Slide #1

6850/6890 Split Animation

Split/Splitless Inlet - Component Identification
Septum
Liner
Liner O-Ring
Gold Seal
Capillary Column
5/4/00
Slide #2
6850/90 Split/Splitless Inlet - Component Identification
Septum
SEPTUM PURGE
VENT
Inlet Split
Port
Slide #3
6850/90 Split Animation - Default Conditions
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
SPLIT
VENT
GOLD SEAL
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
0

ML/MIN
SPLIT VENT
TRAP
0

PSI
Slide #4
6850/90 Split Animation - Total Flow Setting
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
SPLIT
VENT

205 ML/MIN
GOLD SEAL
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
PRIMARY FLOW PATH
REDUCED FLOW PATH
205

ML/MIN
SPLIT VENT
TRAP
0

PSI
Slide #5
6850/90 Split Animation - Inlet Pressure Setting
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
GOLD SEAL
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
PRIMARY FLOW PATH
REDUCED FLOW PATH
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
PRESSURIZED GAS
BACK PRESSURE CONTROL LOOP
Slide #6
6850/90 Split Ready for Injection
Animation
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Mode: Split
Temp 250 250
Pressure 10.0 10.0
Split Ratio 100
Split Flow 200
Tot Flow 205.0 205.0
Gas Saver OFF
Slide #7
6850/90 Split Insert Syringe
Animation
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
GOLD SEAL
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Slide #8
6850/90 Split Inject Sample
Animation
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
GOLD SEAL
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Slide #9
6850/90 Split Sample Vaporizes
Animation
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
GOLD SEAL
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Glass Wool
Slide #10
6850/90 Split Sample is Split -
Animation Good Liner Design?
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Smaller O.D. Liner
Open Split Flow Path
Glass Positioning
Bead
Glass
Wool
Tapered Liner
Agilent Split
Liner - 5183-4647
Slide #11
6850/90 Split Split Continues
Animation
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Slide #12
6850/90 Split Split is Complete
Animation
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Slide #13
6850/90 Split Sample is separated
Animation and Detected
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Slide #14
6850/90 Split Gas Saver - Set to 55 ml/min
Animation After the Injection is complete
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
55

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

50 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Mode: Split
Temp 250 250
Pressure 10.0 10.0
Split Ratio 100
Split Flow 200
Tot Flow 205.0 205.0
Gas Saver ON
Saver Flow 50.0
Saver Time 0.5