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Article history:
Received 7 June 2011
Accepted 1 February 2012
Available online 10 February 2012
Keywords:
tight gas sandstone reservoir
characteristics
recognition criteria
diagenesis
petrophysical properties
Chinese basins
a b s t r a c t
Tight gas sandstone (tight gas) reservoirs have been widely discovered in a number of basins in China including the Sichuan, Ordos, Turpan-Hami (Tuha), Songliao, Junggar, Tarim, Chuxiong and East China Sea basins.
Genetically they are of either primary or secondary accumulations. The tight gas accumulations are mostly
associated with coal strata. The reservoir rocks are mainly lithic arkosic sandstones and feldspathic lithic
arenite. They are characterized by low compositional maturities, low cement contents and moderate petrological textural maturities. The diagenetic evolution of the reservoirs is generally at a high level, reaching
the mid-late diagenesis stages. Reservoir porosities are dominated by secondary intragranular dissolution
porosity and intergranular dissolution porosity with subordinate primary residual intergranular porosity.
The pore throats are sheet like or bending-ake like in geometry and generally have poor connectivity. The
tight gas reservoirs have poor petrophysical properties and show strong heterogeneities. Locally, some moderately porous and low permeable or low porous and moderately permeable sandstone reservoirs are present. Compaction and cementation appear to be key factors contributing to the formation of the tight gas
sandstone reservoirs. Based on the synthesis of a vast data set obtained from some known tight sandstone
gas accumulations from (1) the upper Palaeozoic sandstones in the Ordos Basin, (2) the Triassic Xujiahe
Formation in the Sichuan Basin, (3) the Jurassic sandstones from the foothill belt in the Tuha Basin and (4)
the Cretaceous deep reservoirs in the Songliao Basin, the criteria for recognizing tight gas sandstone reservoirs in China can be established as an in situ permeability of less than or equal to 0.1 mD and with no natural
commercial production.
2012 Elsevier B.V. All rights reserved.
1. Introduction
Tight gas has now become an important component of the wide
hydrocarbon inventory as one of the major unconventional resources.
In 2009 the world annual production of tight gas amounted to 15.3
TCF and one-third of the US gas production for the year was from
tight gas (BP World Energy Statistics, 2009; IEA, 2009). At present
there are over 900 tight gas elds over 40,000 producing wells in
the US with a proven recoverable resource of 459 TCF.
In China tight gas accumulations have been discovered in a number of basins including the Ordos, Sichuan, Tuha, Songliao and Tarim
basins with a total area of 600,000 km 2 and a resource reserve of
over 777 TCF (Jiang et al., 2004; Kang and Luo, 2007; Wang, 2000;
Zou et al., 2010). However, tight gas exploration in China is still in
its infant stage and there are no established criteria for recognizing
and evaluating tight gas sandstone reservoirs. This paper intends
to provide an overview on the major characteristics of the tight gas
sandstone reservoirs in Chinese basins. We also proposed a set of
Corresponding author at: Research Institute of Petroleum Exploration and
Development, PetroChina, 20 Xueyuan Road, Haidian District, Beijing 100083, China.
Tel.: +86 10 83593456; fax: + 86 10 83593456.
E-mail address: zcn@petrochina.com.cn (C. Zou).
0920-4105/$ see front matter 2012 Elsevier B.V. All rights reserved.
doi:10.1016/j.petrol.2012.02.001
C. Zou et al. / Journal of Petroleum Science and Engineering 8889 (2012) 8291
from low permeability reservoirs with porosity b12% and permeability 1 mD. Luo (2007) suggested that tight gas should refer to
those gases that can only be produced commercially via production
intervention such as fracturing and horizontal drilling. Zou et al.
(2010) suggested that tight gas sandstone reservoirs are reservoirs
with porosity less than 10%, in situ permeability of less than 1 mD,
pore throat diameter less than 1 m and gas saturation less than
60%. They also emphasized that tight gas normally cannot be produced naturally to commercial quantity. However, in many countries
tight gas sandstone reservoirs are often dened according to the gas
ow (rates) at well site rather than through the permeability cutoff
values (Schmoker et al., 1996). It has thus been suggested that tight
gas sandstone reservoirs may be best dened from both the petrophysical and economic viewpoints (Holditch, 2006).
Tight gas possesses the following six characteristics: (1) the
source rocks often comprise normally matured coal beds or coal
seam-bearing shale; (2) the reservoirs are usually low porous and
less permeable sandstones with strong heterogeneity and relatively
high water saturation, with the low porosity and permeability being
caused by ne facies, strong compaction and carbonate and siliceous
cementation; (3) sources and reservoirs are in close proximity; (4)
the gas distribution is not entirely controlled by the trap structures
and can occur in structurally low areas; (5) have unique reservoir
migration and accumulation mechanisms complementing the conventional hydrocarbon accumulations; and (6) occur in large scale
with signicant reserves and can have a prolonged sustainable production with proper intervention although there may be low or no
natural production. A number of authors have noticed the uniqueness
of tight gas sandstone reservoirs over the past several decades and
proposed various terms to describe such reservoirs such as deep
basin gas by Masters (1979); tight gas reservoirs by Walls (1982);
basin center gas by Rose et al. (1984) and Law (2002); continuous
gas accumulation by Schmoker et al. (1996); root margin gas by
Zhang and Jin (2005) and continuous hydrocarbon accumulation by
Zou et al. (2009). In this paper the term tight gas sandstone reservoirs
or tight gas is used.
3. Characteristics of tight gas sandstone reservoirs in Chinese
basins
Natural gas occurrence in siliciclastic reservoirs can be classied as
either conventional reservoirs or tight gas sandstone reservoirs.
The two types of reservoirs differ in a number of aspects including
their depositional setting, diagenetic history, pore types, pore throat
structures and pore connectivity and accumulation (Table 1). In
China tight gas sandstone reservoirs are well developed in both the
terrestrial (continental) and marine depositional sequences. Tight
gas sandstone reservoirs can be further classied according to their
formation mechanisms such as (1) primary depositional type or (2)
structurally diagenetically modied type (Zhao et al., 2007; Zou et
al., 2010).
The tight gas sandstone reservoirs in the lacustrine basins in China
are dominated by alluvial fan, uvial and delta front facies. The cause
for the tight nature of the reservoirs is depositional related and due
primarily to the matrix-support nature of the sedimentary facies,
high mud content, poor sorting in the alluvial fan facies, and the
ne grained nature, poor sorting and high mud content in the delta
front facies.
The tight gas sandstone reservoirs of terrestrial origin in China
have generally undergone strong structural-diagenetic alteration
due to their relatively deep burial and high diagenetic evolution
stages (Ying et al., 2004). Most of the tight gas sandstone reservoirs
reached the late diagenetic stage (Lv and Liu, 2009; Zhao et al., 1999)
and are characterized by strong compaction, and the occurrence of
widespread pressure dissolution and cementation. Mechanical compaction and dissolution are widespread in all tight gas sandstone reservoirs
83
Table 1
Differences between conventional and tight gas sandstone reservoirs. Q: quartz; F: feldspar;
R: rock fragment.
Parameters
Conventional sandstone
reservoirs
Rock constituents
Diagenetic
evolution
Type of porosity
and primarily occurred during the early evolution stage. This process
reduces the intergranular porosity signicantly through graingrain or
grainline contacts and compaction. With increasing burial depth mineral dissolution commences when the vertical loading (overburden)
pressure and the lateral tectonic stress become greater than the pore
pressure. With increasing loading and compression the grain contacts
begin to transform from pointpoint contact, through pointline contact, to concaveconvex or sutured contact. Mineral dissolution during
this stage also provides the essential silica solution for cementation.
For example, in the Sichuan Basin, the tight gas sandstone in the
Upper Triassic Xuejiahe Formation is characterized by typical concaveconvex grain contacts with well developed sutures between
quartz grains and exures in some plastic minerals such as lithic fragments and plagioclase (Liu et al., 2011).
The marine tight gas sandstone reservoirs of the structuraldiagenetic origins in China are primarily distributed in the Silurian
sequences of the Tarim Basin, Sichuan Basin and the Carboniferous
Permian sequences of the Ordos Basin (Table 2). They are characterized by braided deltaic, tidal at and offshore bar sedimentary facies.
For example, in the Sichuan basin, the Silurian tight gas sandstone
reservoir is dominated by very ne lithic arenite and arkosic lithic
sandstone with quartz as the predominant lithology. The lithic fragments consist of shale, siliceous materials, schist and eruptive igneous
rock fragments. In the Tarim Basin, the lithology of the Silurian tight
gas sandstone reservoir in the Tadong area comprises very ne, ne
and medium sandstones that have been strongly compacted and
tightly cemented. Carbonate cementation is the predominant process
with some silica cementation. Quartz overgrowth is well developed.
Clay content is relatively high (Dong et al., 2007; Lv and Liu, 2009).
84
C. Zou et al. / Journal of Petroleum Science and Engineering 8889 (2012) 8291
Table 2
Major characteristics of tight gas sandstone reservoirs from main oil and gas bearing basins in China.
Basin
Ordos
Sichuan
South
Songliao
North
Songliao
Tuha
Junggar
Tarim
Stratigraphic
interval
C-P
Xujiahe Fm
Denglouku
Fm
Denglouku
Fm
Shuixigou
Fm
Badaowan Fm
S, Eastern
part
J, Foothill belt
Sedimentary
facies
Rock Type
Fluvial, BS, MS
delta, coastal
Lithic sst, lithic
Qz sst, Qz sst
Fluvial, BS,
MS delta
Ar-lithic sst,
lithic sst
BS, delta, MS
delta
Lithic arkose,
ar-lithic sst
and arkose
BS, delta
BS, delta, MS
delta
Ar-lithic sst and
lithic sst
Shoreline,
BS, delta
Mesograin,
ne grain
lithic sst
Depth (m)
Area (103 km2)
Production
(103 m3/d/well)
Diagenetic stage*
20005200
180
2681a
22003500
50
4150
22003300
30003650
15
4.597.9/39
42004800
45
48006500
240
2956.5
38004900
Pore type
Mesogenetic
A2 to B
RI, interG, intraG
DP, kaolinite
intercrystal pore
20005200
60
Minimum, 2.3
pressurized
Mesogenetic
A to B
RI pore, DP grain
DP, micropore,
microfracture
Mesogenetic
A2
RI, interG
DP,intraG
DP
Mesogenetic
A to late
Miniature
interG,
micropore,
intraG DP
Median (%)
Mean (%)
Sample nos.
Median K (mD)
Mean K (mD)
Sample nos.
6.695
6.93
6015
0.2291
0.6042
5849
4.1998
5.65
39,999
0.0567
0.351
32,351
3.1994
3.35
61
0.0342
0.224
52
5.0121
5.16
25
0.0469
0.1058
25
9.1
9.04
51
0.455
1.25
43
6.5133
6.98
1019
0.2047
3.572
988
2.78
6.49
4720
0.393
1.126
4531
740
1.5110.8
0.011.44
Ar-lithic sst
Bashijike Fm,
west Kuche
deep zone
BS,, BS, delta,
FD
limy ne lithic
sst,
anisomerous
lithic sst
55007000
Minimum66
178.3
(Dabei 1010)
Mesogenetic Mesogenetic
Mesogenetic mesogenetic A to B mesogenetic
B to late
A1A2
A to B
A to B
IntraG and
InterG, grain DP, RI, intraG DP interG, intraG DP,
RI, grain and
interG DP
matrix shrinkgrain DP, microintraG DP, maage, micropore
pore, microfracture trix micropore
3.36
0.06
Qz: quartz; sst: sandstone; ar-lithic: arcosic lithic; sandstone; BS: braided stream; MS: meandering stream; FD: fan delta; RI: residual intergranular pore; DP: dissolution pore;
interG: intergranular; intraG: intragranular.
a
After Ying et al. (2004).
In the Sichuan Basin for example, the Upper Triassic Xujiahe Formation is characterized by a low compositional maturity, low cementation and moderate textural maturity (Fig. 1a). The compositional
maturity indices are around 0.322.45 with a maximum value of up
to 6.14. The quartz content is around 2470% and occasionally up to
86%. Feldspar accounts for 0.518%, while the lithic fragments account for 1265% with a maximum of 75.5%. The lithic fragments
are dominated by igneous rock type and metamorphic quartz arenite
fragments with minor sedimentary fragments or low grade metamorphic rock fragments. The reservoirs are moderately well sorted and
are primarily grain supported, subrounded with the matrix content
being less than 2%. The total amount of authigenic cement and/or diagenetic minerals is low, less than 56%, although they may occasionally take up to 15%. The authigenic minerals include chlorite, silica,
calcite, Fe-bearing calcite,dolomite, siderite and pyrite. Among the
authigenic minerals, chlorite, silica and calcite appear to have the
most effects on the petrophysical properties of the tight gas sandstone reservoirs (Zhu et al., 2009). In the lithic rock fragments, quartz
mineral is the strongest mechanically (Pittman and Larese, 1991).
When the content of quartz falls below 35%, the mechanical strength
of the lithic fragments will be reduced sharply, resulting in poor
reservoir quality (e.g. the Xu-6 interval in the Guangan-102 well).
However, the reservoir quality does not always improve with increasing quartz content (Zhu et al., 2009). When the quartz content
exceeds 75%, the amount of silica cement is doubled, causing extensive cementation and thus reducing the porosity and permeability
(e.g. in the Xu-6 interval of the Guangan-12 well). The mechanic
strength of the feldspar is next to that of quartz. When the feldspar
content is less than 1%, the reservoir quality is poor (e.g. the Xu-6 interval of Well Guangan-102). However, dissolution pores can often be
developed in feldspar grains. There are two contrasting types of lithic
fragments, namely the rigid type and plasticity type (Pittman and
b
1
2 3
N=5643
N=6132
Fig. 1. Ternary plots showing the lithological difference of sandstones from two well known tight gas sandstone reservoirs. Classication scheme after Folk (1968). Q: quartz; F: feldspar;
R: rock fragment; K1q: Cretaceous Qingshankou Fm; K1d: Donglouku Fm; K1y: Yingcheng Fm; K1s: Shahezi Fm.(a). The Upper Triassic Xujiahe Fm in the Sichuan Basin. Data from the
Southwestern Oileld Company, PetroChina. (b) The deep tight gas sandstone reservoirs in the Songliao Basin. Data from the Daqing Oileld Company, PetroChina.
C. Zou et al. / Journal of Petroleum Science and Engineering 8889 (2012) 8291
Larese, 1991). The plastic lithic fragments such as low-grade metamorphic rocks, shale fragments and mica akes, have low mechanic
strength and may affect the reservoir quality greatly. In addition,
the amount of plastic rock fragments of a reservoir is often inversely
related to grain sizes. The ner the grainsize is, the higher the plastic
fragment content will be (e.g. the Xu-6 interval of the Guangan-101
well). The rigid lithic fragments usually comprise metamorphic
quartzose, igneous lithic fragments, silicate and sandstone, among
which the metamorphic quartzose fragment has the highest mechanic strength, while the volcanic lithic fragments have the least
strength. Silicate fragments and sandstone fragments have moderate
mechanic strengths somewhere in between.
In the deep part of the Songliao Basin, the tight gas sandstone reservoirs are characterized by arkosic lithic sandstone and lithic sandstone and arkosic arenite (Fig. 1b; Table 2). The lithic fragments are
dominated by quartz, feldspar and rock fragments with quartz accounting for 9.438.6% (average: 21.833.9%), feldspar accounting
for 15.046.1% (average: 26.738.2%) including orthoclase, microcline and plagioclase. The rock fragments, primarily of igneous rocks
including acidic eruptive rocks and andesite, account for 20.9% to
70.0% with an average content of 28.044.4%. The sizes of the rock
fragments vary from 0.01 mm to 0.25 mm. The cementation is primarily of pore lling type and secondary cementation. The pore lling
material consists primarily of clay and authigenic cements. The clay
matrix is dominated by illite, accounting for 2.329.4%. The authigenic cements consist predominantly of silica (25%), occasionally
up to 10%. The calcite cements are dominated by calcite with minor
amount of limy micrite accounting for 2.28.4% and occasionally up
to 20%. Zeolite cement accounts for 2.37.2% and is often heterogeneously distributed, forming local patches.
In the Ordos Basin, the tight gas sandstone reservoirs are mainly
distributed in the oil bearing He-8 and the Shan-1 reservoir intervals
within the Sulige giant gaseld (Table 2). The main lithology is lithic
quartz arenite. The lithology of the He-8 interval is dominated by lithic quartz arenite with quartz content of 5283%, rock fragment content of 1748% and feldspar content of b1%. The reservoir grains are
moderately well sorted, subrounded to rounded. The grain contact
is primarily of pointpoint contact or pointline contact. The cementation is dominated by pore lling type. The cement consists of clay
with volcanic ashes (412%) with minor calcite (125%) including
Fe-bearing calcite, often in residual forms. Quartz overgrowth is
well developed. The total cement amounts for 528%, while the
poresurface ratio averages around 310%. The Shan-1 interval is
dominated by lithic quartzose arenite with subordinate lithic sandstone. The quartz content is 5987%, while the lithic fragments
account for 1742%. The feldspar content is similar to that of the
He-8 interval, but the sorting is much better. Grain contacts are typical of concaveconvex styles, suggesting a much stronger diagenesis
compared with He-8. The clay content is 48% and the amount of
the calcite is 12%, less than that of He-8 interval. The total cement
accounts for 711%.
In the deep part of the Kuche Depression, northern Tarim Basin, the
Cretaceous tight gas sandstone reservoirs consist of limy ne grained
lithic sandstone, variable grainsized lithic sandstone (Table 2).
Quartz accounts for 4184% (average: 72.2%), feldspar accounts for
1017% (average: 9.6%) and the lithic rock fragments account for
2842% (average: 28.4%). The pore lling materials are dominated
by clay and calcite cement and zeolite, totally accounting for 14
57% (average: 23.2%). Among the pore lling minerals calcite and
zeolite account for 512% (average: 8.5%) and 28% (average: 3%),
respectively. Locally porosities are well developed, consisting of
intergranular pores, intergranular dissolution pores with pore sizes
being mainly around 0.010.1 mm in dimensions (Table 2). The
Palaeogene tight gas sandstone reservoirs consist of limy, limy ne
lithic and medium lithic sandstone or arkosic lithic arenite with
quartz content of 5664%, feldspar of 1118% and lithic fragments
85
of 2129%. The cement, totaling 6.3%, is dominated by clay and calcite with minor quartz overgrowth. The cement calcite accounts for
1028% (average: 20.7%) of the total cement.
86
C. Zou et al. / Journal of Petroleum Science and Engineering 8889 (2012) 8291
b
43839
N=52495
d
N=10643
10643
f
N=1680
1680
Fig. 2. Porosity and permeability ranges of the tight gas sandstone reservoirs in China.(a) and (b) for all tight gas sandstone reservoirs studied in China. (c) and (d) for the upper
Triassic tight gas sandstone reservoirs from the Xujiahe Fm in the Sichuan Basin. (e) and (f) for the upper Palaeozoic tight gas sandstone reservoirs in the Ordos Basin.
Table 3
Classication of pore structures of the tight gas sandstone reservoirs in the deep part of
the Songliao Basin based on MICP data.
Pore structure type
Type I
Type II
Type III
Type IV
Porosity (%)
Permeability (mD)
Maximum pore throat radius (m)
Displacement pressure (MPa)
Maximum mercurial saturation (%)
8.0
1.0
>2.0
b 2.5
>60
8.05.5
1.00.06
2.50.4
2.03.5
8050
5.54.0
0.20.05
0.50.1
3.010.0
7040
4.0
b0.08
b0.10
> 10.0
b 60
C. Zou et al. / Journal of Petroleum Science and Engineering 8889 (2012) 8291
87
c
N=330
N=336
Fig. 3. Characteristics of the pore throat structures of the Xujiahe Fm reservoirs in the Sichuan Basin. a) Pore throat size distribution. b) Correlation between the diameters of pore
throats and permeability. c) Correlation between the diameters of pore throats and porosity.
with an average sorting of 2.73 (sorting coefcient is inversely proportional to and sorting quality). The median displacement pressure
and median saturation pressure are high around 1.20 MPa and
13.2 MPa, respectively, suggesting that oil or gas cannot enter into
the reservoirs easily. For samples with porosity ranges b10% and K
ranges b1 mD, there appears to be a relatively poor correlation between the pore throat diameter, porosity and permeability (Fig. 3b,
c). In general, the Xujiahe Formation in Sichuan Basin is characterized
by narrow and less effective pore throats and a poor pore throat
distribution.
On the basis of the pore structures of the tight gas sandstone reservoirs from the Songliao Basin we have grouped the MICP curves
into four categories: (1) good pore structure; (2) moderately good
pore structure; (3) poor pore structure; and (3) very poor pore structure (Table 3).
4.2. Pore characterization using SEM and BSE imaging
Scanning electron microscope (SEM) with backscattered electron
(BSE) beam has recently been increasingly applied to characterize
micro pore structures in tight gas sandstone. The method enables
the direct observation of the spatial distribution of various micro
pores and their geometries in the rock matrix. The method is able to
detect micro pores in the matrix, within clay minerals and other diagenetic minerals lling micro pores such as dissolution pores in feldspars or lithic fragments and calcite cements. The combined SEM and
BSE capability allows the observation with continuous zooming from
a few tens of magnication to up to a few tens of thousands of magnication. In our work ow, we rstly used the SEM/BSE to acquire
images at magnication of 200010,000. The images were then processed to obtainn the various parameters relating to the micropores
including the porematrix surface ratio, pore diameters, pore throat
sizes, the perimeter of the pores, specic surface area, uniformity coefcient, pore size distribution parameters (Table 4).
The electron microscope used in the investigation is the LEO435VP model with the following operational settings: 20 kV, 100 Pa.
Thirty-nine samples from the Upper Triassic Xujiahe Formation,
Sichuan Basin were analyzed for their micro pore structures using
SEM/BSE image analysis (Table 4; Fig. 4).
The results indicate that the samples are primarily characterized
by micro pores and pore throats (Fig. 4a, b), and the porosity can be
somehow correlated with the average pore size but does not seem
to correlate with the average pore throat size (Fig. 4c, d, e).
4.3. Micro and nano pore characterization using FE-SEM imaging
Field emission SEM (FE-SEM) has the advantage of having extremely high magnication and detection resolution. With the advanced image processing software FE-SEM is able to detect and
characterize nano pores. The technique has recently been widely
used in the pore structure characterization of shale gas reservoirs
(Golab et al., 2010; Zhu et al., 2009). In this investigation FE-SEM
was used to detect and characterize the micro and nano pores developed in the reservoir grains, in the intergrain minerals, pore lling
matrix due to diagenesis or dissolution, which are key storage space
for the tight gas reservoirs (Fig. 5). A variety of sub micro pore
types were observed including (1) Intercrystalline cracks in clay mineral; (2) micro pores and dissolution micro pores in the clay minerals;
(3) micro cracks between chlorite and (4) micropores in mineral
grains.
5. Criteria for recognizing tight gas sandstone reservoirs in China
The criteria for recognizing and evaluating tight gas sandstone reservoirs vary greatly among countries and regions as the amount of
resources and the advancement of technology to produce the tight
gas are different. At present there are yet any agreed criteria for categorizing tight gas sandstone reservoirs. In 1980 in referencing the
NGPA (1978), the US Federal Energy Resource Commission (FERC)
dened that the registration for tight gas reservoirs should be that
the reservoir permeability is less than 0.1 mD for taxation purposes.
Elkins (1981) proposed a threshold value of an in situ permeability
of 0.1 mD to differentiate conventional from the unconventional sandstone reservoirs. Spencer (1989) dened that tight gas should be gasbearing reservoirs with less than 0.1 mD permeability. Surdam et
al. (1997) proposed that the tight gas should refer to the unconventional gases produced from low permeability reservoirs with porosity of b12% and permeability of b1 mD. Nelson (2009) dened the
pore throat diameter for the tight gas sandstone around 20.03 m.
Some authors further divided tight gas sandstone reservoirs into
tight, very tight and ultra tight categories (Table 5). There are
no agreed criteria in China for recognizing tight gas sandstone
88
C. Zou et al. / Journal of Petroleum Science and Engineering 8889 (2012) 8291
Table 4
Summary of the pore structure data and parameters derived from SEM/BSD analysis for the Upper Triassic Xuejiahe Formation, Sichuan Basin.
Well
Strata Depth
(m)
Ying 21
Xu 2
Ying 21
Xu 2
Ying 21
Xu 2
Ying 21
Xu 2
Ying 21
Xu 2
Ying 21
Xu 2
Ying 21
Xu 4
Ying 21
Xu 4
Ying 21
Xu 4
Ying 21
Xu 4
Zhe 2
Xu 2
Zhe 2
Xu 2
Zhe 2
Xu 2
Zhe 2
Xu 2
Zhe 2
Xu 2
Zhe 2
Xu 2
Zhe 2
Xu 2
Long 9
Xu 2
Long 9
Xu 2
Long 9
Xu 2
Long 9
Xu 2
Long 9
Xu 2
Long 9
Xu 4
Yue 2
Xu 4
Yue 2
Xu 4
Yue 2
Xu 4
Yue 2
Xu 4
Yue 2
Xu 4
Yue 2
Xu 4
Yue 2
Xu 4
Yue 2
Xu 2
Yue 2
Xu 2
Yue 2
Xu 2
Yue 2
Xu 2
QiongXi Xu 2
1
QiongXi Xu 2
1
Reservoir
lithology
(%)
Planar
(%)
Max
Ap
(m)
Min
Ap
(m)
mean
Ap
(m)
Max
neck D
(m)
Min
neck D
(m)
Mean
neck D
(m)
P
throat
ratio
Uniform Shape
Grade
coeff
constant factor
Bias
angle
Sharpness
6.33 0.64
58.83
3.42
17.33
10.93
1.52
2.26
7.66
0.30
2.29
1.34
0.24 0.81
7.54 1.74
137.05
5.13
48.51
23.18
2.27
6.63
7.32
0.35
2.00
1.12
0.16 1.14
7.48 2.99
217.60
5.13
55.41
28.75
2.27
6.18
8.97
0.25
1.86
1.32
0.07 1.05
11.63 7.77
180.76
5.13
65.98
27.65
2.27
8.29
7.96
0.37
1.92
0.86
0.21 1.15
7.35 3.19
114.57
5.13
36.08
27.27
2.27
5.94
6.07
0.31
1.81
1.08
0.11 0.62
13.88 8.55
212.34
5.13
71.52
29.11
2.27
7.13
10.02
0.34
1.97
0.99
0.14 1.12
5.82 2.73
128.63
5.13
42.90
22.73
2.27
6.17
6.95
0.33
1.84
1.23
0.28 0.92
4.25 2.97
142.97
5.13
52.22
28.75
2.27
6.95
7.52
0.37
2.00
0.98
0.13 1.16
4.31 1.92
180.61
5.13
45.68
26.50
2.27
6.11
7.47
0.25
1.98
1.11
0.05 1.42
7.98 1.57
152.93
5.13
46.93
28.75
2.27
7.57
6.20
0.31
2.13
1.07
0.09 1.28
3.83 2.44
95.48
3.13
35.25
21.15
1.39
5.33
6.62
0.37
1.98
1.32
0.24 0.87
0.93 1.61
52.81
2.56
21.88
20.33
1.14
6.54
3.35
0.41
1.45
0.65
0.01 1.19
6.86 1.01
55.92
4.34
23.82
25.80
1.92
4.03
5.92
0.43
2.20
0.98
0.46 0.88
9.81 3.74
118.41
5.13
47.41
29.11
2.27
9.74
4.87
0.40
1.73
0.91
0.21 0.93
11.33 4.39
173.89
4.70
57.42
29.46
2.08
7.27
7.89
0.33
1.76
1.01
0.15 1.34
9.65 3.21
128.77
4.51
43.35
25.61
2.00
5.39
8.05
0.34
1.87
1.11
0.26 0.97
1.03 0.34
53.21
4.51
21.26
2.00
2.00
2.00
10.63
0.40
1.52
1.07
0.15 1.22
2.06 1.23
150.83
5.37
63.48
25.64
2.38
6.73
9.43
0.42
1.95
1.05
0.26 1.20
0.96 1.88
75.34
2.56
15.57
11.36
1.14
3.58
4.35
0.21
1.49
1.17
0.34 1.84
1.63 0.31
46.99
2.45
22.35
6.52
6.52
6.52
3.43
0.48
1.35
1.07
0.24 2.04
6.54 1.49
88.21
2.69
36.75
12.82
1.19
4.72
7.79
0.42
1.52
1.15
0.03 1.92
6.40 2.64
156.75
5.37
33.36
28.57
2.38
4.73
7.05
0.21
1.82
1.24
0.10 1.06
1.93 0.57
72.35
5.13
11.86
4.55
2.27
2.39
4.96
0.16
1.97
1.55
0.16 0.70
3.30 0.59
99.45
5.13
38.39
14.37
2.27
7.34
5.23
0.39
1.79
0.34
1.14 0.22
5.91 2.46
143.61
5.13
56.52
28.75
2.27
7.42
7.62
0.39
2.08
1.21
0.28 1.03
4.86 2.06
196.84
6.27
58.36
27.78
2.78
8.72
6.69
0.30
1.88
1.36
0.22 1.19
6.16 1.98
127.81
5.13
50.53
29.11
2.27
9.46
5.34
0.40
1.92
1.05
0.21 1.36
5.64 1.21
125.42
5.13
46.52
14.37
2.27
3.81
12.20
0.37
2.05
1.14
0.07 1.07
5.20 1.58
125.00
5.13
24.89
29.11
2.27
4.31
5.77
0.20
1.80
1.26
0.02 1.15
4.80 0.82
77.14
3.42
19.38
25.71
1.52
7.38
2.63
0.25
1.79
1.36
0.27 0.91
8.72 5.73
210.89
5.94
73.93
26.84
2.63
6.32
11.69
0.35
2.14
1.13
0.19 1.04
7.72 5.27
200.27
5.64
61.87
29.15
2.50
6.72
9.21
0.31
2.12
1.12
0.19 1.17
8.39 5.37
148.92
5.13
53.85
27.65
2.27
6.62
8.13
0.36
2.10
1.15
0.30 1.10
8.04 6.27
147.35
5.37
45.52
28.57
2.38
5.96
7.64
0.31
2.15
1.11
0.22 1.17
0.77 0.60
72.90
5.13
16.37
9.09
2.27
4.82
3.39
0.22
1.73
1.19
0.14 0.96
3.11 0.90
82.86
5.13
28.23
9.09
2.27
5.30
5.32
0.34
1.62
1.00
0.04 1.11
C. Zou et al. / Journal of Petroleum Science and Engineering 8889 (2012) 8291
89
Table 4 (continued)
Well
Strata Depth
(m)
QiongXi Xu 2
1
QiongXi Xu 2
1
QiongXi Xu 2
1
Reservoir
lithology
4230.2 m felsic
arenite
4267.0 m felsic
arenite
4287.4 m felsic
arenite
(%)
Planar
(%)
Max
Ap
(m)
Min
Ap
(m)
mean
Ap
(m)
Max
neck D
(m)
Min
neck D
(m)
Mean
neck D
(m)
P
throat
ratio
Uniform Shape
Grade
coeff
constant factor
Bias
angle
Sharpness
4.41 1.90
45.15
2.56
16.71
8.19
1.14
2.64
6.32
0.37
2.04
1.06
0.29 1.12
3.05 0.94
38.24
2.56
10.19
7.19
1.14
4.16
2.45
0.27
1.65
1.13
0.16 1.04
2.02 0.46
30.99
2.56
8.85
2.27
2.27
2.27
3.89
0.29
1.71
1.15
0.11 0.89
f: ne; m: medium, c: coarse; D: diameter; felsic: feldsparthic; sst: sandstone; Ap: aperture; Uniform coeff: uniformity coefcient.
reservoirs. In the Chinese National Standards for resource exploration such as the Evaluation Methods for Natural Gas reservoirs
(SY/T 560193), the Evaluation Methods for Hydrocarbon Reservoirs (SY/T 62851997) and the Manual for Estimating Hydrocarbon Reserves (DZ/T 02172005), it has been proposed that air
permeability of 101 mD is referred as low permeable reservoirs
and air permeability of less than 1 mD as ultra low permeable reservoirs. In the Natural Gas Classication Manual (SY/T 61681995)
moderately and low porous and permeable reservoirs are dened as
with porosities of 15%10% and effective permeability of 100.1 mD or
absolute permeability of 201 mD. The tight gas sandstone was dened
b
14
3298.85m
30
25
20
15
10
5
0
10
30
20
40
50
60
12
Long-9
10
Yue -2
Qiongxi-1
6
4
2
0
10
20
30
40
50
60
70
80
8
6
4
2
24
36
48
60
72
84
96
16
Zhe-2
10
12
Ying-21
14
2581.3 m
12
70
16
35
Ying-21
14
Zhe-2
12
Long-9
10
Yue -2
Qiongxi-1
8
6
4
2
0
10
12
12
10
8
6
4
2
Ying-21
Zhe-2
Long-9
Yue-2
Qiongxi-1
10
20
30
40
50
60
70
80
Fig. 4. Summary of the distribution of pore throat structures of the Upper Triassic tight gas sandstone reservoirs from the Xujiahe Fm in the Sichuan Basin. (a) Pore throat size distribution
for Sample 3298.85 m. (b) Pore throat size distribution for Sample 2581.3 m. (c) Average porosity vs average pore diameters. (d) Average porosity vs average pore throat diameters.
90
C. Zou et al. / Journal of Petroleum Science and Engineering 8889 (2012) 8291
Fig. 5. Field emission SEM images of some typical tight gas sandstone investigated. (a), (b): Micro pores in tight sandstone from Hechuan-1 at 2124.88 m. The sandstone has a porosity of 5.25% and permeability of 0.0361 mD. (c), (d): Micropores and dissolution pores in clay minerals of tight sandstone from Long-13 at 3541.93 m. The tight sandstone has
porosity of 1.96% and permeability of 0.00231 mD. (e): Microcracks in chlorite mineral from Laoshen-1-10 at 2567.5 m. The tight sandstone has porosity of 7.1% and permeability of
0.388 mD. (f): Micropores within mineral grains in tight sandstone from Laoshen-1-10 at 2567.5 m. The tight sandstone has porosity of 7.1% and permeability of 0.388 mD.
Table 5
Various classication schemes for tight gas sandstone reservoirs.
Elkins (1981)
Alberta Bluesky
Sandstone
Li et al. (1996)
Reservoirs
Fm K (mD)
Res
R50 (m)
Res
K (mD)
R50 (m)
Res
K (mD)
Res
Conventional
Almost tight
Tight
Very tight
Ultra-tight
>1
10.1
0.10.005
0.0050.001
b 0.001
I
II
III
>2.3
2.30.77
b 0.77
Med K
Low K
AlTt
Tight
VTt
UTt
50010
101
10.5
0.50.05
0.050.01
b 0.01
31
10.303
0.3030.137
0.1370.022
Low K
Very low K
Ultra-low K
Tight
U/C tight
Ultra-tight
5010
101
10.1
0.10.01
0.010.001
0.0010.0001
Low K
Very low K
b 0.022
Fm, formation; Res, Reservoir; Tt, tight; AlTt, almost tight; VTt, very tight; U/C, unconventional.
Ultra-low K
Tight
I
IIa
IIb
IIIa
IIIb
IV
Res
K (mD)
5010
105
51
10.3
0.30.1
b0.1
Low K
V low K
1.010
b 1.0
C. Zou et al. / Journal of Petroleum Science and Engineering 8889 (2012) 8291
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Glossary
FERC: Federal Energy Resource Commission.
NGPA: Natural Gas Policy Act.
IEA: International Energy Agency.
MICP: Mercury injection capillary pressure.
SEM: Scanning electron microscope.
BSE SEM: Backscattered electron SEM.
FE-SEM: Field emission scanning electron microscope.
Effective permeability: The ability to preferentially ow a particular uid when other
immiscible uids are present in the reservoir.
Absolute permeability: The ability to ow uids through a rock, conducted when a
single uid is present in the rock (e.g. air permeability).
In situ permeability: Permeability measured under reservoir PTX conditions (e.g.
through DST or interference testing).
Pore throat: In an intergranular rock, the small pore space at the point where two
grains meet, which connects two larger pore volumes.
Pore throat sorting coefcient (Sp): Adopted from the sorting parameter used for characterizing sediments (Folk and Ward, 1957), Sp = (D84 D16) / 4 + (D95 D5) / 6.6
with D84 corresponding to pore throat size at 84% mercury saturation.
TCF: trillion cubic feet.
MPa: mega Pascal.
mD: 10 3 m2.