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The following slides will give you information about analytical methods, performed routinely in the
Analytical Department at Honeywell Specialty Chemicals Seelze GmbH. First pages give an overview
about technical equipments/instruments and possibilities for analyses. Subsequently all analytical
methods for determination of substances, elements etc. are listed.
For detailed information and to discuss analytical problems, you may contact:
+49 (0)5137 999Responsibilities
Name
Phone
Fax
-302
-164
-9230
-164
-561
-164
-306
-164
Analytical Department
The Analytical Department is split into 3 groups dealing with analytical chemistry and one group
taking care of the specifications in the Laboratory Information and Management System (LIMS).
We work like a service center on analytical tasks and support all laboratories at our site Seelze.
The analytical department employs 33 chemists, engineers and well educated and trained lab
technicians.
Some statistical data for 2001:
more than 21.000 analytical orders worked on
206.000 single analyses had been performed + 25.000 measurements for calibration and
verification according to our quality control standards
the average cycle time for analysis of our electronic chemicals (from start of analysis of the
complete specification to the certificate of analysis) was 2,7 days
more than 71.000 certificates of analysis issued
Our LIMS is connected to all internal fabs, production laboratories, purchasing & sales dept., R&D
laboratories and HS&E-dept. (~ 340 user) and enables a fully automated control from A to Z
(printing working sheets, controlling deadlines, comparing results with given specifications, printing
statistical control sheets, informs customer directly).
All analytical data entered in the LIMS since 1988 are directly accessible any time (> 324,000
analytical reports, ~ 3.2 Mio. single data)
Analytical Services Page 2 of 25
Customer
Analytical request
Controlling
Working Sheets
Inspection Methods
Check Intervalls
Statistics
Specifications
Laboratories
Analysis
Results
Supervisor
AL
no
SPC Charts
Trends
others
In
Specification
?
yes
Business
Segments
Customer
Release &
Certificate
October 28, 2002
Responsibilities
Analytical Department & Quality Assurance
Analytical Department
Dr.
Dr. Jens
Jens Gaede
Gaede
Classical
Classical wet
wet
chemistry
chemistry
Product
Product care
care group
group
Organic
Organic instrumental
instrumental
analysis
analysis
Metal
Metal trace
trace analysis
analysis
Dr.
Dr. Hildenbrand
Hildenbrand
Dr.
Dr. Renschen
Renschen (01.12.02)
(01.12.02)
Dr.
Dr. Bldorn
Bldorn
UV/VIS - Spectroscopy
IR - Spectrometry
NMR - Spectroscopy
Fluorescence-Spectroscopy
Flame-AAS (FAAS)
Graphite-Furnace-AAS (GFAAS)
Cold-Vapour-AAS (CVAAS)
Hydride-AAS (HyAAS)
Optical-Emission-Spectrometry using Inductively Coupled Plasma (ICP-OES)
Mass-Spectrometry using Inductively Coupled Plasma (ICP-MS)
Gas-Chromatography (GC)
Gas-Chromatography with mass-selective detection (GC - MS)
High Performance Liquid-Chromatography (HPLC)
HPLC with mass-selective detection (HPLC-MS)
Ion-Chromatography(IC)
Gel-Permeation-Chromatography (GPC)
Voltametry
Polarimetry
Particle-Analysis
Hydride AAS
Cold Vapor AAS
particles
effective
assay
residue on ignition (SO4)
silver (Ag)
aluminium (Al)
arsenic (As)
gold (Au)
barium (Ba)
beryllium (Be)
bismuth (Bi)
calcium (Ca)
cadmium (Cd)
cobalt (Co)
chromium (Cr)
copper (Cu)
iron (Fe)
gallium (Ga)
germanium (Ge)
indium (In)
potassium (K)
lithium (Li)
> 0,5 /m
48.8-49.2 %
max. 2 ppm
max. 0.1 ppb
max. 0.1 ppb
max. 0.1 ppb
max. 0.1 ppb
max. 0.1 ppb
max. 0.1 ppb
max. 0.1 ppb
max. 0.1 ppb
max. 0.1 ppb
max. 0.1 ppb
max. 0.1 ppb
max. 0.1 ppb
max. 0.1 ppb
max. 0.1 ppb
max. 0.1 ppb
max. 0.1 ppb
max. 0.1 ppb
max. 0.1 ppb
magnesium (Mg)
manganese (Mn)
molybdenum (Mo)
sodium (Na)
nickel (Ni)
lead (Pb)
platinum (Pt)
antimony (Sb)
tin (Sn)
strontium (Sr)
titanium (Ti)
thallium (Tl)
vanadium (V)
zinc (Zn)
zirconium (Zr)
chloride (Cl)
nitrate (NO3)
phosphate (PO4)
sulphate (SO4)
sulfite (SO3)