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D 1177 07
7. Refrigerant
7.1 The refrigerant shall consist of solid carbon dioxide in
alcohol or in other suitable bath liquids.
NOTE 4A layer of dry ice, at least 13 mm (12 in.) thick, must be
FIG. 2 Bottom of Freezing Tube Showing Seeding Tip maintained in the bottom or on the top of the cooling bath during a
determination, depending on the bath liquid used. Adequate precautions
stirrer. The length of the stroke is adjusted so that the coil just should be taken against fire hazards or toxic effects of bath liquids, or
clears the bottom of the freezing-point tube at low point of the both.
stroke. 7.2 Liquid nitrogen may be used as the refrigerant when the
6.1.4 Temperature MeasurementA resistance thermom- freezing point of the coolant is 46C (50F) or lower.
eter or a multi-junction copper-constantan thermocouple may (WarningThe liquid nitrogen should be discarded after each
be used with suitable measuring instruments, providing these days use to avoid the possibility of explosion due to dissolved
give an over-all sensitivity of 0.1C (0.2F). The instrument oxygen and inadvertent mixing with organic coolant materi-
shall be calibrated before each series of determinations by als.)
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D 1177 07
FIG. 3 Time-Temperature Cooling Curves for Determining the Freezing Point of an Engine Coolant
NOTE 7The cooling rate must be less than 1C (2F)/min at the time 4
A research report is available from ASTM headquarters. Request
the solution is seeded. RR:D151010.
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