Cdna09875enc 001

Commission of the European Communities
nuclear science and technology
COMPARISON OF THE TENSILE PROPERTIES

OF 9 - 1 2 % CR. STEELS
Parts I and II
Report
EUR 9875 EN
Blow-up from microfiche original
Commission of the European Communities
nuclear science and technology
COMPARISON OF THE TENSILE PROPERTIES

OF 9 1 2 % CR. STEELS
Part I: DATA FILES
Part II: FINAL REPORT
H.C.D. NIEUWLA ND 1 ), G. BRUNRT), E.D. GROSSER3),

P. PETREQUIN"), Y. VANDERBORCK*), D.S. WOODS)
')
2)
3)
*)
5)
)
NERA TOOM, The Hague, (NL)

NIRA , Genova.(l)
INTERA TOM, Bergisch-Gladbach, (FRG)
CEA , Saclay, (F)
BELGONUCLEA IRE, Brussels, (B)
UKA EA -RNL, Risley, (UK)
This work was performed under

the Commission of the European Communities
Part I : Study Contract RA P.011(80)NL
Part II: Study Contract RA P.022(81)NL
for the: WORKING GROUP CODES A ND STA NDA RDS
Activity Group 3 "Materials" within the
FAST REA CTOR COORDINA TING COMMITTEE
Directorate-General Science, Research and Development
1985
EUR 9875 EN
Published by th
COMMISSION OF THE EUROPEAN COMMUNITIES
Directorate-General
Information Market and Innovation
Btiment Jean Monnet
LUXEMBOURG
LEGAL NOTICE
Neither the Commission of the European Communities nor any person acting on behalf
of the Commission is responsible for the use which might be made of the following
information
ECSCEEG EAEC Brussels - Luxembourg, 1985
Summary:
A compilation of tensile properties of 9-12% Cr steels has
been executed by CEC-member states. These data files will
be analyzed en compared under the work, which is agreed
upon as Part II. In the absence of a common data bank the
CEC-member states contributed from their experience with
9%Cr l%Mo steel, 9%Cr 2% Mo steel and 12%Cr steel in order
to form a sound data basis.
England and Italy compiled the information of 75 melts of
9%Cr l%Mo steel. Belgium and France reported 45 melts of
9%Cr 2%Mo steel. Interatom and Neratoom contributed with
36 melts of 12%Cr steel.
The tensile data are compiled between RT and 600C in 50C
intervals and comprise R Q _, R , reduction of area and
elongation. Chemical analysis and condition (heat treatment)
are given. The microstructure is described as far as
possible.
This work is performed under Agreement No. RAP-011-80NL(),
CEC Study Contract.
FRCC Working Group Codes & Standards, Act. No. 3, Materials.
pace
Summary
Contents
Subfile 9%Cr l%Mo steels

a.
b.
II
19
Subfile 9%Cr 2%Mo steels

a.
b.
III
The UKAEA contribution 9%Cr l%iio steel

The NIRA contribution ASTM A 335 9 steel
The Belgonucleaire contribution NF A 498.11 steel

The CEA contribution
NF A 49811 steel
27
59
Subfile 12%Cr steel

a.
b.
The Interatorn contribution X20 CrMoVYi 12 i steel

The Neratoom contribution X20 CrMoV 12 1 steel
67
73
S u b f i l e 9%Cr l%Mo S t e e l e
a.
The UKAEA c o n t r i b u t i o n 9%Cr 1 Mo S t e e l
United Kingdom Atomic Energy Authority

(Northern Division)
CEC STUDY CONTRACT : COMPARISON OF THE TENSILE PROPERTIES

OF 9-122Cr STEELS : PART I (DATA FILES)
UKAEA Contribution
1.
The UKAEA contribution relates exclusively to 9%Crl%Mo steel.
2.
Details of product form, chemical composition and final heat treatment
are given in Table 1.
3.
Information relating to microstructure is not available. In general the
microstructure would be expected to be martensitic without any delta ferrite.
4.
Tensile tests were carried out in accordance with BS3688 Part 1 1963.
Relevant details are given in the Appendix. Note that there is no standard
specimen size or shape.
5.
Data files on the tensile properties at intervals of 50 C over the
temperature range RT-600C are given in Table 2.
D S Wood
UKAEA
Risley Nuclear Labs
8.7.81.
T8LE 1 : DETAILS OF TEST MATERIALS frCHHo
P.rf
1
2
4
9
10
11
12
15
16
17
18
19
Product
Billet
M
H
H
H
H
M
H
H
II
22
26
23
31
36
3S
40
41
42
43
44
45
6
47
53
55
57
59
60
61
64
65
66
67
68
69
70
72
74
76
78
80
82
84
92
93
94
95
96
97
98
II
H
H
Section
254.0
177.8
190.5
6.35
6.35
6.35
6.35
6.35
6.35
6.35
6.35
6.35
7.0
7.0
11.1
8.89
7.62
7.0
Bar
20.64
20.64
20.64
20.64
20.64
20.64
20.64
20.64
20.64
20.64
11.1
II
M
H
H
H
II
H
M
Tube
M
H
II
H
II
Bar
4.9
7.5
7.5
7.5
6.7
6.7
6.0
6.0
6.7
6.7
8.9
7.0
7.0
9.0
6.8
9.0
7.0
9.0
3.25
19.05
19.05
19.05
19.05
19.05
19.05
Steel
Process
HF
HF
HF
BEA
BEA
BEA
HP
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
Che<n1cal Composition, X wt.

Heat Treatment
930C AC 4 720C*
930C AC 4 720C
930C AC 4 720C +
980/1000C AC 4 750C Ih
950C AC 4 750C Ih
980/1000C AC + 750C Ih
950C AC + 750C Ih
980/1000C AC + 750C Ih
980/1000C AC + 750C Ih
950C AC + 750C Ih
980/1000C AC 4 750C Ih
950C AC + 750C Ih
920/950C AC 4 75Q/770C
920/950C AC + 750/770C
920/950C AC + 750
920/950C AC 4 750/770C
92O/950C AC + 750/770C
92Q/950C AC + 750/770C
850C FC to 650C AC then
1000C Ih AC + 780C 2h
As for Ref No 39.
As for Ref No 39.
As for Ref No 39.
As for Ref No 39.
As for Ref No 39.
As for Ref No 39.
As for Ref No 39.
As for Ref No 39.
As for Ref No 39.
960C AC + T 740C
960C AC + T 720C
980C AC 4 T 780C
980C AC + T 780C
980C AC 4 T 780C
1000C AC + T 760C
950C AC + T 760C
1000C AC 4 T 760C
950C AC 4 T 760C
1000C AC 4 T 760C
950C AC 4 T 760C
960/1000C AC 4 T 760/780C
960/1000C AC 4 T 760/780C
960/1000C AC 4 T 760/780C
960/1000C AC 4 T 760/780C
960/1000C AC 4 T 760/780C
960/1000C AC 4 T 760/78OC
960/1000C AC 4 T 760/780C
960/1000C AC 4 T 760/870C
950C AC 4 T 750C Jh
850C JM FC 650C AC then
1000C 1h AC 4 T 780C 2h
As for Ref No 93.
As for Ref No 93.
As for Ref No 93.
As for Ref No 93.
As for Ref No 93.
51
Mn
0.12
0.14
0.13
0.14
0.10
0.51
C.65
0.45
0.40
0.40
0.40
0.40
0.44
0.44
0.44
0.25
0.25
0.42
0.36
0.39
0.44
0.37
0.28
0.56
0.51
0.49
0.51
0.51
0.54
0.54
0.44
0.44
0.44
0.48
0.48
0.40
0.44
0.46
0.48
0.45
0.41
0.13
0.11
0.10
0.09
0.11
0.11
0.09
0.12
0.13
0.12
0.10
0.12
0.13
0.13
0.11
0.09
0.09
0.09
0.09
0.09
0.09
0.09
0.09
0.09
0.09
0.09
0.09
0.09
0.09
0.09
0.43
0.37
0.37
0.29
0.29
0.43
0.43
0.46
0,43
0.33
0.66
0.46
0.40
0.40
0.37
0.47
0.47
0.47
0.47
0.35
0.35
0.35
0.35
0.40
0.40
0.40
0.40
0.40
0.40
0.36
0.10
0.12
0.09
0.11
0.09
0.10
0.29
0.35
0.35
0.39
0.47
0.39
0.1!
0.12
0.13
0.105
0.105
0.095
0.095
0.11
0.11
0.11
0.11
o.n
0.11
,97
0.02
0.C2
0.02
0.02
0.021
0.C21
0.021
0.016
0.016
0.026
0.024
0.019
0.014
0.012
0.021
0.007
0.007
0.007
0.007
0.008
0.008
0.45
0.44
0.46
0.40
0.42
0.45
0.44
0.44
0.48
0.49
0.46
0.49
0.54
0.54
0.44
0.45
0.45
0.45
0.45
0.42
0.42
0.42
0.42
.46
0.46
0.48
0.48
0.49
0.49
0.50
0.014
0.017
0.013
0.015
0.022
0.013
0.015
0.015
0.017
0.016
0.021
0.017
0.018
0.018
0.017
0.022
0.022
0.022
0.022
0.016
0,016
0.016
0.016
0.010
0.007
0.010
0.010
0.009
0.008
0.010
0.022
0.024
0.016
0.018
0.008
0.006
0.006
0.007
0.008
0.008
0.008
0.008
0.010
0.010
0.010
0.010
0.012
0.010
0.42
0.44
0.42
0.46
0.45
0.46
0.018
0.021
0.016
0.009
0.009
0.010
0.020
0.014
0.008
0.009
0.0
0.03
0.03
0.034
0.021
0.013
0.011
0.008
0.029
Cr
9.34
0.99
8.80
8.30
8.30
8.33
8.33
8.64
8.64
8.64
8.68
8.68
9.30
9.10
8.51
8.52
8.24
9.06
Mo
1.0
0.05
0.94
0.93
0.93
0.90
0.90
0.94
0.94
0.94
0.98
0.98
0.99
1.07
0.93
NI
0.23
0.16
0.16
0.18
0.18
0.22
0.2
8.50
8.68
8.64
8.58
8.36
8.70
0.96
0.96
0.99
0.93
0.95
0.93
1.0
0.93
0.93
0.91
0.93
0.98
0.99
0.97
0.96
0.96
0.93
0.95
0.95
0.95
0.95
0.99
0.99
0.99
0.99
0.96
0.96
0.96
0.96
0.96
0.96
0.96
Sn
0.09
0.09
0.C9
0.09
0.025
.0.025
0.025
0.025
0.025
0.025
0.025
0.10
0.09
0.10
0.12
0.11
0.09
0.02
0.019
0.02
0.021
< 0.03
0.021
0.06
0.02
0.015
0.015
0.015
0.015
0.30
1.0
0.97
0.93
0.95
0.98
Co
0.32
0.91
1.04
8.48
8.75
8.52
8.76
8.52
8.52
8.70
8.72
8.62
8.61
9.10
8.82
9.00
9.00
8.75
8.36
8.36
8.36
8.36
8.64
8.64
8.64
8.64
8.70
8.70
8.50
8.50
8.50
8.50
8.32
Cu
0.37
0.13
0.13
0.15
0.15
0.15
0.22
0.22
0.20
0.16
0.17
0.10
0.16
0.16
0.16
0.16
0.17
0.17
0.15
0.15
0.19
0.19
0.15
0.10
0.10
0.10
0.10
0.10
0.10
0.09
0.09
0.09
0.09
0.019
0.37
0.15
0.16
0.16
0.22
0.18
0.13
0.14
0.10
0.09
0.12
0.10
< 0.01
0.01
< 0.01
< 0.02
< 0.02
< O.Ol
0.023
0.023
0.023
0.023
0.030
0.030
0.030
0.030
0.030
0.030
0.03
0.03
0.03
0.03
0.02
0.030
0.030
0.030
0.030
0.006
0.006
0.004
0.004
0.006
0.006
0.010
0.24
0.019
0.020
0.O20
< 0.010
< 0.010
< 0.010
0.010
0.020
< 0.020
0.01
0.01
0.008
0.008
0.007
0.007
TABLE 1 (CONTD)
Ref
99
100
101
102
103
105
107
109
111
113
115
R35
R85
R86
Product
Bar
H
H
Tube
Bar
Section
mn
19.05
19.05
19.05
19.05
19.05
6.7
6.6
7.0
8.9
7.0
8.9
31.0
31.0
12.0
Steel
Process
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA
BEA 1
BEA )
Chemical Compositi on, * Wt
Heat Treatment
C
S1
Mn
Cr
Mo
Ni
Cu
As for Ref No 93.

As for Ref No 93.
900C J h AC 4 T 750C Ih t
900C J h AC 4 T 750C Ih t
900C lh AC + T 750CC lh jr
960/1000C AC 4 T 750/7806C
960/1000C AC 4 T 750/780C
960/1000C AC 4 T 750/780C
9C0/1000C AC 4 T 700/780C
960/1000C AC 4 T 750/780C
9bO/1000C AC 4 T 750/780C
930/970C AC 4 T 730/770C
0.09
0.11
0.11
0,12
0.11
0.09
0.11
0.11
0.11
0.11
0.11
0.10
0.44
0.44
0.23
0.33
0.32
0.47
0.44
0.37
0.37
0.39
0.39
0.66
.0.45
0.44
0.59
0.49
0.48
0.45
0.44
0.44
0.44
0.46
0.46
0.50
0.020
0.021
0.018
0.016
0.019
0.022
0.021
0.017
0.017
0.016
0.016
0.013
0.008
0.008
0.022
0.016
0.017
0.008
0.008
0.007
0.007
0.010
0.010
0,008
8.63
8.64
8.64
8.61
8.68
8.36
8.64
8.75
8.75
8.58
8.58
8.85
0.98
0.94
0.95
0.98
0.92
0.95
0.94
0.93
0.93
0.93
0.93
0.95
0.20
0.26
0.34
0.20
0.52
0.11
0.10
965/985C AC f T 760C
0.09
0.69
0.51
0.023
0.11
9.36
0.99
0.21
Co
0.023
Sn
'V
< 0.020
0.023
0.025
0.030 ,
0.030
0.020
0.020
0.022
0.12
0.02
* Heat tre ste d as 15.9mm.sq se ctions,

* Heat tr eated as 25.4mjn.sq se ctions,
t Heat tr eated to simulate tube.
U3
TABLE 2
TENSILE PROPERTIES
Ref
T e m p e r Q f"o r e
r o e r <^
20
RP . .
m
I 0 0
ta G I C
R of A
'
IO
I!
\1
R p
Rm
A
R of
Ro , . ,
R
Z
SI -L.
fol-5
| 2t.o
i
'
R.PA
RP , . ,
R
A
R *fA
Rp ,.,
Rm"
A
R.f A
Rp , . 5
R
!
5070
1 G2S-7
20
R P.
iGi'/!
6f,lol
R_P^_
1 5 2l-Sl
A
GS7 I
2l0
.i
5l2-q\
f.L.A -3!
2 50
1 3Sd.A
i
;
7 3-.I 3S7-*i! ^ 37-sl

Soi! 1 t i - l /_J5-d
1 s-0 { i f o
AA'ol
2.0cl
-Si-Si
593;i
17cl
|
!
21?-i\
77
37cl
37C.-L
X99
?6ASl
170 1 170
17-0I
65?!
-cj
1S0I
l?o!
L.-iL.-L
??2|!
AS7-cj
-71
37?sl
A lol
2 O
A D 5 I 3 3 3 d 372C
5 0 0 | '75 d A A c J
17oi
i0I
1 Sc
~5U 1 L.S-A
fA S - 2 !
SiS2
17 ol
L.7L-U
52L-7
170
t L M
i
A
;.4?
7-0
3 77.21
-S3
Al?7l
33VA!
/A-0
(70
.;
_P
A
^Jii-5
G U - l ! (,tu-7
j 3 ~ - v
Aio'?!
Sio-1 !
iS -o
170
R o A
II 5"3
R |
22-0
12-0 1
A-C7- ! ^ ^ 1
23-0
-*55
3 5A ol
6.11-3
1 o
4.27Gl
IS.0I
333-A
5 ( ! 5(5-3.1
l-c
R.fA
3 72-3
A
*C
G<?7-2
. -
!
! 3 3 5 -A
AC3.il 795
5.3-3I A 'S S.J
ff5"J
IS
575-7!
33-
Rp
U.SAI
!
1
A 3S.! A o<?o
5"7-2l
SLi-2
5GVH
7 37-J
--cl
R.fA
17
3*.1
X\-S
Ro . R-n
A
e
.7?!
R f A
R*
54931
2J.0
IG
259
! u.00il
1 A ?CA !
R.fA
R f O.
R _
i
1 3&36.
39c-5l
A-S l si
i'/cl
2 3 0 !
1 2<.:.?i
> 3cJ
3ci
!
!
AIC-S I 3
S 3 7 - L I i.. 17-21
25-C
2 1c
!
| G >o
6?
\5
5S C 1
A
R oC A
f-5
ai-s
! A5"I-||
1 1.-..U-.-5I
25!
!
I A G??!
1 c, t. a 71
2.SCI
1
!
I 6I?!
G US
5??t
3A t i
cGll 1
L-IL-yl
5^1}
i
! 5" GL*)!
! "7 11 -5
A S o | 5 0 0 | SSO
i., c i o l
2 15
2.95
Celsius)
3oo
I i.Ll1
5 S C 51
A a3
ideareis
2 00
Sheet 1
u-o\
/ t 7?-G
27A 2 571-5
Slo-1
53t--5
Il e
17-0
34S
A6C?
170
3246
U.CS 1
54 0
I
W/.V
'
Pfttr^.C
el(i)W!
pfc
f (-cl- r
il
TABLE 2
Ref
Tcmpcra'ure
P r o p e r 1"^
20
l
Rf
R~
A
R of A
Ro
Zo
ol
R.fA
Rp
o-l
40
41
4-
21-0 1
(?C..||
553-1
7 SC-al
4*5=
5 2 3-71
511-21
720-S
It-o
C-lo-Sl
l7-e|
73^
iu-0 1
5I7-|
(,7c-?l
5o5c!
(,o.?l
2o-o|
25-0I
Rp .,
p n,
! A SA -c
GJ7-J
P.f A
Re
Rp
Rm
577-G
IS-C
392-3!
4.9,3-sl
? - ??
5S3-S
17-e
1
4.G/-9I
Gc2-il
! A 34.-4
! 53;
i7-o!
1?-cl
!
1
!
1 3<?S-2 2S5-J "U7-7I t - l
33o-5
CM<M 227-5-
Sic1)!
i7?
uld-
1A - C
-,7c-7l
i*-3l
2 1C2
t>c-4
7CC
ucj-i
32?3
2SI-5
'3t4.i
13 -0 |
.
22S-5
273
33-5
55C-e|
22-7
537-d
22-7I
550-2
A
A- l
C-ci
4.011
t3?-3"l
2l-3l
3 5-7-9 1 3 57-11
S35-4 5"i5"-il
2e-!
2I-S
3t-L-2i
5'5->!
I ._
543-3
355-rj
513')
352-il
4<-cJ
3o-5
2 3-7
2C-P
23-sl
4.-0
S 4.
A oi-ll
37-75
5?-
5? *.
Sc-S
24-3
17-5
f? o f A
LT7-2
20--5
**
R
A
R ef A
.sv-i
23-c
R.fA
!
1
R? o; A 32-S
R .?A
502-1 1
G -S 1
ik.o!
1
5"i2-71
707.!
1 G"9.l
I
27-5!
A7J-7
\(..o \
5<?7?
S24.7I
R,
A
355o
5" f 5". !
6 4^-l
1 GGl-ol
1
5?/-3t
7C-I
i-o
Rp . .
R-
13.&
SU-I
2
bj-fl
? 1
5 34-5
33-i'l
IC-ol
Rr.-x,
o.*
ico
U-o 1
tS-o
1-0 1
o-j
ic-o
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l7-o|
A
II 5 3
1 GI2-?!
!
S
R.fA
3?
LS-S
Rm
R -i
R ,
3 79-sl
5I7-$I
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(=23-71
1 7-9
A
R.A
3S
^03*? . 33 7/,
5-
52S-G
G * A-St GS^-cl
20-ol
!
n.-.
31
!
i
5 0 0 ! SSO ! G co'
! AS O
A 3-! A - G t. ? 1 4 . 2 A . I
G 472! G 22-7
5.J
1 765-91
22|
2c-o
Zi-o'\
!
27-0 !
R~
A
Rp
R-,
4.00
!
S4I
-.r
Celsius)
f A
300
A * 3-5
G 74-7
2-G-o
R.1A
2 00
725-7
230
RP
(degrees
R^,
A
R
Z2
...,
1oo
Sheet 2
264?
5.-0 7
16-7
333-4.1
^73-7
322-cl
-511
2 M ! 22-i
3P.
A JQ
2C-S
277*
"iS-ol
31-2
.2S
2?3
32
349.1 I
?3<? i
*27-5
3.4.?
<_0?
2 51-e
371-3
4-3
32-7
ri
,?><
U.7 .!
-i.7-7!
L.U.-1
22-?!
22-5
320
5?24
27<
21-e
/--,.
creen r J
tl
"5
f*cr r t
12
TABLE 2
Ref
T e m p e r a f"ure
P r o p e r 1"^
20
A3>
A l e <7
Go-1
R ..' .,,'. .. ,
R >
1 00
A27-.I
3 ( ,A ? I
4;
25
1 0
25-S I
3(0 i
S 57 0 i
5cr-i I
3tu3-2
5c3-r
.33 3-3
32l-7
2?5
22C-
357')
294
23-Sl
2e-7
4. (.(?
21-3
4.2A-C.I
5-C
25
42(.-|
3- I 37C..G
37C-7
352-1
233-3
31 G - S
2 3-4
G3.d
5(,3?
5<
Sov.c
Ui1-l\
352-1
27-5
fcG
3? 6 A ! 370-7
S 5 C - c | 521-7
fco-i
30-0
2.7-5
2S-I
22-1 1
34t-2
22-0
22-0
27-9
3<
Z7-7-S
L.T-C
34-c
e-3
22.2-6
357.1
34.1
2 "73
2.c
II
531-51
507
23-3
22-3 !
2c-6
2<)
i2r.-Gl
2t-c
1 A GG?
3?5-2 4s!-5
AlG-Sl
595.2!
305-2
37o-7l
iCc-o
219
R~,
G5?-C
UZe-'
7C6-I 1 &2o -31
G3-4.
S7A-7I
I-C5-0
2 S 5-4
A
R . f A .
2,t-5
l -G
15-5
l^-ol
7-5
4-C5
G23-7I
5SC-C
r -
2.6-5!
G4?-2
17-1 1
14-3
43L-J
4.10-7!
377-21
3 70-4.1
3 btM
35lM
3c??
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1 G S 2 - l l
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5tc<5
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A S-J
uit-1
372-7
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21-0
l3c|
15-0 i
5co!
e i
r" p^
A7.J
G36-5
4. 2-11
(,5<?|
24
24-ol
LUS-I A ' - t . l
5?5-5l
55? 1
22-0 1
01
iri
-24-rJ
4?i-s
701-2
642-jl
S?e-f,
2 2 -c |
R.fA
22-c
^0t-il
5ji-5l
4.2 6
Siici
4.24-6
54;
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321-7
327-5
317-7" 1
6 37-4
5?ll
51-2I
423-71
A
R.fA
3o-0
2.7-c
2c-o
loci
IS'c
335-J
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1
2fc3-7
1 S7<?. le
23-0
3 et-e
547-21
Xo
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437-J
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G(,S?
A
R.fA
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2L.-0
274-t
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2o-l
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lil- '
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lil35C
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5,:.4|
I
i.tt-3
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347.7!
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7-0
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4.031
220
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J41.I
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7-c
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-0
37e-7l
4-627
l-o !
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17-0
io-l
515-31
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3-G
A 57-cl
26-0
Rf>
cl
.:
R",
A.33-J
28-1
A
R . f A
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34.6-2
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6.0
20-2.
3.C-9
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5?
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334-4.1
R.fA
57
3?3.
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37-;
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27:2!
2 74 i I
A
R.fA
47
2 5-5
Rm
R.fA
311-7 I 2S7-3I 5 / . . J
3 JC-5
A.C1-7
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Rp c i
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45
3 00 I A . 0 o
2 00
3 tA. 2
S5
Celsius)
370-7
R of A
Rp
(degrees
312-3 1 3 7 J - d
55-el
524.7
Sheet 3
i!.ft..fi'
.f ^
fracvr*
13
TABLE 2
Te,
R e f j P r o p e r }
20
Rp
GA-
1 R~
Ol
A
R of
3
R
R
4-51.1
4.35-.
571-3
5 5 4 1f
24-0
23-0
Rp
eu2.
f^ V
A
R A
4.21.7
uZ(,.(,
G02-I
5GC?
543-3
26 c
2.5c
24.C
21-0
Rp
7o
"
tt 5 4
2I-0
397-21
5/t-?i
351-1
70-7
3c3?
A17-2
4.64-J
313-3
l o
l-0
rv
313-
3 72-7
Sie?
4.77-6.
17-e
e-c
35-A !
i7-o!
2 5-0
27-0
l
3 7C-7
57-71
3 52-1 t
3?5
ice-i
4 S?-4
4.?1-4
A6?
424-6
3 7C--7
2 o-o
2.a-o|
" 2/.0
29-0
il-o
1
3?23
llL-2
357?
^33-S
47S--C
A35-4
It-C
4.S5-.
4.51.1
4-5I-I
6G3 "
6 23-7
S'iti
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23-0
13 0
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wc
2 3-C
-1
4.11.91
54-3
5/.5I
3 7 7
4-77-6
26-7
-41-I.
il-o
2.C-0 I
170
2.4.-0
4.27-5
4.2 3-6
3A-2I
3 57-1
G73-7
ti7-3
571.7
f40-3
5,5-?|
451-e
361.9
^2-C
XL.-*
22-0
2.10
io-ol
17-0
rU-C
R 3 O. '.
Soc* -f
Ati-9
4.26.6
43-4
4.10-9!
36S S
270-7
G*$*-ff
G22-7
571-6
553-0
520-71
uni
362?
23-c
2-J
lo.C
21-0
510-1
/_5c-5
G74.-7
R . f A
R
R~
o l
R . f A
Rp
Rf.
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4 7-si
574-7*
37S-G
.72-7
2Sct
17-0
26
A33-4
1,*^ /
23-C
16 0
20
11-0
4.S5 ^
US c
4.6,1-1
4.244
I_OM|
353-c
G 76-7
6 12-7
577-t.
552
52 4-71
41-1
242-C
J.f-7
2-0
23-0
20
Il-O
ICO
22-0
5 ."f
I 2-0 1
365.3
c
1
n
2.C
4.66 -
PJ.J
r*,
ir-ol
1
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O.
7S
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4.?1
II SS
4.56 c
__4
7G
_1--3
R af A
20
3 72-3
11 - o l
23
R=
7A.
O-
2 1
1
i-43-31
377-2
5/3-3
17-0
G12-3
6 33-5
1
1
is-o !
532-5
2$
A
R.fA
6 6 5")
A
R . f A
7*7-4
.52-1
466 ?
7tL
32-C |
57
,.,
21
l_OI-f
4.41-1
Oi
17-0
5 24-7
AS 3-5
G53-
GOO
Sic-1
3 36-AI
G5S-C
t\ T+\
Rp
-ol
I
SSO
3C2S
w5l.l
0?|
22-e
R.fA
.67
4.13-2
I-C
GS
3 7-Jo
521!
A87A
R.fA
R~
4.01-1 I
545-3
o?
Soo
4,13-
23-c
67
450
4 0 0 !
I
,,
A
R- 0 f A
GG
AS 3 5
653-1
f ^ P R -
&5
3oo
2 0
0 0
Ce 1 si us)
(degrees
p e r o /rc
Sheet 4
N/V
2io
I
'S
i t f t i ' i i C
*.!.
r *:,,
,Ftr
Fr*er r
TABLE 2
Ref
Proper
Te m pera fure
f^
2o
So
R o-7
345 S I
4-72-7
352
270
24.
22-0
2.-0
I 9-0
25<
A 8 C -A
AC3 S
t-52-i
I^L-L
6 84 5
636-5
511-2
56C-
26-0
i.2-0
19 .? !
22 1
52*-f.
I 7-0
37C-7
2 I 1
2.I.I
1
323-4
Z2-3
626 6
593-3
564'/
52 7-4
A?o.S
357-0
23
22-0
l1-0
lS-0
2A-0
24-c
4?5-4
4.75-r.l
4.-2
-Sol
4.0-l.f I
393-1
3 59 -7
3oic
4^2-51
623T-6
575-71
563?!
523-71
Ul6 3
4.52/
3 74-2
2s-ol
23-c|
n-o
l?ol
If.o!
p.;
2*S-
A 1.7I
R.fA
R
(1-e I
I 375-6!
I A 1/-3
4.32-sl
676-71
Rp
334-4
4-C.I-i
2S-C
I-0
R . f A
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-35-4.
4-13-3
3 3 3 4.1
31;|
357-lt
37*-7
321-7
2.4
2 34-4.
Rm
GI7-$I
74-7I
561-1 |
512-1
A3-4.I
S?i-L
C.26-6 1
3C.4.?
2 Si.-4
27-0
26-7
23-0 I
21-0
19.7 |
14..0
2',-7
%0-tl
24-3
A4.52I
4.!7
' 15- 2
3S?-l
37C-7
->J_.-2\
327-5I
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2 > / -4.1
642-31
5-733
556-0
5374!
5!2-ll
A S?-4j
o-51-ii
364?
3C3-C
27-0
25-e t
03-2
210
'7-7,
2l-2!
2i--3l
2-7
2 4-3 {
ri m
Ro
A
0.-
R.fA
0.1
R^
R3
331-3
376-C
3707
3 57-7
3-1-3!
3(6.. ? |
27-3
222-G:
Gc5-ll
553-1
520.7I
S03-I
4 1A - 3 !
^663
AI1-7I
36.1-I
4.13-S
27-5
2S-5
24-5
24-c!
2o-o!
22-c
32-
3?2
4.1I.7
573-31
26-7 I
331.51
543-3I
225
37c.7I
524-7
22-5*1
357-7
34.0-2
337.3!
305-1
2 35
52C-7!
475-61
432-Sl
376-G
4-4
27?
37?
4 . 3 ? / 1.
62.?
27-1
451-1
0?
A A
J -d
6 3'
R~
A
0 i
2!-7 1
5-71-2 1
ACi-l|
376-6
3?3-4.
3 55vO
3^.6-2
3C6-0
55-31
SAC-ij
52?-t
53^-5
4.1/-3
4-5'? -7
392-3
2 2-71
o'S
22-0
2.I.3
23-3
3o-e
2S-A
26-7
6-3
75-6
C-4S-;
43?4
S I'll
A2--5I
4.26(.
3 72-31
3?3-4.
22?'
56-3-31
5??6!
4.7--3
3 55-0
4-<*?;
324-GI
5641?!
377-5J
311.7
2 7-2
2 5-7
23-1
lv5
20 - 5
2.1-0
23-7
3o-7
36-5
J93.1
315-2
4.0'S 0
38C-A
R . f A
o -i
R . f A
io
4.e?-c
(. 5 ? -
f, 1C-5
574-7 1
S?6-
Si.3-3
5A3-3
5A-3
30
26-0
25-l
24/
22-3
2I.7
ZOL.
"
N/IUM'
370.7
T/S?!
364?
I
A30-5
i
R .
Uil-'i
153
pe.i,
ao-9
319-1
R .f A
R p
25-61
R . f A
R 0
R t
II7!
R . f A
256-
t(,1..7
TS
5o5-o|
Rm
R .f
97
G 0 0
521-vi
r.-
Rp
SSo
4-C.9I
<?5
5S4.-I
Rp
*4
S 00
4:15
43-4
R of A
13
ASo
A H -7
562?
R.T,
A
12
A O
of A
S 4-
0 0
Celsius)
6,23-7
0 0
(decrees
663-7
A 97-2
R V
Sheet 5
' J
I
3e
t . Hn
frei
So\
2o-7
21-3
1
fracTure
15 *'
TABLE %
Ref
Proper r^
T e m p e r o ture
20
R o.i
loo
A.
of
1 0 0
decrees
300
2 0 0
A
R of
.60s
*jysl
JOSI
1*36.
614*)
577fc
5CC3
534.5I
SA3
ser?
2S-7
23?
175
2o|
its
A62"
6GG1
2 6 0
o.*
A
9.1
105
lu
3152
3254.
6 3C
S7I7
SL
SS6
515.*
4t1.7
S I 52
2234
377S
2.52
22?
175
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325
507C
A 69 7
4117
177 5
3. M l
24*
,f,
l3
I70
USI-i
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AIV?
G.3AS
5*t2
5?5|
550
544/
A72
A9t|
271
215
20.7I
i t o
?3
221
f r .
3462
2471
" A S 7 -d
556e
5l?3
5 i J . ? 1 4.JI-5 1
7I67
6S?e
fcUS
577-21
235
233
AJ3
4SI
A3G
A 55
5 72
554
537t I
ASA
4.1?
I*?**,
XL'S
33f
17-0
lt-3 I
A4A
4 o :
320
54*
310
226
54.4 I
513
A7
326
*rff ,
32
<M
7*
fir
t&
42
352
15
33
1
|
OS
67
b5
Si
2
C
Uw7
??2
4 02 1
565
**
56A
7A0
GGA
627
24
21
26
24.
17
76
7A
67
7'
.1
366
AG0
f?
R . f A
70
76
R O O.l
fJoo
A fe2
4.2 5
ui
6*6
622
570
SSS
52 I
25
27
22
75
77
7G
1-, I
7G I
s I
72 I
A.0
^4 6
A36
R,
475
4 22
525
A__
2*
S
25
553
2
R *'
f
17
.375

3*6
A75
. 23
2
7
4-S6
A 52
A 53
tÂ
3 5
37*
5 SS
G?A
616
S1<i
SG 7
f?'
A,*'
571
25"
2.3
23
f8
2?
2 *
To
*75
74.
7 6
2I
"TA
7<t
27
R of A
7 7
7A
Rf..., *
7A
2S
R.fA
76
72
25
*?
U27
t t
73
R,
75
AL
*<>*
.3
<f
7 3
47o
6 2 7
ftj|t_
5A
7o
676
R 9
tS3
uil-S
17-J
65
Sos
R35
Aia-sl
lt-3
R.FA
115
5SI-5I
o.l
257
4774
21
a s4
23
R f A
113
1W
1.24 6
*.25
2 6
A
R.fA
III
?*?7
AUS
A 4.52
0 0
A 452
R . f A
Ro
LAI*
R.FA
U7
fW.
So70
feSS5
26I
Rp
$ od
t.254
ASSA
loa
A.50
4 0 0
loi
loj
Celsius)
R o Ol
Ro
Sheet 6
I
I
A*<t
545
TV>
23
2\
TX
75
... 3 ? 5
fcA
27
77
53A
.A3. I
A 4.2
J74,
CIS
SA
563
4v
35
23
70
I
J
IS
4*
I
I
I
72
1 /
R f A
1 f . r c c r . j
J* r *>
I.5N.O
*"*
rfr
.. 3fr
iff
2
*7
, *f
?7*
a
27
GS
f*
ff*r
fV*t*
lb
TABLE 2
Ref
Proper
1"^
T e m p e r o l"uf e
2 0
Rf
R$5
O.
. > m
A
R of A
Rs
R o o 5.
Rm
A
R of A
S'il
AG
28
1 0 0
31
70
3oo
Celsius)
- !
A 37
567
U 16
7.
22
73
71
522
G 5?
(decrees
2 0 0
I
Sheet 7
531
4 5
Soo
SSO
371
66
336
76
S2
337
3 53
Ao<?
-J11
21
1
1
AGf
5"6
4.4-4
52?
z'sr
2?
21
7?
71
TS
32
A6S
! GOO
APPENDIX
...!.....> . . . . . . . .
IB
X.1, l.l.W.V> M . l . ' H O N A C A l l i A
11. " crossscciional :.rc.i hnl! be calculated before (lie let! from invasine
ments of ilic appropriate dimensions will an error of not mo:c than J: 05 per
<cl in cicli dimension. If tin< accuracy cannot icadily be obtained, lhe method
of measurement should bo recti between die interested partici. (Sec Clause 16
concerning measurement of crousectional area after test.)
MAUKivn Tiic OIUUN.U. c\t:cr. LENGTH
12. Kach end of ihr. gauge length may he marked by means of a fine punch dot
or scribed line. Incised markings arc not recommended for notchsensitive
material, .Mid alternative methods wit] be required. It may. be useful to mark
on the surface of the test piece a line parallel to the longitudinal axis. For test
pieces witli flat faces the lir.; should be at the middle of one of the wider faces.
If the parallel length is much in excess of the gauge length, a for instance
in a test piece without enlarged ends, a scries of ovr.'tpping "Jgc lengths,
sonic extending into the gripped portions, should be marked on the test piece.
HEATING OF TZST tlTCt
J3. While attaining the test temperature, the temperature at any point within
the gauge length of the test piece shall not exceed th specified test temperature
by more than 5 degC (see C lause 23/).
The apparatus for heating the test piece shall be such that the test piece
can be luised to a tempera'"re which, at any lime throughout the duration of
lhe tesi .md at any point viiliin the gauge length, does not deviate from the
specified temperature by more than 5 dcgC for temperatures not higher than
rco'c
For temperatures higher than 800*0 the permissible variation shall be
speci5ed by agreement.
lt is recognized that difficulty in temperature control may be encountered
at high strains, but every effort shall be made to comply with the temperature
requirements throughout the duration of the test. Where possible the act'al
temperature at the instant of fracture shall be recorded (see C lause 22a(!L),
and wjth regard to temperature control. Clause 23).
STRAINING OF TEST PC C i
14. When the conditions of C lause 13 have been met, progressive 'ensile strain
ing of the test piece shall commence.
No limitation is imposed on the strain rate during tV; major portion of ths
clastic ran, but before plastic deformation commences the strain rate shall,
if necessary, be adjusted so that the following condition can be met.
When the value of lower yield stress or specified proof stress(cs) is deter
mined, the strain rate shall be within the range 0 001 to 0 003 per minute. The
time intervals used for the estimation of stral.i rate r'om measurements of strain
hould not exceed 6 seconds.
If the test is continued to fracture, higher strain rates may be used beyond
the yield stress or proof stressfes) to enable the test to bs completed within a
convenient time. (See Clause 23/i with regard to rate of straining.)
MEASLTX.NIENT OF STRAIN
IS. A continuous record shall be made, or a sufficient number of strain readings

taken to plot the stressstrain (or load extension) diagram clearly up to lhe
extension corresponding to the lower yield stress or to the highest proof stress
required.
MHASuTMFNT OF TEST AFTE FRAC TUnn
16. If va'jcs of elongation or reduction of area arc required, sufficient measure

ment; .sha!! be taken when the fractured test piece has cooled to room tem
perature to ensure that the elongation and (in tests of round test pieces) lh;
minimum crossSectio nai aron are adequately determined.
Ore shall be taken to ensure proper contact between the broken parts of the
test piece when measuring the fin: length between gauge marks. This is of
particular importance when measuring miniature test pieces and test pieces
havin low elongation values. For sc of measurement a simple jig should be
used which will enable the broker pieces lo be mated axial'y at the point of
- 19
Subfile 9%Cr l%Mo steels

The NIRA contribution ASTM A 335 9 steel
Abstract
This report summarized the available data on tensile
properties on 9%Cr steels.
G. Brunori
NIRA - Genoa
Italy
1.
INTRODUCTION
The activity 3 "materials" of the working group

on "Codes and Standards" of the "Fast Breeder
Coordinating Committee" of the "Commision of Eu
ropean Communities" has begun a joint programme
on "Comparison of tensile properties of 9-12%
Cr steels".
Tensile properties on 9% Cr 1% Mo were determined in Italy and they are collected in this report .
2.
EXTENT
OF DATA
Seven heats were studied, which are avaible:

- chemical composition
- grain size
- tensile properties at room temperature
- tensile properties at 3OO-4O0-500C
Tensile properties were determined on specimens
drawn from forged bars of 20 mm. diameter after
an isothermal annealing heat treatment.
A summary of data is given in Table I.
- 21 -
CHEMICAL COMPOSITION
This steel, corresponding to ASTM specification

A 335-P9, is standardised for pipes for high
temperature service.
Chemical composition of the seven heats are given in Table II.
TENSILE PROPERTIES
Tensile properties at room temperature are given in Table IV.

Tensile properties at 20o-300-400o-500C are
given in Table V.
The load at proportional limit at high tempera
ture was determined in accordance with ISO R
205.
4.
GRAIN SIZE
The grain size was estimated with ASTM metod

E 112.
Grain sizes of the seven heats are given in Ta
ble III.
to I
Table
I - SUMMARY OF DATA
HEAT
NUMBER
HEAT TREATMENT
SHAPE
FURNACE
AIR
DIMENSION COOLING
COOLING
(50C/h)
Forged
bar
0 20 mm.
tl
II
II
II
II
tt
920 b C1 h
720C2 h
CHEMICAL
COMPOSITION
TABLE II
TENSILE PROPERTIES
GRAIN
ROOM
HIGH
SIZE
TEMPERAT.
TEMPERAT.
TABLE III
TABLE IV
TABLE V
X
II
It
II
It
11
It
II
II
II
II
II
II
Table II - CHEMICAL ANALYSIS - VALUES IN % OF WEIGH
" \ ^ ^
ASTM
^^\A335-P9
HEAT ^ " " " \ ^ ^
NUMBER
^ \
r.15
Mn
.30
.60
.030
.030
.09
.55
.034
.019
.07
55
.030
.07
51
.07
Si
.25
1 .00
Cr
8.00
10.00
Mo
.90
1 .10
.78
8.60
1 .00
.010
1 .06
8.80
1 .02
.026
.010
1 .07
8.70
.98
52
.018
.020
.99
8.20
.90
.09
.57
.019
.017
.77
8.80
1 .00
.12
.44
.036
.010
.47
9.00
.96
.12
.50
.033
.024
.71
9.20
.96
ro
co
- 24 -
Table III - GRAIN SIZE
HEAT NUMBER
GRAIN SIZE
ASTM E 112
2
3
4
.7
- 2b -
Table IV - TENSILE PROPERTIES AT ROOM TEMPERATURE
^"\^^
ASTM
HEAT
NUMBER
^J^
^"\
1
R 0,2 (MPa)
^ 207
R (MPa)
^ 414
A (%)
^ 30
287
526
31 .4
274
535
28.0
362
579
33.8
331
57 3
30.0
375
599
29.8
399
593
28.6
291
505
31 .0
292
505
30.8
292
596
26.0
294
593
26.0
237
559
26.4
237
562
28.0
253
581
26.4
250
581
27.0
en
Table
V-
TENSILE
PROPERTIES AT HIGH TEMPERATURE
500 C
400C
300 C
20PC
HEAT
R
(MPa)
R 0.2
(MPa)
R
(MPa)
R 0.2
(MPa)
R
(MPa)
R0.2
(MPa)
R
(MPa)
R 0.2
(MPa)
287
274
526
535
190
204
441
441
165
181
414
414
164
162
369
371
362
331
579
573
231
237
500
486
219
219
486
486
186
186
391
391
375
399
599
593
284
284
521
536
225
219
490
499
186
200
396
415
291
292
505
505
190
200
419
424
169
180
417
414
158
161
353
344
292
294
596
593
200
200
473
475
195
190
444
458
187
178
411
408
237
237
559
562
187
186
468
466
195
191
461
448
173
170
390
393
253
250
581
581
213
200
495
478
187
188
466
451
192
175
427
402
NUMBER
- 27 -
II

a.
The Belgonucleaire contribution NF A 49811 steel

Y. Vanderborck
BELGONUCLEAIRE
Appendix to our letter dated 16.10.81

(ref. 098.10/020/1/036).
CONTRIBUTION TO THE COMPARISON OF

9-12 7. Cr STEELS TENSILE PROPERTIES
FRCC WG C AND S ACT. 3 1980 STUDY CONTRACT
The available data for chemical analysis and tensile properties

of a series of melts are given with the corresponding annealing treatment if
any (1 hour 710C + 10C).
The tensile samples (diameter 3 to 5 mm) are machined identically
from tubes (outer diameter 50 - 60 mm; wall thickness
6 mm) and tested on the
basis of ASTM norms according to the laboratory internai procedure.

No further detailed information is available for these tests
performed a long time ago.
The data files include :
- chemical composition, final heat treatment
- R 0,002
- Rm
- uniform elongation
- reduction of area.
TENSILE PROPERTIES OF 9 12 7. C r STEELS

00
1. '.AMPLE Nr. ( 24459
2. 11 EMI CAL COMPOSITION (7.)

.mple
Si
Mn
Cr
Mo
Ni
Nb
Co
'459
INAL TREATMENT
ENSILE PROPERTIES
.______^ Temperature
ipertlea
~~ '
.. 0.002
100C
150C
530
481
2
iin
/mm
ilnifonn elongation (7.)
726
(7.)
eduction of area (7.)

ftthe basis of the initial
.ample diameter)
eduction of area (7.)
1
on the basis of the dlame
er in the uniform deforma
lon zone of a broken
.imple).
550C
600C
392
353
284
579
495
441
368
4.5
4.5
3.5
12
11
11
13
15
17
70
70
69.5
68.5
71.5
75
79
68
68
67
66
69
73
77
200C
250C
300C
350C
400C
471
466
456
446
441
432
662
638
628
623
618
603
15
10
6.5
19.5
16
15.5
14
13
65
69
69.5
70
60
66
67
67
/mm
lotai elongation
RT
500C
TENSILE PROPERTIES OF 9 12 7. Cr STEELS

1. SAMPLE Nr. ( 2 7434
2. i'UEMICAL COMPOSITION (7.)

;.. imple
7434
0.127
Si
0.28
Mn
0.97
0.004
O.Ol
Cr
Mo
9.34
2.01
NI
0.08
0.08
Nb
Co
0.46
0.02
500C
550C
600 C
.0.32
INAL TREATMENT :
3. ENSILE PROPERTIES
*^____^ Temperature
l... pertica ~~"~~
^______
RT
100C
150C
200C
250C
491
466
451
437
687
633
613
:lniform elongation (7)
12
10
total elongation
23
18.5
69
64
: 0.002
P
:in
/mm
2
N/mm
(7.)
Keduction of area (7.)

>n the basis of the initial
ample diameter)
Keduction of area (7.)
(on the basis of the diame
ter In the uniform deforma
tion zone of a broken
enmple).
300C
350C
400C
427
417
412
407
368
334
294
605
594
579
564
549
491
407
334
6.5
5.5
4.5
7.5
16.5
14.5
12.5
11.5
11.5
13
16
18
20
70
70.5
70
70.5
70
70
69
70
74
79
66.5
67.5
67.5
67.5
67
67
67
68
73
78
TENS ILL PKOt'LIURS Ol- 9 - 12 /. Lr S'l'liliLS

1.
.AMPLE Nr. (
27434 R )
2. IIEMICAL COMPOSITION
,i\ple
,434
(*/.)
Si
0.127
0.28
/[NAL TREATMENT :
1 hour
Cr
Mo
Ni
Nb
Co
0.004
0.01
9.34
2.01
0.08
0.08
0.32
0.46
0.02
Hn
0.97
710C
+ 10C.
3. .ENSILE PROPERTIES
" --^___^^ T e m p e r a t u r e
pertica
" '
__^
RT
100 C
1500C
200C
250C
300C
350C
400C
500C
550 e C
600 e C
486
461
446
432
422
422
412
397
353
314
275
706
638
618
608
598
594
584
549
471
412
353
'Iniform elongation (7.)
11
10
9.5
7.5
;'otal elongation
18
17.5
17
16
14.5
13
12
11
15
18
23
65
68
69
69
69.5
69
69
69
70
72.5
78
62
65
66
67
67.5
67
66.5
67
69
71
77
.'. 0.002
P
.'in
/mm
M /mm
(7.)
Reduction of area (7.)

.in the basis of the initial
nample diameter)
reduction of area (7.)
ter in the uniform deforma
nample).
_j

1.
.l'LE Nr. ( 25587
2.
MICAL COMPOSITION (7.)

le
Si
0.13
0.36
Mn
1.01
0.009
0.008
Cr
Mo
Ni
9.63
1.88
0.07
< 0.05
0.03
Nb
Co
0.63
600 C
:AL TRE ATME NT

SILE PROPE RTIE S
~_______^ Temperature
rties
____^
RT
100C
150C
200C
250C
300C
350C
400C
500C
550C
/mm
491
456
456
461
456
446
437
422
368
324
260
2
/nun
701
633
618
613
608
598
584
559
486
422
334
12
9.5
8.5
7.5
6.5
5.5
5.5
5.5
18
19
18
16
14
14
14
14
16
18
21
auction of area (7.)

Lhe basis of Lhe initial
.ipie diameter)
64
67
68
68.5
69
69.5
69.5
69.5
70
72.5
79
Juction of area (7.)

a the basis of the diame
r in the uniform deforma
un zone of a broken
GO
64
65
67
67.5
67.5
68
68.5
71.5
78
.002
form elongation (7.)

tal elongation
(7.)
ipie).
ILtlblLt
lE_Nv.
25587
1'KOt'tiU it.o ui
-.
O.
I.
V .
LUL.U-J
>
11 CAL COMPOSITION (7.)
Tli
0.13
AL TREATMENT :
3,
l.Ol
0.36
1 hour
710C
:STLE PROPERTIES
/mm
. form elongation (7.)
al elongation
(%)
luction of area (7.)

Lhe basis of the initial
,ple iameter)
luctlon of area (7.)
the basis of the diame
c in the uniform deforma>n zone of a broken
,,ple).
0.009
+ 10C.
0.008
Cr
Mo
Ni
9.63
1.88
0.07
Mb
<
0.05
0.3
0.63
Co

1. SA!: ,K N r . ( 24457
2. Clii CAL COMPOSITION (7.)

Sam.
24.', ,
Fil
Si
Cr
Mo
Ni
Nb
Co
i. TREATMENT
3. TEI. ILE PROPERTIES

_____^^ Temperature
Prop
Lies
Ri.
002
Rrii
_^____
2
/mm
. 2
/mm
orm elongation (7.)
- Uu
.1 elongation
(7.)
- To'
.etion of area (7.)
- Re lie basis of the Initial
( on .
le diameter)
..
- Re. iction of area (7.)

( c the basis of the diame
t e ln the uniform deforma
tl
zone of a broken
.
300C
350C
400C
500C
550eC
600 C
422
417
412
402
363
334
284
594
589
579
564
544
481
417
343
9.5
7.5
6.5
5.5
5.5
17
15.5
14.5
13.5
13
13
13
14
15
17.5
71
73
74
75
75
75
74
73.5
73
76.5
79.5
67.5
70
71
72
73
73
72
72
74
79
RT
100C
150C
200C
91
451
441
427
667
618
603
12
105
20
250C
71
le).
CAJ

UJ
J>
1 , SAM Nr. (
24Sf:
2. CHEMJ.'.Al. COMPOSITION (7.)
Sampl.
Si
Cr
Ni
Mo
Nb
Co
600 C
24458
FINAI. TREATMENT :
3. TENSILE PROPERTIES
______^ Temperature
Propei : Ks ""
______^
RT
100C
150C
200C
250C
300 e C
350C
400C
500C
550C
505
466
456
446
441
437
427
422
387
353
299
706
647
623
613
608
603
594
584
515
451
373
/nun
11
10
9.5
6.5
5.5
5.5
5.5
Uni tonn elongation (7.)
15
16
16
16
15
12.5
10
9.5
12
13
15
Tot, elongation
(7.)
(on the basis of the initial
sample diameter)
(on Lhe basis of the diame
67
69
70
71
71
70
69
68.5
70.5
73
77
63
66
67
68
69
68
67
66
67.5
70.5
76
R O.U02
P
- Rfli
sain;! ;) .
2
/mm
2
TENSILE PROPERTIES OF 9 - 12 7. Cr STEELS

1. SA! : K Nr. (
2.
Cli
24461
''AL COMPOSITION (7.)
Sa.
Si
Cr
Mo
Ni
Nb
Co
24A
RT
100C
150C
200C
250C
300C
350C
400C
500C
550 e C
600 C
510
466
456
446
441
432
427
417
373
343
275
711
652
628
618
613
608
598
569
495
432
358
18
14.5
11
7.5
5.5
11
22
20.5
19
17
15.5
15
14
14
17.5
21
25.5
64
68
69
69
68.5
68
68
68.5
70
73.5
80
59
63
65
67
67
66.5
65.5
65.5
68
72
79
F'i
3 .
. TREATMENT :
:LE PROPERTIES
1
Temperature
Prr,,
2
02
N/mm
N/mm
- li
tm elongation (7.)
elongation
.. )<
(7.)
ilon of area (7.)

basis of the initial
.* diameter)
tion of area (7.)
.he basis of the diametn the uniform deforma. zone of a broken
le).
UJ
TENSILE PROPERTIES Ol- (J - 12 . Cr SLLLb

1. SAMPLE Nr. (
2.
2446IR
C3^
ClIKMICAL C OMPOSITION (7.)
Sam;
24/,,
Si
Cr
Mo
Ni
"
Nb
Co
I
1
FIi .L TREATMENT :
1 hour
7l0C
+ 10C.
3. T) . ILE PROPERTIES
.-.._
Proi-
Mes
Temperature
~~_____^
- R . 002
'
- Riu
/ 2
/mm
2
/mm
400C
500eC
600 e C
550 e C
RT
100C
150C
200C
250C
300C
350'C
491
466
461
451
441
437
422
412
368
334
284
706
652
638
628
618
613
589
569
486
407
348
22
17.5
17
15
14
13
12
12
15.5
18
20
65
66
65.5
66
66
66
67
68
71
75
79
. - Un. io in elongation (7.)

' - Total elongation
(7.)
- Reduction of area (7.)

(ou liL- basis of the initial
ii. : pi diameter)
(,,n the basis of the diame
, ample) .
1
I
1. S. I'lEJJr. (
2 . C l:
2A462
II CAL C OMPOSITION
(7.)
lo
Si
Mn
0.14
0.2
0.79
0.008
0.012
24', 2
1
Cr
Mo
Ni
Nb
Co
9.25
1.9
< 0.1
0.08
0.29
0.41
0.023
600'C
FINAL TREATMENT
~~~~^_____^ Temperature
Properties
~~~________^
2
R 0.002
/nun
''
2
Rui
/mm
Uniform elongation (7.)
Total elongation
(7.)
deduction of area (7.)

. unple diameter)
ier in the uniform dforma
hample).
RT
100C
150C
200C
250C
300C
350C
400C
500'C
550'C
525
486
481
476
471
461
451
441
397
353
304
716
647
633
618
608
598
594
574
505
437
358
15
11
6.5
6.5
21
17
15
14
13
12.5
12
12.5
14
16
18
68
68
69
70
70
70
70
70
71
73
77.5
63
64.5
66
67
68
68
68
.68
69
72
76
UJ
ItMbiLL
1. SAMPLE Nr. (
24462 R
Ol'LIU ILO Oi
. L I
O ^ L J
Co
2 . C 1IEMIG\L C OMPOSITION (7.)
Sample
Si
Cr
Ni
Mo
Nb
Co
I
24462
0.14
0.2
0.79
0.008
0.012
9.25
1.9
<0.1
0.08
0.29
0.41
0.023
600" C
FINAL TREATMENT
1 hour
710C
+ 10C .
""^^_^
' Properties
Temperature
~" ______^
' 1 0.002
M /mm
2
! ...
/mm
, Uniform elongation (7.)
' Total elongation
(7.)

tample diameter)
(on the basis of the dlame
er In the uniform deforma
ion zone of a broken
it imp l e ) .
400C
500 e C
550 e C
427
412
368
348
294
598
579
564
495
441
368
8.5
7.5
7.5
6.5
17
16
14
13
12.5
14.5
17
19.5
68
68.5
69
69.5
69.5
69.5
71
74
80
65
66
67
67
67.5
68.5
72.5
77.5
RT
100 C
150C
200C
505
476
466
451
441
432
706
652
628
618
613
13.5
12.5
10.5
9.5
20.5
20
18.5
67.5
67.5
63
64
250C
66.5
300C
350 C
j
1

1.
.AMPLE U r .
2.
iiiEMIC Al, C OMPOSITION
S....pie
24463
24463
)
(7.)
Si
Cr
Mo
Ni
Nb
Co
550eC
600 C
1 I NAL TREATMENT :
3. 'ir.NSILE PROPERTIES
'~^_
Proporties
Temperature
~~~"^~
RT
100C
150C
200C
250C
300C
350C
400C
500C
481
432
422
417
415
412
407
392
358
324
265
687
628
608
598
603
589
569
549
476
412
324
Uniform elongation (7)
13
12.5
12
10
6.5
., tal elongation
22
20
18.5
17.5
16.5
15.5
15
14.5
16.5
18
20.5
68
70.5
71
71
70.5
70
69.5
69
71.5
74
79
63
67
68.5
68.5
68
68
67.5
67
69.5
72.5
77.5
i 0.002
''
I'm
2
/mm
2
/mm
(7.)
lurt lon of area (7.)

( LIII basis of t lie initial
. nip] e diameter)
.in 1.1 on of area (7.)
.n iLe basis of the diame
r In the uniform deforma
ion .one of a broken
'iip! ).
UJ
VO
TENSILE PROPE RTIE S OF 9 - 12 7. Cr STE E LS

1. SAMPI.; Nr.
2.
CIlKli
24463 R
\L COMPOSITION (7.)
Si
Mn
Cr
Mo
Ni
Nb
Co
24463
FINAI TREATMENT
'IEN'. ..K PROPERTIES
Temperature
opei
fi
Km
.it
ae
2
/mm
2
M /mm
.m elongation (7.)
elongation
(7.)
Lion of area (7.)

( on ti. basis of the initial
a am pi diameter)
Redo tion of area

tuo
1 e:
(7.)
lie basis of the diame
li the uniform deforma
tone of a broken
).
200C
250C
300C
350C
400eC
422
407
402
392
387
633
608
598
594
589
12
11
10
21.5
20
18
16
65
68
68
60
63
64
RT
100C
150C
481
427
697
14
500C
550"C
373
334
299
250
574
549
466
402
319
6.5
6.5
7.5
8.5
10
15
14.5
14.5
14.5
16
19
23
67.5
67.5
66
66
67
70
75
80
64
64
64
64.5
.65
67
72
78
600 C

1. SAMPLE Nr. ( 24464
2. CHEMICAL COMPOSITION (7.)
Sample
24464
C
O.I2
Si
Cr
Mo
0.32
1.05
0,06
0.009
9.1
2.02
Ni
<0.1
0.06
Nb
V
0.23
0.47
Co
0.021
FINAL TREATMENT
.
' Properties
Temperature
' ..
RT
100C
150C
200C
250C
300C
350C
400 e C
500C
550C
600 C
515
466
461
451
446
441
432
417
373
348
294
706
633
618
603
594
584
569
549
491
422
343
/mm
15
10
4.5
3.5
2.5
2.5
Uniform elongation (7.)
23
19
17
15.5
14
13
12
12.5
14
16
18
Total elongation
69
69
69.5
70
70
70
70.5
70
70
74.5
78
65
66
67
68
68
68
68
67.5
68.5
73
77.5
1 R 0.002
P
Kin
/mm
2
(7.)

sample diameter)
tion ..one of a broken
samp)u).
TENSILE PROPERTIES Ol 9 1. SAMPLE Nr.

2.
24464 R
12 V. Cr STEELS
CHEMICAL COMPOSITION (7.)

Sample
24464
Si
0.12
0.32
1 hour
FINAL TREATMENT
Mn
1.05
710C
S
0.006
Cr
Mo
9.1
0.009
Ni
(0.1
2.02
0.06
Mb
0.23
Co
0.021
0.47
+ 10C.
...
Properties
Temperature
- R 0.002
- Rm
/mm
2
/mm
- Uniform elongation (7.)

- Total cloigation
(7.)

(on thu basis of the initial
nample diameter)
nam pi <.-) .
RT
100C
150C
200C
250C
500
456
441
437
432
697
638
618
608
15
11
20
17
63
57
300C
350C
400C
500C
422
412
402
363
324
270
598
589
569
544
481
412
343
7.5
5.5
5.5
7.5
6.5
16
14.5
14
12.5
11.5
11.5
15
17
20
66.5
67.5
68
68
68
68
68
71
74
77
62.5
65
65.5
66
66
66
65
69
72
76
550C
600 C
' I t i l i ILL. l - K u r t i U l L J
1. SAMPLE Hr. ( 24457 R
ur
J -
/. ui
jjuuu
2. Gl EMI CM, COMPOSITION (7.)

'amplc
Si
Mn
Cr
Mo
Ni
Mb
Co
24457
FINAL TREATMENT :
3.
1 hour
7 l O C
10C
TENSILI: PROPERTIES
._
Properties
Temperature
.__
R O.ii.
P
Rjn
2
/mm"
2
/mm
Unifonn elongation (7.)

Total elongation
(7.)
Redu< ion of area (7.)

(on clu basis of the initial
nampl .: diameter)
clon .one of a broken
sampl .) ,
RT
100C
150C
200C
250C
300C
350C
491
461
446
432
422
417
412
687
638
618
598
594
584
10.5
11
10
21
19.5
18
17
67
69.5
70.5
61.5
65.5
67
400C
500C
550 C
600 C
397
363
329
265
569
549
476
407
329
6.5
6.5
5.5
4.5
15
14
14
14
15
17
20
71
71
71.5
72
71.5
71.5
77
82.5
67.5
68.5
69
69
69
69.5
75
81
UJ
*
*.

1. SAMPI
Nr. ( 24460
2 . HE I-.
\L COMPOSITION (7.)
""L
Si
Cr
Mo
Ni
Nb
Co
2446
1
F I / . . TRE ATME NT
i TE U: E
PROPE RTIE S
RT
il." OpC- .
RO.
Rm
-
Unjj
/mm 2
515
476
/mm
711
un elongation (7.)
13
'2
elongation
(7.)
Tor
Red . ion of area (7.)
(on . basis of the initial
oai,
diameter)
Red.
(ou
te.
tl,
U.i.
100 c
lion of area (7.)

ue basis of the diame
r n e of a broken
.).
150C
200C
250C
300C
350 e C
400'C
500C
441
440
437
427
387
353
294
353
550 e C
600 C
451
446
652
633
618
613
603
589
574
505
441
7.5
6.5
6.5
7.5
6.5
3.5
24
18
16
15
14
13
13
13
15
16.5
66
68
69
18
70
70
70
70
70
72
74
79
69
69
69
70
72.5
78
63
65.5
67.5
68
68.5

1. SAMPLE Nr.
2.
24460R
GI EM I CAL COMPOSITION (7.)
Sample
r
Si
Mn
Cr
Mo
Ni
1
I
Nb
"
Co
24460
I
FINAL TRE ATME NT :

3 . TE NSILE
~~ .
Properties
1 hour
710C
+ 10C.
PROPE RTIE S
Temperature
""
^_
R 0.0O2
P
Rm
U/mm
2
/mm
RT
100C
150C
200C
250C
300C
350C
400C
500 e C
550 e C
600 e C
525
481
461
451
441
432
422
412
378
363
299
736
662
638
628
623
613
594
579
505
451
343
21
18
16.5
15.5
15
14
13.5
13
15
Unifoun elongation (7.)

Total elongation
(7.)
16

(on tiu basis of the initial
nnmple diameter)
sample).
18
1
'
66
68.5
70
70
68.5
68
68
68
71
80
75
I
I

1. SAMPLI. Nr. ( 24465
.c
2. ClIEMIi'.L COMPOSITION (7.)

Sample
24465
Si
0.135
0.4
1.03
0.007
0.009
Mo
Ni
2.01
<0.1
Cr
9.24
Nb
0.09
0.23
Co
0.48
0.021
550C
600 C
FINAL TREATMENT
3. TENSI1 I. PROPERTIES
.
Properties
Temperature
~~~-_____^^
RT
100C
150C
200C
250C
300C
350C
400C
500C
- R 0.0".'
2
/mm
2
495
466
451
446
444
441
437
432
397
353
299
687
638
618
608
603
603
594
574
491
427
358
- Rm
/mm
12.5
10
6.5
6.5
- Unifoiui elongation (7.)
20
17
15.5
14
13
12.5
12
12.5
15
17.5
20
- Total elongation
(7.)
- Reduci.ton of area (7.)
(on tiu basis of the initial
sampl, diameter)
- Reduci ion of area (7.)
(on t:.u basis of the diame
ter lu the uniform deforma
tion .-.one of a broken
sampl ).
69
69
69.5
67
64
66.5
68
68
69
73
76
65
65.5
65
62.5
61
63
65
65.5
67
70
73
TENSILE PROPE RTIE S OF 9 1.
AMPI
,i.
2.
ULM'
. COMPOSITION (?.)
l'i
'
24465 R
4465
SI
,,,
Cr
0.4
1.03
0.007
0.009
9.24
Mo
Mi
0.135
1 hour
710C
2.01
(0.1
0.09
i
Mb
FINAL . . :
3 . TENS 11
12 /. Cr STLLLb
Co
0.23
0.48
4 00 C
500eC
550C
600C
0.021
10C.
PROPERTIES
Icmperature
R 0,
Rjn
. elongation
elongation
RT
100C
150"C
200C
250C
300C
350C
2
/mm
495
466
451
437
432
422
407
397
368
334
280
/min
701
647
628
613
608
594
574
549
486
417
343
(7.)
12.5
12
10.5
9.5
8.5
10
(7.)
20 5
20
19
17
15
13.5
12.5
12.5
15
18
22
64
66.5
67
67
67.5
67
66.5
67
69
73
78
60
61
62
63
64
64.5
65
65
67
71
77
on of a r e a
(7.)
e.i r. i s of t h e i n i t i a l
diameter)
J on of a r e a
(7.)
Lr: b a s i s of t h e d l a m e . t h e u n i f o r m do f orina. nie of a b r o k e n
) .
7.5
..
-J
TENSILE PROPERTIES OF 9 1 2
7. Cr STEELS
.AMI'!
Mr. (
III':
L COMPOSITIOM (7.)
,4b,
II..
24466
Si
Cr
Mo
Ni
0.12
0.29
1.01
0.007
O.Ol
9.19
2.01
< 0.1
w
0.08
Nb
Co
0.24
0.45
0.022
TREATMENT
PROPERTIES
Temperature
.:
/mm
2
/nun
. elongation (7)
elongation
(7,)
Ion of area (7,)

diameter)
Ion of area (7.)
e basis of the dlame
the uniform deforma
tine of a broken
).
RT
100C
150C
200C
250C
300C
350C
400C
500C
550C
600 C
510
476
461
451
448
446
432
427
397
368
314
706
643
618
608
606
603
589
564
500
446
373
12.5
9.5
4.5
4.5
18
15.5
14.5
13.5
12.5
12
12
12
13
14
16
69
70.5
71
70
70
70
69.5
70
70
73
76
65
67.5
68
68
67.5
67
66
66
68
71
75
1. SAMI'
2 . CULL
Ur. ( 24466 R
TENSILE l'Kul'LMU li.b ui y u
/. n
Mo
OILI.L,;
'.!, COMPOSITION (7.)
S am
Si
Cr
Mi
Hb
Co
2446..
0.12
0.29
1.01
0.007
O.Ol
9.19
2.01
. 0.1
FIN
TREATMENT
3 . TIA'
1 hour
Temperature
- Rui
Ui.
Tc
Re
( On
il ..
Re
(.
te
t I
n.
0.022
0.24
0.45
400C
500C
550C
600 e C
+ ]0C.
'ROPE RTI ES
Prop.
-Ri,
I-
710UC
0.08
M /mm2
2
N /mm
.... elongation (7.)

ongat ion
(7.)
! on of area (7.)
,.is is o C the initial
. diameter)
; 1 on of area (7.)
M basis of the diame
.one of a broken
).
RT .
100C
510
150C
200C
250C
300C
476
461
446
441
432
427
412
378
338
284
711
657
633
618
613
603
589
564
491
422
343
16
10
8.5
7.5
6.5
5.5
5.5
6.5
20.5
17
15.5
15
14.5
14
13
13
17
19
20.5
64
65.5
66.5
67
68
68
67.5
67.5
70
72.5
78
58
62
63
65
65.5
65
65.5
67.5
70
77
65.5
350C
vC
TENSILE PRO PERTIES O F 9 - 12 'L Cr STEELS

1. SAM. . KJIr. (
2. CUI
25588
,1. COMPOSITION (7.)
Sami :
Si
Mn
2558
0.135
0.35
0.91
0.008
Fi
TREATMENT :
3. TEI
Temperature
RT
2
- Toi
- Re
( Oll
sa.
0.004
9.64
1.9
0.09
< 0.05
0.26
Nb
Co
05
100C
150C
200C
250C
300C
350C
400C
500C
550C
600 C
466
437
441
441
437
422
407
343
299
245
687
618
608
598
594
589
574
540
446
383
314
.. elongation (7.)
13.5
10
2.5
2.5
elo i-ga tion
21.5
18
17
15
13.5
12.5
11.5
12
15
17.5
22
68.5
70.5
71
71.5
71
70
69
68.5
71
74
80
64
67.5
69
69
68.5
67.5
66.5
66.5
69.5
72.5
78
/mm
/nun
(7.)
1 on of area (7.)
nas 1 s of the initial
diameter)
.I.
- Re
(.
te
tl
Ni
495
)'
- Rn,
Uni
Mo
1 I: PROPERTIES
Proi
- R .
Cr
Ion of area (7.)

e basis of the diameLhe uniform deformaone of a broken
).

1. SA; ..lj_N_r. (
2.
Clii
27433
. AL COMPOSITION
Sa.,,,
274
0.137
FI.
TREATMENT :
(7.)
Si
Mn
0.34
1.19
Cr
0.006
0.015
9.92
Mo
Ni
2.1
0.09
0.08
0.34
Nb
Co
0.47
0.02
: K PROPERTIES
ies
R
I'
Temperature
"
-^_____^
t1
fi
250C
300C
350C
400C
500C
550"C
600 C
471
456
446
441
437
427
387
363
299
726
672
647
638
633
623
618
594
515
446
373
m elongation (7.)
11
10.5
9.5
5.5
21
19
17
15
13
12.5
12
12
14
17
20
64
66
66.5
66.5
66.5
67
67.5
67.5
68
71
76
57
61
63
64
65
65
65
65
66
69
74
/nun
(7.)
T..
t.
200C
491
elongation
R
(.
150C
530
/mm
Ui
(.,
fl.
100C
2
'i.'
Ru,
R.
RT
.Ion of area (7.)

. basis of the ini tial
lv' diameter)
ion of area (7.)
'.he basis of the d iame
;
n the uniform deforma
tone of a broken
'<).
I
UT
TENSILE
l'KUl'bKllL
Ol
. u i
iitiiLS
Ul.|
1 SA:
2
CII
Ur.
27433 R
M. COMPOSITION (7.)
Mn
SI
Sa.;
274
0.137
TREATMENT :
3. TI
0.37
1 hour
0.006
1.19
710C
Mb
Cr
Mo
Ni
9.92
2.1
0.09
0.08
0.015
0.34
Co
0.47
0.02
10C.
i. PROPERTIES
Temperature
RT
100C
150C
200C
250C
300C
350C
400 C
500 e C
550C
600C
Pre;
- \'.
,'
- R.
-
Ui
, 2
11 /mm
. 2
M /mm
,,,. elongation (7.)

elongation
(7.)
, 1 on of area (7.)
diameter)
Ion of area (7.)
e basis of the diame.. the uniform deforma
rne of a broken
) .
530
491
481
471
460
441
427
422
383
348
284
746
677
662
647
638
628
608
584
495
422
353
13
11.5
10.5
3. 5
4.5
7.5
16
17
16.5
16
15
14.5
13
12.5
15
19
24
61
63
64
64
64
64
63
63
67.5
72
.
77.5
55
59.5
60.5
61.5
62
61
60.5
60.5
70
75
1
1

1. S/
Nr.
2.
.1 COMPOSITION
CI
27435
)
(7.)
Sa,,
Si
Mn
274
0. 122
0.28
0.96
0.007
O.Ol
Cr
9.57
Mo
Ni
2.02
0.07
0.08
Nb
0.32
0.46
550C
Co
0.018
TREATMENT
3.
,F PROPERTIES
r
Temperature
RT
100C
150C
200C
250C
300C
350C
400C
500C
486
451
437
422
417
417
407
397
353
319
270
687
628
613
603
594
584
574
549
481
407
334
11
10.5
9.5
8.5
7.5
20
19
18
16
14.5
13
12.5
12
14
19
60.5
68
70
70.5
70.5
70
69
69
68.5
72
75
78
64
67
67.5
67.5
67.5
66.5
66.5
67
70
72
77
Pm
- 1'
it'
/nun
- I',
-I
/mm
... elongation (7.)

elongation
(7.)
; lon of area (7)

Las is of the initial
diameter)
1 on of area (7)
, e baste of the diame. the uniform deforma
rne of a broken
) .
600'C
un
u>
TENS I L L
l ' l v O l ' U U J L J -
'J -
' V.I
ol LUL
1. s
I . Ci
II.:.
27435 R
M COMPOSITION (7.;
Sa
0.122
27
Cr
Mn
Si
0.28
0.007
0.96
l
TREATMENT :
hour
l l 0
3.
Pr
H /mm
,. elongation (7.)
elongation
(*/.)
on of area (7.)
,a s is of the initial
diameter)
Ion of area (7.)
i,e basis of the diame.. the uniform deforma
. ,ne of a broken
I
"c
1 0
C'
0.01
9.57
Mo
2.02
Hi
0.07
0.08
Mb
0.32
0.46
Co
0.018

SAMPLE Mr. (
29344
Cl'.i ,11 CAL COMPOSITION (7.)

S.e , U!
. i'..',
Si
0.12
0.37
Mn
Cr
Mo
Ni
0.007
9.55
2.05
0.08
1.04
0.008
RT
100C
150C
471
427
67 7
< 0.05
Nb
Co
0.32
0.42
::\L TREATMENT
. ILE PROPERTIES
--_______^ Temperature
.Lies
' _^__
'..002
/nun2
2
/nun
.i Torrn elongation (7.)

. .il cl ongation
.Liet lon of area
(7.)
(7.)
200C
250C
300C
350C
400C
500C
550C
600 C
417
407
405
402
395
373
343
314
270
613
598
589
585
574
554
530
461
407
343
17
12.5
11.5
10
8.5
7.5
24.5
20.5
19
17.5
16
15
14.5
14.5
17.5
21
26
70
70
70
70
70
70.5
70.5
71
73
75
79
65
66
66.5
67
67.5
67.5
68
68.5
70
73
76.5
t 'ie b .is Is of the initial
.pie diameter)
luction of area (7.)
the baslH of the diame. in the uniform deforma
nti zone of a broken
...le) .
1 bica ILL. r n u t x i u I I , J
1. SAMP
Mr. (
2.
L COMPOSITION (7.)
CHI;
29344 R
j -
i<_ /. . J H . L .
Si
in
Cr
Mo
Ni
1
1
Nb
2934
0.12
1
0.37
1.04
0.008
0.007
9.55
2.05
0.8
< 0.005
0.32
0.42
I
Fil
. TI
Co
TREATMENT
1 hour
710C
H- 10C.
1: PROPERTIES
Temperature
350oC
RT
100C
150C
200C
2
11 /mm
2
M /mm
466
442
412
402
397
387
383
373
682
623
608
594
584
579
559
in elongation (7.)
16
11.5
10.5
10
9.5
I l i .
250C
300C
400 C
500C
550C
600C
334
304
255
535
466
397
319
7.5
6.5
elongation
(7.)
21
19
18.5
17
16.5
16
15
14
16
19.5
23
'..ion of area
(7.)
66.5
67.5
68
68
68
68
68
68
71
"
80
62
64
65
65.5
66
66
66
66
67.5
78

diameter)
ion of area
(7.)
lie basis of the diame

tone of a broken
) .
TENSILE PROPERTIES OF 9
SA.
. Hr. (
29345
12 7. Ci STEELS
I. COMPOSITION (7.)
'
Si
"
'
'
Mn
Cr
Mo
Ni
Nb
Co
1.05
0.008
0.007
9.54
2.05
0.073
C 0.05
0.33
0.42
0. 12
0.36
. TREATMENT :
I ; PROPERTIES
Temperature
RT
100C
150C
200C
250C
300C
350C
400C
500C
550C
600C
471
427
417
402
402
402
397
383
348
314
260
672
613
594
589
598
589
569
540
471
417
343
15
11
7.5
7.5
7.5
7.5
21
19.5
18
16
14
13.5
13
13.5
16
17.5
19
lon of area (7)

ias 1 s of the Initial
diaine ter)
69
70
71
71
70.5
70
69.5
69. 5
72
75.5
80
Ion o area (7.)

e basis of the diame
the uniform deforma
tine of a broken
) .
65
67
67.5
68
68.5
68
67.5
67; 5
70
74
78
/mm
2
'
/mm
elongation (7.)
longa ti on
(7.)
TENSILE PROPERTIES OL y U
/.Li sitt,Lb
UI
O.'
1. SAMPI
Nr. ( 29345 R
2 . GlE Mi
. COMPOSITION
('D
Sampli
Si
Mn
29345
0.12
0.36
1.05
0.008
0.007
Cr
Mo
Ni
Mo
Co
9.54
2.05
0.073
. 0 . 0 5
0.33
0.42
FINA
3 . TE NS
, :
* our
710C
+ 10C.
PROPERTIES
Temperature
RT
100C
150C
200C
250C
300C
350C
400-C
500C
550C
600C
' Propc
ti /mm
. 2
/mm
' - R 0.
?
-
Rjn
- Uni.
, e l o n g a t i o n
,-longation
(7.)
(7.)
' - Tot
-
Red
( on
nan,,
- Ree,
(,
ter
'
ti.
Dilli
Ion of area (7.)

was is of the init ial
diameter)
ion of area (7.)
,: 'oasis of the diame, the uniform deforma
rne of a broken
).
432
412
407
397
392
387
373
334
304
363
471
628
608
594
589
584
574
540
466
402
329
701
18
15
13
11.5
10
22
19
17
16
15
14
13
12.5
15
17.5
21
66
69
69.5
68.5
67.5
67
67.5
72.5
76
81
53
64
67
67
66
64.5
64
65.5
71
74
79
45
7.5
6.5
- 59 II

b.
The CEA contribution NF A 49811 Steel
DEPARTEMENT DE TECHNOLOGIE
Note Technique
"'
. 1QS1
Septembre 1981
SERVICE DE RECHERCHES
METALLURGIQUES APPLIQUEES
GROUPE DE METALLURGIE MECANIQUE
COMPARI SON OF TENSILE PROPERTIES OF 9 - 1255 Cr STEELS

REPORT 1
P. PetrequI
ABSTRACT
This report sunmrri zes the input from France in The data collection
on tensile propertier, of 9-12 Cr steels.
'O
DEPAKlE-ENT bC TEC1N0LOGIL
SERVICE DE FECILERCHES
Note Technique
D.Tech.RMA
Septembre 1981
GROUPE DE METALLURGIE MECANIQUE
COMPARISON OF TENSILE PROPERTIES OF 9 - 12 % Cr STEELS

REPORT 1
P. P e t r e q u i n
CONTRAT SAV
1 - INTRODUCTION
The activity 3 "materials" of the working group on
"Codes and standards" of the "Fast breeder coordinating committee" of the
"Commission of European Communities" has started a joint programme on "Comparison
of tensile properties of 9 - 12 Cr steels".
Tensile properties of 9 Cr 2 Mo steels determined in France
are gathered and collected in this
frame.
This report gives informations on the extent of data and the

collection of tensile properties.
2 - EXTENT OF DATA
26 heats were studied and in some cases, different heat
treatment on the same heat were examined. That leads to a total of 32 different
sets of datas.
Chemical composition was measured on all heats. Microscopic
examinations in order to determine ferrite content and grain size were made
on 11 heats and aie with 2 heat treatment.
Tensile properties at room temperature aregiven
in all
cases., but at high temperature only in 13 cases.

A summary of data is given in Table 1 with some informations
on product shanes-and dimensions when available.
61
- 2
3 - CHEMICAL COMPOSITION - GENERAL CHARACTERISTICS

This steel correspond to a French standard NF A 49811.
This is a steel with a duplex structure ferrite + martensite used in the state
air quenched + tempered. Ferrite content is generally widely controlled by niobium
and carbon contents.
This steel is standardised only for tube and pipes.
Chemical compositions of the 26 heats are given in table 2.
4 - HICTOSTRUCTTJRE
Grainsize and ferrite content are given in table 3 for

11 different heats.
5 - TENSILE PROPERTIES
Table 4 gives tensile properties at room temnerature.
Tensile tests are run following NF standards unless indicated in the table
for the gage length.
Table 5 gives results obtained at 20, 300, 400, 450, 500
550n 600 C on 12 different melts.
(Tv
Shape
Meai:
number -
Heal treat ervt
dimensions
Air cjue.rvf.ri
Chemical
Tn^LLt p r o p e r t i e s
1
L
. . .
compo5irien rcoom lem parar. Hh temperature MicrSiYucluri

Temperi n g Table. I
Tabuni
Table Y
Table
0355
BF
1100 1/2 h
800 1/2 h
0503
T L I 6 I 14
1100* 1/2 h
800 1/2 h
5030
BF
1100 1/2 h
750 1/2 h
5030AC
BF
1100 1/2 h
700 1/2 h
5030AD
BF
1000 1/2 h
750 1/2 h
8178
BF
1100 1/2 h
800* 1/2 h
8234
BF
1100 1/2 h
725 1/2 h
8236
BF
1100 1/2 h
750 1/2 h
TF44 5,4
1 100 1/2 h
800 1/2 h
263961
TF38 5 , 6
1100* 1/2 h
815 1/2 h
263962
TF38 5 , 6
1100 1/2 h
815 1 h
26427A
TF51 6 , 3
1100 1/2 h
810" 4 0 mn
26427B
TF51 5
IIOO* 1/2 h
810* 4 0 nm
26598
TF51 6 , 3
1100* 1/2 h
800 1/2 h
26602
BF
1100 1/2 h
800 1/2 h
26627
BF
1100 1/2 h
775 1/2 h
26630
BF
1100 1/2 h
700 1/2 h
26932
TF51 8
1 100* 1/2 h
8 0 0 * 2 h 1/2
26941IA
TF57 10
1100 1/2 h
8 0 0 * *2 h 1/2
26941IB
TF51 6 , 3
1100* 1/2 h
800 1/2 h
26987
BF
1100 1/2 h
750* 1/2 h
27441
BF
1100 1/2 h
8 0 0 * 1/2 h
28826P6R
TF89 10
Fi lape
775 1/2 h
28826P6T
T F 8 9 10
I I O O ' 1/2 h
7 7 5 ' 1/2 h
29121
TF51 8 , 8
1100 1/2 h
8 0 0 * 1/2 h
29160
TF51 6,3
IIOO* 1/2 h
800 1/2 h
29168
TF51 5 , 6
IIOO* 1/2 h
800 1/2 h
29183
TF51 8 , 8
I I O O ' 1/2 h
800 1/2 h
29196
TF57 4
1100 1/2 h
800 1/2 h
292 79
TF44 8
IIOO* 1/2 h
800 1/2 h
29590
TF63 6 , 3
IIOO* 1/2 h
790* 1 h
TF63 6,3
I I O O ' 1/2 h
790* 1 h
X
1
29592
TABLE I
TABLE
f" DlrTEEMT
PRuCTS
TESTES ,
6F: Forged oar 4>25

TL : rlolleA fute
TF : Extruded, tubes
frtjm
- 63 -
NF A 49 811
0
0
5
8
8
8
355
503
030
178
234
236
J!
E
3
C
-a
=c
26 396
26 427 +
26 598
26 602
26 627
26 630
26 932 +
26 941
26 987
27 441
28 826 +
29 121
29 160
29 168
29 183
29 196
29 279
29 590
29 592
Si
Mn
Cu
Cr
150
700
700
1 400
:
35
4:
'-
8 400
10 650
110
90
90
100
85
105
115
145
1 12
118
125
135
85
127
120
90
130
210
350
280
320
410
390
60
292
340
265
420
380
400
340
350
500
290
360
13
15.
17
16
28
28
13
14
12
I1
18
20
I1
15
13
13
18
18
11
17
1I
8
19
22
10
10
17
14
8
IO
IO
13
18
19
19
22
6
8
8
23
23
7
8
17
1I
17
15
15
21
13
12
13
100
115
150
125
125
125
9 850
9 450
9 200
9 700
9 700
9 800
9 300
9 900
10 070
8 760
9 550
9 450
9 250
10 400
9 550
9 200
9 900
9 370
10 230
10 690
8 550
8 750
8 800
10 030
9 500
9 650
170
1 IO
109
107
85
85
120
1 13
1 15
105
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
4'41
400
365
390
315
401
310
315
+ Chemical analysis
!
1
1
1
1
930
090
080
060
100
090
960
082
100
950
030
100
020
160
960
020
130
950
250
140
975
105
100
090
035
060
35
40
70
105
120
80
60
25
15
IO
10
20
1 650
2 380
250
600
180
430
1
2
2
2
2
2
2
2
2
1
1
2
1
1
1
2
2
I
2
2
2
2
2
2
2
2
120
245
400
350
480
420
400
415
480
371
510
520
420
457
414
440
350
356
272
308
360
315
380
399
410
345
275
350
320
310
260
270
240
240
300
260
300
320
310
335
310
310
360
280
285
340
235
285
245
285
305
365
980
300
080
300
300
200
080
085
030
900
800
050
930
940
950
040
180
940
036
050
020
000
040
022
130
130
on. melt
++ .This, vcdiie Is (Nb+
ahoiA 5.0.-5
Ta is
NS .- urAer[ne.(L i/riJiios are, ixtskie.
TA&LE 31 -
Nb++
Mo
CHEMICAL ANAL/S'S
( T o km/e %
ivie
AFr-lR
.
ach
NFA 4-9&
JALDES
value
ahmaani.
1/4 -t~5
by I000)
- 64 -
Heal n u m b e r
Grain
size.
( AFNIOR )
Lona
"Fransve/-se
""
1 1
22
26 396 - 1
10
14
26 396 - 2
10
16
26 598
10
33
10
20
29 121
30
29 160
10
36
29 168
10
30
29 183
24
26 941 -
29 196
30
29 279
10
34
Ferrite
TABLE 3.
34
0 503
(1)
Ferrite content ['/.)
Curitene' is. aeitrm i neA
STEEL
GRAIN
by micrographie ergami natilo .
2 _
.S E
FERRITE CONTENT
- 65 -
RO,002(MPa)
NF A 49811
R m (MPa)
>, 390
mn
590
L
3
C
OJ
re
(+)
512
538
564
651
539
504
512
548
451
601
558
514
471
487
480
508
490
450
477
613
500
532
550
530
455
534
440
461
381
469
482
480
0355
0503
5030
5030 AC
5030 AD
8178
8234
8236
"X"
263961
263962
26427A
26427B
26598
26602
26fi27
26630
26932
269411A
269411B
26987
27441
28826P6R
2S826P6T
29121
29160
29168
29183
29196
29279
29590
29592
Strain, m e a s u r e a .
Okker
on.
s t r a i n vaLues
TALE 32*. TENSILE
(%)
707
728
710
793
709
687
677
710
633
795
770
693
691
734
676
703
652
662
677
796
651
729
715
693
705
746
637
656
649
695
657
666
Spec.im.en. .
15
740
maxi
20 ( + )
19 (+)
18 (+)
15 (+)
19 (+)
20,5 (+)
18 (+)
18 (+)
27,5
20
19,5
21
24
27
17,5 (+)
18,5 (+)
17,5 (+)
26
24
21
20,5 (+)
19 ( + )
22,5
22,5
25
23
31,5
28
30
24
23
21,5
S^VSQ
are
mezrsurea
PROPERTIES
on.
gage
Lengrrt or
A T K0OM TEMPE FEATURE
5,GS \ / s c
04
04
04
04
04
0
0
0
0
0
0
0
0
4
4
4
4
4
4
4
4
20C
Heat num Ler
0,002
MPa
m
MPa
300C
A
0,002
Rm
m
MPa
400C
A
0,002
MPa
450C
MPa
0,002
MPa
MPa
500C
A
0,002
Rm
MPa
MPa
" "
451
633
27.5
370
508
22
348
491
20
301
MPa
466
263961
601
795
20
489
656
16
482
640
16
458
263962
558
770
19.5
461
637
15
448
614
17
26598
487
734
27
443
640
25,5
408
601
23,5
408
587
269411
613
796
21
538
682
15,5
489
658
16
490
29121
455
705
25
412
622
19
412
595
19,5
29160
534
746
23
479
650
17
473
633
29168
440
637
31,5
378
543
23,5
381
29183
461
656
28
392
572
25
29196
381
649
30
355
581
29279
469
695
24
439
29590
482
657
23
29592
480
666
21,5
TABLE I g " .
TENSILE
550C
A
0,002
MPa
600C
Rm
MPa
MPa
0,002
MPa
24
291
407
26
256
357
37,5
586
18,5
434
519
23
388
433
27,5
424
555
15,5
395
472
20,5
359
408
27,5
19,5
380
537
26
344
463
30,5
305
379
36
629
16,5
436
548
17
438
500
23,5
371
428
29,5
402
578
19
355
519
23
351
471
27
309
382
31.5
14
451
609
16,5
422
555
20,5
39b
496
21,5
340
401
29.5
540
21,5
354
503
22
340
486
27
300
413
27,5
257
321
39,5
404
556
20,5
386
534
17.5
362
489
23
305
410
29.5
265
339
36
23,5
362
555
21
339
539
21
321
510
24,5
294
437
31
253
353
38
607
21
392
555
20,5
410
569
20
379
518
21,5
349
458
25
284
345
34
428
572
17,5
412
556
19
375
494
22
337
436
22
299
363
31,5
379
578
21
401
552
17
360
504
20
324
430
27
298
367
30
PROPERTIES A T
Hl'H
TEMPERA TRE
67
III
Subfile 12% Cr steels

a.
The Interatom contribution X20 CrMoVW 12 1 steel
bv Neratoom
Postbus 93244
2509 A E DEN HA A G
Laan van Nieuw Oost Indie 129-135
Teleoon internationaal + 3 1 70 81 48 21
Telefoon nationaal (070) 81 48 21
Telex 32595 nera ni
Telegramadres Neratoom Den Haag
Datum
.
U w
ref :
Onze rei.:
Qns n r
iErsiti2i
Betreft: FRCC WG C&S Act. No. 3
CEC Study Contract 1980
Agreement No RAP01180 NL()
Comparison of the tensile properties of 912% Cr steels
Part I (Data files)
Interatom Contribution
1.
The Interatom contribution relates exclusively to

X 20 CrMoWV 12.1 (DIN W.N. 1.4922)
The data concerning X 20 CrMoV 12.1 are added to
Neratoom subfile.
2.
Details on product form, chemical composition and

final heat treatment are given in Table 1.
3.
Data files on tensile properties over the temperature

range RT600C are as far as available given in Table 2
68
neratoom
4.
Contents
Specification:
Product:
Number of melts:
X 20 CrMoWV 12.1
vdTV Werkstoffblatt No. 110
Tube (3X), Billet (2X) , Bar (6X)
11
D i s t r i b u t i o n of t e n s i l e d a t a :
Temp ( C)
RT
0,2
m
A
11
Sincerely yours,
B.V. Neratoom
200
300
400
500
550
600
Table 1
Chemical composition % wt.
Ref.
1
2
3
4
5
6
7
8
9
10
11
Product
Section
Heat treatment
Si
Mn
Bar
150
1050C/oil-rT760C 5h AC
.17
.30
.57
.018
Bar
Bar
160
170
1030C 30' oil + 750C 3h AC
.19
.50
.56
.d.*
1030C 30' oil + 750C 2h AC
.20
.34
.50
Mo
12.13 .66
1.06
.37
.13
.d. 11.6
.60
1.08
.35
.59
11.7
.59
1.07
.35
.53
.009
Il
Cr
Ni
Tube
190x25
1030C 3h AC + 750C 3h FC to 600C AC .20
.45
.60
11.5
.62
1.12
.32
.53
Tube
190x25
No 4 + 700 C 100h AC
.20
.45
.60
11.5
.62
1.12
.32
.53
Unknown
.19
.28
.43
12.1
.20
1.04
.28
.45
Bar
18
Tube
57x 7
1050C AC + 780C AC
.19
.28
.43
12.1
.20
1.04
.28
.45
Billet
25 sq
1050C 20' AC + 750C lh AC
.19
.28
.43
12.1
.20
1.04
.28
.45
Billet
25 sq
1050C 20' AC + 750C lh FC
.19
.28
.43
12.1
.20
1.04
.28
.45
25
1050C oil + 775C 3h AC
.25
.46
.45
13.0
.09
1.06
.22
.53
420
1040C oil + 720C 8h FC
.22
.35
.52
12.0
.59
1.35
.31
.40
Bar
Bar
.d.
.011
.014
not determined
o^
VC
- 70 -
Property
*e'
"e"sei;.itv.re (Je. ees Cer.ti i j rade)

20
__-_ _
t-
--
- .o
'
731
21
350
04
687
!
|
!
. _ .- . .
. _.
573
"584" "
- . AJ U L i
R
ROf A
391 _
25
19,3
67
74
18
59
514
R
m
A
.54
V.O-J
492
418
768
.532
444
28
26
64
"p 0.2
514
452
441
418
770
22
636
602
570
21 " "
18
17
61
61
61
56
588
B_P.il
788
m
R of A
R
P 0,2
R
m
A
R of A
" o,2
"~
10
I1473
22"
R " "
m
" A "" "
~T~of "A
70
582
"~~"7
32.7J_
64
415
P. of A
""R of A ~~
I
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59
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70 - + 343
22
R
p ,;
R
Am
706
R of A
415
.21
R
Aa
343
""742
R Of A
j
[
538
59
554
23
-'.5 ,
198
395
23
26
71
488
12
i
1
77
1
1
i
450
798
18
284
352
59
61
62
72
341
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83
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_ 27_
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600
~49
21
348
26
550
5::-
R 'of I" '

"R ' .
_ iL-../R
200
71
1
71
Ref.
Tenpeature ; d e j rees Centri grade)
Property
350
450
4J0
530
_538_
q ?
u Â . . . .
__747__
22
R of A
300 J "
200
20
47
_._.:_r
!
LV
>'
R
550
600
386
317
535.
422__ _*_3_02.
.14.2 _
55
174
22,1
27_-6__.
80_.
89
_-
a
A
I
1
R of A
R
o 0,2
R
R of A
P 0.2
R
m
A
R Of A
P 0.2
r.
A
R Of A
P 0.2
P.
m
A
R of A
I
_
'
LP
o
R
.11
- ,-. - - r
R~oTT~
.Al
R
1
1
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R 0,2
,
R
iI
1
1
'
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R
" 0,2
R
R Of A
L.
I
i
- 73 -
Subfile 12%Cr steels
III
The Neratoom contribution X20 CrMoV 12 1 steel

bv Neratoom
Postbus 93244
2509 AE DEN HAAG
Laan van Nieuw Oo*st Indie 129-135
Telefoon internationaal +-31 70 81 48 21
Telefoon nationaal (O7081 48 21
Telex 32595 nera ni
Telegramadres Neratoom Den Haag
Datum
Uw rel.
Onze ref
Ons nr.
Betreft:
FRCC
WG
c&s
Act
No
CEC Study Contract 1980

Comparison of the tensile properties of 9-12% Cr Steels:
Part I (Subfiles).
This work is performed under Agreement Nr. RAP-011-80NL (B)
Neratoom Contribution
1.
The Neratoom contribution relates exclusively to

X20CrMoV12.1 (DIN W.N. 1.4922). The reference No 23,
24 and 25 are taken from the Interatom contribution
2.
Details of product form, chemical composition and

final heat: treatment are given in Tabel 1.
3.
Information relating to microstructure is not available.

In general the microstructure would be expected to be
martensitic with some delta ferrite and carbides (M23C6^ '
4.
Tensile tests were carried out in accordance with DIN

50140 for tubes and DIN 50145 for solid specimen. A num
ber of tests do not obey 1 = 5.dQ or a prescribed strainrate.
5.
Data files on tensile properties over the temperature

range RT-60GC are as far as available given in Table 2.
Additional heat treatments are indicated.
- 2 -
74
neratoom
Specification :
X 20 CrMoV 12.1
VdTV Werkstoffblatt. No. 110 (Juni 1962)
Product:
Tube (7x), Billet (9x), Bar (3x).
Number of Melts:
25
Distribution of tensile data
Temp (C)
RT
250
300
350
400
80
25
10
m
A
80
25
10
80
25
10
53
24
10
P 0,2
Sincerely yours,
B.V. Neratoom
450
500
550
600
Table 1
Ref. Product Section Steel
Process
1
Tube
2
"
3
"
4
"
5
"
6
"
7
"
8
Billet
9
"
10
"
11
"
12
"
13
"
14
"
15
"
16
"
17
Bar
18
"
H
19
M
20
21
"
22
"
23*
"
24*
"
25*
"
*) VDEh 1969
20.5
2.0
2.0
2.0
2.0
2.0
2,0
100
140
129
15
15
15
15
25
30
25
20
50
125
125
125
20
20
20
?
EA
EA
ESR
ESR
HV
HV
ESR
HV
HV
ESR
ESR
ESR
ESR
ESR
?
EA
ESR
ESR
EA
ESR
HV
?
?
?
Heat Treatment
1030C
1030C
1030C
1030C
1030C
1030C
105CC
1050C
1050C
1050C
1050C
1050C
1050C
Chemical composition % wt
C
Si
S
Cr
Ni
Mo
0.187
.d.
.d.
.d.
.006
11.1
.50
1.0
.32
AC + T 780C
.21
.48
.56
.007
.019
11.43
.50
.95
.32
AC + T 780C + 780C 2h
AC + T 780C
AC + T 780C + 780C 2h
AC + T 780C
AC + T 780C + 780C 2h
AC + T 760C 2h
oil + T 750C
oil + T 750C
AC + T 760C
AC + T 760C
AC + T 760C
AC + T 760C
?
.20
.46
.56
.010
.018
11.45
.50
.95
.32
.19
.39
.57
.009
.005
11.46
.50
.95
.32
.20
.38
.56
.007
.005
11.45
.50
.94
.32
.20
.47
.51
.010
.019
11.46
.50
.95
.32
.20
.47
.49
.006
.019
11.44
.50
.95
.32
.19
.41
.56
.007
.017
11.66
.63
1.07
.29
.21
.31
.40
.023
.007
12.14
.38
.97
.33
.21
.31
.40
.023
.007
12.14
.38
.97
.33
.17
.2
.6
.016
.005
11.0
.9
.9
.22
.13
.2
.6
.016
.005
11.6
.9
.9
.28
.18
.2
.6
.016
.005
11.5
.9
.9
.25
.21
.2
.6
.018
.005
11.3
1.0
.7
.26
.22
.25
.68
.d.
.d.
11.9
.79
1.05
.26
.17
.17
.38
.54
.018
.004
11.32
.58
1.00
.31
.22
.44
.52
.019
.005
11.2
.51
.93
.28
.20
.11
.51
.024
.005
12.4
.51
1.2
.31 < 0 . 2
.20
.11
.51
.024
.005 1 2 . 4
.51
1.2
.30 < 0 . 2
.20
.48
.56
.007
.018
11.4
.50
.94
.32
.20
.36
.56
.009
.004
11.4
.49
.94
.31
.20
.49
.49
.005
.018
11.3
.49
.95
.32
.20
.d.
.d.
.d.
n.d.
11.8
.16
.98
.30
.19
.d.
.d.
.d.
.d.
12.6
.16
1.00
.30
.21
.d.
.d.
.d.
n.d.
10.5
-16
1.02
.30
1050C AC + T 740C 2h
?
?
o,.
Forged + 700~C llh
As for ref.no 20
As for ref.no 20
1050C oil + T 780 C Ih AC
1050C oil + T 750C 2h AC
1050C oil+730C lh AC+780C lh AC
- 76 -
. ,.,...,ty
e* .
Tenpe ;.< tu re (dei.ees
250
300
350
400
t_z:
458
436
418
625
19_
610
590
20
530
755
enti j ' ade)
23
64...
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A
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430
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17
4?
15
402
533
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852
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rp
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429
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j
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82
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74
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69
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29
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17
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20
64
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300
460
535
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560
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350
300
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24
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535
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523
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R
m
49
19
_
384
413
849
l_
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P 0.2
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m
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530
795
600
._.47_.
560
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550
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5%
383
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796
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79
Property
Ref.
20
682" _
807
~"23_"
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" " 62
Ti-peij.iture (dec r e e s
Centi ijrade)
1
250
400
350
450
500
550
600
673
R
r.
798
'~R Of .'
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20
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II
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ir.
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m
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.
653
701
807
'
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R Of A
673"
p 0,2
R
l>.
. ..m
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56
~~ '653
~ 788"
% 0.2
22~
62
P Of A
788
A
R of A
21
f A " """
"692
A
j '
r II56
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j
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23-""
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- 80 -
Te-'^L-. .Iture jdfcjiee
Property
"f.
250
L *
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22
:
6
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72
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Property
250
20
R
p 0.2
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19
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19
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0^.2
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I
1
Cond. 15 with additional 1040C Jh + T 760C 2h

Cond. 15a with additional 760C 2h
I
I
1
1
I
.. .. m
542
7.40
"
ii
__20_
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820
in
'
605
12
635
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15b
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51
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545
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1 445
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R Of A
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64
57
P 0.2
R
m
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13
515
830 . . . .
12
i 425
600
R of A
600
R o f 7
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o
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Ref.
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A
R of A
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R
0.2
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R
p 0,2
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17
62
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i 680
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m
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A
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54
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54
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t
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943
18
52
600
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801
20
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Cond. 18 with additional 780 C
83
Property
Ref.
!ri"pn .iture
20
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301
250
819
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A
400
350
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58
R of A
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m
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26
59
18a Cond. 18 with additional 780C
t
!
400
26
74
351
1I
413
..]_.___
26
76
362
413
29
75
85
PART I I
(FINAL
REPORT)
H.C.D. Nieuwland, P. Petreqain, D.S. Wood
87
Contents
1.
2.
3.
4.
5.
Introduction
Assessment of tensile properties
. Subfile's
. Type of product
. Relative quality of the data files
. Comparison of mean values
Comparison of tensile properties
The effects of product form or steel making practice
Conclusions
Recommendations
Page
. .
89
90
90
90
91
91
93
95
97
98
List of tables
1.0
1.1
1.2
1.3
2.0
2.1
2.2
2.3
3.0
3.1
Chemical composition of 9% Cr-1% Mo-steels; cast (ladle)

analysis or product (check) analysis
Mechanical properties at elevated temperatures of
9% Cr-1% Mo-steels; R Q 2
9% Cr-1% M o - s t e e l s ; R
m
9% Cr-1% M o - s t e e l s ; A 5
Chemical composition of 9% Cr-2% Mo-V-Nb-steels;
cast (ladle) analysis or product (check) analysis
9% Cr-2% Mo-V-Nb-steels; R 0 T
p0,2
9% Cr-2% Mo-V-Nb-steels; R T
m
9% Cr-2% Mo-V-Nb-steels; A 5 T
99
100
101
102
103
104
105
106
Chemical composition of 12% Cr-1% Mo-(W)-V-steels;

cast (ladle) analysis or product (check) analysis . . . . . 107
12% Cr-1% Mo-(W)-V-steels; R Q ^
108
88
Page
3.2

12% Cr1% Mo(W)Vsteels; R T
m
109
12% Cr1% Mo(W)Vsteels; A 5 T
110
4.
Quantities of tensile data
Ill
5.
Listing of mean values at RT and 100 600 C intervals
3.3
T
T
T
D 2
on R . _ , R , A c , R of A and -iL-L
pO, 2
m
5
112
m
6.
7.
8.
9.
Listing
minimum
R _ ,
pO,2
of ratios of mean values divided by specified

values in related standards of specifications
R , A c in 50 C intervals
m
5
T
T
T
Listing of constants A, B, C and D on R _ _ , R , A_
R
R of A and '
for the equation
**
,
P = A + B* T + C * T + D * T
Numbers of heats distributed over classes of sections
the subfiles at RT and elevated temperature
Relative quality figures of the quantities of data in
subfiles
Fig. 1 to 6
Appendix 1
Appendix 2
Appendix 3
on
113
114
in
115
the
116
117
An Evaluation of the Tensile Properties of 9% Cr1% Mo

steel by D.S. Wood RNL UKAEA UK (12 pages; 5 figures,
1 Appendix)
118
Evaluation of the Tensile Properties of 9 Cr 2 Mo Nb V
steels (EM 12 type) (9 pages; 1 table, 4 figures)
by B. Vancampen (C.E.A. I.R.D.I.CENSACLAY) . . . 128
Comparison of the tensile properties of 912% Crsteels
Interim report: Subfile 12% Crsteel; Part II
(RAP022NL) (21 pages; 7 tables, 9 figures,
2 Annexes)
137
89
Introduction
The Activity 3 "Materials" of the Working Group on Codes and
Standards of the Fast Reactor Co-ordinating Committee has set
itself the task of comparing the mechanical properties of
structural steels for use in fast reactor application in the
European Economic Community.
Six member states, namely Belgium, France, Germany, the Nether
lands, Italy and the United Kingdom have contributed to a common
data bank for evaluating the tensile properties of 9-12% Cr-steels.
This work resulted in a report called "Comparison of the tensile
properties of 9-12% Cr-steels, Part I (Data Files)". This work
was performed under Agreement No. RAP-011-80-NL (), and a final
report was issued in December 1981. These data files will be
analysed and compared with current standards under the work known
as Part II. Three member states, namely France, the United
Kingdom and the Netherlands, performed the analyses of the three
subfiles on 9% Cr-1% Mo-steels, 9% Cr-2% Mo-Nb-V-steels and
12% Cr-1% Mo-(W)-V-steels. The subfiles in the data bank were
treated using agreed methods and a comparison of the results was
executed.
This work has been performed under Agreement No. RAP-022-NL CEC
Study Contract.
FRCC Working Group Codes & Standards, Act No. 3, Materials.
90
1. Assessment of tensile properties

. Subfiles
The aim of the study is the assessment of tensile properties
between RT and 600 C at. 50 C intervals. The assessment will
be based on all data in the subfiles. To show the true nature
of the assessment the contents of the data files is evaluated in
the tables 4, 8 and 9. The French only supplied data on extruded
tubes at elevated temperatures, but in the assessment of the
9% Cr-2% Mo-Nb-V tube s+'-.el the Belgian data file dominates by
80% of all data. The numbers of melts f rom billets, bar and tubes
and an indication of scatter in heat treatment and the
distribution of the tensile data at elevated temperature is given
in table 4.
The UK
data relating to 9% Cr-1% Mo-steel cannot be compared
with the Italian data because of the difference in heat treatment.
Only the French and Belgian 9% Cr-steel data and the German and
Dutch 12% Cr-steel data are complementary.
. Type of product
A rough subdivision can be made for different sections and types
of products, viz.
e > 5 mm:
tube
5 - 1 0 mm:
tube/billets
circa 20 - 40 mm: bar
40 - >. 320 mm:
bar/thick sections.
Table 8 shows at RT and elevated temperatures the numbers of
heats distributed over classes of sections. Apparently 9% Cr-1% Mostet:! is characterized in heat-treated sections up to 20 - 40 mm,
whereas 9% Cr-2 %Mo-Nb-V-steel shows sections up to 5 - 10 mm for
extruded tubes at elevated temperature. The amount of heats representing thick sections is limited, viz. one heat of 9% Cr-1% Mosteel and eleven and seven respectively for room temperature and
elevated temperature of 12% Cr-1% Mo-(W)-V-steel.
91
. Relative quality of the data files

Not only the numbers of heats and the absolute quantity of the
tensile data in the subfiles are of interest, but also the
relation between numbers of data related to the same heat. This
relation, called the relative quality figure, is shown in table 9.
If this relative quality figure shows a number a) . 1 or b) << 1,
one might conclude in case a ) : enough data per heat, and in case
b ) : more data per heat are required.
In table 9 all the data files in the subfiles show enough data
per heat for room temperature data. At elevated temperature
the quality of the Belgian data file is consistent with the room
temperature quality, whereas all the other data files differ. The
order in quality is Belgian data, French data, UK-data (but overwhelming in absolute quantity), Italian data, German data and
Dutch data.
The tables 4, 8 and 9 elucidate the versatile data base for
9% Cr-1% Mo-steel and 9% Cr-2% Mo-Nb-V-steel and a data base with
a different character requiring additional data at elevated temperature for 12% Cr-1% Mo-(W)-V-steel. A separate class is the
Italian data file. This steel is furnace cooled after austenitizing
and cannot be fitted in a data file with air cooled or air quenched
steels.
. Comparison of mean values
Bearing in mind the above described particulars in the data files
it is worthwhile to compare the mean values of tensile properties.
The scatter of these properties is shown in the interim-reports
appendices 1, 2 and 3. Instead of assessing confidence limits in
all cases a comparison was made between specified minimum values in
current standards and the assessed mean values.
The tensile properties are expressed in a cubic equation, which
is valid between RT and 600 C.
Property = A + B * T
+ C*T
+D*T"
Property denotes the mean value of a tensile property.
92
Table 7 shows the constants of the cubic equation for the

different subfiles. The data on the reduction of area in the
9% Cr-2% Mo-Nb-V-subfile relating fo French extruded tubes and
Belgian tubes are absent. Table 5 shows the absolute values
of the cubic equations at RT and in 50 C intervals between
LOO C and 600 C.
93
2. Comparison of the tensile properties

Comparison of the tensile properties and related current standards
is given in the figures 1 to 6 and the tables 1 , 2 , 3 and 6.
The basic information of a subfile is given in the tables 1, 2 and
3, respectively for 9% Cr1% Mosteel, 9% Cr2% MoNbVsteel and
12% Cr1% Mo(W)Vsteel. The basic information comprises:
chemical analysis
0.2% proof strength
ultimate tensile strength
elongation
tables
tables
tables
tables
1.0,
1.1,
1.2,
1.3,
2.0,
2.1,
2.2,
2.3,
3.0
3.1
3.2
3.3.
A list of ratios of mean values divided by specified minimum values

or specifications is given in table 6. In this table the ratio of
properties between the 9% Cr1% Mosteels according to the UKdata
file (N + T) and the Italian data file (annealed) is shown.
Important is the observation of ratios < 1. This is the case for
the Italian data file compared with the UKdata file, but the
12% Cr subfile compared with the ISO 2604/Part I F40 specified
minimum values are not in harmony between 100 200 C.
Unfortunately data are scarce in the 12% Cr subfile and the
specified minimum values for ISO forgings F40 are fixed by inter
polation in the lower temperature area, as can be seen
from table 4 and fig. 1.
The behaviour of the three chromium steels is very much alike,
with the exception of the furnace cooled quality.
Fig. 1 shows a comparison of the (absolute) mean value of the
0.2% proof strength. The strongest alloy is the 12% Crsteel with
R n
= 594 MPa. The corresponding minimum specified value for
ISO forgings F40 is added in this figure and compared with mean
values. In fig. 2 the relative shape of the R curves is compared.
pj,
It shows a small scatterbarod at high temperatures. Kere again the

curve for ISO forgings F40 is not in harmony at low temperatures,
not even with the character of the 9% Crsteels curves.
In fig. 3 the specified minima are shown as relative values. In
fig. 2 compared with fig. 3 the same pattern is expected. Here it
can be seen on the 75% line that the specified minimum values at
94
elevated temperature are reached at relatively low temperatures

for ISO tubes TS40 and TS38 in the annealed condition. The
quality R8 is not in accordance with the quality EM12; both
9% Cr-2% Mo-Nb-V tube steels.
Fig. 4 shows the 0.2% proof strength divided by the ultimate
tensile strength, riere a clear tendency is shown for ratios of
about 0.71 - 0.75 over all temperatures with a scatter at 600 C,
except for the UK-data.
Fig. 5 shows the elongation and the reduction of area. The mean
values for the UK-data show the best ductility.
Fig. 6 shows the observed mean values divided by specified
minimum values in related standards. The harmony between UK-data
and ISO tubes TS38 and French and Belgian data and AFNOR A 49 213
tubes is striking. The curves for 12% Cr-steels requiring
additional data, are dotted.
95
3. The effects of product form or steel making practice

The particulars about the type of products in the subfiles are
discussed elsewhere. The steels involved in the assessment comprise many years of steel making practice and do not necessarily
reflect the latest "vogue" regarding to low sulphur content and
low phosphorus content. But an analysis of the average chemical
analysis given in the tables 1.0, 2.0 and 3.0 can be helpful.
Regarding the obtained microstructure the following general
remarks can be made (see table below).
Type of
steel
9% Cr-1% Mo-steel
Data file
UK-data
Grainsize
Delta
ferrite
23 C 6
Carbonitrides/
nitrides
martensitic
(tempered)
bainitic
(tempered)
Italian
data
6-8
9% Cr-2% Mo-Nb-V
12% Cr-1% Mo-(W)-V
French + Belgian
data
German + Dutch
data
11-9
none
(wrought
steel)
30/17% long trans,

direction
traces
CrN 2
CrN 2
with Nb, V
with V
96
The relation between microstructure and tensile properties

sometimes seems confusing. Analyzing ISO 2604/Part I F40, forgings
and ISO 2604/Part II TS40, tubes for 95% lower confidence lines
L
discloses the Rm RT
-value being respectively circa 810 MPa and
circa 720 MPa. Specified is 780 - 930 MPa and 690 - 840 MPa. The
mean value of the 12% Cr-steel subfile is 803 MPa and the lower
Rm RT valuesare measured for air-cooled thick sections, viz. bar
section 160 mm and billet 100 mm fitting in the lowest TS40 range
with 687 and 726 MPa. At 500 C the bar gave the lowest R -values
m
observed, but the R Q 2 -value at 500 C (348 MPa) is in the range

of the minimum value of F40 (344 MPa at 500 C) .
97
4. Conclusions
Comparing tensile properties of different sections and heats of
the ferritic 9 - 12% Cr-steels revealed:
a) The difference between tensile properties of 9% Cr-1% Mo-steel
types of products in air-cooled condition after austenitizing
and 9% Cr-2% Mo-Nb-V extruded tubes in air-quenched condition
after austenitizing is very small between RT and 500 C.
b) The thin-walled tubes, wall thickness: 2 mm, in 12% Cr-steel
cannot be compared with other thin-walled tubes. At 250 C these
tubes are stronger than the mean values obtained from 9% Crsteels .
c) Thick sections in 12% Cr-steel must be evaluated according to
their respective heat treatment, viz. (water-/oil-)quenched or
normalized (air-cooled) and tempered for respectively
ISO 2604/Part I, F40 (forgings) or ISO 2604/Part II TS40 (tubes).
VdTV Werkstoffblatt 110 issued 01.1982 relates to
X 20 Cr Mo V 12 1 (W.No. 1.4922), forgings up to 250 mm in
section and prescribes an oil-/water-quench. The data files for
F40 and X20 are not part of this study.
d) The so-called tempered martensitic structures show the usual ratio
between RpU- ,2
_/Rm for ferritic steels, viz. 0.75 - 0.71.
e) The mean R _ -, values obtained are usually 1.2 times the
p0,2
specified minimum values in related standards.
f) The minimum values are determined and can be seen in the
figures of the interim-reports. The minimum values for R _ 2
are based on the lowest data point per temperature in the case
of the 12% Cr-steel data, whereas the 9% Cr-1% Mo-steel and
the 9% Cr-2% Mo-Nb-V-steel data are analysed at 300 C.
At 300 C the lower confidence limit was calculated and the
mean value curve was translated to this limit.
98
5. Recommendations
a) The versatile Belgian data file of 9% Cr-2% Mo-Nb-V-steel also
gave the data of elongation at maximum load (the so-called
uniform elongation). It is worthwhile to compare these results
with results of the other alloys.
b) It is of general interest to extend the data file for 12% Cr-steel.
The interpolated data between RT a:
and 400 C in a standard like
ISO 2604 should be clearly marked.
c) The 95% lower confidence level as expressed in ISO 2604 in a
figure
showing^ R mRT versus R pO,
~2 was not foreseen in this
^
assessment and is felt as an omission. It is a recommended issue
for future studies of tensile properties. The relation between
ductility properties and the ultimate tensile strength is also
a recommended issue for further study.
Table 1.0. Chemical composition of 9% Cr1% Mosteels; cast (ladle) analysis or product (check) analysis
Standard
Elements in weight percent
relating
to 9% Cr1% Mostsel
* ISO 2604/2T1975(E) 0.15
Mn
max.
S
max.
Cr
Mo
0.25
0.30
0.030
0.030
8.00
0.90
1.00
0.60
0.20
0.30
(corrections according
to table 4c)
1.05
0.63
* (ARNOR) NF A 49213
TU 10 CD 9 (ladle) ^ 0.15
0.25
0.30
1.00
0.60
0.20
0.20
1.05
0.70
0.25
0.30
1.00
0.60
0.105
0.41
0.47
0.018
0.09
0.84
0.52
0.028
TS 38 (ladle)
< 0.16
TS 38 (check)
TU 10 CD 9 (check) ^ 017
Si
* ANS 125.24
ASTM A 33575
P9
(check)
< 0.15
ASTM A 2138la')
T9
\ rela :ed
ASME SA 335
stan ards
0.033
0.030
0.035
0.030
10.00
1.10
7.90
0.86
10.10
1.15
8.00
0.90
10.00
1.10
7.90
0.85
10.15
1.15
8.00
0.9
10.00
1.10
0.012
8.6
0.016
8.8
0.033
0.030
0.035
0.030
Ni
Nb
Co
Cu
others
Al
met
v< 0.30
0.30
^ 0.02
N
0.25) Sr. max. 0.03;

Sn max. 0.04
if
0.251 (Cu+10Sn) <.
0.55
0.96
0.20
0.97
Observed mean values

U.K.data
Italian data
ASTM A 335 75
0.020
0.10
Sr. 0.014;
V 0.008
P9
it
v
Table 1.1
Mechanical properties at elevated temperatures of 9% Cr-1% Mo-steels; R
R ; in degree
Celsius; (MPa)
y
p0,2
Standard relating
to 9% Cr-1% Mo-stael
Reference
heat
350
400
450
500
550
600
RT
50
100
150
200
250
300
TS 38 - condition a
130*
115
98
88
79
78
77
76
75
74
71
- condition b
398*
386
363
348
334
330
326
322
316
311
290
235
205
150
143
136
120
900/950C +
100C/h max.
till 700C
207
"
--
not prescribes
N+T ( T > 6 7 7C]
490
298
462
446
433
426
424
422
215
353
177
311
246
treatment
* ISO 2604/11-1975(E)
(AFNOR) NF A 49-213
TU 10 CD 9
(June 1979)
; * ANS 125.24
ASTM A 335-75
P9
' .
U.K.-data
Italian data
ASTM A 335-75 P9
annealed
(850-950/f)
normalized +
tempered
900-1000C/AC
+ 700-800Q'AC
418
408
195
3 89
RT
RT
or R _
el
p0,2
, d,,.
mi
Table 1.2.
Mechanical properties at elevated temperatures of 9% Cr1% Mosteels; R
R ; in degree Celsius; (MPa)

m
Standard relating
to 9% Cr1% Mosteel
RT
* ISO 2604/211975(E)4
TS 38 condition a 110
* 560
condition b 590
740
* (AFNOH) NF A 49213
TU 10 CD 9
* ANS 125.24
ASTM A 33575
P9
50
100
150
200
250
300
350
400
450
500
550
600
440
(590)
414
(?)
612
591
578
569
534
424
507
467
390
409
331

I
\ U.K.data
Italian data
ASTM A 33575 P9
|
see. table 1.1.

Reference heat
672
563
561
442
551
Table 1.3.
Mechanical properties at elevated temperatures of 9% Cr1% Mosteels; A^
A^
5
Standard relating
to 9% Cr1% Mosteel
50
RT
(L
= 5.65 / S ) ; in degree Celsius;

o
100
150
200
(%)
250
300
3 50
400
45C
500
550
600
* ISO 2604/1975(E)
TS38 condition a
condition b
20
18
* (AFNOR) NF A 49213
TU 10 CD 9
2211
* ANS 125.24
ASTM A 33575
P9 (tube)
30

U.K.data
Italian data
! ASTM A 33575 P9
25.3
28.8
25.2
24.1
22.6
20.9
19.4
Remarks
18.4
18.2
19.2
21.5
25.5
31.5
1
n
R
m
(A-2) >, 10500
Table 2.0.
Chemical composition of 9% Cr-2% Mo-V-Nb-steels; cast (ladle) analysis or product (check) analysis
Standards relating
to 9% Cr-2% Mo-V-Nbsteel
Si
Mn
0.200.65
0.80
1.30
0.17 0.150.70
S
max
Cr
Mo
0.030
0.030
8.50
10.50
1.70
2.30
0.70
1.40
0.035
0.035
8.40
10.65
1.65
2.38
max
others
Nb
Co
S 0.30 0.20
0.40
0.30
0.55
0 . 3 0 0.18
0.43
0.25
0.60
Sn max. 0.03;
Sn max. 0.04
if (Cu+lOSn)
0.C3\ *< 0.55
.3
.6
0.07
0.02
Ni
Cu
* ISO 2604/11-1975(E)
quality: absent
* (AFNOR) NF A 49-213
TU 10 CD Nb V 9.2 ^ 0.15
(ladle)
TU 10 CD Nb V 9.2
(check)
* Superheater tubes
(origin: Belgium)
9% Cr-2% Mo-V-Nb
French data NF A 49 811
Belgian data
0.070.12
0.5
.9
1.2
8.5
10
1.8
2.2
0.25
0.45
0.11
0.13
0.34
0.33
1.1
1.0
0.015
0.009
0.014
0.007
9.6
9.5
2.1
2.0
0.09
0.30
0.29
0.38
0.47
0.03/
0.08
Caubo, M.; "Improve d 9% Cr- Moste 1 for uperhec ter tub es of s team ge lerator "; BNE 3, London (197e), 217 221.
o
OJ
Table 2.1.
Mechanical properties at elevated temperatures of 9% Cr2% MoVNbsteels; R
T
R . ,
T in degree Celsius (MPa)
p0,2
Standard relating to
100
150
200
250
300
350
400
450
500
550
600
390
330
310
290
260
220
* Superheater tubes
9% Cr-2% Mo-V-Nb
(R8)
390
284
275
265
255
24 5

French and Belgian date
498
446
437
432
421
411
395
371
336
289
9% Cr-2% Mo-V-Nb-steel
RT
50
(AFNOR) NFA 49213

TU 10 CD Nb V 9.2
(EM 12)
459
Reference
heat
treatment
1050/1125C/
air +
760/825 C
Table 2.2.
Mechanical properties at elevated temperatures of 9% Cr-2% Mo-V-Nb-steels; R
R ; in degree Celsius; (MPa)

m
Remarks
RT
50
100
150
200
250
300
350
400
450
500
550
600
642
622
610
603
596
586
568
540
497
435
351
(AFNOR) NF A 49-213
TU 10 CD Nb V 9.2
t Superheater tubes
9% Cr-2% Mo-V-Nb

French and Belgian data
590 740
690 800
701
o
ui
Table 2.3
Mechanical properties at elevated temperatures of 9% Cr-2% Mo-V-Nb-steels; Ac
(Lo = 5,65 / S o ) ; in degree Celsius; (%)
Rer.arks
RT
100
150
200
250
300
350
400
450
500
550
600
18.38
11.00
0.60
17.05
9.66
0.57
15.67
8.38
0.53
14.38
7.05
0.49
13.43
6.44
0.48
12.78
5.80
0.45
12.78
5.86
0.46
17.0
15.7
14.9
.14.5
14.6
50
* (AFNOR) NF A 49-213
TU 10 Nb V 9.2
16
* Superheater tubes
9% C r - 2 % Mo-V-Nb
18

French data
1}
fl8.5 2)
)24.33)
20.57
29 Belgian data; A
uniform elongation;A
13.72
i Ratio (A /A 5 )
0.67
French ana Belgian data
21.9
All data
18,6
15.3
16.4
15.14
6.21
0.41
17.53
6.00
0.34
20.47
5.95
0.29
18.2
20.5
23.5
Belgia data
A = A . (m *
u
- n)
nqe
Temper ture r C
3
mxlOn
RT-250 250-475 475-600

1.20
0.783 0.222
1.01
0.686 0.546
1) R (A - 2) > 10 50C
m
2) Lo = 8.16 / So; = 13
3) Lo = 5.65 / So; n= 19
o
Table 3.0
Chemical composition of 12%Cr-l% Mo-V-steels; cast (ladle) analysis or product (check) analysis

Standard relating
to 12% Cr-1% Mo-V-
Si
Mn
max
S
max
Cr
0.200.26
0.190.27
0.150.40
0.10
0.45
0.301.00
0.27
1.04
0.040
0.040
0.701.20
0.045
0.045
10.0012.50
9.9012.65
0.170.23
.$0.50 .$1.00 .030
0.030
0.160.24
>< 0.55 < 1.04
0.C33
0.17- 0.50 $1.00

0.23
0.15- 0.54 < 1.04
0.25
0.17- ,$0.50 ^1.00
0.23
steels
* ISO 2604/1-1975 (E)
F 40 (ladle)
(check)
* ISO 2604/11-1975 (E)
Mo
Ni
.25
0.301.0
0.301.0
0.200.35
0.170.38
10.0012.50
0.801.20
0.300.80
0.250.35
0.033
9.8512.65
0.761.25
0.270.83
0.220.38
0.030
0.030
0.040
0.040
10.012.50
9.8512.65
0.801.20
0.761.24
0.30O.BO
0.270.83
0.250.35
0.220.38
0.030
0.030
10.0012.50
0.801 .20
0.30
0.80
0.250.35
0.010
0.009
11.6
0.97
0.54
0.30
12.0
1.1
0.42
0.30
. -
Nb
Co
0.400.701*
0.400.70
Cu
others
^ 0.701
TS 40 (ladle)
TS 40 (check)
* VdTOV-Werkstoffblatt
110-01.82
X20 Cr Mo V 12 1
(ladle)
DIN Werkstoffnummer 1.4922(check)
DIN 17 175 - 1979
X20 Cr Mo V 12 1
Werkstoff-Nummer
1.4922
Dutch data
.20
.34
.54
German data
.20
.36
.50
0.70 1 1
0.46
1) may be added if so agreed
Table 3.1.
Mechanical properties at elevated temperatures of 12% Cr1% MoVsteels;
R
Standard relating
RT
to 12% Cr1% MoV

steel
* ISO 2604/11975(E)
F40
* ISO 2604/lI1975(E)
TS40
X VdTUVWerkstoffblatt
11001.82
X20 Cr Mo V 12.1
DIN 17 175 1979
Observed mean value
X20 Cr Mo (W) V 12 1
540
435*
eH
0f2
or R T , R n n ; T i n degree Celsius; (MPa)

eL' pO,2
Reference
50
100
150
200
250
300
350
400
450
500
"
508
484
457
434
423
416
408
383
344
349
328
317
310
292
272
425
407
378
305
550
600
10201070C/
oil quenched
+68C"30C
water quenched
102C.070C/air
T68C"30 C/air
10201070C/
WQ cr OQ +
T73C30C/air
V,2
eH
490 l
460
445
490 2 )
594
484
454
360
430
415
390
380
430 3 )
415 3 )
390 31
380 31 360 3)
443
446
454
462
463
Heat treatment
330
290
250
330 3)
290 3 )
250 3 )
446
413
349
249
R . or R
eL
pO,2
1) thickness >< 250 mn
forgings diameter 375 mn1
2) tube wall thicknes s 60 mm max.
3)
"
80 mm max.
o
co
Table 3.2
Mechanical properties at elevated temperatures of 12% Cr1% MoVsteels; R

m
R ; in degree Celsius (MPa)

m
Standard relating
300
35C
50
100
150
200
250
* ISO 2604/11975(E) 780

930
F 40
* ISO 2604/111975 (E)690

840
TS 40
to 12% Cr1 MoVsteel
RT
450
500
550
400
6C0
Remarks
*VdTOVWerkstoffblatt
11001.82
690
X20 Cr Mo V 12.1
840
650
625
600
590
580
545
510
455
400
325
DIN 17 175 1979
690
840
Observed mean value

German and Dutch data
803
672
660
651
638
617
584
533
460
720
690
360
o
VD
Table 3.3
Mechanical properties at elevated temperatures of 12% Cr-1% Mo-V-steels; A^
T
/
A. (Lo = 5,65 / So); T in degree Celsius; %
Standard relating
Remarks
to 12% Cr-1% Mo-V-stee:
RT
50
100
150
200
250
300
350
400
* ISO 2604/1-1975 (E)

F 40
14
* ISO 2604/11-1975 (E)

TS 40
15
"~
14 iJ
21.7
21.1
19.8
18.1
16.4
15.2
500
550
600
""
21.8
28.4
450
*VdTOV-Werkstoffblatt
110-01.82
X20 Cr Mo V 12.1
15
2)
DIN 17 175 - 1979
14
1}
17
2)
Observed mean value
20.2
14.7
15.4
17.6
German and Dutch data
Transversal/TD
2)
Axial/RD
, 1
9% C r 2% Mo
II
(Bar
France
(NF A 49 8J.1)
/Tube
NF A 49 2 1 3 * * *
Tube
Belgium
Tube
10.]
1* .'
1100 C - 0 , 5 h / a i r quenched 13
b
31
31
31
31
***
"~
T : 7 2 5 / 8 1 5 C ; 0 , 5 / 1 h
1 0 5 0 / 1 1 2 5 C ; 7 6 0 / 8 2 0 C
31
18
T:710 C ; 1 h
T o t a l 9% Cr 2% Mo
12% Cr
44
German d a t a
Billet
DIN W.N. 1 . 4 9 3 5
Bar
(old
II
Dutch
d e s i g n a t i o n Tube
data
DIN W.N. 1.4922
Billet
Bar
Tube
DIS*2604/
3i*
Tube Rm >' 720 MPa

(690 - 840)
P a r t I : F 40
P a r t I I : TS 4 0 * * Heavy F o r g i n g s
R - 8 1 0 MPa
m
(790 - 940)
Total s u b f i l e 12%Cr
Total (ISO-data
i n c l u d e d ) 12% Cr
1030 - 1050 C/AC o r OQ
11
T: 720 - 780 C ;
8/- h
11
80
mm
3J
9
:1
19
1030 - 1050 C/AC o r OQ

T:750 - 780 C ; - / 2 h
1020 - 1070 C / a i r cooled

T-680 - 780 C
145
1020 - 1070 C / o i l /water
_
quenched
T:680 - 780 C
91
236
*) DIS now called ISO

at*) BURTON, D.; ORR, J.; MARRIOTT, J.B. "Elevated temperature properties of 2k CrMo, 9 CrMo and 12CrMoV wroughl
steels for international and national standards". BNES, London, 1978, 205 211.
*afc*) new!
p0,2
Table 5: Listing of averaqe values in 50 C intervals of R . , R , A, R of A, and

pO, 2
m
property
TemDerature ( D
Remarks
XX
20
100
150
200
250
300
350
400
450
500
550
600
9% Cr 1% Mo
490
446
433
426
424
422
418
408
389
358
311
246
9% Cr 2% Mo
498
459
446
437
432
427
421
411
395
371
336
289
12% Cr (A+B)
594
484
454
443
446
454
462
463
449
413
349
249
9% Cr 1% Mc
672
612
591
578
569
561
551
534
507
467
409
331
9% Cr 2% Mo
701
642
622
610
603
596
586
568
540
497
435
351
12% Cr
803
720
690
672
660
651
638
617
584
533
460
360
9% Cr 1% Mo
25.3
25.2
24.1
22.6
20.9
19.4
18.4
18.2
19.2
21.5
25.5
31.5
22.7
3.89
9% Cr 2% Mo
21.9
I.6
17.0
15.7
14.9
14.5
14.6
15.3
16.4
18.2
20.5
23.5
17.6
3.04
(%)
12% Cr
20.2
21.7
21.1
19.8
18.1
16.4
15.2
14.7
15.4
17.6
21.8
28.4
19.2
3.87
9% Cr 1% Mo
71.2
75.6
75.9
74.9
73.3
71.4
69.8
69.1
69.8
72.4
77.3
85.2
73.8
4.47
54.6
59.1
59.3
58.2
56.4
54.6
53.4
53.3
55.0
59.1
66.2
76.9
58.8
6.73
9% Cr 1% Mo
0.729
0.729
0.733
0.737
0.745
0.752
0.759
0.764
0.767
0.767
0.760
0.743
0.748
0.0148
9% Cr 2% Mo
0.710
0.715
0.717
0.716
0.716
0.716
0.718
0.724
0.731
0.746
0.772
0.823
0.734
0.0331
12% Cr
0.740
0.672
0.658
0.659
0.676
0.697
0.724
0.750
0.769
0.775
0.759
0.692
0.714
0.0437
V,2
(MPa)
R~
m
(MPa)
R of A
(%)
R
type
of
alloy
Rm
P,02
Rm
AV X
SD
9% Cr 2% Mo
12% Cr
x)
Average value over RT
600 C
xx) Standard deviation (best estimate of the population variance

)
n-1
Table 6: Listing of ratios of average values divided by specified minimum values in related standards or specifications of
R
nf 2o T ' R mmT a n d A-,aT i n 50 C intervals
pO
Temperature (C)
>,
-P
U
RT
u
a,
UK-data versus
ISO 2604/11-1975 (E)
TS 38 cond. b
Italian data versus
NF A 49-213
TU 10 CD 9
Italian data versus U.K.-data
1.23
1.14
1.40
2
p0_f
1.45
1.28
1.31
p0,2
%
A
p0,2
0.61
0.84
0.94
French and Belgian data

versus NF A 49-213
TU 10 CD Nb V 9.2 (EM 12)
R,.2T
*m T
A
1.28
1.19
1.52
French and Belgian cata

versus (R-8)
Rp0,2T
R
Am
1.28
1.02
1 .35
German and Dutch data versus

VdTDV-Werkstoffblatt 110
German and Dutch data versus
ISO 2604/1-1975 (E)
F 40
1.20
150
200
250
300
350
400
450
500
550
1.23
1.24
1.28
1.28
1.29
1.30
1.29
1.25
1.23
1.32
100
Rp0,2
R
Am
A1"
Rm
A
1.13
1.02
1.19
1.20
0.51
0.78
1.37
1.21
1.16
1.26
1.36
0.49
0.84
1.24
1.27
1.28
1.29
1.31
1.45
1.44
1.40
1.32
1.18
1.52
1.53
1.52
""
0.48
0.79
600
1.30
1.30
-
1
R
German and Dutch data, versus

ISO 2604/11-1975 (E)
TS 40
50
1.43
1.49
1.05
1.11
1.02
1.10
1.03
1.12
1.07
1.12
1.16
1.12
1.22
1.17
1.29
1.21
1.35
1.28
1.42
1.33
0.95
0.94
0.97
1.03
1.07
1.11
1.13
1.16
1.20
""
1.40
1.41
114
Table / : L i s t i n g
and
c o n s t a n t s , , C and D for
P -'
R _ - , R , A, R o f A
o0,2' m'
for the equation = A + BT + CT 2 + DT
Property
p0,2
(MPa)
R~~
m
(MPa)
(%)
R Of A
(%)
R
p0,2
R~
m
type
of
alloy
list of constants A, , C and D

A
9% Cr 1% Mo
9% Cr 2% Mo
12% Cr
0.507E+3
0.901E+0
0.334F2
0.427E5
0.5116E+3
0.731F+0
0.240E2
0.300E5
0.6353E+3
0.2234E+1
0.8222E2
0.9283E5
9% Cr 1% Mo
0.693E+3
0.1140E+1
0.378E2
0.481E5
9% Cr 2% Mo
0.7224E+3
0.1150E+1
0.397E2
0.514E5
12% Cr
0.8327E+3
0.1585E+1
0.5194E2
0.6442E5
9% Cr 1% Mo
0.2488E+2
0.259E1
0.269E3
0.407E6
9% Cr2% Mo
0.2286E+2
0.491E1
0.584E4
0.423E7
12% Cr
0.1916E+2
0.5853E1
0.3787E3
0.5112E6
9% Cr 1% Mo
0.691E+2
0.114E+0
0.564E3
0.698E6
12% Cr
0.5245E+2
0.1207E+0
0.6236E3
0.8171E6
9% Cr 1% Mo
0.7325E+0
0.7026E+0
0.7 75 6E+0
0.1477E3
0.1154E5
0.1455E8
0.2832E3
0.1480E5
0.2213E8
0.1723E2
0.1787E5
0.7536E8
9% Cr 2% Mo
9% Cr 2% Mo
12% Cr
Table 8: Numbers of heats distributed over classes of sections in the subfiles at RT and
at elevated temperature
Type of steel
Tempe rature
RT
9% Cr-1% Mo
9% Cr-2% Mo-V-Nb
12% Cr-1% Mo-(W)-V
*
**
Italian data
Belgian data
Section (mm)
e < 5
5-10
10-20
20 - 40
40-80
80-160
160-320
37
14
13 + 7*
37
14
13 + 7*
13+18*
10
12+18**
13
11
e j. 320
> RT
3f)
Table 9: Relative quality figures
of the quantities of data in the subfiles
Type of steel
(subfile)
Data file
Room
temp.
data
9% Cr-1% Mo
UK-data
Italian data
1
1
0.50
0.33
0.54
0.38
34%
23%
9% Cr-2% Mo-V-Nb
Belgian data
French data
1.72
1.23
1.44
0.51
1.46
0.31
100%
35%
12% Cr-1% Mo-(W)-V
German data
Dutch data
(1.4922)
1
3.2
0.20
0.16
0.21
0.38
14%
11%
50 C interval
50 - 600 C
data
All
data
Comparison per
heat at elevated
temperature
*) The relative quality figures indicate the mean number of tensile tests per heat per
temperature indicated, viz. a) room temperature data: 1
b) 50 C interv
interval, 50 - 600 C data: 12
c) all data: 13
117
COMPARISON OF THE TENSILE PROPERTIES OF 912% CrSTEELS AT ELEVETED TEMPERA TURES
100V
100%
90
90
V
X
80
12%Cr1%Mo(W)V
(ISO 2604/11975(E), F40)
V
S
* 12%Cr1%Mo(W)V
(ISO 2604/11975IE); F40)
80
* 12% Cr1% Mo(W) V

(VdTV Werkstoff bltt 110)
70
12%Cr1%Mo(W)V
(ISO 2604/11975(E), F40)
>
**+>+
Afcfc*
70
* ,
12%Cr1%Mo(W)V
(German and Dutch data)
*.\ X \
60
'KS
v ' i n 9% Cr2% Mo
~ W
(French and Belgian data)
50
,9%Cr1%Mo
i*=/(Italian data)
9%Cr1%Mo
(U.K. d a ta)
40
RT
100%
100
200
300
400
500
600
9%Cr1%Mo
(Italian data)
60
cf*9%Cr1%Mo
(UK. data)
50
;*12%Cr1%Mo(W)V
40
RT
100
200
300
RT
'POI
x100%,butinthe
Fig. 2
Relative 0.2 proof strength,
534
12%Cr/F40 curve R p 0
400
500
9%Cr2%Mo(W)V
(EM12;AFNOR NFA 49 213)
600*
RT
100
200
Temperature
Temperature
Fig.l Comparison of 0.2 proof strength,
9%Cr2%Mo
(R8)
9%Cr1%Mo
(ISO 2604/21975(E) ;TS 38)
12%Cr1%Mo(W)V
( ISO 2604/21975(E);TS 40)
t*9%Cr2%Mo
(Frenchand Belgian data)
RT
'P0.2
prr
400
500
6 0 0 C
*> Temperature
Fig. 3
Relative 0.2 proof strength minina specified in related
100%, but in the

standards,
PQ2minx100%
RRT
"PO.2
12%Cr/F40 curve R ' Q ^ is substituted by R p a 2
is substituted by R 0.2 min
300
" P 0.2 min
2.00
u*
100%
90
RofA
80
-9% Cr- 2% Mo
80
*
-*9%Cr-2%Mo
70
*
,.
* 12% Cr1%Mo(W)V
..**
1.60
12%Cr1%Mo(W)V
(German and Dutch Data)
12%Cr/TS40
12%Cr/X20
1.40
9%Cr2%Mo/EM12
' 9%Cr1%Mo
(UK. Data)
12%Cr1%Mo(W)V
20
DU" "
9%Cr1%Mo
(UK Data)
60
40
60
1.80
1.20
9%Cr2%Mo/R8
9%Cr1%Mo/TS38
1.00
9%Cr2%Mo
(French and Belgian Data)
40
RT
100
200
300
400
500
600
100
200
300
*
Temperature
Fig. 4 Ratio of observed mean values 0.2 proof strength devided
pT
2
by the ultimate tensile strength,
100%
'm
400
500
6 0 0 C
RT
Reduction of A rea(RofA ) and elongation(A 5 )
200
300
400
500
600
m Temperature
Temperature
Fig.6
Fig.5
100
Observed mean values compared t o the minima specified

in related standards, R p o 2 / s P e c m m
or
m/Specmin
118
Appendix 1
United Kingdom Atomic Energy Authority
(Northern Division)
An Evaluation of the Tensile Properties

of 9%Crl%Mo Steel
by
D S Wood
Risley Nuclear Laboratories
UKAEA
UK
December 1982
This work has been performed as a sub contract for

B.V. Neratoom in relation to CEC Study Contract
RAP-022-N.
119
An Evaluation of the Tensile Properties of 9%Crl%Mo Steel

by D S Wood
1.
Introduction
B.V. Neratoom are co-ordinating a CEC Study Contract relating

to the tensile properties of 9-12%Cr steels. The work has been
subdivided into two parts, Part I dealing with data collection and
Part II with analysis of the data.
Part I was completed in
December 1981(1) and comprised of contributions from Neratoom, NIRA,

Interatom, CEA, Belgonucleare and UKAEA.
The data were divided into
three sub-files namely 9%Crl%Mo steel, 9%Cr2%Mo steel and 12%Cr

steel.
In Part II of this exercise the UKAEA agreed to evaluate the
9%Crl%Mo data bank in accordance with the technical scope given in

the Appendix.
This document relates to the analysis of the 9%Crl%Mo
data bank.
2.
Extent of Data
Before evaluating the data, the 9%Crl%Mo data bank was examined
in relation to the extent of the data, the type and the values quoted.
This data bank comprised of contributions from UKAEA and NIRA.
Whereas the UK data bank was very extensive, particularly in relation
to proof strength, UTS and elongation, the Italian data file included
data from only seven heats? furthermore most of the data were restricted
to proof strength and UTS and to four temperature levels. Of more
serious consequence however was the fact that whereas the UK data file
related to normalised and tempered material, the Italian data file
related to annealed material resulting in steels with much lower strength
values.
This is illustrated in Fig 1 for the proof strength. As a
result of this large difference in properties and the small amount of

Italian data it was decided to omit the Italian data from the analytical treatment.
3.
Applicability
The data evaluated relate to steel in che normalised and tempered

condition.
The specimens were taken from a range of product forms
including tubes, bars of up to 31mm diameter and plates up to 12mm thick.
The tensile properties appear to be unaffected by product form.

Furthermore, it is probable that similar properties can be
obtained in much larger section sizes since it has been shown that
the microstructure is unaffected up to thicknesses of at least
100mm(2).
Almost all the steels used for the tests were produced
by the basic electric arc process deoxidised with silicon.

4.
Method of Analysis
It has been agreed (see Appendix) that the tensile properties

would be evaluated using a cubic equation of the form
2
3
mechanical property = A + B T + C T + D T
(1)
where = temperature ( C) and varies from RT to 600 C.

5.
Proof Strength
The 0.2% proof strength values are given in Fig 1.
A stat
istical regression analysis was performed using all the data and
an average curve derived as shown, corresponding to the equation
0.2% PS (N/mm2) = 5.07xl02 - 9.01xlO_1T + 3.34xl0_3T2
- 4.27xl0~6T3
(T = temperature, C ) .
2
The standard deviation of the expression is 47.15N/mm
and
hence the 95% confidence limit = 2 SDf at 300 C (the mean temp
erature) this corresponds to 22.3% of the mean stress value. The
upper and lower 95% confidence limits over the full temperature
range have been taken to be jf 22.3% on stress of the average
curve.
6.
Ultimate Tensile Strength
The UTS values are shown in Fig 2.
As in the case of the
proof strength, a regression analysis was performed, the average

2
2
behaviour being given by the expression UTS (N/mm ) = 6.93x10
- 1.14T + 3.78xl0~3T2 - 4.81xlO~6T .
The 95% confidence limits were derived in a similar manner
to that described for the proof strength.
In this case the limits
correspond to + 16% of the average behaviour indicating less

spread in the data points than that observed for the proof strength.
7.
Elongation
The elongation values quoted in the data file may be based

on 4/A or 5.65/A.
It is not possible to establish the criteria
used, but it is thought that most data relate to 4/A.
The results
available are given in Fig 3> the average curve which has been
included is represented by the expression
Elongation (%) = 24.88 + 2.59x10
-2
-4 2
- 2.69x10
+ 4.07xlO~7T3
The 95% confidence limits correspond to _+ 40% of the average
elongation value; this limit is rather wide and may partly be due
to the use of two different elongation criteria.
8.
Reduction of Area
Limited R of A data are given in Fig 4. The average curve

is represented by the expression R of A(%) = 69.1 + 1.14x10
- 5.64xlO"4T2 + 6.98xlO_7T3.
The 95% confidence limits correspond to about +_ 14% of the
average behaviour.
9.
Proof Strength to UTS Ratio
The proof strength to UTS ratio (based on average values) is

shown for the UK data bank on normalised and tempered steel in
Fig 5. Ratio's based on average values from the Italian data
bank on annealed steel have been included in this figure. This
figure indicates that the ratio is relatively insensitive to
temperature (in the range RT-600 C) . It is important to note
however that whereas the ratio is about 0.75 for the normalised
and tempered steel, it is only about 0.5 for the annealed steel.
The differences observed in this ratio between the two heat
treatment conditions could be important in the definition of
allowable stresses if these are based on a consideration of both
the proof strength and UTS.
References
1.
Nieuwland C D et al. Comparison of the tensile properties

of 9-12% Cr steels. Part I data files. Neratoom document,
1981.
2.
Orr J and Beckett A. The physical metallurgy of chromiummolybdenum steels for fast reactor boilers. BNES Conference
on Ferritic STeels for Fast Reactor Steam Generators, London
1977, Paper 16.
122
APPENDIX
"Comparison of tensile properties of 9-12% Cr steels:

Part II (Statistical analysis)"
Technical scope of the study
1.
The contribution of the member states to the 1980 study

contract (Part I, data files) will be evaluated whether
they offer a sufficient basis for statistical analysis.
2.
The tensile properties R n _, R , A and R.of A will be

0,2
m
expressed in a cubic equation of the kind mechanical
2
3
property = A + BT + CT + DT where stands for temperature
between RT and 600C.
The statistical analysis will comprise average values,
minimum values and a 95% lower bound confidence level.
3.
4.
5.
6.
The R n ~/R ratio will be obtained

0,2 m
Effects of product form or steel making practice will
be noticed.
The data files will be divided
into subfiles concerning
steel qualities from different sources of three kinds

9 Cr 1 Mo, 9 Cr 2 Mo and 12 Cr 1 Mo.
7.
A final report v/ill be drafted and the results will be

compared with current standards. Conclusions will be
drawn. Recommendations v/ill be formulated.
RT
700
.,
100
No.
71
OF
DATA
POINTS
200
44
55
400
300
68
56
600
37
34 43
69
600
500
^v
95% CONFIDENCE
LIMITS
vj
E
\
500
^< V
AVERAGE
CURVE
nr
V
*
. ^ S * N X^
U3
.
LU
cr:
*.
400
:
.
* "
s.
.
I
X*
î
..
.
,
^S**N ,
"
.:
v.
N^
.* ^
'
...
\
\
o^
CSI
\**
K*
.*
Q.
_ '.',
:
*^\
**
o
o
cc
*
..;.
**
u_
r O
_".
to
3 00
, \
\
/
\
\.
\
"\
' \
RANGE OF
ITALIAN DA TA
AT RT
200
DATA POINTS
FIG.1
0 RT
100
200
300
400
TEMPERATURE (C)
500
600
9%Cr 1%Mo STEEL (NORMA LISED A ND

TEMPERED) ELEVA TED TEMPERA TURE
PROOF STRENGTH VA LUES
123
124
r-
34
44
NO.OF\7l
DATA
POINTS
700
E
E.
2
600
I
\O
Hi
ce
YU)
DJ
_J
500
UI
95%
CONFIDENCE
LIMITS
f~
UJ
I<
2
400
3 00
DATA POINTS
O 20
IOO
200
300
40C
TEMPERATURE (C )
500
FIG.2 9% Cr STEEL (NORMALISED AND TEMPERED)

ELEVATED TEMPERATURE U.T.S. VALUES
600
125
~i
NO- OF
DATA
POINTS
IO
T
9
T"
4
T
7
90
80
<
ui
70
DC
<
u.
O
60
U
=5
50
95/ CONFIDENCE
LIMITS
c:
40
30
20
IO
RT
200
300
400
TEMPERATURE ( C)
500
FIG.4 9% Cr STEEL (NORMALISED AND TEMPERED)

ELEVATED TEMPERATURE REDUCTION OF AREA VALUES
eoo
126
60
NOOF
DATA
POINTS
too
O 20
' '
300
200
45
56
400
69
60
500
600
40
36
71
45
50
40
_j
AVERAGE
CURVE
ui
UI
;
30
t.
UI
UI
>
20
^^
'
t
m*
"
m
^^^^"Ujjjij/
95%
CONFIDENCE
LIMITS
#*
****.
***
.:
*
**x
o
O
*"
tr
*
*
...
*
*
.r
*m
f*.
* *r
t ' ' n
^^^^^^^^^^^^^^^^ *
m***
"""
* 1*
~~~
<*
9
IO
o 20
100
t
200
300
400
TEMPERATURE ( C )
500
600
F1G.3 9% Cr STEEL (NORMALISED A ND TEMPERED)

ELEVATED TEMPERA TURE DUCTILITY VA LUES
127
0.2%
PROOF STRENGTH
UTS
1.0
UK DATA
FILE
/
0.75 -
cc
<
ex.
ITALIAN
DATA FILE
0.50
/
0.25
j _
100
200
300
500
600
TEMPERATURE (C)
FIG. 5 PROOF
RATIO
400
STRENGTH
9%Cr
TO
1%Mo STEEL
UTS
128
Appendix 2
DEPARTEMENT DE TECHNOLOGIE
DT/13.04
SERVICE DE RECHERCHES
Fvrier 1983
EVALUATION OF THE TENSILE PROPERTIES

OF 9 Cr 2 Mo Nb V STEELS
(EM 12 TYPE)
by B. VANCAMPEN
C.E.A. I.R.D.I. - CEN-SACLAY
This work has been performed as a subcontract SAV for BV NERATOM in relation
to C.E.E. study contract RAP-022-N.
1 -
INTRODUCTION
B.V. NERATOOM are co-ordinating a CEC study Contract relating to
the tensile properties of 9-12 % Cr steels.
The work has been subdivided into
two parts, Part. I dealing w i t h data collection and Part II w i t h analysis of the
data.
Part I was completed in December 1981 (1) and comprised of contributions
f r o m N E R A T O O M , NIRA, INTERATOM, CEA, BELGONUCLEAIRE and U K A E A .

The data were divided into three sub-files namely 9 % Cr 1 Mo steel, 9 % Cr
2 % Mo steel and 12 % Cr steels.
In Part.II of this exercice, the CEA agreed to analyse the 9 Cr 2 Mo
Nb V data bank in accordance w i t h the technical scope given in the appendice.
This document describes the evaluation of the data bank which has been performed.
2. - E X T E N T OF DATA
Data have provided by France (CEA) and Belgium (BELGONUCLEAIRE).
The t w o set of data were very similar and have been analysed all together.
From the Belgium set the t o t a l range of temperature was covered
every 50 C but in the French set, data were only available at room temperature,
and temperatures higher than 300 C.
kk melts have been tested leading to a total amount of *V46 data
points for proof stress and u l t i m a t e tensile strength and 433 data points for
t o t a l elongation.
No values of reduction of area were available.
Only 60 % of
the data were corresponding s t r i c t l y to French standard NF A 49-213 for this

kind of steels for tubes and pipes.
In the analysis, only the melts for which data were available at room
and high temperature have been retained.
uu
3 . - METHOD OF ANALYSIS
It has been decided to use a cubic equation of the f o r m : mechanical
property = A + BT + CT* + D T 3 (1) where is the temperature (C) t o evaluate
the tensile properties.
The temperature range is from room temperature up t o
600 C.
4 . - PROOF STRENGTH - R e 0 . 2
The 0.2 % proof strength values Re0.2 are given on f i g . 1.
The
average curve which was derived using least squares techniques f r o m 427 experimental
data is given by the equation :
R e 0 ? (N/mm2> = 511.60
AV
7.31 10
_1
2.40 10-3
The standard deviation was evaluated at 28.39 N/mm*.
2 - 3.00.10-6
(2)
For evaluating minimum
properties a curve parallel to the average curve was drawn at a distance correspon
ding at 1.97 times the standard deviation (95 % confidence limit) leading to the
equation :
Re 0.2 min.
Re 0.2
A y
- 55.82
(3)
5 . - U L T I M A T E TENSILE STRENGTH - Rm
The analysis has made using 427 data points.
The average curve is
given by the equation :
R m A V ( N / m m 2 ) = 722.39 - 1.15 + 3.97.10" 3 2 - 5.14. ! 0 " 6 3

The standard deviation is estimated to 26.27 N / m m 2 .
again given by a parallel curve :
Rmmin.
R m
A V
51.49
These curves and the data points are given or f i g . 2-
(4)
The minimum values are
131
4 -
6.-
T O T A L ELONGATION .
432 experimental values have been used.

r e l a t i v e l y large.
The scatter appeared to
An average curve is given by :
A ( % ) = 22 86 - 4.91.10" 2 T
AV
+ 5.84.10" 5 T 2 + 4 2 3 . 1 0 " 8 T 3
(5)
This curve is shown on fig. 3,
7.
PROOF STRESS TO UTS. RATIO

The proof stress
f i g . 4.
to UTS ratio calculated on average values is given on
It appears that this r a t i o of about 0.71 a t room temperature is slightly
increasing at temperature
higher
than 500 C and reachs the value of 0 8 2 at
600 C .
8.-
CONCLUSION
The tensile data of the commpn data bank from Belgium and France on
9 Cr 2 Mo Nb V steel (EM 12) have been evaluated. Average values of the d i f f e r e n t
properties are listed in table 1.
#**######**#*
TABLE 1
9 % Cr - 2 % Mo STEEL
(AIR QUENCHED + TEMPERED)
TENSILE PROPERTIES
(C)
R
p 0.2 (N/mm2)
(N/mm2)
A (%)
no
0.2/O
20
100
150
200
250
300
350
400
450
500
550
600
498
459
446
437
432
427
421
411
395
371
336
289
701
642
622
610
603
596
586
568
540
497
435
351
21,9
:s,6
17,0
15,7
14,9
IM
14,6
15,3
16,4
18,2
20,5
23,5
0,701
0,716
0,717
0,717
0,717
0,717
0,719
0,723
0,732
0,746
0,773
0,824
OJ
133
<
CT
c
CNI
ef
50
Temperanne
Fl. 1 ELEVATED
3% O . l i .
600
(*C)
Mo STEEL (Alf? QUtMCHE + TEMPERED }
TEMPERATURE
PROOF STRENGTH VALUES
1J4
J
Oj
ii
C
OJ
40
500
00
bemperuhjre (^c)
FIG. _2__
9%
Cr.
ELEVATED
2*/. Mo
STL
TEMPERATRE
(AIR
UEJ-JCUED 4- TEM P R D )
I S . VALUES .
135
&
C
cn
p
cL
400
500
00
Temperalure ( ? c )
flG. 3
9 % Cr . 2 */. Mc STEEL
( AR UENCHED + TEMPERED )
ELEVATED TEMPERATURE DUCTILITY VALUES
1b
: i'
l)W
_T_
' :
r-
... '.. j....i..
-f-
'
-....LU0,75
...L.
.2
....... ....
'
L....:....{......
/S
- 11
i. ;
!
!
~~ \
:
:
....._..
L ' Ii
j " f" "|
1'
0,25
"'[-"I
4~ ....
..i. 1-
: i
I
!
..... ..
i
"i" '
.LL
""
. 1
: .1
i'
: j : !
1 -:- :
I0
....i. i
!..
1,
300
: ^
j.
PROOF 5TREr4GTM
UZS.
:;
i .:.!
;:_L.
'
.....
' 1 14-LJ....L4-.
400
,..t.-.r
i i ! I
i
1
1
500
. H H _J_|_i
:
. :
600
S*/ C r. l'L Mo STEEL (AIR UENC HD 4 TEMPERED)

PROOF STRENGTH TO UTS RAT/.
R -
i ; 1 1 i
' I" 1 !
Temperakin . ( 'C )
MdL-
!:.!l
L - i - l u i..
..
'
..... ,|
. ._L .-.1(
!
- - - -
I
200
.......
"T
" I IM'
;
i.tl
.
: i
;-.[.. .-. ...
_.i...L.i
:;
T:::f- =!-
' i
.
-:!,.;::
:\:
i ;
....
'
^|-;j
!. i i ;
.... y. . y ... i__.
}:\
[ - !
i
T-m-tp
i: 1
- -j[ i
. iti
.._L-
...:.
_! j . ..
_4- i__i
i
i
""'"
...J.
. .....
_:.:.. .Li...!...;., '--i- t-j-' l i i
""
I l
...,.,...,.,..
......... ~\~~
'Ti
1 '.
1
1 : j ..
..
_...L . . ! . . . . ] . .
TIJT.T.^\
4-i I-
. ..j_..
.1
. .. .. ....: ... ....
"TM
....
... . l_L _ _ -t-frt- y
+-H-
""[""'
i
i
;
;l 1 :
. .
.i
---
i '
!
! li 'i ;
""~' I ir
i
I
- r-)- ---j- -;-
. 1 .
'
:..
FCiJ
I
i. '
........!....: .
r
; :
!
1!
. I
700
137
FRCC WGC&S, Act 3. "Materials"

Comparison of the tensile properties of 9-12% Cr-steels
Interim report: Subfile 12% Cr-steel; Part II
(RAP-022-NL)
by
H.C.D. Nieuwland (Neratoom, The Hague, the Netherlands)
16 February, 1983
Summary
The subfile on 12% Cr-steels was taken from the common data
bank, see Part I (DATA FILES) December 1981, and evaluated.
The data bank comprises 36 melts and yields only 153 tensile
tests divided over two types of 12% Cr steels. Twenty percent
of the tensile test data relate to the tungsten alloyed
X 20 CrMo WV 12.1 with an average of 0,458% W. The mechanical
properties of both types of 12% Cr-steels are characterized
in average, lower and upper confidence levels and ratios
R _ _/R . The chemical analysis of both types of 12% Cr-steels
pO, 2
is also characterized.
This work has been performed under Agreement No. RAP-022-NL

CEC Study Contract
FRCC Working G roup Codes & Standards
138
Contents
Page
Summary
1
1. Statistical calculations
3
2. Evaluation
3
3. References
3
List of tables
Table 1. Distribution of tensile data, ref. 1
4
"
2. Comparison of chemical composition
5
"
3. Minimum tensile properties for X 20 CrMoWV 12.1
6
4. Minimum tensile properties for X 20 CrMoV 12.1
6
"
5. Comparison of the constants of the cubic formulas
of the mean value of the mechanical properties of
12% Cr steel
7
"
6. Constants of cubic equation of R . and R lower
M
p0,2
m
and upper level between RT and 600 C
8
"
7. Constants of cubic equation of R and R -ratio
M
pO,2
m
between RT and 600 C
8
List of figures of all 12% Cr steel data
Fig. AB.01 R 2 (betweenR T a n d 6 0 0 degrees Celcius) .
9
AB. 02 R '
10
m
AB. 03 A
11
"
AB. 04 R of A
12
AB. 05 R . ,/R
13
pO ,2 m
"
AB. 06 R _ lower limit
14
p0,2
AB. 0 7 R lower limit
14
m
"
AB. 08 RQ 2 upper limit
15
"
AB.09 R upper limit
15
Annex 1 Technical scope o f the study
16
Annex 2 X 20 CrMoWV 12.1 versus X 20 CrMoV 12.1
Figures A . 0 1 - B.01 R _ . .
17
^
p0,2
A.02 - B.02 R
18
m
A . 0 3 - B.03 A
19
A.04 - B.04 R of A
20
"
A . 0 5 - B.05 R 0 / R -ratio
21
-2- , m
139
1. Statistical calculations
Mean values of the mechanical properties are calculated with
the aid of a Cyber-175 (Control Data) computer. A least squares
best fitting routine is used for the calculation of the constants
of the cubic formula. The results are given in table 5.
The distribution of tensile tests over the abscis is not uniform.
If the number of data points is more than three a statistical
calculation of upper (95%) and lower (5%) confidence limit was
performed. The variance of the sample was calculated under the
conditions of the "Null Hypothesis". The confidence limit was
calculated after correction of the number of degree of freedom.
In the figures AB.01 up to AB.05 and in Annex 2 in the figures
A. 01 - B.01 up to A. 05 - B.05 the lower confidence _limit (5%)
is denoted by LCL and the upper confidence jLimit (95%) is
denoted by + UCL.
2. Evaluation
The data file contains a very small number of data. The mean
values for the 12% Cr steel with tungsten are heavily inf luenced
by the lack of data between RT and 500 C.
The chemical analysis of one steel shows a significant low
content of molybdenum. The mean values of the two qualities of
12% Cr steel do not show significant differences except for a
slight difference in chromium content, see table 2.
An evaluation of the minimum tensile properties in tables 3 and
4 shows among others exceptions for aged steels and for the
steel with significant low molybdenum content.
3. References
Ref. 1. Nieuwland, H.C.D. etal.
"Comparison of the tensile properties of 9-12% Cr steel"
Part I (data files), Dec. 1981
Ref. 2. Moroney, M.J. "Facts from figures"
Pelican books A 236, Third and revised edition.
-3-
140
Table 1
Distribution of tensile data, ref. 1
Temperature (C)
Steel designation RT
200
250
300
350
400
450
500
550
600
20 CrMoWV 12.1
11
20 CrMoV 12.1
80
24
10
Total
91
24
16
-4-
141
Table 2
Comparison of chemical composition
Designation
Element
X 20 Cr Mo W V 12.1
X 20 Cr Mo V 12.1
average
min.
max.
average
in weight %
min.
max.
in weight %
Carbon
.198
.17
.22
.199
.17
.25
Silicon
.338
. 11
.48
.361
.28
.50
Manganese
.542
.40
.68
.502
.43
.60
Phosphorus
.007
.024
.011
.018
Sulphur
.005
.019
.009
.014
Chromium
11.57
10.5
12. 14
11.98
11.6
13.0
Nickel
.538
.16
1.0
.416
.09
.66
Molybdenum
.972
.7
1.2
1.097
1.04
1.35
Vanadium
.300
.26
.33
.305
.22
.37
Tungsten
.17
.458
.13
.53
< 0.2
Remarks: Evaluation of the average chemical comnosition between

X 20 Cr Mo V 12.1 and X 20 Cr Mo W V 12.1 shows only a
slight difference in chromium content and the
distinguishing difference for the tungsten content.
-5-
142
Temperature
Property
RT
p0,2 ( N / n m 2 )
R
(N/mm2)
A
(%)
R of A
(%)
500 C
550 C
600 C
492 (5)
341 (7)
270 (2)
174 (11)
687 (2)
487 (2)
391 (2)
302 (11)
17 (8)
19 (7)
12 (8)
26 (7)
47 (11)
49 (1)
60 (1)
71 (7)
Table 3
Minimum Tensile Properties for X 20 CrMoWV 12.1
Remarks: the figure between brackets refers to the heat list, ref. 1
N.B. No. 5: aged condition: 100 h/700 C.
Temperature
RT
Property
R
p0,2 (N/mm.2)
500 C
550 C
600 C
429 (3)
435 (5)
385 (14)
342 (1)
691 (5)
500 (14)
400 (23)
10 (7)
10 (2)
44 (3,7)
47 (2)
24
10
Rm
(N/mm )
726 (8)
(%)
15(7,15,18) 15 (2,4,5)
R of A
(%)
Number of data
39 (9)
80
46 (2)
3
Table 4
Minimum Tensile Properties for X 20 CrMoV 12.1
Remarks: The figure between brackets refers to the heat list, ref. 1
N.B. The members 1 up to 7 refer to tubes.
No.'s 3 and 5 are in an aged condition: 2 h/780 C
No. 14 contains an exceptionally low Molybdenum
percentage
-6-
143
Table 5
Comparison of the constants of the cubic formulas of the mean
value of the mechanical properties of 12% Cr steel
= A + BT + CT 2 + DT 3
denotes mechanical property
A, B, C and D denote constants of the cubic equation

denotes Temperature in degree Celcius between RT and 600
Property
12% Cr steel type
R
p0,2
Constants
C * IO 3
D X IO 6
57 3. 0
- 1.853
7.474
- 8.988
638.0
- 1.960
6.703
- 7.277
635.3
- 2.234
8.222
- 9.283
X 20 CrMoWV
779.8
- 1.635
5.683
- 6.970
X 20 CrMoV
830.8
- 1.077
2.910
- 3.826
All data
832.7
- 1.585
5.194
- 6.442
X 20 CrMoWV
20.04
0.059 75
-.3737
.5122
X 20 CrMoV
19.82
0.014 75
-.1619
.2350
All data
19.16
0.058 53
-.3787
.5112
X 20 CrMoWV
56.71
0.142 0
-.7565
.9859
X 20 CrMoV
52.92
0.040 53
-.2353
.3442
All data
52.45
0.120 7
-.6336
.8171
X 20 CrMoWV
X 20 CrMoV
All data
R
R of A
-7-
144
Table 6
Constants of cubic equation of R . and R lower and upper
pO, 2
m
level between RT and 600 C

2
3
Formula: = A + BT + CT + DT
12% Cr steel
c * io3
D * IO 6
All data
R L. L .
p0,2
U.L.
428.6
0.4441
2.509
4.144
782.0
2.496
4.137
L. L.
698.1
0.525
1.612
3.145
U.L.
979.6
2.856
4.543
0.8073
1.021
Table 7
Constants of cubic equation of R ,/R ratio between
*
p0,2' m
RT and 600 C
2
3
Formula: = A + BT + CT + DT
'
12% Cr steel
"
* IO 3
C * io6
D X IO 6
X 20 CrMoWV 12.1
0.7562
2.019
X 20 CrMoV
0.7720
1.611
6.152
.005783
0.7751
1.935
8.128
.008522
All data
12.1
10.10
.01188
145
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11/02/831
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. IN oeeR.CELC.
nr
AO
Ib A , f 7
"" U P P C T L I " I T
STEEL X20C RMOIHV 12.1
450.0
52S.0
152
ANNEX 1
"Comparison of tensile properties of 912' Cr steels:

Part II (Statistical analysis)"
Technical scope of the study
1.
The contribution of the member states to the 1980 study

contract (Tart I, data files) will be evaluated whether
they offer a sufficient basii? for statistical analysis.
2.
_ ,, R , A and R of A will be
The tensile properties R
U f .
expressed in a cubic equation of the kind mechanical

2
3
property A + BT CT + DT whore stands for temperature
between RT and P,00C.
3.
The statistical analysis v/ill comprise average values,

minimum values and
4.
The R
,,/R
\ 95 7 lower bound confidence level.
ratio will be obtained
0, m
5.
Effects of product form or steel making practice v/ill

be noticed.
The data ilos wiJl be divided
into subfiles concerning
steel qua Litio.:: 'rom different source.; of three kinds

9
7.
Cr
! Mo.',
) Cr
1 '!o
.uu!
12
Cr
'.-IJ.
A final report will be draf tei and the results will be

compared with current standards. Conclus ." ons v/ill be
drawn. R.?c .vd o'. r o m v/ill bo f o .mu La ted .
16
NEWT0D1 BV
IU/02/8J1
owToofl ev I
l l / 0 '83'
0.0
75.0
FIG R.01
ISa.O
325.0
300.0
35.0
TEMP. IN OEGR.CELC.
50.0
525.0
RP BETWEEN RT ANO $00 DEGR.CELCIUS

STEEL X20CRM0WV 12.1
0.0
rtn
Y lb
75.0
D ni
. UI
ISO.O
225.0
30O.3
375.0
TEMP. IN OEGR.CELC.
W BETWEEN RT HNO 600
STEEL X20CRM0V 12.1
&0.0
535.0
OEGR.CELCIUS
NERflTOUn Bi
tac2.e3'
tl/oi/l
I ICRflTOOrt BV
i
o
CD
2
o
ur
0.0
75.0
150.0
225.9
300.0
173.0
50.0
57...0
TEMP. IN DCGR.CELC.
cm
a C
lb h.U
*" BETWEEN RT ANO COO OEGR.CELCIUS

STEEL >20CRM0WV 12.1
600.0
>
0.0
cm
lb
1
1
1
1
75.0
IS0.0
225.0
30C.0
375.0
450.0
S25.0
TEMP. I N DEGR.CELC.
ni
t.U
RM BETHEEN RT NO 600 DEGR.CELC I US

STEEL X20CRM0V 12.1
un
.o
NDWTOOfl BV
1 NDWTOON BV
10/02/83'
11/02/831
9a
sr
II
s-
. o
S*
.
Z o
LL"3'
"^^^^
0
^~^^
^~~*"~^
.
S
"
O
_]
e
0
O
"
cr
tr
ISO.O
225.0
300.0
T7S.0
50.0
525.0
600.C
0.0
75.0
TEMP. IN OEGR.CELC.
FIG fi.03
A BETHEEN RT AND 600 DEGR.CELClUS

STEEL X2GCRM0WV 1?.I
150.0
225.0
300.0
375.0
S0.C
525.0
UE.C
TEMP. IN DEGR.CELC.
Fir
SO o
R BETHEEN RT A NO 600 CEGR. CELCIUS

STEEL X20CRM0V 12.1
UI
UI
NEKIIOCI BV :
/*'3?
w/jl
I iftTS BV
si
o
:.4
SO.
225.0
SJO.O
Vi.O
150.0
52S.0
WO. O
0.0
TEMP. IN DEGR.CELC.
A
lb r\.m
R 0 F fl
BETWEEN RT A NO 600 DEGR.CELCIUS

STEEL X20CRM0HV 12.1
I
|
75.0
FIG .04
150.0
225.0
300.0
r
375.0
50.0
525.0
BO.O
TEMP. IN OESR.CELC.
R OF A BETWEEN RT ANO 600 DEGR.CELCIUS
STEEL X20CRM0V 12.1
Ui
Tiowraati Bv !
"U'WBSI
1 tCRMOCn BV I
14/02/831
r*
""*
-,
O
o"
o"
1 'S
UCL
o"
'
x.
1
o"
I
,
:
cc
in
o"
*
O"
o"
rt
0.0
75.0
IS0.0
225.0
300.0
375.0
50.0
525.0
00.:
TEMP. IN DEGR.CELC.
L-i
M b
o ner
H.Ub
RP/RM BETWEEN RT AND 600 DEGR.CELC I US

STEEL X20CRM0WV 12.1
0.0
75.0
150.0
23.0
TEMP.
FIG B.05
300.0
375.0
4S0.0
525.0
600.0
IN 0E6R.CELC.
RP/RM BETWEEN RT A NO 6 0 0 O E G R . C E L C I U S
STEEL X20CRM0V 1 2 . 1
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Commission of the European Communities

nuclear science and technology

COMPARISON OF THE TENSILE PROPERTIES

Commission of the European Communities

nuclear science and technology

COMPARISON OF THE TENSILE PROPERTIES

H.C.D. NIEUWLA ND 1 ), G. BRUNRT), E.D. GROSSER3),

NERA TOOM, The Hague, (NL)

This work was performed under

Directorate-General Science, Research and Development

ECSCEEG EAEC Brussels - Luxembourg, 1985

Subfile 9%Cr l%Mo steels

Subfile 9%Cr 2%Mo steels

The UKAEA contribution 9%Cr l%iio steel

The Belgonucleaire contribution NF A 498.11 steel

Subfile 12%Cr steel

The Interatorn contribution X20 CrMoVYi 12 i steel

The UKAEA c o n t r i b u t i o n 9%Cr 1 Mo S t e e l

United Kingdom Atomic Energy Authority

CEC STUDY CONTRACT : COMPARISON OF THE TENSILE PROPERTIES

The UKAEA contribution relates exclusively to 9%Crl%Mo steel.

T8LE 1 : DETAILS OF TEST MATERIALS frCHHo

Che<n1cal Composition, X wt.

Chemical Compositi on, * Wt

As for Ref No 93.

* Heat tre ste d as 15.9mm.sq se ctions,

7 3-.I 3S7-*i! ^ 37-sl

7C6-I 1 &2o -31

X.1, l.l.W.V> M . l . ' H O N A C A l l i A

IS. A continuous record shall be made, or a sufficient number of strain readings

MHASuTMFNT OF TEST AFTE FRAC TUnn

16. If va'jcs of elongation or reduction of area arc required, sufficient measure

Subfile 9%Cr l%Mo steels

The activity 3 "materials" of the working group

Seven heats were studied, which are avaible:

This steel, corresponding to ASTM specification

Tensile properties at room temperature are given in Table IV.

The grain size was estimated with ASTM metod

Table II - CHEMICAL ANALYSIS - VALUES IN % OF WEIGH

Table III - GRAIN SIZE

Table IV - TENSILE PROPERTIES AT ROOM TEMPERATURE

PROPERTIES AT HIGH TEMPERATURE

Subfile 9%Cr 2%Mo steels

The Belgonucleaire contribution NF A 49811 steel

Appendix to our letter dated 16.10.81

CONTRIBUTION TO THE COMPARISON OF

The available data for chemical analysis and tensile properties

6 mm) and tested on the

basis of ASTM norms according to the laboratory internai procedure.

TENSILE PROPERTIES OF 9 12 7. C r STEELS

1. '.AMPLE Nr. ( 24459

2. 11 EMI CAL COMPOSITION (7.)

eduction of area (7.)

TENSILE PROPERTIES OF 9 12 7. Cr STEELS

2. i'UEMICAL COMPOSITION (7.)

:lniform elongation (7)

Keduction of area (7.)

TENS ILL PKOt'LIURS Ol- 9 - 12 /. Lr S'l'liliLS

'Iniform elongation (7.)

Reduction of area (7.)

TENSILE PROPERTIES OF 9 12 7. Cr STEELS

.l'LE Nr. ( 25587