Professional Documents
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Rev. F
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NOTE: Fann reserves the right to make improvements in design, construction and appearance of our products without prior notice.
Fann Instrument Company PO Box 4350 Houston, Texas USA 77210 Telephone: 281- 871-4482 Toll Free: 800-347-0450 Fax: 281- 871-4358
TABLE OF CONTENTS
SECTION
PAGE
1 2 3 4 5 6 7
Description ............................................................................................................................................................ 1 Safety Considerations .......................................................................................................................................... 2 Filter Press Pressure Sources ............................................................................................................................. 4 Standard Filter Press Test Procedures ............................................................................................................... 9 FREAD Filter Press Test Procedures ................................................................................................................11 Care of Equipment..............................................................................................................................................13 Parts List .............................................................................................................................................................15
FIGURES
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1 2 3 4 5 6 7 8 9
CO2 Cartridge Holder Assembly .......................................................................................................................... 3 No. 207223 - Filter Press with Nitrogen Cylinder (Pressure Source) ................................................................. 4 No. 207290 - Dead-Weight Hydraulic Filter Press .............................................................................................. 6 No. 208594 - Dead Weight Hydraulic Assembly ................................................................................................. 6 No. 208647 - CO2 Pressure Assembly,Exploded View ...................................................................................... 7 No. 208652 - Pressure Regulator Assembly ....................................................................................................... 8 Filter Press and Cell Assembly, Exploded View ...............................................................................................10 Filtration Reduction Evaluation Device-(FREAD)..............................................................................................12 No. 207127 - Filter Press, Standard Frame.......................................................................................................14
10 No. 207174 - Filter Press, Standard Frame w/Regulator ..................................................................................16 11 No. 207224 - Filter Press w/CO2 .......................................................................................................................17 12 No. 207503 - Filter press Wall Mount Frame w/CO2 ........................................................................................20 13 No. 207356 - Filter Press, Wall Mount in Case .................................................................................................21 14 No. 207673 - Filter Press Six-Cell with Manifold ...............................................................................................23 15 No. 208648 - CO2 Pressure Assembly with Top Cap.......................................................................................25
SECTION 1 DESCRIPTION
Filtration and wall-building properties of drilling fluids and cement slurries are determined by a filter press. The 3 filtration rate is a measure of fluid loss measured in milliliters [1 milliliter (ml) = 1 cubic centimeter (cm )] under 100 pounds per square inch (psi) (690 kPa) of pressure through a special filter paper for 30 minutes. Wall-building characteristics are demonstrated by the thickness and consistency of the filter cake (the residue) deposited on the filter paper at the end of this period. The filter cake is measured to the closest 1/32" (0.8 mm). The low pressure filter press assemblies described in this booklet consists of a filter cell mounted in a frame, a pressure source, a filtering medium, and a graduated cylinder for receiving and measuring the filtrate. The filter cell, or drilling fluid cell, is constructed of rustproof anodized aluminum and chrome plated brass, or stainless steel. Pressure sources deliver the required 100 5 psi (690 35 kPa) and may consist of compressed nitrogen or air in cylinders, CO2 gas cartridges, high pressure air or water systems, or a dead-weight hydraulic pressure assembly. CAUTION DUE TO THE HAZARD OF EXPLOSION, COMPRESSED OXYGEN SHOULD NOT BE USED AS A PRESSURE SOURCE. The filtering medium normally is a filter paper that has been especially hardened for filtrate testing. The filtrate receiver is a 10 or 25 ml graduated cylinder. NOTE: A filtration Reduction Evaluation Device (FREAD) is available for use in the Model 300 filter presses. This device adapts the filter press cell to hold a 1/4 inch (6.3 mm) porous ceramic filter which replaces the filter paper.
After making sure the safety bleeder valve is closed, and the regulator adjusting screw is backed out to the closed position (maximum outward), turn the barrel loosely with the fingers until first contact with the puncturing pin is felt. Advance the holder an additional 1/4 turn. The puncture pin, shown in Fig. 1, seals when the cartridge seats. Screw the adjusting screw into the regulator to apply 100 5 psi (690 kPa) pressure to the filter cell as indicated by the test pressure gauge. Start 30-minute timing now. CAUTION WHEN USING SYSTEMS WITH CO2 CARTRIDGES AS A PRESSURE SOURCE, NO INLET PRESSURE GAUGE OR VALVE IS USED. USE CARE WHEN REPLACING SPENT CO2 CARTRIDGES. THERE COULD BE SOME PRESSURE LEFT IN THE CARTRIDGE. KEEP CO2 CARTRIDGES AWAY FROM EXTREME HEAT.
Fig. 2 - NO. 207223 FILTER PRESS WITH NITROGEN CYLINDER PRESSURE SOURCE
B.
NITROGEN CYLINDER PRESSURE SOURCE Follow this procedure to pressurize the filter press with a Nitrogen cylinder pressure source (Refer to the assembly in Fig.2): 1 With the regulator adjusting screw backed out to the closed position (maximum outward), slowly open the pressure valve on the cylinder. The inlet pressure gauge should show the cylinder pressure. Be sure this is greater than 100 psi, (690 kPa). Be sure the hose between the cylinder regulator and the cell is all fittings are tight, and the safety-bleeder valve is closed. Screw the regulator adjusting screw into the regulator to apply 100 5 psi (690 kPa) pressure to the filter cell, as indicated by the test-pressure gauge. Start 30-minute timing now. CAUTION ALWAYS SCREW THE REGULATOR ADJUSTING SCREW TO ITS MAXIMUM OUTWARD POSITION BEFORE OPENING THE RELEASE VALVE ON THE PRESSURE SOURCE. IF THE FULL PRESSURE OF THE PRESSURE SOURCE IS RELEASED TO AN OPEN REGULATOR, THE REGULATOR IS PUT UNDER A SEVERE STRAIN. IF THIS CAUSES THE REGULATOR TO FAIL, THE FULL TANK PRESSURE IS RELEASED TO THE FILTER PRESS AND IT MAY BE DAMAGED. AS AN ADDED PRECAUTION, A SAFETY BLEEDER VALVE THAT RELEASES AT APPROXIMATELY 170 PSI IS PLACED IN THE SYSTEM BETWEEN THE REGULATOR AND THE FILTER PRESS.
C.
DEAD-WEIGHT-HYDRAULICS PRESSURE SOURCE The Dead-Weight-Hydraulic Filter Press is a Series 300 Filter Press equipped with a Dead-Weight Hydraulic Assembly. The Dead Weight Hydraulic Assembly is shown in Fig. 4. Follow this procedure to pressurize the filter press with the deadweight-hydraulic pressure source: 1 2 Fill the water reservoir and cylinder of the dead-weight assembly to the top with clean fresh water. Open the bleed-off valve and place the piston, with the weight attached, in the cylinder. Allow the piston to travel full stroke. Refill the reservoir with clean, fresh water and close the bleed-off valve. Set the unit in place on the filter press frame and tighten the attaching set screws, if not previously attached. Connect the air hose from the dead-weight assembly to the top cap pressure inlet, if not previously attached. Raise the weight to the top of its stroke and allow it to settle. In about two-thirds of the stroke, the delivery pressure gauge will indicate 100 psi. Lift the dead weight back to the top of the stroke. Start the timing of the test when the weight is released. One stroke of the piston will allow a maximum filtration loss of approximately 30 ml.
D.
2. Secure the cell to the base cap by rotating it clockwise. 3. Fill the cell with the test sample to within approximately 1/4" (6mm) of the top. (Filling the cell to this level lessens the volume of pressurizing gas required from the pressure source.) 4. Set the filter press cell assembly in place within the frame. 5. Check the top cap to make sure the rubber gasket is in place. Place the top cap, already connected to the pressure source, onto the filter cell and secure the cell in place with the T-screw. 6. Place a dry graduated cylinder under the filtrate tube, either on the support or in the clip. 7. Depending upon the pressure source being used, apply pressure to the cell following the appropriate pressure source procedure as outlined in Section 3. 8. At the end of 30 minutes (or 7-1/2 minutes - Refer to Note below), close the pressure source valve and back off the regulator, open the safety-bleeder valve. This releases the pressure on the entire system. 9. Measure the volume of filtrate collected in the graduated cylinder and record the filtrate loss in milliliters as the API (30 minute) filtrate loss of the drilling fluid, or milliliters x 2 for the 7-1/2 minute test.
NOTE: The amount of filtrate collected after 7-1/2 minutes can be noted and, when this amount is multiplied by two, it will give a rough estimate of the amount that will be collected in 30 minutes. The estimated valve is usually one or more milliliters short of the actual valve and this estimation procedure should not be attempted on drilling fluids having a filtrate loss of less than 5 ml in the 7-1/2 minute period. 10. Loosen the T-screw, remove the cell top, and then remove the cell from the frame. 11. Discard the drilling fluid. 12. Disassemble the filter cell and carefully remove the filter cake and filter paper from the base cap. 13. With a gentle steam of water (or, in the case of oil drilling fluids, with clean base oil), carefully wash excess drilling fluid from the cake. 14. Measure and record the thickness of the filter cake to the nearest 1/32" (0.8 mm). 15. If desired, record properties of the filter cake such as texture, hardness, flexibility, etc.
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2. Assemble the dry parts of the filter cell in the following order. Refer to Fig. 7 and Fig. 8 omitting filter paper and screen from Fig. 7. a. b. c. d. e. base cap rubber gasket FREAD assembly. Refer to Procedure 1 above. rubber gasket filter cell Secure the cell to the base cap by rotating it clockwise.
3. Fill the cell with the test sample to within approximately 1/4" (6mm) of the top. (Filling the cell to this level lessens the pressure volume required from the pressure source.) 4 5 Set the filter press cell assembly in place within the frame. Check the top cap to make sure the rubber gasket is in place. Place the top cap, already connected to the pressure source, onto the filter cell and secure the cell in place with the T-screw. Place a dry graduated cylinder under the filtrate tube, either on the support or in the clip.
6 7
Depending upon the pressure source being used, apply pressure to the cell following the appropriate pressure sourceprocedure as outlined in Section 3. At the end of 30 minutes close the pressure source valve and back off the regulator, open the safetybleeder valve. This releases the pressure on the entire system. Measure the volume of filtrate collected in the graduated cylinder and record the filtrate loss in milliliters as the 30 minute filtrate loss of the drilling fluid using the FREAD adapter and the micron size of the filter used for the test.
10 Loosen the T-screw, remove the cell top, and then remove the cell from the frame. 11 Discard the drilling fluid. 12 Disassemble the filter cell and carefully remove the FREAD assembly with the cake. 13 With a gentle steam of water (or, in the case of oil drilling fluids, with diesel oil), carefully wash excess drilling fluid from the cake.
14 Measure and record the thickness of the filter cake to the nearest 1/32" (0.8 mm) and note that this test
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12
2 3
Clean and inspect the regulator for evidence of dirt or drilling fluid in the regulator body. An outlet filter (208626) is available to prevent this problem. Replace the pin and seat. Re-assemble the regulator.
5 6 C.
Dead Weight Hydraulic Unit Maintenance Always protect the mirror finish of the stainless steel piston, especially when removing it. Clean the fine mesh screen on the bottom of the water reservoir. If the piston moves sluggishly during a test, remove the piston and O-ring from the cylinder. Clean the O-ring groove in the cylinder. Examine the O-ring carefully for torn or rough places, and, if the surface is damaged, replace it with a new O-ring. Before replacing the O-ring and the piston, apply a light film of high-grade, water-repellent grease. In subfreezing weather, the water in the dead-weight assembly can be replaced by an anti-freeze solution such as propylene glycol and water; this does not adversely affect the operation of the unit.
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2. 207173 Filter Press Assembly PART NO. 207127 207929 205868 206051 DESCRIPTION Standard Filter Press Air Hose, 3 ft. Graduated Cylinder, 25 ml. Filter Paper, (100/box)
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207174 Filter Press (Refer to Fig. 11) PART NO. 207127 207929 208602 208615 208653 205868 206051 DESCRIPTION Standard Filter Press Air Hose, 3 ft. Gauge, 200 psi, (1380 kPa), 1/8" NPT Regulator Safety-Bleeder Valve 170 psi (1100 kPa) Graduated Cylinder, 25 ml. Filter Paper, (100/box)
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4. 207223 Filter Press, Nitrogen (Refer to Fig. 2) PART NO. 207127 207929 208649 208652 208653 205868 206051 DESCRIPTION Standard Filter Press Assembly Air Hose, 3 ft. Air Cylinder, Nitrogen Regulator Assembly Safety-Bleeder Valve 170 psi (1100 kPa) Graduated Cylinder, 25 ml. Filter Paper, (100/box)
5. 207224 Filter Press, CO2 (Refer to Fig.11) PART NO. 207127 208647 205868 206051 DESCRIPTION Standard Filter Press CO2 Pressuring Assembly Graduated Cylinder, 25 ml Filter Paper, (100/box)
Fig. 11 - NO. 207224 FILTER PRESS, STANDARD FRAME, W/ CO2 PRESSURE SOURCE
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DESCRIPTION Standard Filter Press Dead-Weight Hydraulic Assembly Graduated Cylinder, 25 ml Filter Paper, (100/box)
PART NO. 207889 208759 208595 208596 208597 208598 208599 208600 208601 208602 208603 208604 208605 205653 Hex Wrench, 1/8"
DESCRIPTION
Needle Valve, 1/8" NPT Reservoir Elbow, 1/8" Base w/Cylinder Weight Check Valve (2) Tee, 1/8" Hex Nipple, 1/8" x 1/8" Gauge, 200 psi, 1/8" NPT Adapter, 1/8" Air Hose w/connectors, 12" Piston O-Ring for Dead-Weight Piston
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B.
PART NO. 207128 207444 207999 208059 208062 208079 208255 208310 208424 208463 208626 209387 209389 209394 209395 Instruction Manual Pin for Insert
DESCRIPTION
Base Cap and Filtrate Tube Air Hose Adapter, 1/4" NPT x 1/4" Top Cap Cell Cylinder Neoprene Gasket, (6 each) Screen, Monel metal, 60-mesh T-screw, stainless steel Clip for Graduate Felt Filters Frame, Wall Mount Threaded insert Frog Bracket Wall Bracket
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2. 207503 Filter Press Wall Mount, w/C02 Pressure Assembly (Refer to Fig. 12) PART NO. 207391 208608 208647 205868 206051 DESCRIPTION Filter Press, Wall Mount CO2 Cartridges (10/Box) CO2 Pressuring Assembly Cylinder, Graduated 25 ml Filter Paper (100/Box)
Fig. 12 FILTER PRESS, WALL MOUNT FRAME, W/ CO2 PRESSURE SOURCE 3. 207356 Filter Press CO2 Stainless Steel Case (Refer to Fig. 13) PART NO. 207391 208608 208647 209184 205868 205869 206035 206051 DESCRIPTION Filter Press, Wall Mount CO2 Cartridges (10/Box) CO2 Pressuring Assembly Carrying Case, Stainless Steel Cylinder, Graduated, 25 ml Cylinder, Graduated, 10 ml Timer, Interval, 30 minute Filter Paper (100/Box)
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C.
MULTIPLE CELL FILTER PRESS ASSEMBLIES 1. 207785 - Four Unit Filter Press, with manifold PART NO. 207444 207786 207787 207790 207999 208059 208062 208079 208255 208283 208310 208349 208424 208459 208604 208626 208653 208655 209389 205587 205589 205868 206051 Pin for Insert Frame, Filter Press, Four Cell Manifold, Filter Press, Four Cell Preparation Tray, Filter Press Four Cell Base Cap and Filtrate Tube Air Hose Adapter, 1/4" NPT x 1/4" Top Cap Cell Cylinder Neoprene Gasket, (6 each per cell) Support Rod Screen, Monel metal, 60-mesh Thumb Screw T-screw, stainless steel Graduated Cylinder Support Air Hose w/connectors, 12" Felt Filters Safety-Bleeder Valve, 170 psi(1100 kPa) Needle Valve, 1/4" NPT Threaded insert Coupling 1/4 NPT Plug, Pipe 1/4 NPT Cylinder, Graduated, 25-ml Filter Paper (100/Box) DESCRIPTION
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Fig. 14 - 207673 SIX-UNIT FILTER PRESS WITH MANIFOLD 2. 207673 - Six Unit Filter Press, with manifold (Refer to Fig. 14) PART NO. 207444 207674 207675 207678 207999 208059 208062 208079 208255 208283 208310 208349 208424 208459 208604 208626 208653 208655 209389 205587 Pin for Insert Frame, Filter Press, Six Cell Manifold, Filter Press, Six Cell Preparation Tray, Filter Press Six Cell Base Cap and Filtrate Tube Air Hose Adapter, 1/4" NPT x 1/4" Top Cap Cell Cylinder Neoprene Gasket, (6 each per cell) Support Rod Screen, Monel metal, 60-mesh Thumb Screw T-screw, stainless steel Graduated Cylinder Support Air Hose w/connectors, 12" Felt Filters Safety-Bleeder Valve, 170 psi(1100 kPa) Hoke Valve, 1/4" NPT Threaded insert Coupling 1/4 NPT DESCRIPTION
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D.
DESCRIPTION O-Ring 2-5/16 x 2-1/2 Viton Body Adapter for FREAD Ring, Seal for FREAD Nut, Seal for FREAD O-Ring 1/2 x 3/32
PART NO. 210537 210538 210539 210540 210541 210542 210543 210544 Filter 5 Micron Filter 10 Micron Filter 20 Micron Filter 35 Micron Filter 60 Micron Filter 90 Micron Filter 150 Micron Filter 190 Micron
DESCRIPTION
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E.
208648 CO2 Assembly w/Top Cap (Refer to Fig. 15) PART NO. 208647 208062 DESCRIPTION CO2 Pressuring Assembly Top Cap
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208613 205608
Adapter (for external pressure supply) Gauge, 200 psi, 1-1/2" dia., 1/8 NPT back conn.
208616 208617 208618 208619 208622 208623 208624 208625 208626 208628 208643
Seat Diaphragm Adjusting Screw, Spring Case Thrust Plate Spring Button Adjusting Spring Diaphragm Plate Slip Ring Output Filter Screens (2) Regulator Repair Kit consisting of: Retainer Pin O-Ring Seat Seat Holder Spring Spring Guide
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F.
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2.
Nitrogen Supply System PART NO. 208649 208652 208653 208655 208759 207929 207973 208613 209390 209393 DESCRIPTION Cylinder, Nitrogen, (4" Dia. Size D) Regulator, Nitrogen, w/Gauges (Fig. 6) Safety Bleeder Valve, 170 psi (1180 kPa) Needle Valve, Male 1/4 NPT Needle Valve, Male 1/8 NPT Air Hose, 3 Ft., w/Connectors Air Hose, 6 Ft., w/Connectors Adapter, CO2 to Air Hose Speed Coupler or Air Hose Speed Connector for Coupler
G.
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Warranty
Fann Instrument Company warrants its products to be free from defects in material and workmanship for a period of 12 months from the time of shipment. If repair or adjustment is necessary, and has not been the result of abuse or misuse within the 12-month period, please return, freight prepaid, and correction of the defect will be made without charge. Out of warranty products will be repaired for a nominal charge. Please refer to the accompanying warranty statement enclosed with the product
Return of Items
For your protection, items being returned must be carefully packed to prevent damage in shipment and insured against possible damage or loss. Fann will not be responsible for damage resulting from careless or insufficient packing. Before returning items for any reason, authorization must be obtained from Fann Instrument Company. When applying for authorization, please include information regarding the reason the items are to be returned.
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