Professional Documents
Culture Documents
ABSTRACT
The use of radioactive isotopes f o r analysis of fluid
movement within a well bore, a s well a s a review of
the various logging tools, materials, and techniques a r e
discussed in this paper.
Much valuable and pertinent inforination on downhole well problenls can be readily obtained by the proper
use of radioactive logging materials. This paper covers
the major use of isotopes, i.e., the detection of channels
l~ehindcasing, communication between zones, and in
plotting injection profiles. This type of application is
best referred to a s "fluid-movement analysis". Therefore, the isotope, by necessity, must be observed while
INTRODUCTION
G a n ~ n ~r aay detectors f o r use i n oil wells were developed in the late 1930's. Since then radioactive isotopes
have been applied in various manners in the attempt to
chart fluid nlovements within t h e well bore. A variety
of materials, tools, and techniques have been used in
tracer logging and most of the logging tools were satisfactory f o r their specific purpose. However, failure in
understanding the limitations and the improper use of
isotopes has resulted i n a g r e a t volume of erroneous
and misleading information. These errors have implanted a deep mistrust of all "tracer" logging operat i ~ n sin the minds of many people.
The emphasis on secondary-recovery operations, of
wvhich water injection constitutes the major portion, h a s
increased the need and demand f o r valid tracer logging
information. This validity is a direct function of the
knowledge and application of isotopes and detector tools.
Therefore, evers individual concerned with obtain in^
valid data' shoulcl thoroughly analyze the problems an:
become a s familiar a s possible with radioactive materials and detection tools before attempting to use them.
First, who can r u n these surveys? Many service companies, both large and small, offer these services i n
many and varied forms. The personnel doing the logging
and handling of the isotopes must be operating under a
current and valid Atomic Energy Comnlission license.
This means the logging operator must have been
schooled and tested in the basic concepts of nuclear and
atonlic structure, types of radioactive decay, reaction
of matter, health physics, racliation tolerances, preventive safeguards, and first aid f o r over-exposure. I n addi'Carcl~nal Che~mcal.Inc.. Odessa. Texas
?Cardinal Surveys Co., Odessa. Texas
Wresented a t the sgrlng n ~ e e t ~ nofg the Southwestern District. API
Division of Production, March 1964.
RADIOACTIVE MATERIAL
Isotopes to be used f o r surveys should be chosen with
consideration a s to their properties and limitations.
There is no "universal" tracer material t h a t can be
used in all instances. F o r example 1-131 in benzene o r
sylene carrier will not disperse in water. Potassiun~
iodide 1-131 in water solution will not perform properly
in oil. The conditions under wvhich the isotope is to be
used should be considered and made known to the service
company when t h e job is planned. Some factors to be
considered a r e temperature, type of fluid in the well,
acids, and various osidizing agents.
The yardstick f o r computing the length of time the
isotope will continue to emit radiation of measurable
intensity is its "half life". F o r example, 1-192 h a s a
half llfe of 74 clays which means t h a t the racliation
intensity decreases by 50 percent every 74 days. Wells
in which one expects to r u n a series of surveys should
not be subjected to materials of long life. This is particularly t r u e of particle-type o r plate-out materials.
Radiation from these isotopes interferes with f u t u r e
surrey operations f o r the life of the material. Table 1
describes the more commonly used isotopes.
WALLACEJOHNSON
AND BILLY P. MORRIS
142
Table 1
Commonly Used Isotopes
- -
Form
Isotope
Cobalt Co-GO
Solid-spherical particles
25 - 1,000 m i c r o n s i n
diameter
Cobalt Co-GO
Properties
Remarks
INSOLUBLES
5.3 years half life. Temperature
tolerance, 900 F. Gamma emitter
osidizes to radioactive sulfide residue. Half life long enough t o interfere with r a d i o a c t i v i t y l o g g i n g
operations f o r 21 to 26 years.
Cobalt Co-60
Silver Ag-110
270-day half life. Temperature tolerance, 950 F. High-intensity gamm a emitter. Osidizes to radioactive
sulfides. Interferes with radioactivi t y logging operations f o r 3 to 4
years.
Iridium Ir-192
V a r n i s h baked o n t o
Ottawa sand of selected
mesh size
74-day half life. Temperature tolerance, 2,454 F. Medium gamma emitter. Use in oil o r water. No interference with logging a f t e r 1 year.
Iridium 1-192
74-day half life. Temperature tolerance, 212 F in brine carrier. Unstable in oil a t 212 F.
--
Iodine 1-131
OIL SOLUBLES
-
Cobalt naphtenate in
benzene o r sylene carrier
5.3-year half life. High-energy emitter. Con~pletely oil-soluble. Insoluble in water. Stable to 300 F.
Iridium 1-192
Radioactive iridium in
benzene 'or sylene carrier
Iodine 1-131
Solution of elemental
iodine in benzene
Iodine 1-131
L i q u i d - p u r e i o dobenzene CoHiI
Cobalt Co-60
Table 1 (Cont'd)
soto ope
Form
Properties
W A T E R SOLUBLES
Remarks
Iridium Ir-192
Iodine 1-131 .
Radioiodine i n w a t e r
solution
I
Bromine Br-82
Iodine 1-131
Iodine 1-131
GAS TRACERS
Liquid m e t h y l iodide
( C H J ) in sealed glass
ampules
Low-boiling-point g a s tracer f o r
use a s above.
DETECTORS
The detector is one of the basic factors to be considered when planning tracer work. Since down-hole
conditions a r e variable, the effectiveness of the tools
will also vary.
The two most common detectors i n use today a r e t h e
geiger mueller tube and the scintillation crystal. The
scintillation detector crystal is usually sodium iodide
and is coupled optically with a light-sensitive amplifier
tube o r photo-multiplier. Gamma rays striking the
crystal will produce small light flashes t h a t a r e sensed
and amplified by t h e photo-multiplier. It h a s excellent
efficiency (approximately 85 percent) i n the detection
of small amounts of radiation and produces a goodquality correlation log f o r depth control and identification. The photo-multiplier is heat-sensitive and becomes
inoperative a t about 185 F, and requires careful handling to avoid shock damage. The scintillation detector
used i n small through-tubing tools cannot be refrigerated a s is possible i n large-diameter casing type tools.
This 185-deg temperature limit is not a problem in most
water-injection wells. Also, i t does not become a problenl
in producing wells until extreme depths a r e reached in
the Permian Basin.
The geiger mueller tube, which is used in most
through-tubing o r tracer tools, is more rugged. It is
heat-resistant to 350 F , but h a s a low resolution efficiency of 10 to 1 3 percent. This means t h a t i t produces
poor-quality correlation logs. The efficiency can be im-
AND
0C
GAMMA
IONIZING
BUTTON
CAPSUL
RUPTURE
EJECTOR
SOLENOID
PLUNGER
WELL
PRESSURE
PISTON
DISPLACEMENT
a. 1onlxin.g "bz~tton"
A cobalt "button" is attached t o the tool above the
detector. T h e "button" is ionized b y an electrical
current, thereby releasing some radioactive material into the fluid stream.
b. Cnpslcle rziptztre -single a,nd dolcble detector
Several sinall ampules o f radioactive material are
positioned on the tool above the detector. These
are ruptured at will b y an electrical current and
the material released into the well stream.
c. E j c c t o r cylinders - single a d doz~bledetector
This type tool has a cylinder which can be filled
with liquid radioactive material. This material
can be ejected into the fluicl stream b y actuating
an ejector.
There are three types o f ejectors presently i n use: 1,
the solenoid plunger; 2, well-pressure-operated ; and 3,
positive piston displacement. All these types vary i n the
amount o f fluid the cylinder will hold. They also vary
i n the amount o f material that can be ejected at a
single time. W i t h some tools i t is possible t o make the
ejections vary in strength and amount while it is fixed
with others.
W E L L EQUIPMENT
A s with other survey work, the well equipment must
be considered. Injection profiles being the most co~nmoii
application, a typical injection-well arrangement is
shown in Fig. 2. This ideal arrangement is satisfactory
for all work escept for the isotope interface survey
which requires tubing t o the bottom o f the well and no
packer. T h e well head sliould permit the tool t o be run
into the well without altering the injection rate or pressure in any manner. It is also very desirable t o have
the tubing and packer set high enough above the top
perforation or casing seat t o permit tlie location o f at
least two casing collars. In addition, locating a channel
behincl the casing is much more positive when working
below the packer. Channel determination above a packer
becomes very uncertain and confusing.
Prior t o any injection-profile survey the well head
should be esamined for hycl~anlicnipples, bent subs,
BILLYP. MORRIS
STABILIZATION
Stabilization o f injection is o f the utmost iinportance
in injection-profile surveys and i t cannot be over-emphasized. N o t l ~ . i ~ zshould
g
be clone t o the well t o interrupt or
alter the injection rate or pressure for at least 24 hours
prior to running an injection-profile survey. In most
cases it is virtually impossible t o detect unstable clownhole injection with tracer tools.
T o illustrate the point, several examples o f erratic
down-hole fluid behavior are shown. Erratic down-hole
SO'
Fig. 4
- Change
AND
BILLYP. MORRIS
SURFACE S L U G
H O V E TOOL 1 0
P O I 1 1 1 0 , "A"
PASSES TOOL
I0
7 1 M t AS SLUG
MOVE TOOL TO
P O 5 1 T l O t i "C"
1 I - E AS SLUG
P A S S E S TOOL
P O 5 1 T l o t i "D"
T I M E I S SLUG
Fig. 8
DUMP BAILER
- Controlled-interval
Log
148
WALLACE
JOHNSONAND BILLYP. MORRIS
1 1
1 1 1
VELOCITY
SHOT
150
WALLACE
JOHNSON AND BILLYP. MORRIS
ft, and "D" 4,995-5,002 f t ) . There is negligible
spreading of material for two reasons: I , the material is soluble and completely miscible in water;
and 2, the tool is smooth-and without traps.
2
d,
.u
BOTTOM DET.
Fig. 15
cannot be determined whether i t is a channel or
not.
e. Approximate rate-volume calculations based upon
slug travel down hole indicate: 495 BWPD leaving the casing a t or near the top perforation, 75
BWPD leaving the middle set of pel-forations, 170
BWPD leaving near the top of the lower set of
perforations, and the remainder moving down hole
to 5,108 ft-probably
outside the casing.
6. Check the 100-percent injection rate again (ejector
a t 5,002.5 f t ) to make certain t h a t the rate h a s not
changed. The first slug has indicated t h a t a rather
detailed procedure will be necessary to make a complete fluid movement analysis. This Slug No. 2 is not
illustrated.
7. Identify channel a t bottom perforations (Fig. 15).
Tool is positioned a s shown with ejector a t 5,095 f t
which is immediately above the bottom perforation.
Slug No. 3 is ejected and monitored on time drive.
Reaction occurs on bottom detector and no reaction on
the top detector. This indicates fluid moving down,
probably outside the pipe. Note logging runs No. 9
through 11 again show material a s low a s 5,108 ft.
8. Ejector is positioned below l~ottomperforation (Fig.
16). Slug No. 4 is ejectecl and monitored on time
drive. No reaction occurs on either detector. Logging
runs No. 12 and 13 a t 5-min intervals show slug remaining static a t 5,100 ft. This procedure proves
II
SLUO NO. 4
E S S HRS. EJECTOR 5101
Fig. 16
II
Fig. 18
The i?zjectlo?z pvofile is determined a s follows:
a. 185 BWPD leaving the perforations a t 5,096 f t
a s indicated by velocity shot (slug No. 9). The
injection zone behind the pipe is indicated by
slugs No. 3 and 4. This material is approximately
5,106-5,108 ft.
Fig. 17
12. Check f o r channel from top perforation (Fig. 20).
Slug No. 1 did not clearly define the top of the
channel. Tool is positioned a s shown and h e a v y
slug No. 8 is ejected. Note reaction times on both
detectors-the material moves behind the casing a t
a more rapid r a t e u p outside the pipe than downward inside the pipe.
Logging runs 22 through 24 also indicate a highvelocity channel to 4,994 f t ; also a n apparent zone
of injection between 5,014-5,018 ft.
13. All the preceding work h a s defined all channels and
zones of r a t e changes. Velocity measurements must
be made above and below zones where r a t e changes
occur. Measurelnents made in a zone of r a t e change
a r e of little value. Five velocity shots a r e made and
recorded a s shown in Fig. 21.
Fig. 19
154
TIY
DRIVE
*:4l.m
Mas
Fig. 20
TIME D R I V E MONITORS
V E L O C I T Y CHECKS IhSlDE PIPE
S L U G NO. 9
S L U B NO. ll
Yo
19 SEC.
46 S E C
SLUG
N Q 10
Fig. 21
SLUG N Q I3
S L U G NO. 12
CONCLUSION
Tracer logging can be extremely reliable i n diagnosing well problems when properly utilized b y trained
personnel. T w o types o f problems outlined i n the preceding esamples are indicative of the information
obtainable f r o m tracer logs.
In planning a tracer-logging operation, the conlpany
engineer has a considerably more involved task than
he has i n planning a primary-logging operation. First,
he must consider the physical equipment of the well t o
be certain it will accommodate the logging tools. N e s t
he should be thoroughly familiar w i t h the reservoir
conditions, injection rates and pressures and the iaformation on lithology, porosity, and permeability as
reflected b y pertinent primary logs. Also, he should
determine what specific information is desired from
tracer logs. T h e n the company engineer should consult
with the logging engineer and discuss the foregoing
factors before a proper isotope can be selected and
correct tools and techniques be used t o adequately collect
and evaluate tracer-logging data.
A f e w basic rules for successful tracer logging can be
stated as follows: 1 , Have masimuln control over fluid
movement; 2, reduce variables t o a minimum ; 3, avoid
use o f compressible gases; 4, use isotopes of short half
l i f e ; 5, use only miscible isotopes that are compatible
with we!l fluids t o avoid plate-out or settling; 6 , observe
the isotope i n transit; 7, carefully note clock times o f
each r u n or operation; 8, let each logging operation set
the stage for following operations; and 9, double check
each operation i f possible.
W h e n a trained logging engineer and a company representative confer on location as t o what information
is desired and what data have been obtained as the logging job progresses, a complete picture as presented b y
tracer logging can usually be obtained and a preliminary
interpretation afforded b y the time the well logging
has been completed. I n this manner rapid planning o f
any necessary remedial work on the well can be
accoinpllshed.