Professional Documents
Culture Documents
THE SUPERIOR
TECHNICAL GUIDE
*These services have been developed with you in mind. If you have any issues or comments arising from them,
please contact us in the first instance.
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03 Research, Development
and Partnership
Consultation
Seal Integrity
Testing
Seal Performance
Optimising
Tooling
Staying Ahead
22 Quality
Standards Compliance
04 Specifying Compounds
Important Environmental Parameters
Temperature
Approvals
Media Compatibility Rating
Elastomer Properties
Certification
Hardness
Environmental Compliance
Compression Set
Ageing
Low Temperature Flexibility
Fitting Aids
Tensile Strength
Elongation
Cleanliness/Cleaning Materials
Tear Strength
Gas Permeability
Light
Abrasion
Humidity
Colour
Contaminants
Media Table
Producing an Order Specification
13 Seal Design
Introduction
Precision O rings
Sealing Types
Groove Layouts
Static Sealing Axial and Triangular
Static Axial Face Housing
Static Triangular Housing
Static/Dynamic Sealing Radial
O ring Stretch in Piston Sealing
Reduction of Cross-Section due to Stretch
Gough-Joule Effect
O ring Size & Compound Selection Program
Pressure
Stress
Temperature
Oxygen and Ozone
Shelf Life
28 Going Forward
TESTING
We control all aspects of seal test and development programs closely with our customers.
All testing procedures are carried out under ISO 9001 accreditation.
We offer a diverse range of compounds, to satisfy the vast majority of market needs.
If a customer has specific working parameters that cannot be met within our existing elastomer
range, we will develop new compound grades at our in-house laboratory even for unique needs.
We are able to conduct extensive test programs to fully validate specific elastomers to customer
parameters (eg, temperature/media exposure and mechanical property testing).
Also we will validate to specific accreditation standards (eg, EN681, WRAS, DVGW, ACS, KIWA,
NSF, EN 549).
OPTIMISING
and application.
Seal Engineering
State-of-the-Art Manufacturing
Through the customer partnership exchange, we can assist with optimised seal profile design
TOOLING
Our Tooling Manufacture Department designs and machines precision prototype and production
moulds to exceed conventional tolerancing. Pilot tooling can be provided economically and rapidly
to further expedite customer test programs.
With our extensive tooling expertise, we can optimise critical surface features to facilitate reliable
function with mating parts.
STAYING AHEAD
Our continuous capital investment program allows us to remain at the leading edge of our field.
We continually implement latest technology systems, ensuring batch-to-batch consistency
throughout the manufacturing process.
With such broad customer support facilities, Superior will always strive to provide added value
with our customer programs.
Indeed, we find that each new project challenges our thinking and creates a springboard to
increasingly enlightened manufacturing practices.
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SPECIFYING COMPOUNDS
IMPORTANT ENVIRONMENTAL PARAMETERS
TEMPERATURE
All dynamic and shock loads should be avoided at temperatures below the minus limit of a
given compound.
However, elastomers stored in static conditions, below the low temperature flexible range,
At elevated temperatures, consideration must be given to the long term running limit and the
short term peak limit of each elastomer.
Elastomers exposed to the extreme limit can suffer an accelerated loss of flexibility, resulting in
excessive compression set. This can dramatically shorten effective sealing life. Also there is an
influence in volume swell and age hardening at high temperatures, dependant on compound type.
SPECIFYING COMPOUNDS
APPROVALS
The degree of change depends upon media composition in combination with the elastomer exposed.
Aggressive media become more active with subsequent increase in temperature. Physical changes
become apparent in two ways and can occur simultaneously;
Pharmaceutical:
USP Class XI
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Material
Nitrile
Butyl
Epichlorohydrin
Polyacrylate
Designation
NBR
IIR
ECO
ACM
BB
ECO
PA
40 90
40 80
50 80
50 80
Colours
Limited Range
Black
Limited Range
Limited Range
120
130
135
150
Heat Resistance C
Peak
Normal
100
110
120
135
Low Temp C
-30
-50 low temp version
-50
-20
-20
Oxidisation
Ozone
Weathering
Radiation
Tear Strength
Compression Set
Abrasion Resistance
Resilience
Gas Permeability
Resistances
Integrity
Electrical Insulation
Inflammability
Rating
Very Good
Good
Fair
Unsuitable
SPECIFYING COMPOUNDS
Ethylene Propylene
Hydrogenated Nitrile
Ethylene Acrylate
Fluorosilicone
Silicone
Fluorocarbon
EPDM
HNBR
AEM
MFQ
MVQ
FPM
EP
TH
VA
FSIL
SIL
VF, VP
40 90
50 90
50 80
40 80
30 80
55 85
Limited Range
Limited Range
Limited Range
Limited Range
Full Range
Limited Range
160
170
175
230
230
250
140
150
150
200
200
200
-50
-40
-40
-55
-60
-20
-35 low temp version
Grade Dependant
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ELASTOMER PROPERTIES
COMPRESSION SET
This is the measurement of a compounds loss of elastic memory. A standard cylindrical test piece of
rubber is subjected to a deformed pre-load at given temperature/time parameters (eg, 24hrs/100C).
The test deformation is usually 25% of the original height.
The measured recovery of the cross-section is carried out at ambient temperature. The end result is
recorded as the height not recovered, expressed as a percentage of the amount by which the part
was compressed.
Usually it can be stated that the better the elastomeric memory, the lower is the compression set. This
is regarded as an important feature of any compound, as leakage will occur if high set (and therefore
loss of memory) occurs.
% Compression Set =
x 100
SPECIFYING COMPOUNDS
AGEING
TENSILE STRENGTH
This is the force necessary to rupture a standard test piece at a given rate of elongation and expressed
In practical terms this property result does not assist the end user to select a compound, because
a correctly assembled O ring does not rely on its tensile strength to achieve effective sealing.
original properties.
Air and relevant fluid ageing over standard
ELONGATION AT BREAK
Elongation at break is measured at the moment of rupture of a test piece under tensile load
expressed as a percentage.
NBR
TEAR STRENGTH
FPM
Resistance to tear propagation from a point of initial damage, sustained for example during assembly.
MVQ
GAS PERMEABILITY
If elastomers are pushed beyond their ageing
resistance parameters, they will suffer from
Elastomers allow gas to enter into the structure. They will diffuse or permeate through and escape via
To reduce permeability:
The rate of permeation is governed by temperature, pressure, gas type and elastomer type. This may be
ABRASION
Abrasion resistance is a general term indicating wear resistance.
NBR, EPDM and CR have relatively good abrasion resistance. FPM has a lower abrasion resistance.
Abrasion resistance improves with hardness (up to 80 IRHD). However, Silicone and Fluorosilicone
have poor properties and should only be applied to static environments.
COLOUR
Rubbers are usually formulated with the addition of carbon black fillers. Hence, the majority of
compounds are black in colour. Rubbers gain much of their strength and heat resistance from the
However, at Superior we have the expertise to formulate and produce colour pigmented compounds
for most of the elastomer range.
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10
MEDIA TABLE
Recommended
Compound
Superior Designation
LN/MN
HN
ECO
PA
EP
TH
VA
FS
SIL
VF/VP
100
-45/-30
100
-20
120
-20
135
-15
150
-50
150
-40
160
-40
200
-55
200
-60
230/200
-20/-35
x
x
x
x
x
x
x
x
/
/
* /
* / x
WN70/3
EP1/1/5, WN12/7/1
EP7/3/7
VF12/99/3, EP11/7/4
x
x
x
x
/ *
/ *
/ *
/
/
/
EP10/00/2
EP10/00/2
EP10/00/2
VF3/00/10
EP10/00/2
VF3/00/10
x
x
o
o
o
/
/
/
EP7/3/7
EP7/3/7
EP7/3/7
x
x
x
x
x
x
/
/
x /
EP70, MN70
EP70, MN70
EP70, MN70
o
o
x
x
x
o
o
o
x
x
x
x / *
x/
x/x
EP7/3/7
EP7/3/7
EP7/3/7
x
x
o
o
o
o
/
/
/
/
EP7/3/7
EP7/3/7, MN70
EP7/3/7, MN70
EP7/3/7, MN70
Rating
*Conditions Apply
SPECIFYING COMPOUNDS
Superior Designation
Fluids Resistance (continued)
Gases
Butane
Carbon dioxide (dry)
Chlorine (wet)
Freon 12 (R12)
Freon 21 (R21)
Freon 22 (R22)
Freon 134a (R134a)
Natural gas
Methane
Propane
Oils and Fuels
ASTM No 1 oil
ASTM No 2 oil
ASTM No 3 oil
ASTM fuel A
ASTM fuel B
ASTM fuel C
Diesel oil
Diesel oil + RME (10%)
Mineral oil (low aromatic)
Hydraulic oils (petroleum base)
Lubricating oils
Paraffin
Petrol
Silicone oil / grease
Transformer oils
Vegetable oils
Solvents
Acetone
Benzene
Carbon tetrachloride
Dimethyl formamide
Ethyl acetate
Methyl ethyl ketone
Tetrachloroethylene
Toluene
Turpentine
Xylene
Miscellaneous
Ethylene glycol
Detergents
Dioctyl phthalate
Formaldehyde
Hydrogen peroxide (90%)
Phosphate esters
Potassium nitrate
LN/MN
HN
ECO
PA
EP
TH
VA
FS
SIL
VF/VP
Recommended
Compound
x
x
o
x
x
o
o
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
o
x
x
/
/
/
/
x/x
x/x
x/x
/
/
/
TH5/03/1, HN75
TH5/03/1
VF75B
HN75
EC0391
EP7/3/7
EP7/3/7
TH5/03/1, HN75
TH5/03/1, HN75
TH5/03/1, HN75
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
o
o
x
x
x
x
x
x
/
/
/
/
/
/
/
/
/
/
/
/
/
/
/
/
MN70
HN75
HN75
HN75
VF75B
VF75B
HN75
VF5/4/4, TH8/5/6
MN70
MN70
MN70
MN70
VF75B
EP7/3/7
MN70
FN70
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
o
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
o
o
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x/x
/
/
x /
x/x
x/x
/
/
/
/
EP7/3/7
VF75B
VF75B
EP7/3/7
EP7/3/7
EP7/3/7
VF75B
VF75B
HN75
VF75B
x
x
x
x
o
o
x
x
x
x
x
o
x
x
o
o
/
/
x / *
x/x
/
/
/
EP2/9/10
EP7/3/7
EP7/3/7
EP7/3/7
VF3/00/10
Consult
MN70
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11
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12
System Pressure
Colour/hardness requirements
Quality and Documentation requirements
Lead time plan
Size of seal (in the case of O rings, inside diameter and cross section)
SEAL DESIGN
13
SEAL DESIGN
INTRODUCTION
PRECISION O RINGS
These are the most versatile and economical form of sealing device available. O rings will conform
most readily to general design guideline recommendations, as they have the most extensive record
of service life in diverse conditions.
O rings are mainly used in static applications, sealing against liquids, gas and general environments.
Our Engineering Department is able to assist in specifying for dynamic applications, with special
SEALING TYPES
The various configurations can be defined according to the type of sealing, as described below:
Radial Compression
Axial Compression
Face sealing
Type C & D
Piston sealing
Type A
Rod sealing
Type B
A correctly designed housing with the appropriate sized seal is important. However, this function is
not solely responsible for an effective seal: the compound used influences the sealing performance.
In all applications, where possible the largest O ring cross section diameter d2 should be specified
for the application to overcome tolerances and rolling.
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14
GROOVE LAYOUTS
To identify each feature of the housing standard letter symbols can be applied in all cases.
Letter symbols:
Radial clearance
r1 Corner radius
r2 Edge radius
in circumferential length.
A maximum outside diameter interference of 3%
is considered optimum but on small diameters
this could be up to 8%.
SEAL DESIGN
15
d4 /d10
d5 /d9
d7
d8
H8
f7
H11
H11
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16
r1
t
Axial Compression or Face Seal
is difficult.
35
30
25
s
45
min.
15
h8
Installation in a
triangular groove
max.
20
10
squeeze %
0
d2 (mm)
static-axial
SEAL DESIGN
17
GOUGH-JOULE EFFECT
An O ring can be used as a rotary seal in some short running applications, however the following
points should be observed;
When using a stretched elastomer in a rotary application, it will contract because of the Gough-Joule
effect. This states that when a stretched elastomer is heated, it will try to regain a less stressful state.
Bearing this phenomenon in mind, this effect can be prevented by ensuring that the O ring
internal diameter is approximately 2-5% larger than the shaft to be sealed.
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18
Typical O ring housing data for piston and rod sealing applications
squeeze %
25
20
max.
15
10
min.
5
0
1.8
2.65
3.55
5.3
squeeze %
20
25
max.
15
10
min.
1.8
2.65
3.55
5.3
squeeze %
25
20
15
min.
10
5
0
1.8
2.65
3.55
5.3
*BS4518 Recommendations
NOTE: All dimensions in mm
SEAL DESIGN
19
PRESSURE
When exceeding the recommended gap size (in accordance with the below graph) an anti-extrusion
device is required.
Recommended extrusion gap is based upon radial clearance if eccentricity is zero, or diametral
clearance if concentricity of mating diameters cannot be assured.
It should be noted that Silicone and Fluorosilicone (due to low tensile strength) should only
Temperature
be applied in grooves with extrusion gaps at half the recommended radial clearance for other
compounds.
If a selected radial clearance will not achieve a given pressure, then the next hardness range
should be considered.
If a 90 IRHD rubber compound does not satisfy the given parameters, then a PTFE or Thermoplastic
back-up ring should be selected.
Anti extrusion rings are required when considering conditions to the right of the hardness curve.
For temperatures above 100C use the curve for the next harder rubber.
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Moulded Gaskets
the lips
Lower assembly force than the equivalent
O ring
Lower dynamic running force than the
equivalent O ring
Require less space than the equivalent
O ring
Less creep in housing
Able to cope with larger tolerances
Able to cope with eccentric conditions
Tailored profile
Able to cope with larger tolerances
Able to cope with out flatness
Plastic housings
Retention
Axial (face) sealing
Multiple sealing ports
Customer Information
Location tags
Stabilising features
Eccentric conditions
Tolerances
Special Conditions
Profile
21
SEAL INTEGRITY
We are focused on the fact that our precision O rings and
special mouldings are a crucial part of the bigger picture.
The integrity and quality of Superior products are fundamental
DESIGN
SEAL
INTEGRITY
COMPOUND
MANUFACTURING
PROCESS
Traditional Method
SEAL PERFORMANCE
Design
CHANGE
Mould Making
Sample Production
System Media
Seal Design
Hardware
Seal Compound
Service Conditions
Getting involved at the earliest possible stage of development, our engineering department aim to
Does sample
meet specifications?
become an integral part of our customers team, providing services such as;
NO
YES
Successful completion
of development
Seal Design
FEA/CAD
Housing recommendations
Problem Solving
Advice
Design
FEA Investigation
NO
That is why Superior uses mathematical models for describing complex material properties and
special measuring methods for determining compound parameters. In addition to enabling static
load tests, these tools allow temperature influences to be considered.
Material parameters can be determined by standardised tests performed on material samples and
are valid for a wide spectrum of operating and/or simulated conditions.
Mathematical modelling is based on stress versus strain data for each material. The stress strain data
is generally non linear.
To simulate elastomeric or plastic components as well as composite parts we use the non
linear finite element analysis method. In certain cases, we combine numerical tools, like the FEA
method with conventional analytical techniques.
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QUALITY
STANDARDS COMPLIANCE
and tolerances, but will still allow for the principle of a more accurate cross-section. Superior can also
supply O rings to customers specifications.
A continually updated version of the Superior Size List can be downloaded from the website
www.superiorltd.com
QUALITY
23
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CERTIFICATION
Certification can be provided with the product, but must be stated at point of order.
ENVIRONMENTAL COMPLIANCE
Superior is able to provide materials compliant to current European and worldwide legislative
requirements e.g ROHS, REACH and IMDS.
25
FITTING AIDS
Suitable assembly tools, as detailed, aid location and avoid contact with sharp edges. The aid should
be made from materials which will not damage sealing locations and surfaces (eg, plastic or brass).
For manual assembly or removal of an O ring from a groove (eg, in small runs or when servicing) a
spatula-type tool can be manufactured from a soft material such as brass. All edges should be
smooth, rounded and free from burrs.
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O rings are at risk from rolling when fitted over a diameter. This risk can be accentuated on large
inside-diameter/small section O rings. This can result in spiral failure with additional leakage risk.
To assist, we recommend that suitable initial lubrication be applied to the O ring.
27
STRESS
Always store O rings in their unstressed, free state, avoiding distortion and the risk of ozone attack.
Large rings should never be hung on pegs.
TEMPERATURE
Finished components should be stored below 30C and preferably below 25C.
Extended exposure to higher temperatures in air can accelerate ageing effects and cause distortion,
hardening, elongation loss and impairment of low temperature flexibility.
If inadvertent freezing has occurred, the apparent hardening effect can be reversed by warming to
normal ambient temperatures.
LIGHT
Ozone is present in low concentrations in the atmosphere and at much higher levels near some
electrical equipment. It will attack rubber components based upon particular elastomers when they
are stretched or distorted. This appears as cracks at right angles to the direction of distortion.
Of all common O ring elastomers, only nitrile (NBR) is significantly prone to ozone attack.
Once again, storage in the original sealed polythene bags in dark or very low-intensity artificial
light conditions offers full protection.
SHELF LIFE
HUMIDITY
It is practically impossible to define a specific maximum shelf life for finished elastomeric products.
CONTAMINANTS
Airborne contaminants deposited on the surface
of O rings prior to installation can promote
surface attack. Examples include cutting oil
mists, powders and active chemicals used in
production processes.
To achieve the best results, always rotate stock and store as recommended.
The following table of suggested shelf life is for guidance only.
3 years
7 years
Superior FN
Superior EP
Superior WN
Superior SIL
5 years
Superior LN
Superior MN
Superior HN
Superior PA
Superior TH
Superior VA
Superior VF/VB/VP
These storage times are more conservative than those proposed in BS 3574, 1989,
Controlled storage and packaging of vulcanised rubber and rubber products.
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G O I N G F O RWA R D
All technical information included in this document is provided free of charge for guideline purposes only and is based on technical data which
Superior believes to be reliable.
This information is intended for use by suitably skilled and qualified persons entirely at their own discretion and risk. As the end use of our
product is beyond our control, we make no warranties express or implied and no liability can be accepted in connection with the use of this
information, which is subject to revision without prior notice as additional knowledge and experience are gained.
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