Lye from wood ash: Journey to Forever

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Making lye from wood ash

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Lye made from wood ash is potassium hydroxide, not sodium hydroxide -- there's 10 times
as much potassium as sodium in wood ash.
The process makes lye water. If you boiled off all the water you could use it as the catalyst
to make biodiesel, but you'd need more accurate pH measures than those listed below. The
usual pH meter or litmus papers would do. See also Natural test papers.
If you try this, we'd be very interested to know the results -- please contact us.

Making the lye

Drill a lot of holes in the bottom of a small wooden barrel, make sure it's waterproof before
you drill the holes!
Stand the barrel on blocks leaving space beneath the barrel for a container. Use a waterproof
wood or glass container. Lye can burn through some metals.
Put a layer of gravel in the bottom of the barrel over the holes, then put a layer of straw over
the gravel. Fill the rest of the barrel with hardwood ash (NOTE: hardwood -- NOT
softwood), leaving a couple of inches at the top clear. Then pour rainwater into the barrel.
After a long time the water in the barrel will start to drip into the container. Leave it until it
stops, then replace the container with another in case of odd drips.
Use an old iron pot, or a steel pan (One you will not be using for anything else!). Boil the
liquid until it is so concentrated that a fresh egg (still in it's shell please!) will float on top.
Then destroy the egg. Remember to take all precautions not the let the liquid touch your skin
or clothing.
To test the strength of the lye you need a saturated solution of salt. Dissolve chemical-free
salt in a pint of water until no more salt will dissolve. Take a stick and put a small weight on
the end of it and float it in a pint of the salty water. The weight will sink to the bottom, while
the top of the stick will float. Make a mark on the stick where it reaches the water line. Then
float the stick and weight in a pint of lye. The mark on the stick will probably be above the
water mark of the lye. If so, stir in some more rainwater until the mark on the stick is in
exactly the same place it was in the salt water. You now have the correct distillation of lye
for making soap.

Making "Lye Water"

Soap making uses a caustic solution known as "Lye Water".
When available, Caustic Soda is used. Here we will make Lye Water out of certain wood
ashes and "soft water".

1) White Ashes
Dried palm branches, dried out banana peels, cocoa pods, kapok tree wood, oak wood, (or
for really white soap, apple tree wood) make the best lye ashes. Ordinary wood used in
cooking fires will do.

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Lye from wood ash: Journey to Forever

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Whatever wood is used, it should be burned in a very hot fire to make very white ashes.
When cold, these are stored in a covered plastic bucket or wooden barrel, or stainless steel
container. If these are not available, a clay pot-jar which has been fired in a pottery making
kiln (not just dried in the sun).
A wooden drum or barrel which has a tap at the right is best.

2) Soft Water

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Water from a spring or from showers of rain is called "soft water", because it does not have
metallic or acidic chemicals in it.
This makes it useful for soap making, as there are no other chemicals in it which would get
in the way of making soap.
"Ordinary" bore, well, or river water can be used for making soap, but this will sometimes
need to have a "washing soda" or "baking soda" added to it. Otherwise some of the
chemicals in the water will get in the way of making the soap.
If you are using "ordinary" water and you want to test it to see if some soda needs to be
added, simply try to make soap bubble up (foam) in it.
If the soap easily foams up, the water is probably ok as it is.
If not, try adding a little bit of soda at a time stirring it to make it disappear, until the water
will foam the soap up.
Then add the same amount of soda to the same amounts of the water that you wish to use to
make the soap. For example, if you were testing a 1/4 (a quarter) of a bucket of water, and
you ended up needing 1/8 (an eighth) of a cup of soda, then you would need 4/8 ( or
1/2-half) a cup of soda for a full bucket of "ordinary" water.
However you have got it, store the "soft water" in covered wooden, plastic, or stainless steel
buckets or containers. (Again, a clay-jar as described above can be used if needed.)

"Safe" Containers
Any of the types of containers, buckets, barrels or jars described in the White Ashes or Soft
Water sections are called "safe containers".

Making "Lye Water"

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If you are going to use a large barrel or drum to make the lye water in, and it has a tap or
hole at the right, place some kind of filter on the inside of the barrel around the opening.
Fill the barrel with white ashes to about four inches (10 cm or 0.1 metre) below the top.

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Boil half (1/2) a bucket full of soft water (about 10 pints or six litres), and pour over the
ashes.
Slowly add more cold soft water until liquid drips out of the barrel. Close the tap or block
the hole.

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Lye from wood ash: Journey to Forever

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Add more ashes to top the barrel up again, and more soft water. Do not add so much water
that the ashes swim.
Leave to stand for four or more hours (or overnight if you have the time). Later pour the
brownish lye water into a plastic or other "safe" container(s). Then pour back through the
ashes again. Let the lye water drip into "safe" containers.
When the brown lye water stops coming out of the barrel, or ash container, then pour four to
five pints (2-1/2 to three litre) of soft water through the ashes, collecting the lye which
comes out in a separate "safe" container (as this lye may be weaker than the first lot).
Repeat this using two to three pints (one to two litres) of soft water, until no more brown
liquid comes out of the ashes.
Either put the lye into "safe" bottles, or cover the "safe" containers which it is in. Dig the
ashes into the vegetable garden.

Lye Water Strength

If an egg or potato will float just below halfway, or a chicken feather starts to dissolve in it,
then the lye water is at the right strength.
If the egg will not float, then the lye water could be boiled down if you want it to be
stronger.
If the egg seems to pop up too far, add a little bit of soft water (a cup at a time) stirring the
lye water, until the egg floats so that its head pops up.

Make The Lye

From Soap Making - Traditional Methods: Lye Rain Water Wood Ash by Paul Norman
In making soap the first ingredient required was a liquid solution of potash commonly called
lye.
The lye solution was obtained by placing wood ashes in a bottomless
barrel set on a stone slab with a groove and a lip carved in it. The
stone in turn rested on a pile of rocks. To prevent the ashes from
getting in the solution a layer of straw and small sticks was placed in
the barrel then the ashes were put on top. The lye was produced by
slowly pouring water over the ashes until a brownish liquid oozed out
the bottom of the barrel. This solution of potash lye was collected by
allowing it to flow into the groove around the stone slab and drip
down into a clay vessel at the lip of the groove.
Some colonists used an ash hopper for the making of lye instead of the
barrel method. The ash hopper, was kept in a shed to protect the ashes
from being leached unintentionally by a rain fall. Ashes were added
periodically and water was poured over at intervals to insure a
continuous supply of lye. The lye dripped into a collecting vessel
located beneath the hopper.

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9/11/15, 11:34 AM

Lye from wood ash: Journey to Forever

file:///Users/saumitre/other/read/house/soap/lye-from-ash-.html

The hardest part was in determining if the lye was of the correct strength, as we have said. In
order to learn this, the soap maker floated either a potato or an egg in the lye. If the object
floated with a specified amount of its surface above the lye solution, the lye was declared fit
for soap making. Most of the colonists felt that lye of the correct strength would float a
potato or an egg with an area the size of a ninepence (about the size of a modern quarter)
above the surface. To make a weak lye stronger, the solution could either be boiled down
more or the lye solution could be poured through a new batch of ashes. To make a solution
weaker, water was added.
From Colonial Soap Making: Its History and Techniques -- The Soap Factory
http://www.alcasoft.com/soapfact/history.html
"When a fresh egg floats with a nickel-sized to quarter-sized area above the surface, the
liquor is ready for soap making." -- Homestead mailing list.
Nickel = 2 cm diameter
Quarter = 2.5 cm diameter
At the turn of the last century lye was obtained by leaching water through wood ashes. At
best, the concentration of potassium hydroxide in the resulting lye water was always
questionable. My grandmother said that she could tell if the lye water was the right strength
by using the wing feather pulled from her favorite goose. She would pour the lye water into
a 30 gallon cooking pot and heat the solution. Next she would touch the feather to the
heating lye. If the feather dissolved, the lye was strong enough to dissolve pig fat.
-- Soap Making Today

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Biodiesel resources on the Web
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Food or fuel?
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Lye from wood ash: Journey to Forever

file:///Users/saumitre/other/read/house/soap/lye-from-ash-.html

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