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Procedure 2. c- Place the crucibles in a 250- mL labeled beaker ready for the oven
Procedure 2. e- Let your crucibles cool for at least 30 minutes in the dessicator before weighing Procedure 2. d- TAs place all beakers with the crucibles on a designated rack in the oven for drying
e- No more precipitate!
b- Continue to add more 2M NH4CH3COO until the precipitate stops dissolving with stirring
d- Parafilm your beaker and let the precipitate digest overnight in your 4 drawer
Attach black hose to the vacuum line Attach black hose to the vacuum line
Crucible
Vacuum adapter
Procedure 6. b- Set the filter paper in place by wetting it with DI water (vacuum is on)
All perforations must be covered at the bottom of the crucible and the filter paper must not be creased
Procedure 6. c- Add the solution to the ceramic crucible with pre-determined mass
Procedure 6. c- Use a stirring rod to guide the solution onto the filter paper
The filtrate in the filter flask should be clear (i.e., with no solid particles ) and light yellow in color
Procedure 6. d- Wash the beaker quantitatively with water, adding the wash to the crucible
Procedure 6. h- Place your crucibles in a 250 mL labeled beaker ready for the oven
TAs place all beakers with the crucibles on a designated rack in the oven for drying 7
Procedure 6. i- After drying , let your three crucibles with product cool for at least 30 minutes in the dessicator before weighing Procedure 6. j- Weigh each of the cooled crucibles with the product