Professional Documents
Culture Documents
PETROCHEMICAL ENGINEERING)
Qualitative and quantitative analysis, Principle of gravimetry and steps involved in gravimetric analysis,
digestion and its importance, favourable conditions for precipitation.
Titration, titrant, analyte, primary and secondary standards. Basic requirements of a titrimetric method,
classification of titrations (acid-base, oxidation-reduction, precipitation and chelometric titrations with
examples).
Absorption Spectrophotometry : Beer and Lamberts law (definition and units of terms involved.
deviaton from Beers Law) Block diagram of single bean UV-Visible Spectrophotometer.
Definition of chromatography and chromatographic system (stationary and mobile phase), classification
of chromatography on the basis of physical mode (planar and column chromatorgrahy) and mechanism
(sorption, partition and ion exchange chromatorgrahy). Calculation of RF Value, separation factor,
resolution and capacity factor from chromatorgram.
UNIT-II: WATER TRATMENT
Hardness of water (units of hardness, calculation on hardness, determination by soap and EDTA
methods). Sludge, scale priming and foaming. Boiler corrosion and caustic embrittlement (causes, defects
and prevention). Lime-soda, zeolite and ion exchange processes. Calculations based on Lim-soda and
zeolite proesses. Sedimentation, coagulation and filtration. Disinfection, requirements of a good
disinfecting agent and types of disinfecting agents, (bleaching powder, liquid chlorine, ozone, UV
radiation and chloramines). Break point chlorination:
UNIT-III FUELS
Classification of fuels and characteristics of a good fuel, calorific value and its determination by Boom
Calorimeter and Dulongs formula (Numerical problems). Analysis of coal (Proximate Ultimate analysis)
Composition and classification of petroleum. Important factions of petroleum and their uses. Synthetic
petrol ( Polymerizations and cracking, Fisher Tropsch and Bergius processes). Advantages and
disadvantages of gaseous fuels, composition and uses of natural gas, CNG, LPG, Combustion
calculations on solid and gaseous fuels.
UNIT-IV LUBRICANTS
Definition and classification of lubricants Mechanisms of lubrication. Mineral oils, fatty oils,
compounded oils and silicone fluids. Testing of liquid lubricants, Viscosity, and index Flash and Fire
points. Cloud, pour and setting Point, Saponification value, Aniline point, Types of greases and
conditions for their use. Consistency test, and Drop Point of Greases.
UNIT-V CORROSION AND ITS PREVENTION
Definition, significance and classification of corrosion. Mechanism of oxidation metals, PillingBedworth rule. Nernst equation, electrochemical and galvanic series. Cathodic and anodic reactions.
Factors affecting corrosion. Corrosion control (design and selection of materials, cathodic protection,
metallic coatings, galvanizing and tinning anodized coating). Paints definition, compositions and the
function of each component).
UNIT-VI POLYMER
Definition and classification of Polymers. Polymerization (addition and condensation), mechanism of
free radical addition polymerization.
Definition, preparation, properties and uses of thermoplastic (PMMA Teflon), and thermosetting plastics
(Bakelite, Polyesters) synthetic fibres (Nylon 66, or lon). Natural rubber and vulcanization.
AP111
APPLIED PHYSIC
UNIT 1.
Semiconductors Elemental and compound semiconductors, Energy bands, Direct and indirect
semiconductors, Electrons and holes, Effective mass, Intrinsic material, Extrinsic material, Fermi
level Electron and hole concentration at equilibrium, temperature dependence of carrier
concentrations, compensation and space charge neutrality, conductivity and mobility, hall effect in
semiconductors
Superconductivity Zero resistivity, Meissner effect, Type I and Type II Superconductors, High
Temperature Superconductors, BCS theory (Qualitative), Josephson effect, SQUIDS.
UNIT II.
Masers and lasers, Basic principle, Einstein coefficients for induced absorption, Spontaneous
Emission and induced emission, Ammonia maser and its applications, Ruby and He-Ne Lasers,
Semiconductor laser, spatial and temporal coherence, characteristics of lasers and its applications
based on these characteristics (such as in Industry, Science, Medicine, Communications, Surveying,
Holography, Fusion reactors, Isotope separations etc).
Fibre Optic, Basic principle, Fibre construction and dimensions light Propagation in fibres,
Numerical aperture of the fibre, Step index and graded index fibres signal distortion in optical fibres,
Transmission losses, light wave communication in optical fibres, Fibre Optics in medicine and
industry.
UNIT III.
Particles and waves, Mechanism of X-ray production (continuous and characteristic X-rays, DuaneHunt limit Compton effect, Pair production, Phase and group velocities, Uncertainty principle.
Quantum Mechanic, Introduction to quantum mechanics wave function, conditions necessary for
physically acceptable wavefunction, Probability density and probability, Schrodinger equation (Time
dependent form and steady state or time independent form), Eigen values and eigen functions,
Expectations values Particle in a box (Infinite potential well), Tunnel effect.
UNIT IV
Statistical Mechanics, Statistical distributions, Maxell- Boltzman statistics, Molecular energies in an
ideal gas, Quantum statistics, specific heats of solids, free electron in a metal Electron-energy
distribution.
Nuclear Physic, Q value and threshold energy of nuclear reactions, Cross section of nuclear reaction
and reaction rate, Breeder reactors, Fusion reactors, Nuclear detectors (names and general working
principle), gas filled detectors, Scintillation detectors.
Text Books
1. Ben G. Streetman, Solid State Electronic Devices 5th edition(2000), Prentice-Hall of India
Private Limited New Delhi
2. Arthur Beiser, Concepts of Modern Physics 6th edition (2003), Mc. Graw Hill Inc. International
Edition.
3. M.R. Wehr, J.A. Richards. Jr. and TW AdairIII, Physics of the Atom 4th editions (1984), Addison
Wesley / Narosa.
4. M.R. Srinivasan, Physics of Engineers 1st Edition (1996), New age International (P) Limited
Publishers.
AM111 MATHEMATIC
UNIT 1.
Rank of a matrix with applications to consistency of system of linera equations, Eigen-values and
Eigen vectors of a matrix, Cayley-Hamilton Theorem.
UNIT 2.
Asymptotes and simple curve tracing. Successive Differentiation, Leibnitzs Theorem, Taylor
and Maclaurin series with remainder terms.
UNIT 3.
Applications of integration to lengths of curves, surfaces and volumes of solids of revolution.
UNIT 4.
Solutin of exact differential equations, Linear differential equations of second and higher order
with constant coefficients. Homogeneous differential equations. Simultaneous linear differential
equations, Applications to physical problems.
AM112 MATHEMATIC
UNIT 1.
Partial differentiation, Eulers Theorem, Total differential, small errors, change of variables,
Jacobians.
UNIT 2.
Taylor series for functions of two variables approximate calculations Maxima and minima of
functions of two variables, lagranges multipliers.
UNIT 3.
Double and triple integrals, change of variables, change of order of integration, Applications of
areas and volume.
UNIT 4.
General equations of second degree, Tracing of conics introduction to polar form of conics.
UNIT III.
Water Quality Physical, Chemical and Biological parameters water quality standards,
Biochemical (BOD) and Chemical Oxygen Demand (COD). BOD/ COD Calculations.
EN101 ENGLISH
UNIT I
Text. Comprehension Questions, Summary Type as well as short answer type and questions on
Vocabulary for 10 passages of the Basic Scientific English by Ewer and Latorre (Longman).
Units are 1,3,4,5,8 & 11 from main book and passages 4,11,13,17 from the supplement.
UNIT II
Comprehension questions, summary or short answer type from the following supplementary
readers:
1. Animal Farm by George Orwell
2. The time machine by HG Wells retold by Margery Gree Macmillan)
UNIT III
Note taking, note making exercises, report and process writings.
UNIT IV
Precis writing
UNIT V
Composition and spoken English.
UNIT I
Dimensions and units system boundary types of systems and boundaries property cycle
thermodynamic equilibrium and quasi-static process.
Pressure and its measurement, zeroth law of thermodynamics, temperature and its measurement,
numerical problems.
UNIT II
Thermodynamic and mechanics definition of work. Displacement work and its expressions
engine indicator and indicated work, introduction to 2-stroke and 4stroke engines, heat, work and
heat as energy interactions, Joules experiment & mechanical equivalent of heat, firs law of
thermodynamics for cycle and non cyclic processes.
Definition of energy as a property, internal energy, enthalpy, specific heats, first law for a control
volume, steady flow energy Equation (SFEE) and its applications, numerical problems.
UNIT III
Pure substance, different phases of pure substance, tow property rule property diagrams, tables
and charts equation of state of an ideal gas t, tp, pv, and tv diagrams, phase boundaries, SL-V region, CP and TP, dryness fraction and its measurement using throttling calorimeter,
limitations of throttling calorimeter, separating & throttling calorimeter, numerical problems.
UNIT IV
Limitations of first law , heat engine heat pump refrigerator, second law of thermodynamicskelvin plancks and Clausius statements and their equivalence efficiency of heat engine and
coefficient of performance of heat pump and refrigerator, reversible and irreversible processes.
Carnot cycle and its efficiency corollaries of second law, the thermodynamic scale. Inequality of
Clausius, entropy, principle of increase of entropy, isentropic process, ts and hs diagrams
(Mollier chart), second law applications, air standard otto, diesel, dual simple Brayton and steam
power cycles (Rankine cycle) numerical problems.
UNIT V
Modes of heat transfer, Fouriers law of steady state heat conduction (one dimensional
conduction), thermal conductivity and its unit, conduction through slab or plane wall, conduction
through composite walls and hollow cylinders, convective heat transfer, Newtons law of
cooling, combine heat transfer, electrical analogy and overall heat transfer coefficient radiation,
black body emissive power emissivity, Kirchoffs law Stefan Boltzmanns law. Numerical
problems.
Book
1. Thermodynamics, An Engineering Approach by yunus A. Cengel and Michael A Boles
2. Engineering Thermodynamics by D. B. Spalding and E.H.Cole.
3. Engineering Thermodynamics by R. Joel
4. Engineering Thermodynamics by P.K.Nag.
5. Engineering Heat Transfer by C.P. Gupta and R. Prakash.
ME111
APPLIED MECHANIC
UNIT 1
Fundamental concepts and principles of Mechanic, Reduction of a system of forces to a force
couple system, free body diagrams, equilibrium of rigid bodies in 3 Dimensions, Reactions,
loading indeterminacy and solvability. Friction forces and laws of dry friction principle and
application of virtual work.
UNIT 2
Analysis of Multiple particle system application of Newton;s laws, linear and angular
momentum, kinetic energy and work energy principle, principle of impulse and momentum to a
system of particles.
UNIT 3
Translation and rotation about a fixed axis, general plane motion absolute and relative velocity in
plane motion angular momentum of rigid body in plane motion. Problems of motion of rigid
bodies and system of rigid bodies principle of work and energy, conservation of energy for rigid
body and a system of rigid bodies.
UNIT 4
Analysis of stress and strain Mechanical properties analysis of simple state of stress and strains,
elastic constant, example of state of tension compression and shear
UNIT 5
Bending shear and torsion: Concept of bending and shear forces in shear forces in simple beams,
relationship between load, bending moment and shear force. Bending and shear stresses in simples
beams, concept of torsion in circular shafts.
Text Books
1. Beer Ferdinand P. and Johnston Jr. E Russel, Vector Mechanics for Engineering Statics and
Dynamic Metric edition, Mc Graw Hill, New Delhi.
2. Popov E., Engineering Mechanics of Solids, PHI, Delhi.
Reference Books
1.
Merium, JL, Engineering Mechanics (Volume I and II), 3rd edition, (SI version) John Wiley and sons,
Inc, NT
THIRD SEMESTER
AM-
UNIT I: Vector differentiation, scalar field, gradient of a scalar field, vector field, divergence & curves
of vector fields, solenoidal angle and irrotational field. Determination of potential function.
UNIT II: Vector integration, line integral, conservation fields, Gauss divergence theorems, Greens
theorem and Stokes theorem.
UNIT III: Laplaces transformation, shifting theorems, transforms of derivatives and integrals.
Differentiation and Integration of transforms. Inverse transforms, Application with single and system of
linear differential equations.
UNIT IV: Boundary Value Problems, solution of 2D laplace equation in Cartesian and polar coordinates, solution of one dimensional diffusion and wave equation by method of separation of variables.
BOOKS:
1. Prasad, C., Mathematics for Engineers, Prasad Mudranalaya, New Delhi, 1985.
PK-214: REACTION KINETICS AND REACTOR DESIGN
UNIT I: Rate of Reaction , elementary and non-elementary reactions molecularity and order of reaction,
thermodynamics formulations of rates, mechanism of reaction, Temperature dependency from
thermodynamics, arrhenius, collision and activated complex theories, Introduction of industrial reactors.
UNIT II: Integral and differential methods for analyzing kinetics data, interpretation of constant volume
batch reactor data for zero, first second and third order reactions, half life period, irreversible reactions in
parallel and series, auto catalytic reaction, shifting order reactions enzyme catalyzed and surface
catalyzed reactions. Interpretation of variable volume batch reactor data for zero, first and second order
reactions.
UNIT III: Design equations for batch, plug flow, back mix, flow and semi batch reactors for isothermal,
adiabatic reactions holding time and space time for flow system Design of batch plug flow and mixed
flow reactors for first and second order single reactions. Optimum reactor size plug flow reactors in series
/ parallel Equal and different size of mixed reactors in series and finding the best system for a given
conversion recycle reactor
UNIT IV: Multiple reactions, independent, parallel and series reactions; mixed reactions, instantaneous
and over all fractional yield, choice of reactors for simple and complex reactions and multiple reactor
system; Introduction to thermal stability of reactors; temperature and pressure effects and optimal
temperature progression for first order reactions. Introduction to Residence time Distribution of fluid in
Vessel.
BOOKS:
1. Levenspiel, O., Chemical Reaction Engineering, John Wiley and Sons, New York, 3/e, 1998
2. Fogler, H. S., Elements of Chemical Reaction Engineering, Prentice Hall, USA 4/e, 2005
3. Smith, J. M., Chemical Engineering Kinetics, McGraw Hill Publications, New York, 1981
Unit-III: Transportation of fluids; types of pumps, centrifugal and positive displacement pumps
compressors, fans, blowers, types of valves, pipes and tubes.
Unit-IV: Metering of fluids; orifice meter, venturimeter, pitot tube, rotameter, notches, gas flow meters,
coefficient of discharge
BOOKS
1. McCabe, W.L., Smith, Julian C. & Harriett, Peter, Unit Operations of Chemical Engineering,
McGraw Hill, New Delhi, 7/e,2005.
2. Kumar, K.L., Engineering Fluid Mechanics, Eurasia Publishing House (P) Ltd, New Delhi, 17/e,
2008
3. Bansal, R.K, A Textbook of Fluid Mechanics, Laxmi Publications(p) LTD, New Delhi, 2008
Unit I: origin and formation of Petroleum, Reserves and deposits, Indian Petroleum Industry, Composition of crude
Oils, ultimate and chemical composition , non-hydrocarbons in petroleum, Asphltenes and Resins, classification of
petroleum, evaluation of crude oil, Bench mark crudes.
Unit II: characterization of crude oils : TBP and ASTM distillation, Classification by chemical composition,
Correlation Index, Density, API gravity, Viscosity, UOP characterization factor, etc. Physical & Thermal properties
of petroleum, ASTM, TBP, EFV distillation curves.
Unit III: Distillation: Pretreatment, Electric desalting, atmospheric and vacuum distillation, petroleum products
and their quality control tests.
Unit IV: Value addition of petrochemicals from feedstock to consumer end products, chemical reactions of
hydrocarbons like Decomposition (Thermal & Catalytic), Halogenations, Isomerization, Hydrogenation, Alkylation,
Nitration, Sulfonation, etc. with chemistry and reaction mechanism.
BOOKS:
1.
2.
3.
4.
5.
6.
Speight, J.C.; The Chemistry and Technology of Petroleum, Marcel Dekkar, New York, 3/e1999.
Lucas, A.G. (ed.), Modern Petroleum Technology, Vol. 2, Downstream, John Wiley & Sons Limited,
New York, 6/e, 2000.
Simanzhenkov, V. and Idem, R., Crude oil Chemistry, Marcel Dekker Inc., New York, 2003.
Hobson, G.D., Modern Petroleum Technology Vol I & II, John Wiley & Sons, New York, 5/e, 1984
Rao, B.K.B., Modern Petroleum Refining Processes, Oxford & IBH Co. Pvt. Ltd., New Delhi, 4/e, 2002,
Prasad, R., Petroleum Refining Technology, Khanna Publishers, New Delhi, 2000
FOURTH SEMESTER
AM-: NUMERICAL METHODS AND OPTIMISATION
UNIT I: General iteration method, Newton Raphson method, application of Newton Raphson method,
Solution of system of linear equation by Gauss elimination method and Gauss Siedel method,
Convergence of iteration.
UNIT II: Interpolation-Finite difference operator, Central difference operator, backward difference
operator, relation between operators, Newtons forward Interpolation formula, Newtons backward
Interpolation formula, Newtons Interpolation formula for unequal interval, Lagranges Interpolation
formula for unequal interval.
UNIT III: Numerical Differentiation- Newtons divided difference formula; Numerical integrationTrapezoidal rule, Simpsons rule, Weedles rule; Numerical Solution of differential equation-Solution
with Taylors series, Eulers method, modified Euler method, Runge-Kutta method, Boundary value
problems.
UNIT IV: Graphical and analytical methods of optimization, Numerical search methods, search of
optimum over single and several design variables, Optimum of process systems, linear programming.
BOOKS :
1. Sastry, S.S., Introductory Methods of Numerical Analysis, Prentice Hall of India Pvt. Ltd., 2004.
Equilibrium: The nature of equilibrium, the phase rule-Duchems theorem, VLE Quantitative behaviour,
VLE by modified Raoults Law, VLE from k-value correlations.
UNIT III: Solution thermodynamics: theory, fundamental property relation, the chemical potential and
phase equilibria, partial properties, ideal-gas mixtures, fugacity and fugacity coefficients, pure species,
species in solution, generalized correlations for the fugacity coefficient, the ideal solution, excess
properties. Application ; liquid phase properties from VLE data, models for the excess Gibbs energy,
property changes of mixing, heat effects of mixing processes.
UNIT IV: Chemical Reaction Equilibria: The reaction coordinate, application of equilibrium criteria to
chemical reactions, the standard Gibbs. Energy change and the equilibrium constant, effect of
temperature on the equilibrium constants, relation of equilibrium constants to composition, equilibrium
conversions for single reactions, phase rule and Duhems theorem for reacting systems.
BOOKS:
1. Rao, Y.V.C. , Chemical Engineering Thermodynamics, Universities Press, India 2/e, 2001.
2. Rao, Y.V.C., Theory and Problems of Thermodynamics, New Age International (P) Ltd, New
Delhi, 2000
3. Smith, J.M., Van Ness, H.C. and Abbott, M.M., Chemical Engineering Thermodynamics, Tata
McGraw-Hill Publishing, New Delhi, 6/e, 2003.
4. Kyle; B.G., Chemical and Process Thermodynamics"; Prentice Hall, New York, 3/e, 1999
PK 223
UNIT I: Principles of process synthesis: reaction path synthesis, species allocation, separation task selection, task
integration.
Unit II: Diagrams for understanding chemical processes: Block Flow Diagram, Process Flow Diagram,
Piping & Instrumentation Diagram. Structure and synthesis of process flow diagrams.
Unit III: Chemical product design, tracing chemicals through the process flow diagram, understanding
process conditions.
UnitIV: Introduction to design codes, design of cylindrical and spherical shells, design of storage tanks,
designs of tall vertical vessels, selection and design of flanges and supports for equipment.
BOOKS:
1. Turton, Richard, Bailie, Richard C., Wallace B. Whiting, Shaeiwitz, Joseph A.; Analysis,
Synthesis and Design of Chemical Processes, Prentice Hall, USA 3/e, 2009.
2. Douglas, J.M., Conceptual Design of Chemical Processes, McGraw-Hill, 1988
3. Joshi, M.V. and Mahajani, V.V.; Process Equipment Design, 3/e, 1996, MacMillan India Ltd,
New Delhi
4. Bhattacharya, B.C. Introduction to Chemical Equipment Design Mechanical Aspect, Chemical
Engineering Education Development Centre I.I.T Madras.
2. Viswananthan. B., Sivasankar and Ramaswamy, A.V. (ed.), Catalysis Principles and
Applications, Narose Publishing House, New Delhi, 2002.
3. Thomas, J.W. and Thomas, W.U., Introduction to the Principle of Heterogeneous Catalysis,
Academic Press, 1967.
UNIT I: Behavior of Chemical Reactors: Ideal & Non-Ideal Flow; Classification of Reactors:
Isothermal, Ideal batch, CSTR, PFR, Multiple Reactors, Non-isothermal Reactors,
Multiplicity, Non-ideal reactors, Fluid Solid Non-Catalytic reactions, Fluidized Beds.
UNIT II: Introduction to Reactor Design; Detailed Design of Batch Reactors.
UNIT III: Flow Reactors; Detailed Design for CSTR; CSTR Design; Single CSTR Battery; CSTR at
Differential Temperature etc.
UNIT IV: Detailed Design for Plug Flow Reactor: Single; Series And Parallel; Mixed Reactor
(Combination); Reactor stability, Design aspects for Non-ideal Reactors.
BOOKS:
1. Octave Levenspiel, Chemical Reaction Engineering, 3rd Edition, John Wiley &Sons (Asia)Pte Ltd.
(1998), ISBN: 978-0-471-25424-9.
2. H. Scott Fogler, Elements of Chemical Reaction Engineering 3rd Edition November,
Prentice Hall of India Pvt Ltd (1998).
3. L. D. Schmidt, The Engineering of Chemical Reactions, Oxford Press (1998).
4.J.M. Smith, Chemical Engineering Kinetics, 2nd, McGraw-Hill (1981).
FIFTH SEMESTER
PK-311: PETROLEUM REFINING PROCESSES
Unit I: Thermal conversion processes like Visbreaking, Delayed Coking, Fluid coking, Flexicoking, etc.
Unit II: Catalytic conversion processes - fluid catalytic cracking, RFCC, DCC, Hydrocracking,
Hydrotreating processes, etc.
Unit III: Reforming, hydrogen production, Alkylation, Polymerization, Isomerisation etc.
Unit IV: Evaluation of crude for LOBS, Production of lubes and waxes.
BOOKS:
1. Speight, J.G. and Ozum, B. Petroleum Refining Processes, Marcel Dekker Inc, New York, 2002.
2. Gary, J.H. and Handiwerk, G.E., Petroleum Refining Technology and Economics, Marcel Dekker,
Inc., New York, 2001.
3. Hobson, G.D., Modern Petroleum Technology Vol I & II, John Wiley & Sons, New York, 5/e,
1984
4. Rao, B.K.B., Modern Petroleum Refining Processes, Oxford & IBH Co. Pvt. Ltd., New Delhi, 4/e,
2002,
5. Prasad, R., Petroleum Refining Technology, Khanna Publishers, New Delhi, 2000
Unit I: Natural Gas-origin and occurrence, properties of natural gases, phase behavior of Natural Gas
systems, vapor liquid equilibrium calculations.
Unit II: Natural gas- liquid separation, separation principles, separation equipment, low temperature
separation.
Unit III: Water-hydrocarbon phase behaviour, measurement of water content in Natural gases, Hydrate
formation and prevention of hydrates, Gas dehydration- types of processes.
Unit IV: Acid gases in natural gas, acid gas treatment, types of processes. Natural gas storage, Natural
gas liquids removal, Transportation of Natural Gas, LNG chain.
BOOKS:
1. Kumar, S., Gas Production Engineering, Gulf Publishing Company Book Division, London, 1960.
2. Mokhatab, S., William, A.P. and Speight, J.G., Handbook of Natural Gas Transmission and
Processing, Gulf Professional Publishing, Oxford, 2006.
3. Francis, S.M. and Thompson, R.E., Oil Field Processing of Petroleum, Volume one: Natural Gas,
Penn Well Books, Penn Well Publishing Company, Oklahoma, 1995.
UNIT IV: Equipment for Gas-Liquid Operations: Sparged vessels, mechanically agitated vessels.
BOOKS:
1. Treybal, R.E., Mass Transfer Operations, Mc. Graw Hills, New York, 3/e, 1983
2. Geankoplis, C.J., Transport Processes and Unit Operations, Prentice Hall of India, New Delhi, 4/e,
2003.
3. Mc. Cabe, W.L., Smith, J.C., and Harriot, P., Unit Operations of Chemical Engineering, Mc.
Graw Hills, New York, 6/e, 2001
4. Skelland, A.H.P., Diffusional Mass Transfer, John Wiley and Sons, New York, 1974
PK- 312: HEAT TRANSFER OPERATIONS
UNIT I: Steady State heat conduction in one dimension: heat conduction through plane wall, composite
wall, single layer cylinder, multi layer cylinder, sphere, Fouriers Law of conduction and thermal
conductivity, critical thickness of insulation, overall heat transfer coefficients. Forced Convection: forced
convection past planar surface, inside cylindrical pipes and tubes and in non-circular sections, forced
convection for external flow normal to tubes, tube banks.
UNIT II: Heat Transfer by Free Convection: Governing equation for free convection, working
correlations for free convection, analytical solution of free convection past vertical plane surfaces. Heat
Transfer in Boiling and Condensing: working correlations of film condensation, dropwise condensation,
heat transfer for boiling of a liquid, working correlations for pool boiling, forced convection boiling.
UNIT III: Heat transfer by radiation: basic definition, laws of radiation, black body, gray body, shape
factors. Heat Exchangers: Various types, general characteristics, overall heat transfer coefficient of heat
exchanger, heat exchanger mean temperature difference, heat exchanger effectiveness and number of
transfer units, performance of heat exchanger and design of heat exchanger.
UNIT IV: Evaporation and Evaporators: types of evaporators, their construction and operation,
evaporator auxiliaries, principles of evaporation, single effect evaporator, multiple effect evaporator,
modes of feed supply to the evaporator, evaporator selection, effect of boiling point on multiple effect
evaporator.
BOOKS
1. Chapman, A.J.,Heat Transfer, Mc Millan Publishing Company, New York, 4/e, 1984.
2. Holman, J.P., Heat Transfer, Tata McGraw Hill Publishing Company, New Delhi, 9/e, 2009.
1.
2.
3.
Van Vlack L.H. Elements of Materials Science and Engineering ed 6th Addison Wesley Inc New York
E.d. Dyson R.W Engineering Polymers, Blackie, New York.
Smith C.O The Science of Engineering Materials third edition, Prentice Hall Inc New Jersey.
SIXTH SEMESTER
PK-323: TRANSPORT PHENOMENA
UNIT I: General Introduction to Transport Processes: analysis of momentum transport process, principle
of shell balance, laminar, rectilinear steady flow of incompressible fluids in conduits and thin layer. Flow
of falling film, flow between parallel plates, flow through circular pipes, capillary flow viscometer, flow
through annular, adjacent flow of two immiscible fluids.
UNIT II: Analysis of thermal transport processes: Fouriers law of heat conduction, steady one
dimensional heat conduction without and with internal heat source, conduction through plane wall,
hollow cylinder, composite wall, multilayer cylinder, overall heat transfer coefficient, critical thickness
of insulation, heat conduction with internal electrical/nuclear/viscous and chemical heat.
UNIT III: Analysis of species transport processes: Definition of concentration, velocity, flux in multi
species system, Ficks Law of diffusion, continuity equation for binary system and transport of species
through annulus.
UNIT IV: Macroscopic Analysis of momentum, heat and species transport: Macroscopic mass balance,
momentum balance, mechanical energy balance, use of macroscopic balance equations, power
requirement for pipeline flow, efflux time of tank. Interphase transport of momentum/ heat/ species in
turbulent flow: definition of friction factor, heat transfer coefficient, binary species transfer coefficient,
interphase momentum/ heat/ species transport in circular tubes.
BOOKS:
1. Bird, R.B., Stewart, W.E., and Lightfoot, E.N., Transport Phenomena, John Wiley and Sons, New
Delhi, 2008.
2. Geankoplis, C.J., Transport Processes and Unit Operations, Prentice Hall of India, New Delhi, 4/e,
2003.
UNIT II: Petrochemicals from C1, C2, C3, C4, Syngas & aromatics.
UNIT III: Chemistry and technology for the production of Methanol formaldehyde, Ethylene oxide , glycol and
Vinyl Chloride
UNIT IV: Chemistry and Technology for the Production of Acetone, Cumene, Acrylonitrile, Linear alkyl benzene
etc
BOOKS:
1
2
3
4
Waddams, A.L., Chemicals from Petroleum, 4th edition, Gulf Publishing Company, London, 1980.
Lewis F. Hatch & S Matar, From Hydrocarbon to Petrochemicals
Chauvel and B. Lefebvre, Petrochemical Processes 1 & 2; Gulf Publishing Co. Houston, Texas, USA.
M. Gopala Rao and Marshall Sitting, Outlines of Chemical Technology, 3/e, Affiliated East West Press Pvt.
Ltd, New Delhi.
(DE-II)
Unit-I: Fuels from coal development of synfuels, Properties & principles of coal conversion,
thermodynamic of coal conversion Low, medium & high BTU gas from coal Clean liquid from coal
Pyrolysis, liquefaction, coal & oil processing Environmental issues, CTL.
Unit-II: Liquid fuels from NG, GTL, DME, Methanol, MTBE.
Unit-III: Fuels from Biomass Biomass thermal conversion processes, Biological conversion processes,
Lignocellulosic conversion processes.
Unit-IV: Fuels from oil shales & tar sands, Properties of oil shales & tar sand above ground processes &
insitu processes, Constraint in commercial production for oil shales & tar sands.
BOOKS:
1. Anderson, L.L. and Tillman, D.A., Synthetic Fuels from Coal: Overview and Assessment, WileyInterscience, New York, 1979.
2. Lee, S., Speight, J.G. and Loyalka, S.K., Handbook of Alternative Fuels Technologies, CRC Press,
2007.
UNIT II: Steps in organizational design (division of work, departmentation, hierarchy, co-ordination),
span of control or span of management, Garicunas theory, approaches to organizational design,
classiscal approach, task technology approach, environmental approach. Leadership-source of power
(Reward power, Coercive power, legitimate powers, expert powers, referent power), theories of
leadership (trait theories, behavorial theory, situation theory and contingency approach)
UNIT III: Types of behavior (status-meritorial, etc), leadership (democratic, autocratic, lessen free),
motivation. Engineering economy (Law of supply and demand), Laws of diminishing return, unit cost
function, elements of cost, overheads, break-even analysis and charts.
UNIT IV: Forecasting and techniques, kinds and types of forecasting, methods of forecasting,
qualitative methods (consumer survey model, composite sales team method, Delphi method). Statistical
Approach - time series models, components of TS models, trend, seasonal variation, cyclic variation,
Random variables, least square method, moving average method, weighted moving average method,
semi-average method, and exponential smoothup. Casual Models regression analysis, correlation
analysis, standard deviation, Depreciation, cash flow diagrams and various numerical problems based on
it. Present worth method, future worth, annual worth, ERR worth and ERR worth methods.
BOOKS:
1. Barthwal, R.R., Industrial Economics, New Age International Pvt. Ltd., New Delhi, 2/e, 2000.
2. De Garmo, P.E., Engineering Economy, Printice Hall Inc., New Jersey, 10/e, 1997
3. Stoner, A.F., Freeman, E.R., Gilbert, D.R., Printice Hall Inc., New Jersey, 6/e, 1995
SEVENTH SEMESTER
PK - 411: PROCESS DYNAMICS AND CONTROL
Unit I: Process Control systems, Basic Concepts in Process Control., Process variables, control
configurations & physical elements of a control System, Block diagrams, Dynamic Modeling of
processes, Linearization of Non-linear systems,
Unit II: Response of first order system, Response of first order system in series (Interacting and noninteracting systems) , Second order system, Dynamic Response of second order system Transportation
Unit III: Closed loop transfer functions, Modes of control action, Classification of Controllers, Transient
response of some simple control systems. Stability analysis of control systems, Root locus Method,
Controller Tuning, Frequency response analysis, Bode diagrams, control system design by frequency
response, Bode stability criterion, Nyquist plots.
Unit IV: Introduction to Advance Control Systems, Control systems with multiple loops, feed forward
and Ratio Control systems. Process Control using Digital Computers, Reconstruction of continuous
signals from their discrete-time values, conversion of continuous to discrete time models, Z- transforms.
BOOKS:
1. Coughanowr, D. R., Process Systems Analysis and Control, McGraw Hill, New York, 1991.
2. Stephanopoulos G., Chemical Process Control, Prentice Hall of India, 1991.
3. Weber, T.W., An Introduction to Process Dynamics & Control, John Wiley & Sons, New
York, 1976.
4. Bequette, B.W., Process Control-Modeling, Design and Simulation, Prentice Hall of India Pvt.
Limited, New Delhi, 2003.
5. Luyben, W.L., Process Modelling Simulation and Control for Chemical Engineers, McGraw
Hill, New York, 2/e, 1990.
6. Seborg, D.E., Edgar, T.E. and Mellichamp, D.A., Process Dynamics and Control, Wiley New
York ,1989.
7. Luyben, M.L. & Luyben, W. L., Essentials of Process Control, McGraw Hill, New York, 1997.
8. Palm, W.J., Modelling, Analysis and Control of Dynamic Systems, John Wiley and Sons, New
York, 1983.
UNIT II: Chemistry and technology for the production of DMT, Terephalic acid, Acrylic acid, Methyl
methacrylate etc
UNIT III: Properties, applications and production technologies of the following commodity polymers
polyethylene, LLDPE, HDPE, polypropylene, polystyrene, PVC.
UNIT IV:Properties, applications and production technologies of the following engineering and thermoset
polymers: ABS plastic, nylon-6, polycarbonate, epoxy resin, unsaturated polyester resin, rubber
BOOKS:
1
2
3
4
5
Waddams, A.L., Chemicals from Petroleum, 4th edition, Gulf Publishing Company, London, 1980.
Lewis F. Hatch & S Matar, From Hydrocarbon to Petrochemicals
B.K. Bhaskara Rao, A Text on Petrochemicals, 2/e, Khanna Publishers, Delhi, 1998.
Mall, I.D., Petrochemical Process Technology, Macmillan India Limited, Delhi, 2007.
F.A. Lowenheim and M. K. Moran; Industrial Chemicals, John Wiley & Son
Inc.,USA.
PK-491A: PROJECT
Techno-economic feasibility analysis, presentation and report
EIGHTH SEMESTER
(DE-IV)
UNIT I: Transportation and storage of crude oil and petroleum products, Types of tanks, Pressure
vessels and underground storage.
UNIT II: Sweetening processes, hydrogen sulphide removal, Sulfur conversion processes, Solvent
Deasphalting, Gasification
UNIT III: Ammonia, Nitric Acid, Ammonium Nitrate, Urea.
UNIT IV: Phosphatic fertilizers, super phosphate, Triple super phosphate, Mono and diammonium
phosphate, Nitro phosphate, Mixed Fertilizers.
BOOKS:
1. Speight, J.G., The Chemistry & Technology of Petroleum, CRC Press, New York, 4/e, 2007.
2. Speight, J.G. and Ozum, B. Petroleum Refining Processes, Marcel Dekker Inc, New York, 2002.
3. Gary, J.H. and Handiwerk, G.E., Petroleum Refining Technology and Economics, Marcel Dekker,
Inc., New York, 2001.
4. Hobson, G.D., Modern Petroleum Technology Vol I & II, John Wiley & Sons, New York, 5/e,
1984
5. Chauvel, A. and Lefebvre, G., Petrochemical Processes, Gulf Publishing Company, Houston,
1989.
6. Matar, S., Chemistry of Petrochemical Processes, Gulf Publishing Company, Houston, 2/e, 2000
7. Waddams, A.L., Chemicals from Petroleum, Gulf Publishing Company, London, 4/e, 1980.
8. Mall, I.D., Petrochemical Process Technology, Macmillan India Limited, Delhi, 2007.
9. Meyers, R.A. (ed.), Handbook of Petrochemicals Production Processes, McGraw Hill, New York,
2005.
PK-491B: PROJECT
Techno-economic feasibility analysis, presentation and report.
FIRST YEAR
FIRST SEMESTER
AM 641: ADVANCE MATHEMATICS
Vector space matrix solution of ODE (IVP), partial differential equations. Sturm louiville
theory, separation of variables, Greens function, transform techniques, non linear equation,
continuous methods, bifurcation and Chaos Runge Kutta, multistep methods, Gears algorithm,
Finite difference, finite elements, shooting methods.
BOOKS
1. Sastry, S.S., Introductory Methods of Numerical Analysis, Prentice Hall of india Pvt. Ltd.,
1983.
PK 601: FLUID FLOW AND HEAT TRANSFER
Fluid flow phenomena, Equation of continuity and continuity and momentum transfer, Navier
Strokes equation and its solution to practical situation. Boundary layer theory, Von Karmann
theorem of integral momentum, Universal velocity profile. Turbulent boundary layer, Non
Newtonian Fluid Flow. Flow of two phase gas liquid mixture in pipes two phase two flow
model and governing equations, flow transition pressure drop calculation.
Forced Convection heat transfer, Introduction to compact heat exchanger employing extended
surfaces, heat transfer by conduction, heat transfer to solids in packed and moving / fluidized
beds. Heat transfer to boiling liquids, Pinch Technology and its application, concepts of energy
conservation and its application in process equipment.
BOOKS
1. F.A. Holland, Fluid Flow, Chemical Publishing Company, New York.
2. D. Butterworth & G.F. Hewitt, Two phase Flow and Heat Transfer, oxford university
Press, London
PK 602: PETROLEUM PROCESSING
Origin, occurrence, exploration, drilling & Production of Oil/ Gas Evaluation of oil, Petroleum
refining in India, Refinery tests and crude distillation column, catalytic reforming for Gasoline
upgrading and for aromatic production.
BOOKS
1. Speight, J.C.; The Chemistry and Technology of Petroleum, Marcel Dekkar, New York,
1991.
2. Ram Prasad , Petroleum Refining Technology , Khanna Publishers , Delhi 2000
3. Rao, B.K.B; Modern Petroleum Refining Processes, 4/e, 2002, Oxford and IBH Company
Pvt. Ltd.
4. G.D. Hobson, W. Pohl, Modern Petroleum Technology (Part I &II), John Wiley & Sons,
N.Y., 1986.
PK 603 DISTILLATION AND EXTRACTION
Thermodynamic equilibrium diagrams for binary and ternary system, analytical and graphical
methods of calculation in distillation and extraction design of extractors key components bubble
points and dew point, stage and extraction examples from petroleum refining, Azeotropic and
extractive distillation.
BOOKS
1. Henley E.L., J.D. Seeder, Equilibrium Stage separation operation in chemical engineering,
John Wiley
2. King C.J. Separation Process, TMH New Delhi (1962)
PK 611: ELECTIVE I
Modeling and Simulation of Separation Processes
Thermodynamics of separation Processes: Property Calculation from various models. Single
equilibrium stage and flash separation calculation. Modeling and separation cascades. Modeling
of batch distillation. Advanced topics in Multicomponent staged separation processes such as
distillation, absorption, extraction etc. Approximate (Shortcut) methods, rigorous methods, Rate
based models for distillation, enhanced distillation and supercritical extraction modeling of
membrane separation.
BOOKS
1. Smith B.D. Design of Equilibrium Stage Processes, McGraw Hill Book company, New York
(1985)
2. Holland C.D. and A.I. Liapis Computer Methods For Solving Dynamic Separation
Problems, McGraw Hill Book company, New York (1983)
3. Seader, J.D. and E.J. Henley, Separation Processes Principles, John Wiley and Sons Inc.
New York (1983)
impact or air, water noise and biological environment, socioeconomic environment method of
impact analysis.
BOOKS
1. M.N. Rao and HVN Rao Air Pollution Tata McGraw Hill Publication Co, Ltd. New Delhi
2. L.Hodges Environment Population (Halt) and Winston Inc. New York 1973.
3. S.H. Stroke and S.L. Seager, Environment Chemistry Air and Water Pollution (Scott
Foresman & Co. New York)
Petroleum Engineering
Overview of petroleum engineering including geological and geophysical aspects. Presentation
of the various stages of development of a petroleum reservoir including exploration drilling
reservoir rock & fluid production and processing highlight of the petroleum industries.
BOOKS
1. Nontechnical Guide to Petroleum Geology, Exploration, Drilling and Production, 2/e, 2001,
Penn Well Corporation, Oklahoma, USA.
2. The Petroleum Industry-A Nontechnical Guide, Charles F. Conaway, Penn Well
Corporation, Oklahoma, USA.
3. Modern Petroleum Technology , edited by Richard A. Dawe , Volume 1 , sixth edition , John
Wiley & Sons Limited , New York
SECOND SEMESTER
PK 604 PROCESS DYNAMICS & CONTROL
Development of dynamic models for physical system. Analysis of Pumped parameters system
using transfer function and state models response of multistage process. Analysis of industrial
system response of thermal and mass transfer methods with and without diffusion using exact
and transfer system methods Classical control methods for linear system stability and optimum
controller setting. Multiline loop multivariable feed forward, time optional and direct digital
process control. Introduction of computer control of petroleum and chemical process industries.
BOOKS
1. J.M. Douglas, Process Dynamics and control Vol I Analysis of Dynamic system Vol - II
Control System Synthesis, Prentice Hall (1972)
2. Donald R. Coughnowr and L.B. Koppel, Process System Anaysis and control, McGraw Hill
3. W.L. Luyben Process Modeling, Simulation and control for Chemical Engineers, McGraw
Hill Book Co. (1993)
4. John & Fredly, Dynamic Behavior of Process, Prentice Hall
J.M. Thomas and W.J. Thomas, Introduction to the Principles of Heterogeneous Catalyst,
Academic Press (1976).
J.M. Smith, Kinetics for Chemical Engineers, McGraw Hill 1981.
Kramer H. and Westertrap, Elements of Chemical Reactor Design and Analysis
Danbigh, K.C. and Turnar, J.CR Chemical Reactor Theory, University Press, Cambridge
BOOKS
1. Gas Production Engineering, Sanjay Kumar, Gulf Publishing Company Book Division,
London.
2. Natural Gas Engineering Production & Storage, Donald L. Katz, Robert L. Lee, Mc. Graw
Hill International Edition, New York.
3. Francis, S.M. and Thompson, R.E., Oil Field Processing of Petroleum, Volume one:
Natural Gas, Penn Well Books, Penn Well Publishing Company, Oklahoma.
SECOND YEAR
THIRD SEMESTER
PK-721: ELECTIVE-II
Petroleum Refinery Engineering
An overview to petroleum refining industry in India., distillation fractions and their quality control
Thermal Conversion processes, Thermal cracking, Visbreaking delayed & flexicoking. Catalytic
conversion processes, catalytic cracking, FCC,
catalytic reforming, Hydrocarcking, Hydrodesulphurization, Reside upgradation. etc.
BOOKS
1. Modern Petroleum Technology: G.D Hobson by. Who (Part I& II)
2. Petroleum reining Technology & Economics, J.H. Garry, G.E Handiwork, Marcel & Dekker
Inc. New York.
R&D evaluation and estimated material and energy balance equipment cost estimate waste study
flow diagram Plot Plans Planning and Scheduling the project.
Rheology and Testing of Polymers
Analysis and characterization of the flow of non-Newtonian fluids, Rheology measurements on
polymers and their interpretation viscoelasyiccoelastic material analysis of experimental data on and
characterization of viscoelastics material. Mechanical, thermal electrical and optical properties of
polymers and their evaluations.
Multiphase Reactors
Gas-liquid-solid catalytic and non-catalytic reacting systems Interaction of Physical and chemical
inter-and interparticle transport Development of Kinetic models. Isothermal systems Stability
criteria. Flow Modeling Hydrodynamic, deterministic and stochastic description. Evaluation of
Model parameters. Interfacial area Bubble/ Drop breakup, distributions, coalescence and dynamics.
Mixing and Fluid Agitation
Basic concepts of fluid mixing Impeller characteristics power correlation Pumping capacity of
impeller Mixing in agitated vessel scale up and operating characteristics of liquid mixing system
Heal and Mass transfer in agitated vessels Mixing Chemical reactions.
Advanced Mass Transfer
Molecular transport properties steady state diffusion Diffusitives in solids liquids gasses and
electrolytes. Interphase mass transfer mechanism multicomponent system Ordinary diffusion in
multicomponent system Convective Mass Transfer, in Laminar
flow Turbulent Flow. Hatta and Dankwerts models.
BOOKS
1. Hanley E.L.J.D. Seader, Equilibrium Stage Separable Separations in Chemical Equilibrium
John Wiley and Sons New York (1981).
2. Holland, C.D. Fundamentals of Multicomponent Distillations McGraw Hill Book Company New
York (1981).
3. Watking R.N. Petroleum refinery Distillations and Publishing Company Houston (1979).
4. King C.J. Separation Processes TMH New Delhi (1982), S. Skelland A.H.P. Diffusional Mass
transfer New York McGraw hill Book Company (1974).
Coal Conversion Process
Origin and Classification of Coal, Characteristics and industrial uses, Carbonization Processes Coke
areas by Product recovery systems liquid fuels from coal and tar. Theory of Gasification reaction,
Industrial gasification of Coal with oxygen and
steam.
BOOKS
1. Considine, D.M. Energy Technology Hand Book/ McGraw Hill Book Company, New York.
2. Sarkar S. Fuels and Combustion Second edition Orient Longman Ltd. Kamani Marg Ballard
Estate, Mumbai-400001
3. Lowenhien, F.A. and Moran, M.K. Industrial Chemicals, John Willey and Sons, New Delhi.
Heterogeneous Catalysts
Review of Chemical kinetics, Homogeneous acid catalysts heterogenic catalysts Physical and
chemical, surface area pore size and determination, reaction rates and selected diffusion in catalysts
polymerization in emulsions selection preparation and evaporation of catalysts.
BOOKS
1. J.W. Thomas and W.J. Thomas Introduction to the principles of heterogeneous catalysts
academic Press 1967.
2. C.N. sattereed and T.I. Sherwood The role of diffusion in catalysts Addition Wesley 1963.
Safety & Hazard Assessment of Hydrocarbon Plants
industrial Safety & Loss trends, Loss Prevention, Major Hazards, legislation law, Technologies for
hazard identification & assessment. Safety aspect of combustion, self heating, flame propagation,
limits of flammability, Explosion, detonation & deflagation, toxic materials, dosage, acute &
Chromic effects, Threshold limits, Instrumentation and Safety devices for temperature, flow, level
composition and pressure, plant layout, fabrication & Inspection, Operability Steady, Hazard
analysis, Safety effectiveness, Personal safety.
BOOKS
1. Frank P. Less, Loss Prevention in the process industry, Butter worth Heinmann.
2. Roy E. A Saders, Chemical Process Safety learning from case History, butter worth Heinamann.
3. Klctz, Trevor A, Critical Aspects of Safety & Loss Prevention, Butter worth London & Boston.
hybridomas, dynamics of mixed culture and unstable recombinant microbial strains plant and
animal tissue culture lines and bio transformation.
PK-612 / CE - 625 Air Pollution & Control
Classification and sources of air pollutants, Principles of meteorology and diffusion of pollutants, Dispersion models,
Theory and description of control devices and their applications, Sources and effects of noise pollution. Kinetics of
noise, Measurement and control of noise pollution.
THIRD SEMESTER
PK731
Elective- III
PK780P
General Seminar
PK791P
Lab/ Project
PK781P
FOURTH SEMESTER
PK782P
PK798P
Dissertation