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Journal of Manufacturing Processes 25 (2017) 201211

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Journal of Manufacturing Processes


journal homepage: www.elsevier.com/locate/manpro

Dimensional accuracy and surface nish of biomedical implant


fabricated as rapid investment casting for small to medium quantity
production
Jaspreet Singh a,b , Rupinder Singh c, , Harwinder Singh d
a
I.K Gujral Punjab Technical University, Kapurthala 144601, India
b
Lovely Professional University, Phagwara 144411, India
c
Production Engineering Department, GNDEC, Ludhiana 141006, India
d
Mechanical Engineering Department, GNDEC, Ludhiana 141006, India

a r t i c l e i n f o a b s t r a c t

Article history: In this work the feasibility of combined route of fused deposition modelling (FDM), chemical vapor
Received 5 May 2016 smoothing (CVS), vacuum casting (VC) and investment Casting (IC) for the development of customized
Received in revised form 4 August 2016 implant for small to medium quantity production has been investigated. Further, an effort has been made
Accepted 28 November 2016
to optimize the dimensional accuracy and surface nish of the implant (hip joint) prepared by varying
two controllable factors (namely: drying time of primary coating and mould thickness) each at three
Keywords:
levels of the IC process. The master pattern of the hip joint has been prepared by FDM followed by the
Fused deposition modelling
CVS process to enhance the surface nish and multiple replicas were produced by the VC process for
Chemical vapor smoothing
Vacuum casting
batch production. The tolerance grades for the selected dimension of the implant/castings were found
Investment casting to be acceptable as per the ISO standard UNI EN 20286-I (1995). Also, the Cpk value greater than 1.3
indicated that the proposed process is statistically controlled.
2016 The Society of Manufacturing Engineers. Published by Elsevier Ltd. All rights reserved.

1. Introduction ing manufacturing of customized or specialized component, during


design iterations or optimizations, the high cost of wax pattern tool-
The demand for specialized and tailor made product like ing makes the IC process expensive [8,9]. Rapid prototyping (RP)
biomedical implant is increasing day by day all around the world becomes one of the feasible solutions used widely in which man-
at high rates [1]. These implants should be biocompatible as well ufacturing facilities are being utilized for specialized, customized
as bioactive within the human body [2]. Also, these implants must and low volume production [10,11]. Fused deposition modelling
have excellent surface quality and dimensional accuracy [3]. Devel- (FDM) is the most diffused RP technique to construct prototypes
opment of these implants using an appropriate route so that they and parts that can be used directly as nished products [1214].
can satisfy all the requirements is the need of todays world. Invest- FDM process begins by creating a 3D CAD model of the component
ment casting (IC) also known as lost wax casting or precision and given as an input to the FDM machine [15]. Then, the materials
casting occupy a key position in the modern metal casting tech- like acrylonitrile butadiene styrene (ABS) or polycarbonate were
niques and is widely used for producing complex, intricate shaped fed into the FDM extrusion head, where they are heated to a semi-
and precision metallic components that requires excellent sur- liquid state [16]. The head then deposits the material in thin layers
face nish and dimensional accuracy [46]. The term IC refers to and each layer bonds to the previous layer by particular material
the use of ceramic slurry applied or invested around a disposable fabrication technology until the 3D physical model is built [17,18].
pattern usually wax to form a mould with extremely smooth sur- This 3D plastic model can be used to replace sacricial wax patterns
face qualities [7]. However, IC is considered economical only for in the traditional IC process without any major modications in the
mass production [8]. If the volume is low like in prototyping, dur- process [18,19] and thus eliminate the expensive tooling required
for making the patterns [20]. The process of employing RP tech-
niques to fabricate sacricial patterns for the IC process is known
as rapid investment casting (RIC) [9]. Also, it enables the engineers
Corresponding author. to make changes in design readily [21,22]. Although, FDM process
E-mail addresses: rupindersingh78@yahoo.com, singhrupinder@gndec.ac.in has been implemented successfully to reduce the product build
(R. Singh).

http://dx.doi.org/10.1016/j.jmapro.2016.11.012
1526-6125/ 2016 The Society of Manufacturing Engineers. Published by Elsevier Ltd. All rights reserved.
202 J. Singh et al. / Journal of Manufacturing Processes 25 (2017) 201211

terion is that the optimum settings were not restricted to the


experimental values as in case of grey Taguchi method, so true
optimum settings were achieved using this approach. Galantucci
et al. [31] employed a post-processing technique to improve the
surface nish of FDM fabricated ABS parts by immersing them in a
dimethyl-ketone and water solution (ratio 9:1) and concluded that
by this treatment exural strength as well as surface nish of the
components has improved signicantly along with small variations
in prototype dimensions. Nunez et al. [32] examined the effect of
part density and layer thickness on dimensional accuracy, atness,
and surface texture obtained in FDM with ABS-plus as the model
material and concluded that minimum dimensional deviation was
obtained with layer thickness of 0.254 mm and with solid density.
The Z axis exhibited the worst dimensional behaviour and density
of model interior ll was found to be the parameter affecting most
dimensional precision even more than the layer thickness on the
Z axis. Katatny et al. [33] made investigations regarding the errors
generated during the fabrication process on FDM3000 system by
comparing the dimensions with actual models and concluded that
high level of accuracy has been achieved by the FDM process in
comparison with other RP techniques. Garg et al. [23] investi-
gated the improvement in surface nish and change in dimensional
accuracy of FDM fabricated parts when subjected to cold vapor
treatment of dimethyl-ketone and concluded that by this vapor
treatment the surface nish of the components improved dramati-
Fig. 1. Benchmark component. cally with minimal variations in part dimensions. From the review
of literature, it has been observed that orientation, layer thickness
time and cost, but the surface quality and dimensional accuracy and part density (part interior style) are the main factors that affect
of the FDM prototypes suffers badly even for basic part geometries the dimensional accuracy and surface nish of FDM prototypes
[23]. So, for effective use of RP technology, it becomes necessary [23,26,27,29,30,32] and a lot of work has been done to improve
that improvement in surface quality, dimensional accuracy and part the surface nish and dimensional accuracy of by employing var-
strength are the key issues that have to be addressed [24,25]. ious techniques such as by optimizing the input parameters, by
Many researchers have directed their effort to improve the utilizing the optimum slicing strategy, or by optimizing part build
surface nish and dimensional accuracy of FDM prototypes by opti- orientations. Also, some work has been reported that reveals that
mizing the process parameters and part build orientation while the surface nish of ABS replicas improved signicantly by exposing
few of them have employed advanced techniques such as barrel them to suitable chemicals at the expense of dimensional accu-
nishing and chemical vapor smoothing. Thrimurthulu et al. [26] racy [23,31]. But still lot of scope has been observed to determine
developed a model to improve surface nish and to reduce build the effect of combined process of FDM and CVS on dimensional
time by optimizing part deposition orientation using adaptive slic- accuracy and surface nish of fabricated replicas.
ing scheme for the FDM process. Surface nish and build time are Another challenge with RP technologies is that they are not pre-
the most important concerns and these two generally contradict ferred for small to medium quantity production due to the high cost
with each other. A coded genetic algorithm was used to obtain involved and also have limited range in terms of material selec-
the optimal solution. Anitha et al. [27] investigated the effect of tion [34]. This requires the need of developing rapid tooling (RT),
three process parameters, namely layer thickness, road width and which is an extension of RP. It is the technology that utilizes the RP
speed of deposition on the surface quality of the FDM fabricated and applies them to the manufacturing of various tools [24,35]. RP
components and concluded that layer thickness was the most dom- cuts down product development time and RT cuts down the pro-
inating factor affecting the surface roughness. Chakraborty et al. duction time [36]. Further, RT can be classied as either direct or
[28] described a method for the FDM process, in which the lay- indirect. Direct tooling techniques are those which utilize additive
ers are deposited along curved paths instead of horizontal paths manufacturing (AM) techniques for the fabrication of the mould
and concluded that this method has the potential to increase the and then these moulds are used for producing prototypes of var-
strength of parts and to reduce the stair-step effect, number of ious materials [37]. Indirect tooling involves fabrication of mould
layers, and ultimately build time. Sood et al. [29] examined the from an AM master pattern, which is then used to manufacture mul-
effect of ve parameters (layer thickness, part build orientation, tiple prototypes. Silicone rubber tooling (RTV), epoxy resin tooling
raster angle, air gap and raster width) on the dimensional accu- and spray metal tooling are some common examples of indirect
racy of length, width, thickness and diameter of FDM-made ABS RT. Silicone moulding (SM) is an established prototyping technique
parts using the Taguchi method. The results indicated that opti- widely used in industry to produce wax patterns [38,39] and vari-
mum parameter that minimizes the variation in all the responses ous types of plastic parts due to high chemical resistance of silicone
were different. So, the common factor settings that simultaneously rubber and low interfacial energy of its surface [38]. Some studies
show minimum deviation in all the responses had been obtained have been reported as an indirect approach for producing wax pat-
using grey Taguchi method. Mohamed et al. [30] tried to study the terns via silicone rubber moulding from RP based master pattern
inuence of six FDM process parameters (layer thickness, air gap, to reduce the costs associated with single-part or small-quantity
raster angle, build orientation, road width and number of contours) production during the investment casting process [8]. Yarlagadda
on the percentage change in length, width and thickness using I- et al. [40] compared the accuracy of wax patterns produced by hard
optimality criterion. The optimum parameter settings for all the (PU mould) and soft tooling (RTV mould) and concluded that for soft
three responses were different and the best solution was achieved tooling, injection temperature is the only parameter that affects the
by I-optimality criterion. The main advantage of I-optimality cri- dimensional accuracy. Singh et al. [41] fabricated the plastic com-
J. Singh et al. / Journal of Manufacturing Processes 25 (2017) 201211 203

Fig. 2. Methodology of the study.

Table 1
Input parameters, their levels and optimal parameter settings for the two stages.

Stage 1 Process Parameters Unit Levels Range of Ra and d Optimal settings

1 2 3

Stage 1 FDM Orientation degree 0 90 Ra : 5.006-8.742 m 90
d: 0.040.19 mm
Part density High Low Solid High
CVS No. of cycles 3 4 5 Ra : 0.144-0.159 m 5
Cycle time sec 4 6 8 d: 0.010.14 mm 4

Stage 2 VC PU material 6130 PX223 PX223


Hardener % 90 95 100 Ra : 0.3191.640 m 100

Curing temperature C 70 80 90 d: 0.080.58 mm 70
Curing time min 45 55 65 45

ponent using SM process and highlighted the process capability of on vacuum casting (VC) process to fabricate polyurethanes (PU)
SM in-terms of dimensional accuracy. Further, many researchers replicas for RIC applications. Also, it has been suggested by the
successfully fabricate sacricial wax patterns for IC process by RTV researchers that the dimensional accuracy of the traditional IC pro-
mould process [40,42,43] but very little work has been reported cess for complex and intricate shapes can be increased by replacing
204 J. Singh et al. / Journal of Manufacturing Processes 25 (2017) 201211

Fig. 3. Specimens after casting.

Table 2
Parameters and their levels for IC process.

Stage 3 Mould thickness B number of layers 7 8 9


Drying time of primary coating A min 330 360 390
Parameters Symbol Unit Levels

1 2 3

conventional wax based pattern with the modern plastic based hip joint is replaced with metal, plastic or ceramic components.
patterns [20]. Generally, the ball (femoral head) is removed and replaced with
Keeping in mind gaps in the literature, the researcher rst tried new and durable articial synthetic part. The CAD model of the
to investigate the feasibility of the combined route of FDM, CVS, VC component has been made using Solidworks software and then
and IC process for the development of specialized or customized converted into .STL le. The master pattern of the hip joint has been
products such as biomedical implant for small to medium quan- fabricated from the .STL le by FDM technique followed by CVS
tity production. After that, an effort has been done to investigate process to enhance its surface nish. After that, multiple replicas
the inuence of two input parameters of IC process, namely drying of PU material were manufactured by vacuum casting (VC) process
time of primary coating and mould thickness on the dimensional that reduces the cost of RP and also acts as sacricial pattern in IC
accuracy and surface nish of biomedical implant (hip joint) fab- process. IC begins with joining the PU replicas to a wax tree fol-
ricated as RIC. The optimization of process parameters has been lowed by number of layers of stucco coating of ceramic material
done to obtain the optimum parameter settings and it has been also for imparting strength to the mould. Baking of the mould is then
checked that whether the tolerance of the casted components is carried out in a furnace at around 900 C. During the baking process,
consistent with the permissible range of tolerance grades as per ISO the PU replica suddenly come out of the mould in the gaseous state
standards. In order to check the repeatability and consistency of the and leaves the shell for pouring the molten metal. Before pouring,
process, the process capability analysis for the selected dimension compressed air was passed through the shell for removing any ash
has also been done. content that left during the baking process. Castings were produced
with a biocompatible grade of stainless steel (316L) under recom-
2. Methodology and experimentation mended parameters. Experiments were conducted twice in order
to check the repeatability and to minimize the error. The complete
In this research work, a component of biomedical application methodology of the study has been shown in Fig. 2.
(hip joint) as shown in Fig. 1 has been selected as the benchmark. The controllable factors and their levels during each process
The hip joint is basically a ball-and-socket joint. The socket is made have been decided on the basis of an extensive literature review
of bone and cartilage, and the ball is the head of the thigh bone and pilot experimentation. From the review of literature, it has been
(femoral head). During the hip replacement surgery, the damaged observed that orientation, layer thickness and part density (part
J. Singh et al. / Journal of Manufacturing Processes 25 (2017) 201211 205

Fig. 4. Surface roughness (Ra ) graphs of each casting.


206 J. Singh et al. / Journal of Manufacturing Processes 25 (2017) 201211

Table 3 (SR) has been taken to represent the dimensional accuracy and sur-
Control log of Experimentation.
face nish respectively (Fig. 3). One selected dimension of all the
S.No Drying time of primary Mould thickness PU replicas and corresponding castings was measured by coordi-
coating (min) (number of layers) nate measuring machine (CMM) and deviation has been identied.
1 330 7 Surface roughness (Ra value) of all the castings has been measured
2 330 8 at femur part by Mitutoyo SJ-210 roughness tester at 0.5 mm/sec
3 330 9 stylus speed, cut-off length at 0.25 mm and X at 5. The reason
4 360 7
for selecting Ra value in order to measure the surface roughness
5 360 8
6 360 9 was that it employs an algorithm that averages the absolute val-
7 390 7 ues of the prole height deviations from the mean line on the
8 390 8 entire surface within the sampling length and then neutralizes the
9 390 9
few outlying points so that the extreme points have no signicant
impact on the nal results (as described in ASME B46.1). Also, it is a
interior style) are the main factors that affect the surface nish and simple and effective method for monitoring the surface texture and
dimensional accuracy of FDM prototypes. Layer thickness has been ensuring consistency in measurement of multiple surfaces. The sur-
kept constant (0.254 mm) in this study because it has very little face roughness (Ra ) graphs obtained during each experiment have
effect on surface roughness after chemical treatment [44]. Simi- been shown in Fig. 4.
larly, one of the parameter selected to be varied in CVS process Signal to noise (S/N) ratio has been calculated in order to predict
was number of cycles i.e. number of times the prototypes were the variation caused by each factor. The advantage of using S/N ratio
exposed to chemical vapors and the second was cycle time. The is that it uses a single measure, mean square deviation (MSD), which
optimal replica obtained after the model fabrication stage (FDM & incorporates the effect of changes in mean as well as the variation
CVS process) with regard to dimensional accuracy and surface nish (standard deviation) with equal priority [20]. The main objective of
would act as a master pattern for the VC process. The input param- this research work is to obtain both the d and SR to be minimum.
eters varied during the creation of multiple replicas by VC process Therefore, S/N ratios were calculated using Eq. (1) on the basis of
were PU material, hardener percentage, curing temperature and lower is better approach for both the responses.
curing time. The level selected for various parameters along with  
1 2
r
the optimum results with regard to dimensional accuracy and sur-
face nish during the two stages (model fabrication and creation of S/N = 10 log Yi (1)
r
multiple replicas) have been shown in Table 1. i=1
In IC process, there is no direct way to control the thickness
of the mould except by controlling the number of ceramic slurry Yi = Observed value of the response characteristic, r = Number of
layers. Higher the number of slurry layers more will be the thick- repetitions.
ness of the mould. The mould thickness affects the strength of the Analysis of the experimental results has been made by using
mould as well as the cooling rate of the castings [45]. Observation MINITAB 17 statistical software package [46]. The d and SR along
made from pilot experimentation indicates that with less than 7 with signal to noise ratio for both the responses has been shown in
number of slurry layers, the IC shell gets cracked while pouring Table 4. Analysis of Variance (ANOVA) has been performed on S/N
the molten metal. Based on the pilot experimentation and liter- ratio of both the responses for testing and analyzing the results.
ature review, level for the two selected parameters in IC process It helps in predicting the signicance of each input factor and its
has been shown in Table 2. Taguchis orthogonal array has been percentage contribution on the desired response. In ANOVA, the
selected to plan and analyze the experiments. In this study, the sum sum of squares (SS), degree of freedom (DOF), variance (V), F-Ratio
of number of degrees of freedom for the selected two parameters and the percentage contribution of each factor are calculated. SS is
is 4; accordingly the most suitable orthogonal array with three- a measure of deviations of the experimental data from the mean
level variables was distinguished as L9 with 8 of freedom. Since data value. Percentage contribution denes its signicance rate
the experimental design requires only 4 of freedom, the remain- on the output response. Higher the percentage contribution, the
ing dofs has been utilized to measure the experimental error. The more will be the effect of the input factor on the output. By con-
control log of experimentation is shown in Table 3. trolling the factors with high contribution, the total variation can
be reduced leading to improvement of process performance. The
3. Results and discussion ANOVA result for the S/N ratios of d and SR has been shown in
Tables 5 and 6 respectively. The P-value less than 0.05 (i.e. = 0.05,
After casting, the effect of selected input parameters has been or 95% condence) in Tables 5 and 6 indicates that the model terms
studied on the dimensional accuracy and surface nish. In this are signicant. So, in case of d, B is the signicant model term and
research work, dimensional deviation (d) and surface roughness in case of SR, A is the signicant model term. Larger F-value for any

Table 4
d and SR along with S/N ratio.

S.No Dimensional deviation (mm) S/N ratio Surface roughness, Ra (m) S/N ratio

R1 R2 Average R1 R2 Average

1 0.305 0.301 0.303 10.37 2.140 2.156 2.148 6.64


2 0.180 0.188 0.184 14.70 2.235 2.257 2.246 7.03
3 0.060 0.062 0.061 24.29 2.088 2.120 2.104 6.46
4 0.324 0.320 0.322 9.84 1.921 1.875 1.898 5.57
5 0.159 0.165 0.162 15.81 1.822 1.788 1.805 5.13
6 0.091 0.093 0.092 20.72 1.753 1.759 1.756 4.89
7 0.360 0.354 0.357 8.95 1.666 1.602 1.634 4.27
8 0.242 0.246 0.244 12.25 1.531 1.499 1.515 3.61
9 0.102 0.10 0.101 19.91 1.584 1.602 1.593 4.04
J. Singh et al. / Journal of Manufacturing Processes 25 (2017) 201211 207

Table 5
ANOVA results for d.

Source DOF Adj SS Adj MS F-value P-value % Contribution

A 2 11.647 5.823 3.39 0.138 4.94


B 2 217.327 108.663 63.18 0.001 92.15
Error 4 6.880 1.720 2.91
Total 8 235.853

Model summary

S R-sq R-sq (adj) R-sq (pred)

1.3014 0.9708 0.9417 0.8523

Table 6
ANOVA results for SR.

Source DOF Adj SS Adj MS F-value P-value % Contribution

A 2 11.2826 5.6412 52.86 0.001 94.80


B 2 0.1992 0.0995 0.93 0.465 1.67
Error 4 0.4269 0.10673 3.59
Total 8 11.9087

Model summary

S R-sq R-sq (adj) R-sq (pred)

0.3266 0.9642 0.9283 0.8185

Table 7
Calculations of IT grades.

Exp No Nominal Measured Fundamental Tolerance value IT grade


dimension (mm) dimension (mm) tolerance i (m) n

1 24.945 24.642 1.3072 231.78 IT13


2 24.945 24.761 1.3072 140.75 IT12
3 24.945 24.884 1.3072 46.66 IT9
4 24.945 24.623 1.3072 246.31 IT13
5 24.945 24.783 1.3072 123.92 IT11
6 24.945 24.853 1.3072 70.37 IT10
7 24.945 24.588 1.3072 273.08 IT13
8 24.945 24.701 1.3072 186.64 IT12
9 24.945 24.844 1.3072 77.26 IT10

Table 8
Constraints and optimum values suggested by the software.

Name Goal Lower limit Upper limit Weight Importance

Drying time of primary coating Constraint to region 330 390 1 1


Mould thickness Constraint to region 7 9 1 1
S/N ratio for d Maximize 8.95 24.29 1 1
S/N ratio for SR Maximize 7.03 3.61 1 1

Optimum values

Drying time of primary coating Mould thickness S/N ratio (d) S/N ratio (SR) Desirability

390 9 20.14 3.81 0.828

factor indicates that variation in this factor causes large variation drying time of primary coating and was minimum with time of
in performance characteristics. 390 min. This was due to the removal of moisture present in the
Figs. 5 and 6 shows the main effect plot of various factors on ceramic shell with increase in drying time of primary coating. It
d and SR respectively. Fig. 5 shows that d decreases with is similar to the results obtained by [48]. Ra value also improves
increase in mould wall thickness and was minimum with 9 number slightly with an increase in mould thickness and this may be due
of layers. With 7 number of layers d was maximum and this was to variation in heat transfer rate but its effect was not signicant as
due to the lesser mould wall thickness which resulted into higher observed from lesser F-value in Table 6.
heat transfer rate and ultimately more shrinkage occurs. As the
number of layers increases, heat transfer rate as well as shrinkage
decreases which results in lesser deviation. The results are in line 3.1. Calculation of tolerance grades
with the observations made by other investigators [47]. Also, d
increases slightly with increase in drying time of primary coating, In order to nd the tolerance grades, rst the measured dimen-
but its effect was not signicant as observed from lesser F-value sion have been used to evaluate the tolerance unit n that derives
in Table 5. Fig. 6 shows that Ra value decreases with increase in from the fundamental tolerance i, as dened in ISO standard UNI
EN 20286-I(1995). Also, the fundamental tolerance i is not eval-
208 J. Singh et al. / Journal of Manufacturing Processes 25 (2017) 201211

Fig. 5. a) Mean S/N ratios for d b) Mean graph for d.

Fig. 6. a) Mean S/N ratios for SR b) Mean graph for SR.

uated separately for each nominal size, but for a range of nominal
sizes. The fundamental tolerance i and tolerance unit n is calcu-
lated as follows [11,49]:

3 n = 1000(24.94524.642)/1.3073 = 231.77
i = 0.45 D + 0.001D (2)
D D 
N M
n = 1000 (3)
i
Similarly, the values of n for all the experimental runs were
Where: D is the geometric mean of range of nominal size, DN is calculated and the corresponding IT grades have been obtained as
the nominal dimension, DM is the measured dimension, i is the shown in Table 8.
fundamental tolerance in m. It has been observed from Table 7 that in all the experiments,
In this research work, the linear dimension as shown in Fig. 1 the measured dimension is less than the nominal dimension. It is
(24.945 mm after VC process) has been taken as nominal dimen- due to the shrinkage that occurs during solidication of the cast-
sion. The standard basic step for this dimension is 1830 mm. For ing as the metal changes state from liquid to solid. This shrinkage
experiment 1, the value of n is calculated as follows: is generally compensated by providing shrinkage allowance to the
pattern. Further, the IT grades of the component prepared by this
D = (18 30)1/2 = 23.237 mm
rapid investment casting (RIC) are consistent with the permissi-
ble range of tolerance grades as per ISO standard UNI EN 20286-I
i = 0.45(23.237)1/3 + 0.001(23.237) = 1.3072 (1995).
J. Singh et al. / Journal of Manufacturing Processes 25 (2017) 201211 209

Fig. 7. Histogram of observed values along with Cp and Cpk values of the process.

Fig. 8. Normal distribution curve for observed values.

4. Optimization and conrmation experiments parameter levels for the two responses are also different. So, instead
of optimizing the individual response in an arbitrarily manner, it
Higher the S/N ratio, more favourable is the effect of input vari- has been desirable to obtain the parameter settings that simulta-
able on the response. From Figs. 4 and 5, the optimum factor levels neously minimizes the d and SR. In order to achieve the above
with highest S/N ratio have been identied in order to achieve the objective, the response optimization module of Minitab 17 soft-
maximum dimensional accuracy and surface nish. So, the opti- ware has been used. The constraints set and the optimum values
mum parameter settings for maximum dimensional accuracy are along with the desirability suggested by the software have been
A1 and B3. Similarly, the optimum parameter settings for maxi- shown in Table 8.
mum surface nish are A3 and B3 . From Tables 5 and 6, it has been The calculated d and Ra corresponding to S/N ratio of 20.14
observed that signicant factors and their percentage contribution & 3.81 are 0.098 mm & 1.550 m respectively. In order to check
for the two output responses are different. Similarly, the optimum the validity of the results suggested by the software, two conrma-
210 J. Singh et al. / Journal of Manufacturing Processes 25 (2017) 201211

Table 9 The Cpk value greater than 1.3 for the same dimension indicated
Observations of selected dimension at optimum parameter setting.
that the proposed process is highly capable.
S.No Observations IT grade

1 24.842 IT10
Acknowledgements
2 24.846 IT10
3 24.851 IT10
4 24.839 IT10 The authors are thankful to Manufacturing Research Lab
5 24.849 IT10 (GNDEC, Ludhiana) and IKGPTU, Jalandhar for providing the
6 24.845 IT10 research facilities. The authors are also thankful to Mr. Gurpreet
7 24.850 IT10
8 24.846 IT10
Singh Phull (Associate Dean, Lovely Professional University) and
9 24.841 IT10 Mr. Puran Singh (Lab technician, GNDEC, Ludhiana) for providing
10 24.835 IT10 their technical support.
11 24.848 IT10
12 24.847 IT10
References

[1] Singh R, Singh G. Process capability analysis for replication of FDM based
tion tests were performed at optimum parameter values as given
patterns by vacuum moulding in biomedical applications. In: Proceedings of
in Table 8. The d and Ra for the two conrmation tests were International Conference on Smart Technologies for Mechanical Engineering
found to be (0.096 mm, 0.099 mm) & (1.593 m, 1.581 m) respec- (STME-2013). 2013.
[2] Gibson I, Cheung LK, Chow SP, Cheung WL, Beh SL, Savalani MM, et al.
tively. This conrms excellent reproducibility of the experimental
The use of rapid prototyping to assist medical applications. Rapid Prototyp J
conclusions. 2006;12:538.
[3] Gu P, Li L. Fabrication of biomedical prototypes with locally controlled proper-
ties using FDM. Ann CIRP 2002;51(1):1814.
5. Calculation of process capability [4] Liu Q, Sui G, Leu MC. Experimental study on the ice pattern fabrication for the
investment casting by rapid freeze prototyping. Comput Ind 2002;48:18197.
[5] Konrad CH, Brunner M, Kyrgzaev K, Volkil R, Glatzel U. Determination of heat
Further, in order to check whether the process is statistically transfer coefcient and ceramic mold material parameters for alloy IN738LC
controlled or not, 12 samples were casted with optimum parame- investment casting. J Mater Process Technol 2011;211(2):1816.
ter settings. The selected dimension of nal castings measured with [6] Amira S, Dube D, Tremblay R. Method to determine hot permeabil-
ity and strength of ceramic shell moulds. J Mater Process Technol
CMM along with calculated IT grade was shown in Table 9. After that 2011;211(8):133640.
the Cp and Cpk values of the process and histogram of observed val- [7] Babu M, Kayala J, Martin P, Chowdiah PM. Standardization of invest-
ues have been obtained by QI Macros 2015 software as shown in ment casting process using modied binder hydrolysis. Bull Mater Sci
1990;13(3):22734.
Fig. 7. Basically, Cp and Cpk are the process capability indices used [8] Cheah CM, Chua CK, Lee CW, Feng C, Totong K. Rapid prototyping and tooling
to measure the potential ability of a process to produce acceptable techniques: a review of applications for rapid investment casting. Int J Adv
output by meeting the specied requirements [50]. The prerequi- Manuf Technol 2005;25(34):30820.
[9] Pattnaik S, Karunakar B, Jha PK. Developments in Investment casting processa
site for computing Cp and Cpk is that the process is required to be
review. J Mater Process Tech 2012;212:233248.
under statistical control and that the data are normally distributed [10] Ainsworth I, Ristic M, Brujic D. CAD-based measurement path planning for free
[51,52]. form shapes using contact probes. Int J Adv Manuf Technol 2000;16:2331.
[11] Singh JP, Singh R. Investigations for statistically controlled rapid casting solu-
In this work, corresponding to Cpk value of 1.44 for the selected
tion of lead alloys using three dimensional printing. J Mech Eng Sci (Proc IMechE
dimension, area under the normal curve is 0.99997973 and non- Part C) 2009;223:212534.
conrming parts per million is 20.27. It means that the process will [12] Wohlers T. Wohlers report 2012: executive summary. Fort Collins CO: Wohlers
produce conforming products as long as it remains in statistical Associates; 2012.
[13] Singh R, Verma M. Investigations for reducing wall thickness of aluminum
control. Further, normal probability plot (Ref. Fig. 8) shows that shell casting using three dimensional printing. J Achiev Mater Manuf Eng
the data are normally distributed. The observed values are plotted 2008;31:659.
on the X-axis against a theoretical normal distribution (z-scores) on [14] Singh R. Three-dimensional printing for casting applications: a state of art
review and future perspectives. Adv Mater Res 2010;42:836.
the Y-axis [52]. A regression line is drawn from these XY pair which [15] Greul M, Pintat T, Greulich M. Rapid prototyping of functional metallic parts.
shows points closer to the regression line and thus indicating a good Comput Ind 1995;28(1):238.
t. [16] Chhabra M, Singh R. Rapid casting solutions: a review. Rapid Prototyp J
2011;17(4). In-Press.
[17] Noorani R. Rapid prototypingprinciples and application. NewJersey: John
Wiley & Sons Inc.; 2005.
6. Conclusions [18] Upcraft S, Fletcher R. The rapid prototyping technologies. Assemb Autom
2003;23:31830.
From this research work, the following conclusions have been [19] Kumar P, Ahuja IPS, Singh R. Application of fusion deposition modelling for
rapid investment castinga review. Int J Mater Eng Innov 2012;3:20427.
made:
[20] Kumar P, Singh R, Ahuja IPS. Investigations on dimensional accuracy of the
components prepared by hybrid investment casting. J Manuf Processes 2015,
The combined route of FDM, CVS, VC and IC has been found fea- http://dx.doi.org/10.1016/j.jmapro.2015.07.008.
[21] Chua CK, Chew TH, Eu KH. Integrating rapid prototyping and tooling with vac-
sible for the development of specialized or customized products uum casting for connectors. Int J Adv Manuf Technol 1998;14:61723.
such as biomedical implant for small to medium quantity pro- [22] Chua CK, Feng C, Lee CW, Ang GQ. Rapid investment casting: direct and indirect
duction. approaches via model maker II. Int J Adv Manuf Technol 2005;25:2632.
[23] Garg A, Bhattacharya A, Batish A. On surface nish and dimensional accu-
Mould thickness affects the dimensional accuracy signicantly
racy of FDM parts after cold vapor treatment. Mater Manuf Processes 2015,
and d decreases with increase in mould wall thickness and http://dx.doi.org/10.1080/10426914.2015.1070425.
was found to be minimum with 9 number of layers. [24] Rosochowski A, Matuszak A. Rapid toolingthe state of art. J Mater Process
Drying time of primary coating affects the surface nish signif- Technol 2000;106:1918.
[25] Hopkinson N, Hagur RJM, Dickens PH. Rapid manufacturing: an industrial rev-
icantly and Ra value decreases with increase in drying time of olution for the digital age England. John Wiley & Sons Inc; 2006.
primary coating and was minimum with time of 390 min. [26] Thrimurthulu K, Reddy NV, Pandey PM. Optimum part deposition orientation
The tolerance grades for the selected dimension of the castings in fused deposition modeling. Int J Mach Tools Manuf 2004;44:58594.
[27] Anitha R, Arunachalam S, Radhakrishnan P. Critical parameters inuencing
were found to be acceptable as per the ISO standard UNI EN the quality of prototype in fused deposition modeling. J Process Technol
20286-I (1995). 2001;118:3858.
J. Singh et al. / Journal of Manufacturing Processes 25 (2017) 201211 211

[28] Chakraborty D, Reddy A, Roy B, Choudhury A. Extruder path generation for [41] Singh R, Singh B. Process capability of rapid manufacturing for plastic
curved layer fused deposition modeling. Comput Aid 2008;40:23543. components. Germany: LAP Lambert Accademic publication; 2010. ISBN 978-
[29] Sood AK, Ohdar RK, Mahapatra SS. Improving dimensional accuracy of fused 3-8433-8735-4, pp. 76.
deposition modelling processed part using grey Taguchi method. Mater Design [42] Rahmati S, Akbari J, Barati E. Dimensional accuracy analysis of wax patterns
2009;30:424352. created by RTV silicon rubber molding using Taguchi approach. Rapid Prototyp
[30] Mohamed OA, Masood SH, Bhowmik JL. Optimization of fused deposition mod- J 2007;13(2):11522.
eling process parameters for dimensional accuracy using I-optimality criterion. [43] Zamani J, Hemati MH, Morsaluie R. An experimental comparison on dimen-
Measurement 2016;81:17496. sional accuracy of wax patterns of gas turbine blades produced by rapid tooling.
[31] Galantucci LM, Lavecchia F, Percoco G. Experimental study aiming to enhance Arab J Sci Eng 2014;39:728997.
the surface nish of fused deposition modeled parts. Ann Manuf Technol [44] Galantucci LM, Lavecchia F, Percoco G. Quantitative analysis of a chemical treat-
2009;58:18992. ment to reduce roughness of parts fabricated using fused deposition modeling.
PJ, Rivas A, Garca-Plaza E, Beamudb E, Sanz-Lobera A. Dimensional and
[32] Nunez CIRP Ann Manuf Technol 2010;59:24750.
surface texture characterization in Fused Deposition Modelling (FDM) with ABS [45] Kumar P, Singh R, Ahuja IPS. Experimental investigations on hardness of the
plus. Proc Eng 2015;132:85663. biomedical implants prepared by hybrid investment casting. J Manuf Processes
[33] E-Katatny I, Masood SH, Morsi YS. Error analysis of FDM fabricated medical 2016;21:16071.
replica. Rapid Prototyp J 2010;16(1):3643. [46] MINITAB 17 Statistical software package, User Manual. Copyright 2015
[34] Boparai K, Singh R, Singh H. Development of rapid tooling using Minitab Inc.
fused deposition modeling: a review. Rapid Prototyp J 2016;22, [47] Singh R, Singh J, Singh S. Investigation for dimensional accuracy of AMC
http://dx.doi.org/10.1108/RPJ-04-2014-0048, 2. prepared by FDM assisted investment casting using nylon-6 waste based rein-
[35] Kruth PJ. Material increases manufacturing by rapid prototyping techniques. forced lament. Measurement 2016;78:2539.
Ann. CIRP 1991;40(2):60314. [48] Singh R, Singh S, Kapoor P. Investigating the surface roughness of implant
[36] Karunakaran KP, Bernard A, Suryakumar S, Dembinski L, Taillandier G. Rapid prepared by combining FDM and investment casting. Proc IMechE Part E
manufacturing of metallic objects. Rapid Prototyp J 2012;18(4):26480. 2014;0(0):18.
[37] Pal DK, Ravi B. Rapid tooling route selection and evaluation for sand and invest- [49] Bassoli E, Gatto A, Luliano L, Violentte MG. 3D printing technique applied to
ment casting. Virtual Phys Prototyp J 2007;4:197207. rapid casting. Rapid Prototyp J 2007;13:14855.
[38] Smith BJ, St Jean P, Duquette ML. A comparison of rapid prototype techniques [50] Singh R, Singh G. Cast component hardness comparison for investment casting
for investment casting Be-Al. Proc Rapid Prototyping and Manufacturing Con- prepared with wax and ABS patterns. Trans Indian Inst Met 2015;68:1721.
ference, 2325. 1996. p. 111. [51] Singh R. Effect of work piece volume on statistically controlled rapid casting
[39] Chung S, Park S, Lee I, Jeong H, Cho D. Replication techniques for a metal micro- solution of aluminum alloys using three dimensional printing. Mater Manuf
component having real 3D shape by microcasting process. Microsys Technol Processes 2012;27(4):37782.
2005;11:4248. [52] Singh R. Process capability analysis of fused deposition modelling for plastic
[40] Yarlagadda P, Hock TS. Statistical analysis on accuracy of wax patterns used in components. Rapid Prototyp J 2014;20(1):6976.
investment casting. J Mater Technol 2003;138:7581.

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