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To cite this article: Glay zkan , Gray rkmez & Gksel zkan (2003) Application of BoxWilson Optimization Technique
to the Partially Oriented Yarn Properties, Polymer-Plastics Technology and Engineering, 42:3, 459-470, DOI: 10.1081/
PPT-120017964
To link to this article: http://dx.doi.org/10.1081/PPT-120017964
ABSTRACT
A static model for partially oriented yarn (POY) production was
examined in a commercial POY spinning plant. A two-level factorial,
industrial experimental design was used to identify a statistical model.
Three independent variables effecting the elongation at break (a POY
property of interest) were selected. Namely, yarn winding speed,
spinneret flow rate, and spinneret hole diameter. Elongation at break was
chosen as the dependent variable. A first-order statistical model was
considered to show the dependence of the elongation at break on the
operating parameters: 145%; for elongation at break, the optimum values
of yarn winding speed, spinneret flow rate, and spinneret hole diameter
zkan, U
zkan
rkmez, and O
O
460
were found to be as 2938 m/min, 49.74 g/min, and 205 mm, respectively.
The statistical model and Box Wilson steepest ascent method were used.
INTRODUCTION
A synthetic polymer needs to have fiber characteristics for its use as a textile
material, suchas high-softening and low-melting points thatallow ironing,enough
load at break, elongation at break, and reasonable boiling shrinkage. Polyethylene
terephthalate (PET) is an important synthetic fiber that is classified as a polyester.
The yarns produced from POY (partially oriented yarn), a semi-finished product of
the first production stage of polyester yarn, have a wide range of use. For the
polymer to gain these characteristics in the production stage, its degradation must
be under certain values and enough orientation has to be reached by the time it
comes to the spinning beam.
Fiber spinning is a complex manufacturing process in which the final
properties of the spun fiber depend on the polymer and the process operation. The
latter includes the details of the heat transfer, the aerodynamics, and the stress
development, all of which are ultimately related to a variety of factors that include
both the spinning speed and the polymer properties at the spinneret. The
uniformity and birefringence of the spun fiber are the process variables that are
probably of the greatest interest; both are directly related to product quality and
generally correlate with final product properties such as elongation.[1]
Small changes in polymer properties or in operating variables are
sometimes known to cause large changes in fiber properties, thus an
understanding of the interrelationships is essential. This understanding is
becoming increasingly important as fiber properties move to polymer
modifications and to new process conditions that may provide increased
productivity or improved properties at the expense of process sensitivity.[2]
By considering these effects on the POY productivity and quality, we aimed
to find the optimum values of important parameters for 100 denier and 96
filaments in a commercial POY spinning plant with a capacity of 70 ton/day.
To determine the optimal operating conditions, we used a statistical
model. The experimental data used in the preparation of this model were
obtained according to the use of a two-level, factorial experimental design.
This is called a statistical experimental design technique that has been used
over a wide range of industrial process, such as ternary composites based
461
462
zkan, U
zkan
rkmez, and O
O
Figure 1. The yarn production system, which is similar in the direct spinning system
and the yarn production system with extruder.
463
Table 1.
Maximum (+1)
Minimum (-1)
Spinneret hole
diameter U1 (mm)
Spinneret flow
rate U3(g/min)
Winding speed
U2 (m/min)
250
170
52
47
3100
2850
X0
X1
X2
X3
X1X2
X1X3
X2X3
X1X2X3
Y
1
2
3
4
5
6
7
8
1
1
1
1
1
1
1
1
1
1
1
1
21
21
21
21
1
1
21
21
1
1
21
21
1
21
1
21
1
21
1
21
1
1
21
21
21
21
1
1
1
21
1
21
21
1
21
1
1
21
21
1
1
21
21
1
1
21
21
1
21
1
1
21
136.6
146.2
133.8
144.3
137.8
153.8
135.1
149.1
Experiment
number
zkan, U
zkan
rkmez, and O
O
2003 Marcel Dekker, Inc. All rights reserved. This material may not be used or reproduced in any form without the express written permission of Marcel Dekker, Inc.
464
465
Xi
U i 2 U iav
DU i
i 1; 2; . . .. . .. . .; n
U iav
U max:
U min:
i
i
2
i 1; 2; . . .. . .. . .; n
DU i
U max:
2 U min:
i
i
2
i 1; 2; . . .. . .. . .; n
B X T * X21 X T * Y
The design matrix has orthogonal properties, the coefficient matrix (X*X)
becomes diagonal, and its diagonal elements are equal to the number of
experiments, N. For this reason, X* X21 N1 and the values of the constants
in the regression equation were calculated by the following equation:
N
X
bi
N
X
Xij Y i
j1
N
X
X2ij
Xij Y i
j1
; i 0; 1; . . .N
j1
In this work, the model coefficients, b0 b7, by using experimental data, were
calculated using MATLAB code. And then, Students t and Fishers F tests
were applied using the following equations. The error mean square was
zkan, U
zkan
rkmez, and O
O
466
S2e
y0i 2 y 0
i1
n0 2 1
ti
10
11
Fishers F test was applied to see the fitness of the new estimated regression
equation, which was obtained by the removal of the insignificant coefficient
from the experimental data. According to this, the F value was determined by
using the following equation:
F
Sr 2
Se 2
12
In this equation, Sr2 is the residual mean square, and it was determined as
N
X
S2r
yi 2 y^ i 2
i1
13
N2l
RESULTS
By applying the design matrix given in Table 2, the productivity values
were used to evaluate the values of the constants in a linear regression model
as illustrated previously. The identified statistical model is given by Eq. (14)
Table 3.
MATLAB m files.
467
zkan, U
zkan
rkmez, and O
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468
below:
Y 141:7125 2 1:4875X1 1:1375X2 2 5:8875X3
0:0375X1 X2 0:8625X1 X3 0:2375X2 X3
14
2 0:0125X1 X2 X3
0:8625X1 X3 0:2375X2 X3
Uncoded : E 487:65 2 0:5487* U1 2 1:82* U2 2 0:121* U3
16
0:00017* U1 U3 0:000768* U2 U3
This equation was validated against new data, which is given in Table 4, and it
was seen that the model was suitable for this process.
After the identification of the statistical model for the process, Box
Wilsons steepest ascent optimization method was applied theoretically on the
Table 4.
Elongation at
break E (%)
(theoretical)
141.8
New data.
Elongation at
break E (%)
(experimental)
Spinneret hole
diameter: U1
(mm)
Winding
speed U3
(m/min)
Spinneret
flow rate U2
(g/min)
142.3
170
3000
49
469
basis of the statistical model using the model constant by applying 2 0.50
change to the growth medium spinneret hole diameter and 145% for
elongation at break, the optimum values of yarn winding speed, spinneret flow
rate, and spinneret hole diameter were then found as 2938 m/min, 49.74 g/min,
and 205 mm, respectively.
CONCLUSION
In the present study, an orthogonal, two-level, factorial experimental
design technique was found suitable for the first-order regression equation.
Model constants were calculated using MATLAB coded and Students t and
Fishers F test were applied to see whether the identified statistical equation fit
the experimental data. Then, with the help of the identified model coefficient
for 145% elongation at break, the optimal operating parameters of the process
were determined by the Box Wilson steepest ascent optimization technique
as follows: spinneret flow rate 49.74 g/min, spinneret hole diameter 205 mm,
yarn winding speed 2938 m/min.
NOMENCLATURE
bi
D
E
l
Q
S
Sbi
Sr 2
Se 2
Ui
Uiav
Ui*
DUi
Xi
Xi*
X1
X2
X3
Yi
zkan, U
zkan
rkmez, and O
O
470
v 1, v 2
Y
Degrees of freedom
Estimated value of the elongation at break
ACKNOWLEDGMENT
.B.A.P. 2002 07 45
Ankara University Research fund through project A.U
009 is gratefully acknowledged.
REFERENCES
1.
2.
3.
4.
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6.
Denn, M.M. Spinning: where are we and where are we going? Fiber Prod.
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Davis, G.W.; Everage, A.E.; Talbot, J.R. Polyester fibers: high speed melt
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Lopez-Manchado, M.A.; Arroyo, M. Effect of the incorporation of pet
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