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novAA 350

Operator:

Page 1/4

22/04/2016 14:59
Laboratory:
De Benikhalled

Mm Farida Karoui

Method Parameters Technique: Flame


Name:
Created:
Comment:

fe04016
22/04/2016 14:18

Version:
Operator:

1
Mm Farida Karoui

Lines
Line

Elem. Wavel.
[nm]
Fe
248.3

Fe248

Optic. mode Lamp

Current
[mA]
4

Single-beam HCL

Boost
[mA]
-

Slit [nm]
0.2

Meas time. PMT [V]


[s]
3.0
300

Evaluation/Background correction
Line
Fe248

Background corr.
D2 background

Int.mode AZDK
Mean
off

Smooth
strong

D2 cur. [mA] HC/BC rat.


-

Flame Parameters
Type:
Burner type:
Line

C2H2/air
50 mm
C2H2/air
[L/h]
65

Fe248

Ox. control:
Burner angle:

off
0 deg

Nebulizer rate:

0 mL/min

Burner height
[mm]
6

Sample Transport
Autosampler:
Dilution if conc.
exceeded:
Injection switch:
Wash:

Yes
none

Delay time:

5s

No
after sample

Wash time:

5s

std. cal.

Std. prep.:

manual

Mixing cup cycles: 1

Calibration
Method:

Calibration Curve Parameters


Line
Calib.func.. Intercept
Fe248
linear
calculate
Calibration table

Weighting
none

No.

Type

Pos

Rec

1
2
3
4

Cal-Zero1
Cal-Std1
Cal-Std2
Cal-Std3

1
2
3
4

Check
none

Unit
mg/L

Fe
[mg/L]
0
2
3
4

Statistics Parameters
Statistics:
Repl./sample:
Pre-runs:
ASpect LS 1.5.0.0

Mean stat.
3
0

CI calc.:
absolute
Repl./calib.sample:
3
Grubbs test:
off

conf. level:
Repl./QC:

95.4%
3

Analytik Jena

novAA 350
Operator:

Page 2/4

22/04/2016 14:59
Mm Farida Karoui

Laboratory:
De Benikhalled

QCS Parameters
No entries exist

QCC Parameters
RSD/RR% check:

ASpect LS 1.5.0.0

Calib. check:

Recal. check:

Analytik Jena

novAA 350
Operator:

Page 3/4

22/04/2016 14:59
Laboratory:
De Benikhalled

Mm Farida Karoui

Results
Results file:
Instrument:
Comment:
Line
Load method

C:\Use...\Results-16-04-22 1426.tps
novAA 350 #
Technique:
Mean
fe04016 (1)

SD

Flame

RSD[%]

Flame on

CI

Unit
Date:

Rem.
22/04/2016 14:26

Date:

22/04/2016 14:26

Autozero

fe04016(1)

SIM

Date:

22/04/2016 14:27

Fe248
Cal-Zero1

fe04016(1)

SIM

Date:

22/04/2016 14:27

Fe248
Conc.1
Abs.

0
0.00011

mg/L
0.00010

89.4

Single values (Abs.): #1: 0.00001 #2: 0.00012 #3: 0.00021 (SEV: 300V)
BG (Abs.): #1: -0.00007 #2: 0.00010 #3: -0.00013
Cal-Zero1 Fe248
0.004
Abs.

0.003
0.002
0.001
0.000
0

Time [s]

Cal-Std1

fe04016(1)

Fe248
Conc.1
Abs.

2
0.47514

SIM

Date:

22/04/2016 14:27

mg/L
0.00039

0.1

Single values (Abs.): #1: 0.47551 #2: 0.47475 #3: 0.47517 (SEV: 300V)
BG (Abs.): #1: 0.00010 #2: 0.00016 #3: -0.00010
Cal-Std1 Fe248
0.5

Abs.

0.4
0.3
0.2
0.1
0.0
0

Time [s]

Cal-Std2

fe04016(1)

Fe248
Conc.1
Abs.

3
0.71241

SIM

Date:

22/04/2016 14:27

mg/L
0.00047

0.1

Single values (Abs.): #1: 0.71278 #2: 0.71256 #3: 0.71189 (SEV: 300V)
BG (Abs.): #1: -0.00011 #2: -0.00003 #3: 0.00005
0.8

Cal-Std2 Fe248

Abs.

0.6
0.4
0.2
0.0
0

Time [s]

ASpect LS 1.5.0.0

Analytik Jena

novAA 350

Page 4/4

22/04/2016 14:59

Operator:

Laboratory:
De Benikhalled

Mm Farida Karoui

Line
Cal-Std3

Mean
fe04016(1)

Fe248
Conc.1
Abs.

4
0.95036

SD

RSD[%]
SIM

CI

Unit
Date:

Rem.
22/04/2016 14:28

mg/L
0.00022

0.0

Single values (Abs.): #1: 0.95014 #2: 0.95036 #3: 0.95057 (SEV: 300V)
BG (Abs.): #1: -0.00006 #2: 0.00008 #3: 0.00004
Cal-Std3 Fe248
1.00

Abs.

0.75
0.50
0.25
0.00
0

Time [s]

Compute calib.

Fe248

Date:

22/04/2016 14:28

Date:

22/04/2016 14:28

Fe248
R(adj.): 0.999999442 Slope: 0.23753 Abs./mg/L Char.conc.: 0.01836 mg/L/1%A
Method SD: 0.00090 y=a+bx
a=0.0000623 b=0.2375303
mg/L
Fe248
1.00

Abs.

0.75

0.50

0.25

0.00

Z
0

Sample

2
Conc. [mg/L]

fe04016(1)

Pre-DF: 1
Fe248
Conc.1
Conc.2
Abs.

SIM

Wt.[g]:
2.946
2.946
0.69990

Vol.[mL]: 100
0.0026
0.0026
0.00062

AS-DF: 1.0

0.1
0.1
0.1

0.0028

Blank corr.:

off

mg/L
mg/L

Single values (Abs.): #1: 0.70049 #2: 0.69997 #3: 0.69925 (SEV: 300V)
BG (Abs.): #1: 0.00025 #2: 0.00009 #3: 0.00004
0.8

Sample Fe248

Abs.

0.6
0.4
0.2
0.0
0

Time [s]

Flame off

Date:

22/04/2016 14:28

Lamp off

Date:

22/04/2016 14:28

Cleaning

Date:

22/04/2016 14:28

Clean system

Date:

22/04/2016 14:28

Clean system

Date:

22/04/2016 14:28

ASpect LS 1.5.0.0

Analytik Jena

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