [Ca(NO3)2 (s)] sodium nitrate [NaNO3 (s)]
copper (II) nitrate [Cu(NO3)2 (s)] strontium nitrate [Sr(NO3)2 (s)]
iron (III) nitrate [Fe(NO3)3 (s)] unknown salts (A and B)
lithium nitrate [LiNO3 (s)] wooden splints
Safety Considerations
Wooden splints must be soaked in a waste beaker after being used, otherwise they can set
trash can contents on fire.
Avoid inhaling any fumes given off by the burning salts.
Be sure you wear your goggles for the entire lab. You may also want to wear a lab apron.
Always report spills and splashes to your teacher.
Some of the salts are toxic; be sure to wash your hands after youve completed the experiment
and before you leave the lab.
Procedure
1. Fill a 250-mL beaker halfway full of tap water to use as a
soaking beaker for the wooden splints.
2. Fill a 400-mL beaker halfway full of tap water to use as a
waste beaker.
3. Light the Bunsen burner.
4. Obtain one sample of salt from the supplies table.
5. Test a small portion of the salt sample in the flame by using a
pre-soaked wooden splint. Be careful not to let any of the salt
fall into the Bunsen burner. Do not allow the splint to burn, as this will affect your results. Record
the color of flame generated by the salt.
CP Chemistry Theodore Roosevelt High School Lab #1-4
Data you should create a data table in your lab write-up that looks something like this:
Metal Ion Flame Color
barium
calcium
Questions
1. Do you think that flame tests would be a valid means of detecting metal ions present in a mixture
of ions? Why or why not?
2. The energy of visible light increases from the least energetic color, red, to the most energetic
color, violet. List the ions used the flame tests in increasing order of the energy of their emitted
light.
3. What conclusion can you make about the relationship between metal ions and the emission of
light?
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
identifying the unknown metal ions.
CP Chemistry Theodore Roosevelt High School Lab #1-4
Purpose
To observe chemical reactions in order to determine their types; to practice writing chemical equations.
Prediction
Based on the directions, which reaction do you think will be the most interesting? Why do you think so?
Equipment
beaker (600 mL) test tube holders
Bunsen burner tongs
forceps wash bottle
small test tubes watch glass
stirring rod well plate
striker
Materials
aluminum foil copper (II) sulfate solution [CuSO4 (aq)]
candle lead (II) nitrate solution [Pb(NO3)2 (aq)]
pH paper magnesium ribbon [Mg (s)]
wooden splints potassium iodide solution [KI (aq)]
calcium [Ca (s)] silver nitrate solution [AgNO3 (aq)]
calcium oxide [CaO (s)] sodium chloride solution [NaCl (aq)]
copper (II) carbonate, basic [CuCO3 Cu(OH)2 (s)] zinc [Zn (s)]
copper (II) sulfate, pentahydrate [CuSO4 5H2O (s)]
Safety Considerations
Several of the chemicals in this lab are slightly to moderately toxic. YOU MUST WEAR
GOGGLES AT ALL TIMES.
The silver and lead-based chemicals are toxic; DO NOT POUR THEM DOWN THE SINK.
Instead, pour them in the specially marked waste containers.
DO NOT look directly at the magnesium ribbon while burning.
When heating test tubes, keep them slightly tilted and pointed away from yourself and other
students; DO NOT LOOK DOWN INTO THE TEST TUBE.
CP Chemistry Theodore Roosevelt High School Lab #1-5
Procedure
Part E Combustion
1. Place a candle upright on the center of a foil-covered watch glass.
a. Carefully lower a beaker over the lighted candle.
b. Observe and record until no more changes are evident.
c. Light a splint, carefully lift one edge of the beaker and insert the lighted end into the beaker
next to the candle. Record your observations.
CP Chemistry Theodore Roosevelt High School Lab #1-5
Data you should create a data table in your lab write-up that looks something like this:
Reactants Reaction Products
Experiment
(before) (during) (after)
A1
single
replacement
A2
single
replacement
B1
combination
Questions
1. What evidence do you have that the color of copper (II) sulfate pentahydrate is related to the
presence of water in the crystal?
2. Would you predict that the ash formed when magnesium burned would have a greater or lesser
mass than the original piece of magnesium metal? Why?
3. What evidence do you have that the product of calcium oxide and water is basic rather than
neutral or acidic?
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
identifying the unknown metal ions.
CP Chemistry Theodore Roosevelt High School Lab #1-5
In the reaction between zinc (Zn) and copper (II) sulfate (CuSO4), the more reactive zinc replaces
copper and combines with the sulfate ion. The less reactive copper is released from the compound and
becomes a free element. Likewise, when a metal is placed in hydrochloric acid (HCl), a single
replacement reaction can occur. If the metal is more reactive than the hydrogen in the acid, the metal
will replace the hydrogen, and bubbles of hydrogen gas (H2) will be produced. The more reactive a
metal is, the more vigorously it will react with hydrochloric acid.
In this lab, you will determine whether or not various metals undergo single-replacement reactions
when placed in hydrochloric acid. Based on your observations of these reactions, you will then rank the
metals by reactivity.
Purpose
To determine the reactivity series of common metals; to observe single replacement reactions.
Prediction
Which metal will be the most reactive? Why do you think so?
Equipment
graduated cylinder (10 mL) test tubes, 5 small
marker test-tube rack
Materials
aluminum [Al] iron [Fe]
copper [Cu] magnesium [Mg]
hydrochloric acid, 1M [HCl] zinc [Zn]
Safety Considerations
Hydrochloric acid is damaging to the eyes; YOU MUST WEAR GOGGLES AT ALL TIMES.
Some of the metals may not completely react; DO NOT POUR THEM DOWN THE SINK.
Instead, pour them in the specially marked waste beakers.
Procedure
1. Use the glass marker to label each test tube with the symbol for each metal used in the lab.
Place the test tubes in a test-tube rack.
2. One at a time, place the appropriate metal in each test tube. Using a small graduated cylinder,
carefully measure and pour 5 mL of hydrochloric acid into each of the five test tubes.
CP Chemistry Theodore Roosevelt High School Lab #1-6
3. Observe what happens to the metal in each test tube and feel each test tube as the reaction
proceeds. Record your observations.
Data you should create a data table in your lab write-up that looks something like this:
Aluminum
(Al)
Copper
(Cu)
Questions
1. The rate at which hydrogen gas is produced as a result of these single-replacement reactions is
an indication of the relative reactivity of the metals. List the metals in order of their reactivity from
the most reactive to the least reactive.
2. Were these reactions endothermic or exothermic? Explain.
3. What could you do to determine whether the gas produced by these reactions is hydrogen?
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining the reactivity of each metal.
CP Chemistry Theodore Roosevelt High School Lab #1-6
In this lab, you will determine the electrochemical production potentials of various metals using citrus
fruit and a multimeter. Based on your observations, you will then rank the metals by reactivity and
compare it to their known ranking in your textbook.
Purpose
To determine the activity series of metals using fruit.
Equipment
Determine all equipment you will use and list it in your lab write-up.
Materials
Determine all materials you will use and list them in your lab write-up.
Safety Considerations
None for this lab beyond standard lab safety procedures.
Procedure
As you perform the lab, record your procedure steps, and then describe them in your lab write-up.
Data
Record all pertinent data and include it in your lab write-up.
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing and explaining your results, as well as critically analyzing
your procedure methods.
CP Chemistry Theodore Roosevelt High School Lab #1-7
Laboratory Activities
CP Chemistry Theodore Roosevelt High School Lab #2-0
Purpose
To become familiar with the measurement scale of electronic balances, graduated cylinders, and rulers;
to make several different kinds of measurements and compare the uncertainty between them.
Equipment
balances (0.1, 0.01, and 0.001) graduated cylinder (10 mL and 100 mL)
ball meter stick
beaker (100 mL and 250 mL) ruler
Erlenmeyer flask (125 mL) SmartBoard w/projector
Materials
Chemistry textbook silicon metal
pre-1982 pennies
Safety Considerations
Sometimes chemicals from previous labs still remain in glassware and on other lab equipment.
Wash all lab equipment before performing this lab.
Procedure
Station A Length
1. Using a ruler, measure and record the length, width and height of a lab station in centimeters.
Repeat this measurement with a meter stick and record.
2. Using a ruler, measure and record the length, width and height of a Chemistry textbook in
centimeters. Repeat this measurement with a meter stick and record.
3. Using a ruler, measure and record the thickness of the pages of a Chemistry textbook (not the
covers). Count and record the number of pages you measured.
4. Using a meter stick, measure and record the width, length and height of the Chemistry classroom
in meters.
Station B Mass
1. Obtain a piece of silicon metal that is small enough to fit inside a graduated cylinder. Weigh the
piece once on each of the three balances and record the measurement for each balance. Save
this piece for use at Station C.
2. Obtain a pre-1982 penny. Weigh it once on each of the three balances and record the
measurement for each balance.
CP Chemistry Theodore Roosevelt High School Lab #2-0
3. Obtain nineteen more pre-1982 pennies, for a total of twenty. Using a beaker, weigh them once
on the 0.01 balance and record.
Station C Volume
1. Obtain a pre-1982 penny. Using a ruler, measure and record the width and thickness of the
penny.
2. Fill a 100-mL graduated cylinder with exactly 50-mL of tap water (be sure the bottom of the
meniscus, or curve of the water, is exactly on the 50 mL line). Place the penny in the water and
record the new volume. Dump out the water in the sink.
3. Repeat step 2 with 20 pennies and record.
4. Repeat step 2 with the small piece of silicon metal from Station B and record.
5. Fill a 100-mL beaker to the 50-mL line with tap water. Pour this water into your graduated
cylinder and record. Dump out the water in the sink.
6. Repeat step 5 with a 250-mL beaker and a 125-mL Erlenmeyer flask.
Lab station
w/meter stick
Textbook
w/ruler
Textbook
w/meter stick
Room 207
w/meter stick
Silicon
One penny
20 pennies
One penny
20 pennies
Silicon
100-mL beaker
250-mL beaker
125-mL flask
Calculations
1. Calculate the volume of your lab station using your ruler data. Repeat this calculation with your
meter stick data.
2. Calculate the volume of your textbook using your ruler data. Repeat this calculation with your
meter stick data.
3. Calculate the volume of the classroom using your meter stick data.
4. Using your textbook pages data, calculate the thickness of one page of your book.
5. Using the combined mass of twenty pennies, determine the average mass of one penny.
Calculate the percent error of this average based on the accepted mass of pre-1982 pennies of
3.11 g.
6. Using the width and thickness of a penny, calculate its volume using the equation V = r2t, where
r is radius and t is thickness. Using the combined volume of twenty pennies, calculate the
average volume of one penny. Calculate the percent error for these two values using the
accepted volume of a pre-1982 penny of 0.3516 cm3.
7. Using your mass and volume measurements of zinc, calculate its density. Calculate the percent
error using the accepted density of silicon of 2.329 g/cm3.
CP Chemistry Theodore Roosevelt High School Lab #2-0
8. Using your volume measurements for the beakers and flask, calculate the percent error for each
compared with the accepted value of 50.0 mL.
Errors
Think of two possible errors you may have committed in this lab that may have somehow affected your
results and record them below. Explain the specific steps you will take to avoid each of these errors in
the future.
1.
2.
Conclusion
Describe what you learned while doing this lab:
CP Chemistry Theodore Roosevelt High School Lab #2-1
Purpose
To become familiar with SI units, measurement, and conversion.
Prediction
What would you predict the dimensions of the classroom are (length x width) in meters?
Equipment
electronic balance meter stick
graduated cylinder (100 mL) ruler
Materials
various (see procedure)
Safety Considerations
None for this lab beyond standard lab safety procedures.
Procedure:
Part A Length
1. Determine the length of a teammate's foot, in meters.
2. Determine the width of the classroom, in centimeters.
3. Determine the thickness of a calculator, in millimeters.
4. Find a person in the class who is approximately 1.6 meters tall and determine his or her exact
height, in millimeters.
Part B Volume
1. Determine the volume of a paperback book, in cm3.
2. Determine the volume of one coin, in mm3.
3. Determine the volume of a piece of jewelry, in mL.
4. Find an object with a volume of around 100 cm3 and determine its volume, in cm3.
CP Chemistry Theodore Roosevelt High School Lab #2-1
Part C Mass
1. Determine the mass of a dollar bill, in grams.
2. Determine the mass of a ring, in centigrams.
3. Determine the mass of a piece of chalk, in milligrams.
4. Find a single object different from those already used that has a mass between 100 and 200
grams and determine its mass, in grams.
5. Find a single object different from those already used that has a mass between 10 and 25 grams
and determine its mass, in grams.
Part D Density
1. Determine the density of a coin, in g/mL.
2. Determine the density of a piece of jewelry, in g/cm3.
3. Find a single object different from those already used that is more dense than water and
determine its density, in g/mL.
Data you should create a data table in your lab write-up that looks something like this:
Station Measurement Calculation Result
A1
A2
Calculations
A1. Calculate the length of your teammates foot in decimeters.
A2. Calculate the width of the classroom in millimeters.
A3. Calculate the thickness of the calculator in meters.
A4. Calculate the height of the person measured in Procedure A4 in micrometers.
B1. Calculate the volume of the paperback book in milliliters.
B2. Calculate the volume of the coin in cm3.
B3. Calculate the volume of the piece of jewelry in microliters.
B4. Calculate the volume of the object measured in Procedure B4 in Liters.
C1. Calculate the mass of the dollar bill in milligrams.
C2. Calculate the mass of the ring in kilograms.
C3. Calculate the mass of the piece of chalk in grams.
C4. Calculate the mass of the object measured in Procedure C4 in micrograms.
C5. Calculate the mass of the object measured in Procedure C5 in decigrams.
D1. Calculate the density of the coin in g/L.
D2. Calculate the density of the piece of jewelry in kg/mL.
D3. Calculate the density of the object measured in Procedure D3 in kg/L.
Questions
1. What method did you use to determine the volume of jewelry used in Procedure B3? Why did you
use this method?
2. What method did you use to determine the density of the coin used in Procedure D1? Why did
you use this method?
3. Do you find it difficult to use SI units as compared to American customary units? Why or why not?
CP Chemistry Theodore Roosevelt High School Lab #2-1
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
describing what you learned while doing this lab.
CP Chemistry Theodore Roosevelt High School Lab #2-1
In this lab, you will take the measurement challenge by first determining the
volume of a plastic block, and then predict its mass using the known density of
that block. Success in this challenge depends on your ability to take accurate measurements!
Purpose
To practice the calculation of density while demonstrated both accurate and precise measurement
skills.
Prediction
Can density be used to identify an unknown substance? Explain.
Equipment
balance ruler
Materials
plastic blocks, 4
Safety Considerations
None for this lab beyond standard lab safety procedures.
Density
Block Color
(g/cm3)
white 0.541
black 0.985
milky-white 0.908
clear 1.18
gray 1.42
4. After predicting the mass of the block, take it to your teacher, who will measure its mass for you
using a high-precision balance. Record this value in your data table.
5. Determine the accuracy of your mass calculation by calculating the percent error between your
predicted mass and the actual mass of the plastic block.
Data you should create a data table in your lab write-up that looks something like this:
Block # and Color Length Height Width Mass Volume* Density*
8 - Grey
11 - Clear
Questions
1. How did you use density to identify an unknown substance?
2. Do you think you could accurately use volume displacement to determine the volume of these
plastic blocks? Why or why not?
3. Identify two things you learned about density as a result of this lab activity.
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining your calculations.
CP Chemistry Theodore Roosevelt High School Lab #2-2
Nuclear chemists have discovered what is believed to be element number 119. The researchers have
named this element Beanium. There are three naturally occurring isotopes of beanium: beanium-
white, beanium-brown, and beanium-green. Your job is to determine the atomic mass of each individual
isotope, the percentage abundance of each isotope, and ultimately the average atomic mass of
beanium. One unique property of beanium that should make this determination particularly easy is that
beanium atoms are very large, so sorting the isotopes of this element should be accomplished with little
difficulty.
Purpose
To determine the average atomic mass for the fictitious element beanium.
Prediction
In this lab, you will determine the average mass of all the beans together, and then the average mass
of each type of bean based in their abundance. How close do you think these values will be to each
other?
Equipment
balance beaker (100 mL)
Materials
beans, various types
Safety Considerations
None for this lab beyond standard lab safety procedures.
Procedure
1. Obtain a sample of beanium isotopes by scooping up a beaker full of beans from the bean
container.
2. Separate the beans by isotope and count them. Record the total number of each type of bean.
3. For each isotope sample of beanium, determine and record its total mass.
4. Determine and record the total mass of your entire sample of beanium.
5. For each isotope, calculate its average mass by dividing the total mass of that isotope by the
number of beans of that isotope.
6. For each isotope, calculate its percent abundance by dividing the number of beans in each
isotope by the total number of beans.
7. Calculate the total % abundance of beanium isotopes by summing their abundances.
CP Chemistry Theodore Roosevelt High School Lab #2-3
8. Calculate the average atomic mass of beanium by dividing the total mass of the entire sample by
the total number of beans.
9. Calculate the average atomic mass of beanium again by first multiplying each isotopes average
mass by its percent abundance and then adding these values together.
Questions
1. What is an isotope? How is it related to beanium?
2. Compare your average mass of beanium with that of two other groups. How does your average
mass compare to theirs? Why do you think this happened?
3. Neon-20 has a mass of 19.9924 amu, neon-21 has a mass of 20.9940 amu, and neon-22 has a
mass of 21.9914 amu. The relative abundance of Ne-20 is 90.92%, while Ne-21 is 0.257% and
Ne-22 is 8.82%. Using the same techniques that you used in this lab, calculate the average
atomic mass for neon. How does this compare to the value for neon found on the periodic table?
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining your calculations.
CP Chemistry Theodore Roosevelt High School Lab #2-3
In this lab, we will determine the percent composition of a modern (post-1982) penny by using a strong
acid to react and dissolve the zinc core, leaving only the copper coating. Once only copper remains,
we will compare its mass to the entire mass of the penny to determine how much of a penny is copper
and how much is zinc.
Purpose
To practice calculating percent composition.
Prediction
What percentage of your penny do you think will be made of zinc? Why do you think so?
Equipment Materials
beaker, 100 mL hydrochloric acid, 1M [HCl]
metal file penny (1983 or later)
oven
Procedure
Day 1:
1. Obtain a clean post-1982 penny.
2. Measure and record the mass of the penny in your lab notebook.
3. Using a metal file, file three, oppositely-placed small grooves into the edge of the penny. The
grooves must be deep enough so that the zinc is exposed, but not so deep that the penny's mass
is greatly affected.
4. Obtain a small beaker and label it with your name, your partners name and your period.
5. While wearing gloves, carefully pour 75 mL of 1M HCl into a 100-mL beaker.
6. Carefully place the penny in the acid. Observe the effect the acid has on the copper outside of
the penny.
7. Place your labeled beaker under either fume hood to react overnight.
CP Chemistry Theodore Roosevelt High School Lab #2-4
Day 2:
1. After the penny has reacted overnight, carefully pour some water from another beaker into the
acid to dilute it.
2. Carefully remove the remainder of the penny with a pair of tongs.
3. Gently rinse the penny with water from a wash bottle and pat it dry with paper towels.
4. If any zinc inside the penny remains unreacted, repeat steps #5-7 from Day 1 and check again the
next day.
5. Put the penny in a small beaker and place it in the oven for 5-10 minutes to allow it to dry
completely.
6. Dispose of the acid in the large waste beaker in the fume hood (DO NOT POUR IT DOWN THE
SINK).
7. Remove the penny and measure and record its new mass in your lab notebook.
8. Dispose of the penny in the trash and clean all used glassware.
Data you should create a data table in your lab write-up that looks something like this:
Day 1 Mass Day 2 Mass Mass of Zinc* % Composition* % Error*
Calculations
1. Calculate the mass of zinc in the penny that was reacted.
2. Knowing the total mass of the penny and the mass of both copper and zinc in the penny, calculate
the percent composition of your penny.
3. According to the United States Mint, pennies are 97.5% zinc and 2.5% copper. Calculate the
percent error for your experimental percent composition of zinc.
4. Using the accepted density of zinc (7.140 g/cm3) and the accepted volume of a penny
(0.360 cm3), calculate what the mass of a penny would be if it were made of solid zinc.
Questions
1. Why is the mass of your penny so close to the mass of the hypothetical solid zinc penny
calculated in Calculation #4?
2. Copper and zinc are next to each other on the period table. How is it possible that one of them
would react with hydrochloric acid, but not the other?
3. Why is it necessary to use a post-1982 penny for this lab?
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
describing what you learned while doing this lab.
CP Chemistry Theodore Roosevelt High School Lab #2-4
Stoichiometry Lab
Introduction
In chemical reactions, the actual masses of substances used are
proportional to their molar masses. Therefore, its possible to predict the
number of grams of a given product that will be formed in a reaction if you
know the mass of any one of the reactants.
In this lab, you will start with a known mass of basic copper (II) carbonate and determine the mass of
copper (II) oxide formed by decomposition due to heat. Using stoichiometry, you will then calculate the
theoretical mass of copper (II) oxide that should form in this reaction. The difference between the
actual yield obtained from the experiment and the theoretical yield calculated using stoichiometry can
then be used to determine the percent error and percent yield of your product.
Purpose
To use stoichiometry to calculate the theoretical mass for the product of the reaction and compare it to
the actual yield using percent error and percent yield.
Prediction
Do you think you will be able to achieve 100% yield with this lab? Explain.
Equipment
balance iron ring
Bunsen burner ring stand
clay triangle stirring rod
evaporating dish tongs
Materials
copper (II) carbonate, basic [CuCO3Cu(OH)2 (s)]
Safety Considerations
Basic copper (II) carbonate is TOXIC, with a lethal dose of 140 mg per kg of body mass. This
means that a 125-lb. student could die from ingesting as little as 8 grams. Avoid contact with
basic copper (II) carbonate and wash your hands after completing the lab!
Safety goggles must be worn at all times.
Sometimes chemicals from previous labs still remain in glassware and on other lab equipment.
Wash all lab equipment before and after performing this lab.
Procedure
1. Determine the mass of a clean evaporating dish. Record this value.
2. Obtain as close to one gram of basic copper (II) carbonate as possible and determine its mass.
Record this value in a data table.
3. Add the basic copper (II) carbonate to the empty evaporating dish.
4. Place the evaporating dish on the clay triangle supported by the ring stand. Heat the evaporating
dish using the Bunsen burner until all of the basic copper (II) carbonate has been converted to
black copper (II) oxide. You may want to stir the materials toward the end of heating to make sure
all the reactant has decomposed, but be careful not to allow anything to stick to your stirring rod.
CP Chemistry Theodore Roosevelt High School Lab #2-5
5. After you have finished heating, CAREFULLY remove the evaporating dish with tongs and gently
place it on your lab station to cool. If you drop your evaporating dish and spill your product, you
will have to start the lab over from the beginning.
6. Once the evaporating dish has cooled enough to touch, determine the mass of the dish and the
contents together and determine the actual yield of copper (II) oxide. Record this value.
3. Compare your actual yield of copper (II) oxide in Calculation #1 to the theoretical yield in
Calculation #2 by calculating the percent yield and percent error for your reaction using these
equations:
Questions
1. In the reaction we saw in this lab, would you expect your solid product (copper (II) oxide) to have
a greater, equal, or smaller mass than the reactant? Why?
2. What relationship did you notice between percent yield and percent error? Describe a situation
for each where one value may be more useful than the other.
3. Based on your observations of green basic copper (II) carbonate during this lab and drawing from
your previous experiences with blue copper (II) sulfate pentahydrate crystals, what general
conclusion can you draw about other hydrates such as these?
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining your calculations.
CP Chemistry Theodore Roosevelt High School Lab #2-5
Because this reaction could also form either iron (II) sulfate or iron (III)
sulfate, you will use both observations and stoichiometry to determine
the chemical reaction that occurred. Through calculations, you will also
determine the theoretical mass of copper metal that should form from this
reaction and determine its percent yield.
Purpose
To use stoichiometry calculations to calculate theoretical mass and percent yield.
Prediction
Which reactant copper (II) sulfate or iron will be the limiting reagent? Explain why you think so.
Equipment
balance permanent marker
beaker, 250 mL ring stand
Bunsen burner stirring rod
iron ring wire gauze
Materials
copper (II) sulfate (anhydrous) [CuSO4 (s)] filter paper
distilled water iron filings [Fe (s)]
Safety Considerations
Safety goggles must be worn at all times.
Sometimes chemicals from previous labs still remain in glassware and on other lab equipment.
Wash all lab equipment before and after performing this lab.
Procedure
1. Measure 7.00 g of anhydrous copper (II) sulfate and place it in a 250 mL beaker.
2. Add about 50 mL of distilled water and heat gently over a Bunsen burner until the solid has
completely dissolved. DO NOT ALLOW THE SOLUTION TO BOIL.
3. Once the crystals have dissolved, remove the beaker from the heat. Record your observations of
the solutions appearance.
4. Measure 2.00 g of iron filings and slowly add them to the beaker while stirring the hot CuSO4
solution.
CP Chemistry Theodore Roosevelt High School Lab #2-6
5. Allow this solution to sit for at least 10 minutes. Record your observations of the solutions
appearance.
6. Obtain a piece of filter paper and label it with your lab group members names using a permanent
marker. Determine and record its mass.
7. Fold the filter paper in quarters and place it in a funnel, wetting it with distilled water to keep it in
place.
8. Filter the solution through the funnel and filter paper to collect the copper product. Wash the
product with distilled water. Let the filter paper and copper sit overnight.
9. After allowing the filter paper to dry overnight, determine and record its mass.
Data you should create a data table in your lab write-up that looks something like this:
Item Mass (g)
2. The other possible unbalanced chemical equation for this reaction is:
copper (II) sulfate (aq) + iron (s) copper (s) + iron (III) sulfate (aq)
If this were the correct reaction, what mass of copper should be produced in this lab?
3. What mass of copper was formed? What was the percent yield of this reaction?
Questions
1. What are some of the clues you observed that suggested a chemical reaction occurred?
2. Which reactant limited the reaction? What observations support this conclusion?
3. Based on your data, which product was formed along with the copper metal: iron (II) sulfate or
iron (III) sulfate? How do you know?
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining your calculations.
CP Chemistry Theodore Roosevelt High School Lab #2-6
Purpose
To determine how many antacids are necessary to produce 500 mL of gas when reacted with 100 mL
of vinegar.
Equipment
Determine all equipment you will use and list it in your lab write-up.
Materials
Determine all materials you will use and list them in your lab write-up.
Safety Considerations
None for this lab beyond standard lab safety procedures.
Procedure
As you perform the lab, record your procedure steps, and then describe them in your lab write-up.
Data
Record all pertinent data and include it in your lab write-up.
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing and explaining your results, as well as critically analyzing
your procedure methods.
CP Chemistry Theodore Roosevelt High School Lab #2-7
Laboratory Activities
CP Chemistry Theodore Roosevelt High School Lab #3-0
Purpose
To observe the effects of changes in pressure, temperature and volume on gases.
Materials Equipment
aluminum cans, empty beaker tongs plastic tray
balloons beakers, 1000-mL, 2 stopper, one-hole
ice Bunsen burner syringe, 20-cc
tap water dropper vacuum apparatus
electronic balance, 0.001g Vernier gas pressure sensor
Erlenmeyer flasks, 125-mL, 2 Vernier LabQuest
hot plates, 2 2-Liter bottle
netbook or laptop
Safety Considerations
Wash your hands thoroughly after completing this lab.
Procedure
For each of the following stations, follow the directions and record your observations in the data
table. You may complete the stations in any order.
Station A
Station B
Station C
Station D
Station E
Station F
Station G
Station H
Errors
Think of two possible errors you may have committed in this lab that may have somehow affected your
results and record them below. Explain the specific steps you will take to avoid each of these errors in
the future.
1.
2.
Conclusion
Describe what you learned while doing this lab:
CP Chemistry Theodore Roosevelt High School Lab #3-1
Purpose
Based on the introduction above, determine the purpose of this lab and include
it in your lab write-up.
Prediction
Do you think the lauric acid will freeze quickly or will it take a long time? Why do you think so?
Equipment
beaker (400 mL) utility clamp
large test tube w/wire stirrer Vernier LabQuest
ring stand Vernier temperature probe
Materials
lauric acid [CH3(CH2)10COOH] (in test tube) tap water
Safety Considerations
Lauric acid is mildly irritating avoid contact with the skin and eyes.
Safety goggles must be worn at all times.
Sometimes chemicals from previous labs still remain in glassware and on other lab equipment;
wash all lab equipment before and after performing this lab.
Wash your hands thoroughly after completing this lab.
Procedure
1. Turn on the Vernier LabQuest and connect the temperature probe. Tap on the settings box on
the right of the sensor screen and set the collection time to 40 minutes and the frequency to 10
times per minute. Save the settings by tapping the Done button.
2. Fill a 400 mL beaker with about 250 mL of cold tap water. Place the beaker on the lab counter
next to a ring stand.
3. Attach a utility clamp to the ring stand and place it above the beaker.
4. Obtain a large test tube with melted lauric acid and a wire stirrer from the hot water bath in the
back of the room. Place the large test tube in the beaker and hold it in place using the clamp.
Make sure the water level is above the level of the lauric acid in the test tube; add water to the
beaker if necessary.
5. Place the temperature probe in the test tube, making sure it does not touch the glass, and begin
recording data by pressing the play button.
6. Gently stir the lauric acid with the wire stirrer with constant motion. Continue stirring the lauric
acid throughout the experiment.
7. Record the time at which the lauric acid started to freeze and the time when it was
CP Chemistry Theodore Roosevelt High School Lab #3-1
completely frozen.
8. Continue stirring the lauric acid and recording temperature readings with the LabQuest until the
temperature of the material has fallen below 40C. When most of the lauric acid has solidified,
you will no longer be able to stir the contents.
9. Return the lauric acid test tube to the hot water bath in the back of the room.
10. Using the LabQuest stylus, highlight as much of the flat section of the curve as possible. Record
the average of these data points (shown on the right) as the melting point of lauric acid.
11. Turn off the LabQuest (discard the data) and return it to the supplies table.
Questions
1. Based on your lab results, does the temperature of a substance vary while it is freezing? Explain
why or why not.
2. Would increasing the amount of lauric acid used affect your curve? Explain why or why not.
3. In this lab, you recorded temperature readings every 6 seconds. Between temperature and time,
which is the manipulated variable and which is the responding variable? Explain.
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining your calculations.
CP Chemistry Theodore Roosevelt High School Lab #3-1
Calorimetry Lab
Introduction
Much like in the previous lab where we melted an ice cube, you can
use q = CmT to calculate the heat change that occurs when you
dissolve an ionic solid. You can then determine the molar heat of
solution, Hsoln, in kJ/mol by dividing the heat change by the moles of
chemical dissolved. Positive molar heats represent endothermic
changes, which cause a decrease in the temperature of the
surroundings, while negative molar heats have the opposite effect.
In this lab, you will compare the calculated heat change of each chemical to its accepted value to
determine your percent error. Be sure to work quickly, measure accurately and keep your calorimeter
lid secure to ensure the best possible data!
Purpose
Based on the introduction above, determine the purpose of this lab and include it in your lab write-up.
Prediction
During the winter, calcium chloride is used to melt ice from streets and sidewalks. Do you think this is
an endothermic or an exothermic reaction? Explain.
Equipment
beaker, 250 mL Styrofoam cups, 2
cardboard lid Vernier LabQuest
electronic balance, 0.01 g Vernier temperature probe
graduated cylinder, 100 mL
Materials
ammonium chloride [NH4Cl] calcium chloride [CaCl2]
Safety Considerations
Safety goggles must be worn at all times.
Sometimes chemicals from previous labs still remain in glassware and on other lab equipment;
wash all lab equipment before and after performing this lab.
Wash your hands thoroughly after completing this lab.
Procedure
1. Turn on the Vernier LabQuest and connect the temperature
probe. Tap on the settings box on the right of the sensor screen
and set the collection time to 10 minutes and the frequency to 60
times per minute (once per second). Save the settings by
tapping the Done button.
2. Assemble your calorimeter per the diagram shown to the right.
3. Using a graduated cylinder, measure out exactly 100.0 mL tap
water and pour it into your Styrofoam cup calorimeter.
4. Using the LabQuests temperature probe, measure the starting
CP Chemistry Theodore Roosevelt High School Lab #3-2
Data you should create a data table in your lab write-up that looks something like this:
Mass Starting Final
Chemical q* Hsoln* % error*
Temp Temp
calcium chloride
Questions
1. Why is the molar heat of solution (Hsoln) of calcium chloride a negative value? Why is the molar
heat of solution (Hsoln) of ammonium chloride a positive value?
2. Compare your results to those of another lab group. Were their values for Hsoln similar to or
different from yours? Explain why or why not.
3. How do you think you might apply this technique to determining the amount of chemical potential
energy stored in food?
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining your calculations.
CP Chemistry Theodore Roosevelt High School Lab #3-2
Purpose
Based on the introduction above, determine the purpose of this lab and include it in your lab write-up.
Prediction
Will the heat change for the combustion of paraffin have a positive or negative value? Explain.
Equipment
Erlenmeyer flask, 125 mL thermometer
graduated cylinder, 100 mL tin can
ring stand utility clamp
rubber stopper
Materials
matches paraffin candle [C25H52]
Safety Considerations
Sometimes chemicals from previous labs still remain in glassware and on other lab equipment;
wash all lab equipment before and after performing this lab.
Wash your hands thoroughly after completing this lab.
Procedure
1. Obtain a candle; measure and record its mass.
2. Measure out exactly 100.0 mL tap water into a 125-mL Erlenmeyer flask. Use a stopper with a
hole to seal the flask make sure the number on the stopper matches the number on the flask!
3. Using a ring stand, attach the flask to a utility clamp so that its bottom is 1-2 inches above the tin
can.
4. Measure and record the starting temperature of the water.
5. Away from the flask, use a match to light the candle and quickly slide it underneath the flask. DO
NOT PLACE USED MATCHES IN THE SINK.
6. Allow the candle to burn for around 5 minutes or until the temperature of the water reaches 30C,
whichever comes first.
7. Gently blow out the candle and record the peak temperature of the water.
8. Allow the candle to cool for several minutes; measure and record its mass.
9. Repeat steps #2-8 for two additional trials, using new water each time. Record the starting
temperature, final temperature, and mass change for each trial.
CP Chemistry Theodore Roosevelt High School Lab #3-3
Data you should create a data table in your lab write-up that looks something like this:
Starting Starting Final Final
Trial H* q*
Mass Temp Mass Temp
Trial #1
Trial #2
Questions
1. Why is the heat change for the combustion of paraffin a negative value? Why is the heat change
for the water a positive value?
2. One of the products of the combustion of paraffin is water. What sort of experiment could you
design to show this is formed?
3. When a candle burns, is it the wax or the wick that burns? Explain why.
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining your calculations.
CP Chemistry Theodore Roosevelt High School Lab #3-3
Butane is a gas at normal room conditions, but it is a liquid in disposable lighters under high-
pressurized conditions. When the lighter is opened, the container is depressurized, allowing the butane
to escape as a gas. In this experiment you will collect a butane gas sample in a container by the water
displacement method, allowing direct measurement of the volume of butane gas collected.
Purpose
Based on the introduction above, determine the purpose of this lab and include it in your lab write-up.
Prediction
Do you think 100 mL of butane gas is enough to accurately determine the molar mass of butane? Why
or why not?
Materials Equipment
butane lighter [C4H10] electronic balance, 0.001 g plastic trough or dishpan
tap water gas pressure sensor thermometer
graduated cylinder, 100 mL Vernier LabQuest
Safety Considerations
Butane is toxic and highly flammable. No open flames should be used in this experiment!
Sometimes chemicals from previous labs still remain in glassware and on other lab equipment;
wash all lab equipment before and after performing this lab.
Wash your hands thoroughly after completing this lab.
Procedure
1. Place the lighter under water. Remove the lighter, shake off
the excess water, and dry the outside with a paper towel.
Using the balance, determine the mass of the lighter and
record.
2. Fill the plastic trough two-thirds full with water.
3. Fill a 100-mL graduated cylinder to the brim with water.
Using the palm of your hand, completely cover the opening of
the graduated cylinder and invert it into the trough. Once the
opening is under water, remove your hand, keeping the
opening of the graduated cylinder under water at all times. If This diagram shows a similar setup
there are any noticeable air bubbles in the graduated cylinder, using an Erlenmeyer flask; you will
you must remove the cylinder and repeat this step. use a graduated cylinder instead.
CP Chemistry Theodore Roosevelt High School Lab #3-4
4. Hold the lighter under the opening of the graduated cylinder and release the butane gas by
depressing the lever. Collect exactly 95.0 mL of butane gas. Do not to allow any bubbles of
butane to escape outside the cylinder. Do not exceed 95.0 mL since this may prevent you from
making an accurate volume measurement.
5. Determine the temperature of the water in C and record.
6. Carefully raise or lower the graduated cylinder until the water level inside the cylinder is the same
as the water level in the trough. Be careful not to pull the cylinder out of the water! While
maintaining equal water levels, read the exact volume of the butane gas to the nearest 0.1 mL
and record.
7. While keeping it upside down, remove the graduated cylinder and take it to the fume hood to
release the collected butane gas safely.
8. Remove the lighter from the water, shake off the excess water, and dry the outside with a paper
towel. Determine the mass the lighter and record.
9. Record the barometric pressure from the Vernier LabQuest.
Data you should create a data table in your lab write-up that looks something like this:
Property Value
water temperature
Questions
1. Explain how butane, which can be stored as a liquid in lighters, comes out as a gas.
2. Butane gas does not dissolve well in water. Why is this critical to performing this experiment?
3. The diagram on the first page shows this experiment being performed with an Erlenmeyer flask
instead of a graduated cylinder.
a. Why is it preferable to use a graduated cylinder instead of a flask in this lab?
b. Imagine you performed this lab and collected the gas with a flask instead of a graduated
cylinder. How might you attempt to accurately determine its volume?
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining your calculations.
CP Chemistry Theodore Roosevelt High School Lab #3-4
Purpose
Based on the introduction above, determine the purpose of this lab and include it in your lab write-up.
Prediction
Do you expect that the atmospheric pressure in the lab will be above or below standard atmospheric
pressure (101.3 kPa)? Explain.
Materials Equipment
copper wire [Cu] beaker, 400 mL pipette
hydrochloric acid, 3.0 M [HCl] gas pressure sensor rubber stopper, one-hole
magnesium ribbon [Mg] graduated cylinder, 10 mL ruler
latex gloves thermometer
Safety Considerations
3M hydrochloric acid is dangerously caustic! Avoid contact with the
skin and eyes.
Safety goggles must be worn at all times; gloves must be worn in
Steps #5-8.
Sometimes chemicals from previous labs still remain in glassware and
on other lab equipment; wash all lab equipment before and after
performing this lab.
Wash your hands thoroughly after completing this lab.
Procedure
1. Using a ruler, measure and record the exact length of a small
piece of magnesium ribbon. The length of the ribbon piece
should be between 0.6 and 0.8 cm.
2. Wrap the copper wire around the magnesium ribbon,
making a cage that surrounds the ribbon as shown in the
first figure to the right. Leave a handle of copper wire
approximately 6 cm long.
3. Insert the handle end of the copper wire into the one-hole
rubber stopper as shown in the second figure to the right.
4. Fill the 400 mL beaker approximately half full with tap water.
5. While wearing latex gloves, use a pipette to add
approximately 3 mL of 3.0 M hydrochloric acid to the
graduated cylinder.
6. Using the pipette, gently fill the graduated cylinder by
drizzling water down the inside wall of the cylinder to avoid
CP Chemistry Theodore Roosevelt High School Lab #3-5
mixing with the acid. Since HCl is more dense than water, it will stay at the bottom of the cylinder.
7. Gently insert the stopper into the graduated cylinder while keeping the copper wire cage at the top
of the cylinder.
8. While holding your finger over the hole in the rubber stopper, quickly but carefully turn the
graduated cylinder upside down and place it into the beaker of water as shown in the third figure
to the right. Once the top of the cylinder is underwater, remove your finger and rest the cylinder in
the beaker while the reaction proceeds.
9. When the magnesium ribbon is no longer reacting, tap the side of the cylinder to release any
trapped gas bubbles.
10. Let the cylinder sit for 5 minutes so that the temperature of the system returns to room
temperature. Measure and record the temperature of the water in the beaker.
11. Using the gas pressure sensor, measure and record the atmospheric pressure in the lab.
12. Lift the graduated cylinder slightly until the levels of water inside and outside the cylinder are the
same. Measure and record the volume of gas in the cylinder.
13. Remove the cylinder from the beaker, remove the stopper from the cylinder, and dispose of the
liquid in both containers in the sink. Clean all lab equipment used and return each item to its
proper place.
Data you should create a data table in your lab write-up that looks something like this:
Property Value
length of Mg ribbon
water temperature
moles).
2. Using the balanced equation for the reaction between magnesium and hydrochloric acid,
determine the number of moles of hydrogen gas that were produced.
3. Determine the pressure of the hydrogen gas by subtracting the water vapor pressure of the
system from the atmospheric pressure.
4. Convert the volume of hydrogen gas produced from milliliters into Liters.
5. Convert the temperature of the system into Kelvins.
6. Using the pressure, volume, temperature and moles of hydrogen gas in this system, calculate
your experimental value of the ideal gas constant, R.
7. Using the accepted value for the ideal gas constant, R, determine the percent error for your
experimental value of the ideal gas constant.
Questions
1. Using your experimental value of R, determine the molar volume of a gas at STP (solve for n if V
= 1 L). How does this compare to the accepted value, 22.4 L/mol?
2. Describe three observations from your lab that showed a chemical reaction took place.
3. When exposed to hydrochloric acid, the copper wire reacted very differently than the magnesium
ribbon. What chemical explanation can you give for why this occurred?
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining your calculations.
CP Chemistry Theodore Roosevelt High School Lab #3-5
Purpose
Based on the introduction above, determine the purpose of this lab and include it in your lab write-up.
Prediction
On average, what percentage (%) of pennies should show heads up for each shake of the shoe box?
Why do you think so?
Materials Equipment
pennies, 100 shoe box or other cardboard box
Safety Considerations
None for this lab beyond standard lab safety procedures.
Procedure
1. Count out 100 pennies and place all of them tails up into the shoe box. Close the box.
2. While securely holding the lid closed, shake the box for several seconds.
3. Open the box and remove all of the pennies that are heads up.
4. Count the number of pennies remaining in the box and record. DO NOT PUT ANY PENNIES
BACK IN THE BOX!
5. Close the box and repeat Steps #2-4 until only one penny remains or the box is empty.
6. Perform two additional trials by repeating Steps #1-5.
Questions
1. In this lab, what did the pennies represent? What did one trial represent?
2. In your graph, which variable went on the x-axis? Which variable went on the y-axis? Explain
why for both.
3. Theoretically, 50% of the pennies should decay with each shake. Did this actually happen?
Explain why or why not.
CP Chemistry Theodore Roosevelt High School Lab #3-6
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining your calculations.
CP Chemistry Theodore Roosevelt High School Lab #3-6
Your team will test all four food types using a method known as calorimetry. During
this process, you will burn a food sample positioned below a test tube containing a
known amount of cold water. By calculating the temperature change of the water,
you will determine how much energy was released when the food sample burned.
Purpose
To determine how much chemical energy is stored in several different food samples.
Equipment
Determine all equipment you will use and list it in your lab write-up.
Materials
Determine all materials you will use and list them in your lab write-up.
Safety Considerations
Sometimes chemicals from previous labs still remain in glassware and on other lab equipment;
wash all lab equipment before and after performing this lab.
Wash your hands thoroughly after completing this lab.
Procedure
As you perform the lab, record your procedure steps, and then describe them in your lab write-up.
Data
Record all pertinent data and include it in your lab write-up.
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
CP Chemistry Theodore Roosevelt High School Lab #3-7
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing and explaining your results, as well as critically analyzing
your procedure methods.
CP Chemistry Theodore Roosevelt High School Lab #3-7
Laboratory Activities
CP Chemistry Theodore Roosevelt High School Lab #4-0
Purpose
To observe the properties of water in various situations.
Materials Equipment
beaker, 250-mL laundry detergent, conductivity meter pipette
corn syrup powdered graduated cylinder, plastic spoon, plain
dish detergent salt [NaCl] 100-mL plastic spoon w/
isopropyl alcohol, sugar [C12H22O11] paper clip, small Magic Sand
green vegetable oil paper cup rubber band
Kool-Aid solution water, distilled penny stirring rod
water, tap Petri dish well plate
Safety Considerations
Sometimes chemicals from previous labs still remain in glassware and on other lab equipment;
wash all lab equipment before and after performing this lab.
Wash your hands thoroughly after completing this lab.
Procedure
For each of the following stations, follow the directions and record your observations in the data
table. You may complete the stations in any order.
5. Repeat step #B3 using the salt solution. Record your observations in the data table.
6. Discard the paper cup in the trash; return the paper clip to the supplies table.
Station A
Station B
Station C
Station D
Station E
Station F
Station G
Station H
Errors
Think of two possible errors you may have committed in this lab that may have somehow affected your
results and record them below. Explain the specific steps you will take to avoid each of these errors in
the future.
1.
2.
Conclusion
Describe what you learned while doing this lab:
CP Chemistry Theodore Roosevelt High School Lab #4-1
In this lab, we will take a sample of a chemical and treat it as if it is polluted water. We will then dilute
the sample five times, decreasing its concentration by ten times for each step, all the way down to one-
hundred thousandth of the original concentration. Finally, well test each sample with a drop of
chemical indicator to attempt to detect pollution at each concentration.
Purpose
Based on the introduction above, determine the purpose of this lab and include it in your lab write-up.
Prediction
Do you that you will be able to dilute the samples in this lab to levels that are no longer detectable?
Materials Equipment
distilled water graduated cylinder, 10-mL
iron (III) chloride [FeCl3], 0.1M medium test tubes, 6
phenolphthalein indicator solution, 1% plastic pipettes, 3
potassium thiocyanate solution [KSCN], 0.1M test tube rack
silver nitrate solution [AgNO3], 0.1M
sodium chloride [NaCl], 0.1M
sodium hydroxide [NaOH], 0.1M
Safety Considerations
Silver nitrate and potassium thiocyanate are toxic; sodium hydroxide is caustic! Avoid contact
with the skin and eyes.
Safety goggles must be worn at all times; gloves are optional but highly recommended.
Silver nitrate can stain light-colored clothing; you may want to wear a lab apron during this lab.
Sometimes chemicals from previous labs still remain in glassware and on other lab equipment;
wash all lab equipment before and after performing this lab.
Wash your hands thoroughly after completing this lab.
Procedure
1. Obtain six medium test tubes and a test tube rack. Place the test tubes in the test tube rack.
2. Obtain one of the three solutions representing polluted water: NaOH, FeCl3, or NaCl. Note its
color in your observations.
3. Using a small graduated cylinder, measure out exactly 10 mL of polluted water.
4. Pour the 10 mL of polluted water into the first test tube on the left. Rinse out the graduated
cylinder thoroughly.
5. Return the original sample of polluted water to the supplies table.
CP Chemistry Theodore Roosevelt High School Lab #4-1
6. Using a plastic pipette, remove enough polluted water from the first test tube to make 1 mL in the
graduated cylinder.
7. Pour the 1 mL of polluted water in the second test tube. Rinse out the graduated cylinder.
8. Using the small graduated cylinder, measure out exactly 9 mL of distilled water.
9. Pour the 9 mL of distilled water into the second test tube. This dilutes the polluted sample to a
concentration ten times less than the original.
10. Repeat Steps 6-9 for each test tube, each time using the previous test tube to obtain your 1 mL
sample until all six test tubes have polluted water samples like this:
Data you should create three data tables in your lab write-up that look something like this:
Test Tube # Concentration Observations
0.1 M NaOH
1
(original)
2 0.01 M NaOH
Questions
1. What trend did you notice in the colors of the chemical reaction as your solutions became less
concentrated or more dilute? Why do you think this happened?
2. What specific steps would you take to dilute one of these solutions down to one-billionth of its
original concentration?
3. Do you think it would be possible to remove pollution from a water source by simply diluting it?
Why or why not?
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining your calculations.
CP Chemistry Theodore Roosevelt High School Lab #4-1
Supersaturation Lab
Introduction
Under certain conditions, a solution may contain more solute than is
normally contained in a saturated solution at the same temperature. This
type of solution is unstable and is called supersaturated. The solubility of
most substances decreases as temperature decreases. As a solution
cools, any excess solute may or may not crystallize out. If the excess
solute remains in solution, that solution becomes supersaturated.
Purpose
Based on the introduction above, determine the purpose of this lab and include it in your lab write-up.
Prediction
What do you think will happen when you add more solute to the supersaturated solution?
Materials Equipment
distilled water beaker, 100 mL
ice Bunsen burner
sodium sulfate decahydrate [Na2SO410H2O] electronic balance
graduated cylinder, 10 mL
test tube holder
test tube, medium
test tube rack
Safety Considerations
When heating a test tube, never point the mouth of the tube at yourself or anyone else!
Safety goggles must be worn at all times.
Sometimes chemicals from previous labs still remain in glassware and on other lab equipment;
wash all lab equipment before and after performing this lab.
Wash your hands thoroughly after completing this lab.
Procedure
1. Place 5.0 g of Na2SO410H2O in a clean medium-sized test tube. Add 10 mL of distilled water.
2. Hold the test tube in a test-tube holder and heat it in a burner flame, agitating the mixture gently
until all of the solid has dissolved. Place the test tube in a test-tube rack. Add one more crystal of
Na2SO410H2O to the warmed solution and gently agitate it. Record your observations.
3. Place the test tube in a beaker of ice water to cool. Be careful not to disturb the test tube during
the cooling process. If crystals begin to form as the tube is cooling, gently reheat the tube to re-
dissolve the crystals; cool the tube again.
4. When the solution is cold, gently remove the tube from the ice water bath and put it in the test-
tube rack. Add one small crystal of Na2SO410H2O. Touch the bottom of the test tube to the palm
of your hand. Record your observations.
Questions
1. Why is it necessary to heat the mixture in step #2 of the procedure?
2. How could you test whether a solution is unsaturated, saturated or supersaturated? Explain how
interpret the results.
3. Based on the results of this lab, what hypothesis could you develop relating the effect of the rate
of cooling to the stability of a supersaturated solution?
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining your calculations.
CP Chemistry Theodore Roosevelt High School Lab #4-2
In this lab, we will determine the pH of several common household chemicals using both universal
indicator and a natural indicator extracted from red cabbage leaves. We will then use the pHs of these
chemicals to compare the colors produced by universal indicator with the colors produced by red
cabbage indicator in order to determine its effective range.
Purpose
Based on the introduction above, determine the purpose of this lab and include it in your lab write-up.
Prediction
Which of the household chemicals do you think will be the most acidic? Basic?
Materials Equipment
distilled water beaker, 250 mL pipettes
red cabbage beaker tongs ring stand
universal indicator Bunsen burner stirring rod
various household chemicals Erlenmeyer flask, 125 mL well plate
iron rings, 2 wire gauze
Safety Considerations
Be careful not to place bleach and ammonia in adjacent wells this can generate
poisonous chlorine gas!
Although you will not have to wear safety goggles, some of the household chemicals are irritating
to the eyes and skin.
Sometimes chemicals from previous labs still remain in glassware and on other lab equipment;
wash all lab equipment before and after performing this lab.
Wash your hands thoroughly after completing this lab.
Data you should create a data table in your lab write-up that looks something like this:
Household Universal Indicator Red Cabbage Indicator
Well # pH
Chemical Color Color
1
Questions
1. Using your data table, determine the pH range for each color of the red cabbage indicator.
2. As an acid-base indicator, do you think red cabbage indicator is more effective, less effective, or
about as effective as universal indicator? Why?
3. What effect did bleach and/or Oxi-Clean have on the red cabbage indicator? Why do you think
this happened?
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining your calculations.
CP Chemistry Theodore Roosevelt High School Lab #4-3
During the first stages of the titration, the NaOH will be completely neutralized, and an excess of acid
will remain. However, at the theoretical endpoint, the acid and the base will have neutralized one
another exactly, and the phenolphthalein indicator will turn pink when the acid is completely neutralized
and a slight excess of base is present. In this titration, a successful endpoint is achieved if one drop of
base turns the solution in the flask from colorless to a very faint pink, and at this point, the number of
moles of NaOH used will be equal to the number of moles of HCl in the unknown solution.
Purpose
Based on the introduction above, determine the purpose of this lab and include it in your lab write-up.
Materials Equipment
sodium hydroxide solution [NaOH], 0.1M beakers, 250 mL Erlenmeyer flask, 250 mL
hydrochloric acid [HCl], unknown buret, 25 or 50 mL ring stand
phenolphthalein indicator buret clamp
Safety Considerations
Hydrochloric acid and sodium hydroxide are caustic! Avoid contact with the skin and eyes.
Safety goggles must be worn at all times; gloves are optional but highly recommended.
Sometimes chemicals from previous labs still remain in glassware and on other lab equipment;
wash all lab equipment before and after performing this lab.
Wash your hands thoroughly after completing this lab.
Procedure
1. Obtain approximately 120 mL of NaOH in a 250 mL beaker.
2. Rinse the buret with approximately 10 mL of the NaOH solution, and let the liquid drain through
the buret tip into an empty 250 mL "waste" beaker. Repeat this procedure twice more, using new
10 mL samples of NaOH solution each time.
3. Refill the buret so that the meniscus of the solution is above the 0 mL mark. Position the buret in
a double buret clamp on a ring stand. Let some of the solution run rapidly from the buret to expel
all air bubbles from the tip and to bring the level of the solution down to the calibrated region of
the buret. If there is a drop of solution hanging on the tip of the buret, remove it by touching the
drop to the inside wall of the 250 mL beaker.
4. Read the initial volume of the NaOH solution at the bottom of the meniscus. Your eye must be at
the same level as the meniscus.
5. Pour 20.0 mL of HCl into a clean 250 mL Erlenmeyer flask. Add two drops of phenolphthalein
indicator.
CP Chemistry Theodore Roosevelt High School Lab #4-4
6. Place the Erlenmeyer flask under the tip of the base buret; a piece of white paper placed under
the flask will make it easier to see the color changes. While continuously swirling the flask to
ensure thorough mixing, run in the NaOH solution from the buret. Initially, a pink color will appear
at the point where the NaOH comes in contact with the solution in the flask, but this color
disappears quickly. As the endpoint nears, the color will disappear more slowly. Eventually, the
NaOH should be added drop by drop until one drop turns the entire solution in the flask pink. This
pink color should remain for at least 15 seconds while the solution is being swirled.
7. If you overshoot the endpoint, you will have to discard the solution and begin again. When you
have reached a satisfactory endpoint, read the final volume of the buret and record the volume of
NaOH used in your data table.
8. Refill the buret and repeat steps #3-7 twice more, using a clean Erlenmeyer flask.
Data you should create a data table in your lab write-up that looks something like this:
Trial Initial NaOH Titrated Amount Total
Questions
1. Why does the pink color, which forms at the point where the NaOH comes into contact with the
solution in the flask, disappear more slowly near the endpoint?
2. Why is it a good idea to carry out titrations in triplicate?
3. Would the addition of several milliliters of distilled water to the Erlenmeyer flask during the titration
affect the results of the titration? Explain your answer.
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining your calculations.
CP Chemistry Theodore Roosevelt High School Lab #4-4
In this lab, we will test two brands of antacids to see which can neutralize the most acid. We will use
the familiar titration technique with a new indicator, phenol red, which is a pink-red color when basic
and a yellow color when neutral or acidic.
Purpose
Based on the introduction above, determine the purpose of this lab and include it in your lab write-up.
Prediction
Which antacid brand will be the most effective? Why?
Materials Equipment
antacids, various beakers, 250 mL Erlenmeyer flask, 125 mL
hydrochloric acid [HCl], 0.01 M buret, 25 or 50 mL mortar & pestle
phenol red indicator buret clamp ring stand
Safety Considerations
Hydrochloric acid is caustic! Avoid contact with the skin and eyes.
Safety goggles must be worn at all times; gloves are optional but recommended.
Sometimes chemicals from previous labs still remain in glassware and on other lab equipment;
wash all lab equipment before and after performing this lab.
Wash your hands thoroughly after completing this lab.
Procedure
1. Obtain approximately 100 mL of 0.01M hydrochloric acid solution in a 250 mL beaker.
2. Rinse the buret with approximately 10 mL of the HCl solution, and let the liquid drain through the
buret tip into an empty 250 mL "waste" beaker. Repeat this procedure twice more, using new
samples of HCl solution each time.
3. Refill the buret with HCl so that the meniscus of the solution is above the 0 mL mark. Position the
buret in a double buret clamp on a ring stand. Let some of the solution run rapidly from the buret
to expel all air bubbles from the tip and to bring the level of the solution down to the calibrated
region of the buret. If there is a drop of solution hanging on the tip of the buret, remove it by
touching the drop to the inside wall of the 250 mL beaker.
4. Read the initial volume of the HCl solution at the bottom of the meniscus. Your eye must be at the
same level as the meniscus. Record this initial volume in a data table in your data table.
5. Obtain an antacid tablet and measure its mass. Record this information, along with the brand
name and active ingredients, in the data table.
6. Using a clean mortar and pestle, crush the tablet into a fine powder. Pour all of the antacid
CP Chemistry Theodore Roosevelt High School Lab #4-5
Data you should create a data table in your lab write-up that looks something like this:
Antacid Mass Initial HCl Titrated Amount Total
Tums
Rolaids
Questions
1. What advantage does phenol red have over phenolphthalein in this lab?
2. Does it matter how much distilled water you add to the antacid powder? Why or why not?
3. What difference is there between the active ingredients of the antacids? What effect, if any, do
you believe this has on their ability to neutralize acid?
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results, examining the validity of your prediction, and
explaining your calculations.
CP Chemistry Theodore Roosevelt High School Lab #4-5
where R and R represent carbon chains, RCOOH represents an organic acid, HOR represents an
alcohol, and RCOOR represents an ester. Esters are named by using the alcohol name with the acid
name after its suffix has been changed to -ate. For example, ethyl alcohol and acetic acid produce
the ester ethyl acetate.
In this lab, you will prepare three types of fragrant ester molecules from their original components. You
will also name these fragrances using your knowledge of organic chemistry.
Purpose
Based on the introduction above, determine the purpose of this lab and include it in your lab write-up.
Prediction
Which fragrance do you think will smell the most like what it is supposed to?
Materials Equipment
alcohols: beaker, 400 mL
n-amyl alcohol (C5H11OH) graduated cylinder, 10 mL
methyl alcohol (CH3OH) hot plate
ethyl alcohol (C2H5OH) small test tubes, 3
organic acids:
salicylic acid (C7H6O3)
butyric acid (C4H8O2)
glacial acetic acid (CH3COOH)
sulfuric acid, concentrated (H2SO4)
Safety Considerations
Concentrated sulfuric acid is EXTREMELY dangerous! You must wear goggles, gloves and a lab
apron at all times while working with chemicals. Your teacher will dispense the sulfuric acid for
you.
Glacial acetic acid is also VERY dangerous! Take special care not to inhale its vapors or spill any
on your skin.
Because some of the fragrances may have acid remaining after they have reacted, you must use
the wafting method when sampling the odor of your product as shown:
CP Chemistry Theodore Roosevelt High School Lab #4-6
Procedure
1. Prepare a water bath by filling a 400 mL beaker half full with tap water. Place the beaker on a hot
plate to begin heating it.
2. Using the following table, determine three ester fragrances you will produce in this lab:
3. For your first fragrance, obtain 2 mL of the necessary alcohol and add it to a small test tube.
4. If your ester fragrance requires solid acid, obtain 1.0 g of acid and add it to the test tube. If your
ester fragrance requires liquid acid, obtain 2.0 mL of acid and add it to the test tube.
5. Carefully add 1.0 mL of concentrated sulfuric acid to the test tube. (Your teacher will perform this
step.)
6. Gently tap the bottom of the tube to mix the reactants in a safe manner.
7. Place the test tube in the water bath and allow it to be heated for one minute.
8. Check for any possible odor of an ester by using the wafting method. Record your observations.
If no odor is detected, allow the test tube to remain in the water bath for 5-10 more minutes.
9. Repeat steps #3-8 for your second and third ester fragrances.
10. If an odor still cannot be detected, cover the test tube with a small piece of aluminum foil, label it
with your or your lab partners name, and leave it to sit overnight.
Questions
1. Show the balanced reaction for the production of each of the esters that you formed in this lab.
2. Using the directions in the introduction, name the three esters that you produced in this lab.
3. What is the purpose of using concentrated sulfuric acid, which is dangerous, instead of dilute
sulfuric acid or a weak acid, which would be safer?
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing your results and examining the validity of your prediction.
CP Chemistry Theodore Roosevelt High School Lab #4-6
In this capstone lab, you will first research and then perform a chemical purification procedure to
produce clear water using a sample from the Cuyahoga River. You will then judge your success based
on your waters clarity/turbidity, odor, pH, total dissolved solids, and the overall complexity of your
chemical procedure. You will NOT drink your water; you would need to apply additional treatment in
order to make it potable, or safe for drinking.
Purpose
To remove impurities from a sample of water from a local water source.
Equipment
Determine all equipment you will use and list it in your lab write-up.
Materials
Determine all materials you will use and list them in your lab write-up.
Safety Considerations
Sometimes chemicals from previous labs still remain in glassware and on other lab equipment;
wash all lab equipment before and after performing this lab.
Wash your hands thoroughly after completing this lab.
Procedure
As you perform the lab, record your procedure steps, and then describe them in your lab write-up.
Data
Record all pertinent data and include it in your lab write-up.
Errors
Describe two possible errors you may have committed in this lab that may have somehow affected your
results. Explain the specific steps you will take to avoid each of these errors in the future.
Conclusion
Write two or more paragraphs summarizing and explaining your results, as well as critically analyzing
your procedure methods.
CP Chemistry Theodore Roosevelt High School Lab #4-7
(base unit) 1
To convert FROM a base unit TO a prefix unit, MULTIPLY by the Base Unit Multiplier.
To convert TO a base unit FROM a prefix unit, DIVIDE by the Base Unit Multiplier.
To convert FROM a prefix unit TO another prefix unit, first MULTIPLY, then DIVIDE.
From http://www.essex1.com/people/speer/large.html:
"When the metric system was devised in the late 1700's there was no particular need for very large or very small
numbers. It was already customary to count in thousands and millions, and to use commas to set off the extra zeros in groups
of three, as we still do today. In the two centuries since that time we have learned to measure objects and distances, both
large and small, to the limits of nuclear particles and astronomical bodies, and to count from pennies to the US national debt.
The metric measurements are all in decimal form, and are used very consistently from one parameter to another. (Parameters
are things that you measure, such as: length, mass, charge, density, heat, temperature, etc.)
The mass of the earth is 5983 Yg (yottagrams), and it gains another 40 Gg (gigagrams) every year from captured
meteorites and cosmic dust. The average distance to the moon is 384.4 Mm (megameters). The average distance to the sun
is 149.5 Gm (gigameters). The wavelength of yellow light is 590 nm (nanometers). The diameter of a hydrogen atom is about
70 pm (picometers). The mass of a proton is about 1.67 yg (yoctograms), and that of an electron about 0.000 91 yg
(yoctograms).
Converting within the metric system becomes very easy with a little practice. It is simply a matter of moving the
decimal the proper number of places, in the correct direction! For example: 27 000 000 000 grams would be 27 gigagrams,
and 0.000 000 045 meters would be 45 nanometers. If you try to do similar problems in the British system, it becomes much
more difficult. Try the following: How many inches are there in 186,000 statute miles? How many avoirdupois ounces are there
in 82 dry tons? (Realize that there are also nautical miles, troy ounces, and liquid tons in the British system.) Answers:
11,785,000,000 and 2,624,000."
Chemistry
Useful Equations and Constants
theoretical - actual
% error = x 100%
theoretical STP = 0 C at 1 atm
actual
% yield = x 100%
theoretical
Stoichiometry
A
log f
Concentration of Solutions Ai
n=
1
log
2