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Asphalt Additives
Feipeng Xiao1*, Ph.D., P.E., Wenbin Zhao2, and Serji N. Amirkhanian3, Ph.D.
1
Research Assistant Professor, Asphalt Rubber Technology Service, Department of Civil
Engineering, Clemson University, Clemson, SC 29634-0911 U.S.A., Tel: 001-864-6566799,
Fax: 001-864-6566186, E-mail: feipenx@clemson.edu
2
Graduate Research Assistant, Department of Civil Engineering, Clemson University, Clemson,
SC 29634-0911
3
Professor, Department of Civil Engineering, Clemson University, Clemson, SC 29634-0911
ABSTRACT:
The long-term performance of pavement is associated with various factors such as pavement
structure, materials, traffic loading, and environmental conditions. Improving the understanding
of the fatigue behavior of the specific rubberized warm mix asphalt (WMA) is helpful in
recycling the scrap tires and saving energy. This study explores the utilization of the
conventional fatigue analysis approach in investigating the fatigue life of rubberized asphalt
concrete mixtures containing the WMA additive. The fatigue beams were made with one rubber
type (-40 mesh ambient crumb rubber), two aggregate sources, two WMA additives
(Asphamin® and Sasobit®), and tested at 20ºC. A total of 8 mixtures were performed and 29
fatigue beams were tested in this study. The test results indicated that the addition of crumb
rubber and WMA additive not only reduced the mixing and compaction temperatures of
rubberized asphalt mixtures offset by crumb rubber but also effectively extended the long-term
performance of pavement when compared with conventional asphalt pavement. In addition, the
exponential function forms are efficient in achieving the correlations between the dissipated
energy and load cycle as well as mixture stiffness and load cycle.
Keywords: Rubberized asphalt concrete; Warm asphalt additive; Mixing and compaction
temperature; Stiffness; Dissipated energy; Fatigue Life.
*: Corresponding author
Xiao et al. (2008)
INTRODUCTION
Fatigue cracking, called alligator cracking and associated with repetitive traffic loading, is
considered to be one of the most significant distress modes in flexible pavements. The fatigue
life of an asphalt pavement is directly related to various engineering properties of a typical hot
mix asphalt (HMA). The complicated microstructure of asphalt concrete is related to the
gradation of aggregate, the properties of aggregate-binder interface, the void size distribution,
and the interconnectivity of voids. As a result, the fatigue property of asphalt mixtures is very
Understanding the ability of an asphalt pavement to resist fractures from repeated loading
condition is essential for developing superior HMA pavement designs. Previous studies have
been conducted to understand the occurrence of fatigue and how to extend pavement life under
repetitive traffic loading (3-4). However, reaching a better understanding of fatigue behavior of
The recycling of scrap tires has been of interest to the domestic and international asphalt
industry for over 40 years. The utilization of crumb rubber modifier (CRM) in asphalt binders
has proven to be beneficial from many stand points. The use of CRM, expanded to HMA,
continues to evolve since the CRM binders enhance the performance of asphalt mixtures by
increasing the resistance of the pavements to permanent deformation and thermal and fatigue
cracking. Many researchers have found that utilizing crumb rubber in pavement construction is
Recently, the “warm mix asphalt” (WMA) is widely being used in the hot HMA industry as
a mean of reducing energy requirements and lowering emissions. WMA can significantly reduce
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Xiao et al. (2008)
the mixing and compacting temperatures of asphalt mixtures, by either lowering the viscosity of
asphalt binders, or causing foaming in the binders. Reduced mixing and paving temperatures
decreases the energy required to produce HMA, reduces emissions and odors from plants, and
makes for better working conditions at both the plant and the paving site (10-15).
However, the influence of crumb rubber and WMA additives mixed with virgin mixtures
together has not yet been identified clearly. The interaction of modified mixtures is not well
understood from the standpoint of binder properties and field performance. It has been shown
that the WMA additives reduce the mixing and compaction temperatures and achieve ideal
workability of HMA without significantly affecting the engineering properties of the mixtures
(10-13). While the addition of crumb rubber increases the demand of asphalt binder and
increases the mixing and compacting temperatures, it is helpful in resisting the high temperature
deformation and extending the long-term performance of HMA. Because of the complicated
relationships of these two materials in the modified mixtures, detailed information will be
beneficial to help obtain an optimum balance in the use of these materials. Very few fatigue
studies of modified asphalt mixtures, including crumb rubber and warm asphalt additives, have
been performed in recent years (16). However, the utilization of these materials will enable the
engineers to find an environmentally friendly method to deal with these materials, save money,
The objective of this study was to gain an improved understanding in the long-term
containing WMA additives through a series of experimental tests. Experiments were carried out
to evaluate rheological properties of the modified binder (unaged and aged binders) as well as
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Xiao et al. (2008)
the engineering properties of the mixture, such as the stiffness and fatigue life performed by
BACKGROUND
between the initial stress or strain and the number of load repetitions to failure-determined by
using repeated flexure, direct tension, or diametral tests performed at several stress or strain
levels. The fatigue behavior of a specific mixture, characterized by the slope and relative level of
the stress or strain versus the number of load repetitions to failure, may be defined using the
N f a(1 / 0 ) b (1 / S 0 ) c or N f a (1 / 0 ) b (1 / S 0 ) c (1)
Where N f = number of load application or crack initiation, 0 , 0 = tensile strain and stress,
In recent years, several researchers have used the energy approach for predicting the fatigue
behavior of the asphalt mixtures. The dissipated energy per cycle, Wi, for a linearly viscoelastic
n n
W Wi i i sin( i ) (2)
i 1 i 1
i = stress amplitude at load cycle i, i = strain amplitude at load cycle i, and i = phase
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Xiao et al. (2008)
Research has shown that the dissipated energy approach makes it possible to predict the
fatigue behavior of mixtures in the laboratory over a wide range of conditions based on the
results of a few simple fatigue tests. Such a relationship can be characterized in the form of the
W A (N f )Z (3)
Materials
One virgin binder (PG 64-22) and one crumb rubber modified (CRM) binder (PG 64-22 +
10% -40 mesh rubber) were used in this study. The PG 64-22 binder was a mixture of several
sources that could not be identified by the supplier. One type of rubber, -40 mesh ambient rubber,
was used in this study. Previous research and field projects conducted in South Carolina
indicated that the -40 mesh ambient rubber is effective in improving the engineering properties
of rubberized mixtures.
Asphamin® and Sasobit® were used in this study as two WMA additives. Aspha-min® is
contains approximately 21% crystalline water by weight. By adding it to an asphalt mix, the fine
water spray is created as all the crystalline water is released, which results in volume expansion
in the binder, therefore increasing the workability and compactability of the mix at lower
temperatures. Sasobit® is a long chain of aliphatic hydrocarbons obtained from coal gasification
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Xiao et al. (2008)
using the Fischer-Tropsch process. After crystallization, it forms a lattice structure in the binder
which is the basis of the structural stability of the binder containing Sasobit® (10-11).
Two aggregate sources (A and B) were used for preparing the samples (Table 1). Aggregate
aggregate B (schist) is a metamorphic rock. Hydrated lime, used as an anti-strip additive, was
added at a rate of 1% by dry mass of aggregate. A total number of eight mixtures were evaluated
in this research. In this paper, the mixtures made from aggregates A and B without rubber and
WMA additive are referred to as ACO and BCO; and the mixtures with rubber but no WMA
additive are referred to as ARO and BRO. In addition, the mixtures with rubber and Asphamin®
are designated as ARA and BRA, and the mixtures with rubber and Sasobit® are labeled as ARS
The combined aggregate gradations for the 12.5 mm mixtures were selected in accordance
with the specification set by the South Carolina Department of Transportation (SCDOT). The
gradations for each aggregate source (A and B) are shown in Figure 1, which shows that the
design aggregate gradations for each aggregate source are the same when using different WMA
additives (Asphamin® and Sasobit® ) at the same percentages of rubber (0% or 10% rubber),
while the gradations are similar when comparing mixtures from both aggregate sources.
Superpave mix design defines that the laboratory mixing and compaction temperatures can
be determined by using a plot of viscosity versus temperature. While there are no previous
specifications available regarding the mixing and compaction temperatures for rubberized
mixture containing WMA additives, some researchers have developed guidelines for mixing and
6
Xiao et al. (2008)
compaction temperatures when using either WMA or rubber (10-11, 23-24). The temperatures,
shown in Table 3, were determined in accordance with previous research projects (16, 24).
Though the mixing and compaction temperatures increase as the percentage of crumb rubber
Fatigue beams were made in the laboratory and two-four beams of each mixture were tested
for this study (Figure 2). All tests were performed in a temperature-controlled chamber at 20 ±
0.5°C. In this study, a repeated sinusoidal loading at a frequency of 10 Hz was used; in addition,
the controlled strain mode was employed. The control and data acquisition software measured
the deflection of the beam specimen, computed the strain in the specimen and adjusted the load
The test apparatus also recorded load cycles, applied load, and beam deflections. Failure is
assumed to occur when the stiffness reaches half of its initial value, which is determined from
the load at approximately 50 repetitions; the test is terminated automatically when this load has
diminished by 50 percent. The flexural stiffness and dissipated energy of fatigue beam are
aP(3l 2 4a 2 )
S / (4)
4bh3
Where, = tensile stress, in Pa; = maximum tensile stain, in m/m; P = applied peak-
to-peak load, in Newton; a = space between inside clamps, in meters; b = average beam
width, in meters; h = average beam height, in meters; Δ= beam deflection at neutral axis,
7
Xiao et al. (2008)
Where, f = load frequency, in Hz; and = time lag between Pmax and max , in second
i n
W= Di (6)
i 1
Statistical considerations
Results of the stiffness, cumulative dissipated energy, and fatigue life values were
statistically analyzed with 5% level of significance (0.05 probability of a Type I error) with
respect to the effects of aggregate sources and WMA additive types. For these comparisons, it
should be noted that all specimens were produced at optimum binder content.
Binder analysis
Table 3 shows that the viscosity of rubberized asphalt binder decreases while the high
temperature performance (G*/sinδ) of overall binders increase with the addition of WMA
additive. The unaged binder test result shows that the Asphamin® and Sasobit® can improve
the workability (viscosity) and rutting resistance (G*/sinδ) of mixtures. While the aged
rubberized binders show that the G*sinδ values decrease with the addition of rubber, these values
increase slightly as the WMA additives are added. It also can be seen that the stiffness values of
binders have similar trends with G*sinδ values due to the addition of these materials. Aged
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Xiao et al. (2008)
binder properties show that the WMA additives produce a slightly effect on the long-term
Testing data were analyzed using Equations 4-6 presented earlier to compute the stress,
strain, stiffness, phase angle, the dissipated energy per cycle as the function of the number of
load cycles, and the cumulative dissipated energy to a given load cycle. In this study, fatigue life
was defined as the number of repeated cycles corresponding to a 50 percent reduction in initial
stiffness, which was measured at the 50th load cycle. Several fatigue beam specimens were
utilized to characterize the fatigue behavior of a mixture in order to avoid too much or too little
loss in stiffness. This procedure involved testing control specimens (ACO and BCO samples) at
a 500 micro strain level with the controlled strain mode of loading at a frequency of 10 Hz.
Table 4 presents a typical analyzed fatigue test results which were computed at various
cycles from the raw data. It can be seen that the stress value and dissipated energy per cycle
generally decrease as the number of cycle increases. That is, at the same strain level, the greater
stress is needed to reach the desired strain values at the beginning of fatigue test than at the end
of the test. At the same time, the dissipated energy per cycle during the first thousands of cycles
is remarkably greater than those during the final cycles (50% loss of initial stiffness). As
expected, the asphalt pavement in the field rapidly releases the potential energy within the first
several years, followed by the further reduction of pavement performance caused by micro-
cracking under repeated traffic loading conditions. Previous research also presents this similar
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Xiao et al. (2008)
The test results presented in Figure 3(a) show that the fatigue life of fatigue beams made
from aggregate A has a greater value than those made from aggregate B, though the aggregate B
has a lower LA abrasion loss and absorption values. Conversely, the standard deviations of the
fatigue test results for each mixture are large since the variability of fatigue life is generally
based upon the micro-structure of beams (e.g. the aggregate-binder interface, the void size
distribution, the interconnectivity of voids, distribution of aggregate particles, film thickness and
the aged status of binder). Through previous research, which also determined that large
variabilities exist in the fatigue test results, the authors found that increasing the number of the
repeated specimens reduced the variability (24). Moreover, in comparison with the control
fatigue beam (without rubber and WMA additive), the rubberized fatigue beam without WMA
additive or with Sasobit® additive has a slightly greater fatigue life while the rubberized fatigue
beam with Asphamin® additive has a slightly lower fatigue life, regardless of aggregate sources.
Figure 3(a) shows that the addition of crumb rubber and/or Sasobit® slightly benefits the long-
term performance of asphalt pavement while the Asphamin® results in a slight decrease of the
fatigue life, though these additives are critical in reducing the mixing and compaction
temperatures of mixture. In addition, the statistical analysis (t-statistics) in Table 5 indicates that,
with respect to the effect of aggregate source, there is a significant different fatigue life value
between any two aggregate sources regardless of mix types. As shown in Table 6, the influence
of a WMA additive on the fatigue life is generally not significant (p-value > 0.05) for overall
mixtures
The flexural stiffness of an asphalt pavement, associated with repetitive traffic loading
and pavement thickness, is related to the various aspects of HMA, such as rutting, resilient
modulus, and fatigue life. In this study, the fatigue beams were made with a height of
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Xiao et al. (2008)
approximate 50 mm and the values were competed from Equation (3), defined as the ratio of
tensile stress-to-tensile strain. The test results shown in Figure 3(b) show that the aggregate A
mixture has greater stiffness values since under the repeated loading the induced micro-strain of
the mixture from aggregate A is smaller. This greater stiffness may be the result of different
aggregate sources producing different interfaces among the binder, voids, and aggregate, thus,
affecting the corresponding fatigue behavior of the pavement. Previous research indicates that
while the initial stiffness of rubberized mixture is less than the conventional mixture (19), the
initial stiffness values of mixtures in this study showed no obvious trend when the additional
crumb rubber and WMA additive were blended together. Moreover, the statistical analysis in
Tables 5 and 6 indicates that aggregate source has a significant influence on the stiffness values
generally while the effects of rubber and WMA additive is not significant for all four types of
mixtures.
The dissipated energy, computed from Equations 5 and 6 was used as an indicator of
fatigue cracking in the asphalt layer (19-22). As shown in Figure 3(c), the cumulative dissipated
energy of mixture made from aggregate B is slightly higher than that of mixture from aggregate
A. However, the statistical results in Table 5 indicate that, except for the mixture with Sasobit
additive, other mixtures from two aggregate sources have no significant different cumulative
dissipated energy values. With respect to the effect of rubber and WMA additive, Table 6 shows
that there is a significant different value between control and rubberized mixture in general, but
the influence of WMA additive on cumulative dissipated energy is not significant for all
rubberized mixture.
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Xiao et al. (2008)
G*sinδ, strongly associated with fatigue life of the mixture, has become a basic parameter
used to describe fatigue characteristics of asphalt binder. Thus, the study of G*sinδ is beneficial
for researchers and engineers to analyze fatigue behavior of asphalt pavements. Table 3 indicates
the effect of rubber and WMA additive on G*sinδ of binder. In Figure 4(a), it can been seen that
the fatigue life decreases remarkably with a corresponding increase of G*sinδ regardless of
aggregate source. Figure 4 indicates that the binder aging process, for the materials used in this
research, does shorten the fatigue life of asphalt pavement. However, the addition of crumb
The correlations between the stiffness of the beam and binder are shown in Figure 4(b).
Similar to Figure 4(a), it can be seen that the stiffness values of the beam do not have a large
alteration with an increase in binder stiffness. Table 3 shows that the rubberized binders have
lower stiffness values than original asphalt binder. However, the stiffness values of the
rubberized mixture do not exhibit a similar trend. In addition, as shown in Figure 4(b), two
aggregate sources also show the different effects on mixture stiffness in terms of binder stiffness
in this study.
AASHTO T321 assumes that the fatigue life depends on the accumulation of dissipated
energy from each load cycle. Thus, the dissipated energy may be plotted against load cycles for
the particular load cycles where the data was collected. As shown in Figure 5, the correlations
between the dissipated energy per cycles with load cycles indicate that the dissipated energy
increases at a negative exponential growth as the number of load cycles increase, in other words,
the dissipated energy decreases insignificantly initially and then it reduces rapid prior to reaching
the 50% stiffness. For example, as shown in Figure 5(a), the dissipated energy of three fatigue
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Xiao et al. (2008)
beams exhibits a slightly decrease before the number of the repeated loads is less than 10,000
cycles, after that, the dissipated energy decreases quickly until the final load cycle accomplishes.
Figure 5 indicates that the individual fatigue beam from each mixture has different
dissipated energy values per load cycle, regardless of the mixture types (i.e. ACO, ARO, etc) and
these values are greater when using aggregate B. The results in Figure 5 also show that the
crumb rubber and WMA additive do not affect the dissipated energy per cycle.
The initial stiffness of fatigue beam, determined by the initial tensile stress and strain, can
be plotted using stiffness (S) against load cycles (n) and best fitting the data to exponential
S A ebn (7)
coefficients.
As shown in Figure 6, it can be noted that, in most cases, the stiffness values of various fatigue
beams from same mixture present similar results, and the mixture from aggregate B has a greater
stiffness value. However, the addition of crumb rubber and WMA additive do not exhibit a
The correlations between the repetition number of fatigue beam and cumulative
dissipated energy are shown in Figure 7(a). Although these two linear models can be used to
determine the predicted values, it was hard to obtain accurate results due to the limited test
specimens and variability of materials. Similarly, as shown in Figure 7(b), the loss of stiffness
under repeated loading, as expected, is also related to the cumulative dissipated energy though
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Xiao et al. (2008)
CONCLUSIONS
The following conclusions were determined based upon the limited experimental data
presented regarding the fatigue life of the modified binder and mixtures for the materials tested
The combination of the crumb rubber and WMA additive in asphalt binder is beneficial
for improving the rheological properties of both the unaged and aged binders (e.g.
increase G*sin δ and reduce G*/sin δ values), The increase in the mixing and
compaction temperatures due to the addition of crumb rubber can be offset by adding the
warm asphalt additives, which lowers the mixing and compaction temperatures of
The experimental results indicated that fatigue life and stiffness of the rubberized WMA
mixture from aggregate A is greater than aggregate B while the cumulative dissipated
energy of mixtures made from aggregate A is slightly lower. Moreover, the fatigue life
of the mixtures made with crumb rubber and WMA additive is greater than the control
mixtures (no rubber and WMA additive), except the mixtures containing Asphamin®
additive.
Statistical analysis results illustrated that there are no significant differences in the
stiffness and cumulative dissipated energy values for overall mixtures (control,
rubberized, or WMA mixtures) while fatigue life values from control mixtures are
presented the aggregate sources play a key role in determining fatigue life, stiffness and
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Xiao et al. (2008)
There are good correlations between the fatigue life and G*sin δ as well as mixture and
binder stiffness values. The exponential function forms are efficient in achieving the
correlations between the dissipated energy and load cycle as well as mixture stiffness
ACKNOWLEDGMENTS
Control (SC DHEC) is greatly appreciated. However, the results and opinions presented in this
paper do not necessarily reflect the view and policy of the SC DHEC.
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Xiao et al. (2008)
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19
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100
80
40
Agg. A
20 Agg. B
Low Range
Up Range
0
0.075 0.15 0.60 2.36 4.75 9.5 12.5 19.0
Sieve size (mm)
20
Xiao et al. (2008)
21
Xiao et al. (2008)
800000
8x10 5
Aggregate A Aggregate B
600000
400000
4x10 5
2x10 5
200000
00
CO RO RA RS
Mixture type
(a)
2.0x10 7
20000000
Aggregate A Aggregate B
1.5x10 7
15000000
Stiffness (kPa)
1.0x10 7
10000000
5000000
0.5x10 7
00
CO RO RA RS
Mixture type
(b)
1,000
Cumulative dissipated energy (J/m 3 )
Aggregate A Aggregate B
800
600
400
200
0
CO RO RA RS
Mixture type
(c)
Figure 3 Mechanical properties (a) Fatigue life; (b) Stiffness; (c) cumulative energy
22
Xiao et al. (2008)
1000000
10 6
100000
10 5
10 3 y A = -141.59x + 562241
1000
y B = -19.604x + 96617
100
10 2
10
10
Aggregate A Aggregate B
10
1000 2000 3000 4000
G*sinδ (kPa)
(a)
100000000
10 8
Stiffness (kPa)
10000000
10 7
y A = 4095.5x + 8E+06
10 6
1000000 y B = -15759x + 2E+07
Aggregate A Aggregate B
100000
10 5
100 150 200 250
Binder stiffness (MPa)
(b)
Figure 4 Correlations, (a) fatigue life and G*sinδ; (b) mixture stiffnes and binder stiffness
23
Xiao et al. (2008)
Figure 5 Dissipated energy versus load cycles (repeatition) (a),(e) control beam (aggregate A
and B); (b),(f) rubberized beam (aggregate A and B); (c),(g) rubberized Asphamin® beam
(aggregate A and B); (d),(h) rubberized Sasobit® beam (aggregate A and B)
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Xiao et al. (2008)
10 8
1.0E+08 10 8
1.0E+08 10 8
1.0E+08 10 8
1.0E+08
y A = 9E+06e-6E-06x y A = 9E+06e-6E-06x y A = 9E+06e-5E-06x y A = 1E+07e-3E-06x
y B = 8E+06e -5E-06x
y B = 8E+06e-4E-06x y B = 8E+06e-7E-06x y B = 9E+06e-5E-06x
y C = 8E+06e-1E-06x
Stiffness (kPa)
Stiffness (kPa)
Stiffness (kPa)
Stiffness (kPa)
y C = 8E+06e-2E-06x
y D = 9E+06e-6E-06x
10 7
1.0E+07 10 7
1.0E+07 10 7
1.0E+07 10 7
1.0E+07
ARO-A
ACO-A ARO-B
ACO-B ARO-C
ARO-D ARA-A ARA-B ARS-A ARS-B
ACO-C
10 6
1.0E+06 10 6
1.0E+06 10 6
1.0E+06 10 6
1.0E+06
10 10 2 10 4 100000 10 6
10 10
10 2
100 1000 10 4 100000
10 3 10000 10 6
10 5 1000000 10
10 10 2
100 1000 10 4 100000
10 3 10000 10 6
10 5 1000000 10 10
10 2
100 1000 10 4 100000
10 3 10000 10 6
10 5 1000000 10 10 3 10000
100 1000 10 5 1000000
Cycles Cycles Cycles Cycles
Stiffness (kPa)
Stiffness (kPa)
Stiffness (kPa)
Stiffness (kPa)
y D = 2E+07e-3E-05x
10 7
1.0E+07 10 7
1.0E+07 10 7
1.0E+07 10 7
1.0E+07
BRO-A
BRO-B
BRO-C
BCO-A BCO-B BRO-D BRA-A BRA-B BRS-A BRS-B
10 6
1.0E+06 10 6
1.0E+06 10 6
1.0E+06 10 6
1.0E+06
2
10 10100 10 4 10000 10 6
10 10 31000 10 5 100000 10 10
10 2
100 1000 10 4 100000
10 3 10000 10 6
10 5 1000000 10 2
10 10100 10 4 10000
10 31000 10 6
10 5 100000 10 10
10 2
100 1000 10 4 100000
10 3 10000 10 6
10 5 1000000
Cycles Cycles Cycles Cycles
25
Xiao et al. (2008)
1000000
10 6
Repetition (cycle)
100000
10 5
10000
10 4 y A = 63.372x + 243145
y B = 163.28x - 40713
Aggregate A Aggregate B
10 3
1000
100 600 1100
Cumulative disspated energy (J/m 3 )
(a)
100000007
10
Loss of stiffness (kPa)
1000000
10 6
y A = 11.92x + 7E+06
y B = 2121.7x + 3E+06
Aggregate A Aggregate B
100000
10 5
100 600 1100
Cumulative dissipated energy (J/m 3 )
(b)
Figure 7 Cumulative dissipated energy versus (a) repetition and (b) stiffness
26