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Heat treatment effect on microstructure and phase transformation and
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4- PROPOSAL SUMMARY
Title of the Project
Effect of aging treatment on microstructure and martensitic transformation
and magnetic properties of NiGaFeTi smart shape memory alloys
Principal Investigator: Dr. Nader El-Bagoury
Name of the College: Science
Name of the Department: Chemistry
Heat treatment processes like annealing, solution and quenching, homogenization, and ageing
affect the microstructure, phase transformations, mechanical and physical properties of alloys.
The heat treatment process factors are the applied temperature and the duration of time for the
heating cycle as well as cooling rate after heat treatment process using water or air or cooling
inside used furnace. Using different temperatures and also variant times, volume fraction of
different phases in the microstructure, martensitic phase transformation temperature, mechanical
properties such as hardness and tensile strength and physical properties like magnetic properties
will be influenced and investigated. In this study, a combination of heat treatment processes;
homogenization, solution and ageing treatments will be accomplished for the Ni-Ga-Fe-Ti shape
memory alloys to find out the changes can be occurred for the its microstructure, phase
transformations, martensitic-austenitic reaction temperature and magnetization.
Ferromagnetic Shape Memory Alloys (FMSMAs) have drawn much attention as promising
magnetic actuator materials, since magnetic-field- induced strains (MFISs) as larger as several
percent were found in Ni2MnGa Heusler alloys. Some new Hueslr alloys such as Co-Ni-Al, Co-NiGa and Ni-Fe-Ga were explored up to now some other alloy systems have also been developed as
FMSMA candidates, such as Fe-Co-Ni-Ti, Fe-Pt, Fe-Pd, Co-Ni as well as two Co=based ternary
alloys, i.e Huesler-type Co2NiGa and Co-Ni-Al (B=2 structure) alloys. The occurrence of MFIS can
be attributed to two actuation mechanisms. One is the magnetic-field-induced martensite
transformation from the parent phase, and another is the magnetic-field-induced reversible
redistribution of martensite twin variants. In general the former needs a huge magnetic field, e.g.
in Fe-Co-Ni-Ti systems, and the latter is responsible for the large MFIS to Ni 2MnGa Heusler alloys
under a moderate magnetic field. The MFIS formed due to the latter actuation mechanism has
been well described by a phenomenological model with such parameters as Zeeman energy,
magnetic anisotropy energy, an internal elastic energy and an external stress.
Similar to Ni2MnGa alloy, other Heusler alloys with a reversible martensitic transformation may
also possess the capability of MIFS. A very recent study on Ni 54Ga27Fe19 alloy has demonstrated the
Ni-Fe-Ga alloy as a Heusler-type FMSMA.
The most important problem of Ni-Mn-Ga alloys to be used in practical engineering fields is how
to increase the martensitic transformation temperatures, that is, the operating temperature must
increase. Progress is being made in this direction. The main method is to adjust the alloys
compositions. For the newly-explored Huesler alloys, few researchers have been conducted and
they are still not sufficient for designing alloys with proper martensitic transformation
temperatures.
In this research, the effects of ageing heat treatment process on the martensitic transformation
5
and microstructure of Ni-Ga-Fe-Ti smart shape memory
alloys will be investigated. Additionally,
influence of heat treatment variables such as temperature and time on magnetic properties of NiGa-Fe-Ti will be studied as well.

 -5

The process of heat treating is the method by which metals are heated and cooled in a series of
specific operations that never allow the metal to reach the molten state. The purpose of heat
treating is to make a metal more useful by changing or restoring its mechanical properties.
Through heat treating, we can make a metal harder, stronger, and more resistant to impact.
Also, heat treating can make a metal softer and more ductile. The one disadvantage is that no
heat- treating procedure can produce all of these characteristics in one operation. Some
properties are improved at the expense of others; for example, hardening a metal may make it
brittle.
The various types of heat-treating processes are similar because they all involve the heating
and cooling of metals; they differ in the heating temperatures and the cooling rates used and
the final results. Most nonferrous metals can be homogenized, annealed, solutions, aged but
never tempered, normalized, or case- hardened.
STAGES OF HEAT TREATMENT
Heat treating is accomplished in three major stages:
Stage l: Heating the metal slowly to ensure a uniform temperature.
Stage 2: Soaking (holding) the metal at a given temperature for a given time and cooling
the metal to room temperature.
Stage 3: Cooling the metal to room temperature.
Most documented studies exploring the aging effect on shape memory alloys have been
associated with AuCd [1], CuAlNi [2] and TiNi systems [39]. These studies can essentially
be classified into two major categories: martensite aging effect and aging-induced
precipitation.
The first category provides a means to understand the rubber-like behavior and martensite
stabilization with respect to the change in Af/As by martensite aging (aging at < As) [13]. The
other category explores the precipitation process as well as the effect of precipitates on
martensitic transformation behavior or the shape memory effect [49]. However, few relevant
studies on aging have been documented for FSMAs [1013], and those that have are
inadequate. Our previous work on Mn2NiGa alloys has demonstrated that aging cannot only
provide an alternative way to enhance magnetization but can also induce Mn-rich
precipitates within a certain temperature range [1, 14].
In conventional shape memory alloys (SMAs), which are paramagnetic, the martensitic
transformation underlying the shape memory effect is induced by changes in temperature or
stress or both. The same transformation in ferromagnetic shape memory alloys (FSMAs) can
be triggered not only by changes in temperature and stress, but also by changes in the applied
magnetic field. Therefore, it has attracted much attention as high performance solid-state

actuator materials. Many FSMAs systems have been developed from Heusler alloy system,
such as Ni2MnGa [15-18], Ni2MnAl [19], Co-Ni-Ga (Al) [20, 21], and Ni-Fe-Ga [22, 23].
There have been many reports on their structure, magnetic properties, martensitic
transformation, magnetically controlled shape memory effect, super plasticity and magneticfield-induced strains (MFIS).
Shape memory alloys have the ability to perform both sensing and actuating functions. As
commercial functional materials, TiNi and Cu-based SMAs have been applied in mechanical,
electronic, medical and dental areas etc. [24, 25]. The operating temperatures of most SMAs
depend on their themo-elastic martensitic transformation (MT) temperatures. The MT
temperatures of TiNi and Cu-based alloys are below 150C, so the devices made with SMAs
can only be applied in low temperatures [26, 27]. Many applications, such as aircraft and space
industry, automobile industry, oil and gas exploration, and nuclear industry etc., require a
shape memory transformation temperature between 150 and 400C with structural stability
when heated for long periods up to 600C [28]. Therefore, it is necessary to develop SMAs that
have the high MT temperatures and the good stability of the microstructure, the mechanical
properties and the shape memory behavior over a long time at elevated temperature. A
number of alloy systems have exhibited transformation temperatures at or above 150C,
showing promise as high-temperature SMAs. These include alloys of the TiNiPd(Pt, Hf) [29,
30], RuTa(Nb) [31, 32] and NiAl-based [33, 34] systems. Among these alloys, NiGaFe alloy has
high thermal conductivity, good high temperature strength, and excellent oxidation and
corrosion resistance. Furthermore, it has the shape memory effect (SME), high transformation
temperatures, and low cost, and is a potential high temperature SMA [35].
Heusler alloys have attracted much attention for their unique potential as actuators in
microelectromechanical systems [36], especially Ni-Mn-Ga, in which a magnetic-field-induced
strain up to 6% has been reported [37]. Subsequently, some new Heusler alloys, such as Co-NiAl, Co-Ni-Ga and Ni-Fe-Ga were explored [38, 39].
Recently, Oikawa et al. have found the Ni-Ga-Fe alloys to be promising FSMA candidates [40,
41]. According to their study, the parent phase with the B2 and /or the L2 1 structure
martensitically transforms into a seven-layer modulated structure (14M) and a five-layer
modulated (10M) structure up on cooling. More recently, some additional investigations have
been reported. However the atomic and magnetic orderings and the martensitic
transformations in the Ni-Ga-Fe B2 phase alloys have not been reported yet. The atomic
ordering that associated with the transformation of B2 to L2 1 and the martensitic
transformation from L21 to the modulated layer 14M and/or 10M revealed that the shape
memory effect take place in the ferromagnetic state.

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Materials and Characterization Techniques:

Materials:
Ni Ga Fe Ti smart shape memory alloys (SMAs) will be investigated in this study.

Melting and casting:

To obtain clean cast polycrystalline Ni Ga Fe Ti (Ti= 2.0 % at) shape memory

alloys (SMAs). These alloys will be made using arc-melting under argon
atmosphere (the purity of the elements is higher than 99.99%). The cast alloys will
melt many times to ensure the homogeneity. The as-cast alloys will be used in
this investigation.

Heat treatment processes:

Solution treatment: 24 h homogenization treatment at1170 K in under Ar atmosphere
followed by quench in iced water.
Ageing treatment: Subsequently, the solution-treated samples were aged within a
temperature range of 573 - 973 K for various durations and then quenched into iced
water.

Microstructure investigation:
Light optical microscopy (LOM), X-ray diffraction (XRD), and scanning electron
microscopy (SEM), Energy dispersive X-ray spectroscopy (EDS) will be used to
determine local chemical composition of alloying elements, grain size, recognition
of different phases exist in the microstructure, volume fraction of these phases.
Additionally X-ray tests will be used to detect and prove the existence phases in
the microstructure.

Evaluation of phase transformations:

Differential Scanning Calorimetry (DSC) instrument will be used to investigate the
phase transformation of SMAs especially the hysteresis of martensite and austenite
phase transformations.
11

 Evaluation of mechanical properties:

Mechanical properties like hardness, tensile and ductility will be carried out to
evaluate the effect of different additions of Co on mechanical properties.

Monitoring of magnetization of tested alloys

Magnetization of Ni Ga Fe Ti smart shape memory alloys will be measured to
know to what extent that the variables of heat treatment influenced the Magnetic
properties of these alloys.

Results evaluation:
The results that come out from the different tests that will be carried out will be
analyzed and evaluated. Final report will be prepared.

Publication:
The final outcome results of the project will be published in a high reputation
international journal with high impact factor.

12

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12. REFERENCES
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37. W.D. Collins, R.E. Weyers, I.L. Al-Qadi, Corrosion 49 (1993) 74.

16

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nader_elbagoury@yahoo.com

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M.Sc. title: Microstructure and Solidification Mode of Austenitic and
Martensitic Stainless Steels.
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Ph.D. title: Microstructure and Mechanical Properties of Ni Base
Superalloys, Inconel 718 Alloy.

9/4/1995 9/3/1999 .
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Journal of Materials Transactions A

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Superalloys 2003 .2006

20

2007 -
2007 -
2008 -
2008 -

1.
Moustafa I. M., Nader El-Bagoury, A. A. Amar, S. A. Ibrahim, A. A. Nofal, Solidific
Conditions of Martensitic Stainless Steels, Egyptian Journal of Chemical Engineering, E
July 1999, Vol. 25, No. 2, p 64.
2.
Moustafa I. M., Nader El-Bagoury, A. A. Nofal, Interdendritic Ferrite in Solidificatio
Austenitic Stainless Steels Egyptian Journal of Chemical Engineering, Egypt, Oct. 2000 Vo
No. 4, p 197.
3.
Moustafa I. M., Nader El-Bagoury, A. A. Amar, S. A. Ibrahim, A. A. Nofal, Solidific
Mechanism of Martensitic Stainless Steels Ironmaking and Steelmaking, 2001, Vol. 28, No
404.
4.
Nader El-Bagoury, Kaoru Yamamoto, Keisaku Ogi, Effect of Rhenium
Solidification of Inconel 718 Alloy Journal of Materials Science and Technology, London,
21, No. 2, 2005, p 204.
5.
Nader El-Bagoury, Kaoru Yamamoto, Hirofumi Miyahara, Keisaku Ogi, Influenc
Rhenium and Cooling Rate on the Solidification of Ni Base Superalloys, Inconel 718, Journ
Materials Transactions, Vol 46, No. 5, May, 2005, p 909.
6.
Nader El-Bagoury, Toru Matsuba, Kaoru Yamamoto, Hirofumi Miyahara and Kei
Ogi, Influence of Heat Treatment on the Distribution of Ni 2Nb and Microsegregation in
Inconel 718 Alloy, Journal of Materials Transactions, Vol. 46, No. 11, Nov, 2005, p 2478 .
7.
Mohamed Ramadan, Mitsuharu Takita, Hiroyuki Nomura and Nader ElBagoury "S
solid processing of ultrahigh-carbon steel castings" Materials Science and Engineerin
Volume 430, Issues 1-2, 25 August 2006, p 285.
8.
Nader El-Bagoury, M. A. Waly, A. Nofal Effect of various heat treatment condition
microstructure of IN738LC alloy, Materials Science and Engineering A 478, 2008, 152-16
9.
Nader El-Bagoury and A. A. Nofal "Investment casting of Ni Base Superalloys", Jo
of Geisserei Praxis, June, 2008, 197-210.
10.
Nader El-Bagoury An investigation on a failed turbocharger turbine blade, Journ
Materials Science; An Indian Journal, Vol 6, Issue 2, 2010, 32-36.
11.
Nader El-Bagoury, Mohamed Ramadan, Mohamed Waly and Keisaku
Microstructure control of HIPed Inconel 718 alloy, Journal of Materials Science; An In
Journal, Vol 6, Issue 2, 2010, 36-40.
12.
Nader El-Bagoury and Adel Nofal Microstructure of an experimental Ni
21

superalloy under various casting conditions Journal of Materials Science and Engineerin
527, 2010, 7793- 7800.
13.
Kh. M. Ibrahim, Nader Elbagoury and Y. Fouad, Microstructure and marten
transformation of cast TiNiSi shape memory alloys Journal of Alloys and Compounds
(2011) 3913 3916.
14.
M. Ramadan, N. El-Bagoury*, N. Fathy, M. A. Waly, and A. A. Nofal, "Microstruc
Fluidity and Mechanical Properties of Semi-Solid Processed Ductile Iron" , J Mater Sci (2
46:40134019.
15.
Khaled ElSabawy and Nader El-Bagoury, Structure Visualization and Sur
Microstructural Investigations on Ni-Ti-O Mixed Oxide With ABX3-Structure of Cast
Superalloy, Advances in Applied Science Research, 2011, 2 (2): 38-47.
16.
Nader El-Bagoury Influence of Casting Conditions on Microstructure of sol
treatment of Ni base superalloys, J. Heat Treatm. Mat. 66 (2011) 3.
17.
N. El-Bagoury and Q. Mohsen, "Gamma Prime and TCP Phases and Mecha
Properties of Thermally Exposed Ni Base Superalloy", Phase Transition, Vol. 84, Nos. 11
November-December 2011, 1108-1122.

18.
Nader El-Bagury, Microstructure and Mechanical Properties of Aged Ni B
Superalloys, Archives of Applied Science Research, 2011, 3 (2):266-276.
19.
Khaled M. Elsabawy, Nader H. Elbagoury and Mohamed A. A. Moussa, "Computat
Modeling and Structure Visualization of Ni2X3 ( X= Cr, Ti, W, Co and C ) Structure
Possibility of Cast Ni-Base Superalloy", J. Comput. Method. Mol. Design, 2011, 1 (4): 46-5
20.
N. El-Bagoury, Mohammed A. Amin, Q. Mohsen, "Effect of Various Heat Treat
Conditions on Microstructure, Mechanical Properties and Corrosion Behavior of Ni B
Superalloys", Int. J. Electrochem. Sci., 6 (2011) 6718 6732.

1. Nader El-Bagoury, A. A. Alameldin, Kiesaku Ogi, Role of Rhenium on Solidification

Microstructure and Mechanical Properties of Inconel 718 Alloy, Microstructure, Metallogr
and Analysis, Feb. 2012.
2.
Mohammed A. Amin, N. El-Bagour, A.A. Omar and Adel S. Megahed, "Influenc
rhenium as an alloying element on the pitting corrosion behavior of cast TiNiRe sh
memory alloys I", Int. J. Electrochem. Sci., 2012.

1. A. A. Omar, N. El-Bagoury, "Heat Treatment Influence on Microstructure and Mecha

Properties of Al Alloy, 6061".
2. N.El-Bagoury, Q. Mohsen, Sahar Fadallah, Rasha" Influence of Ni on protein adsorptio
on oxidized surface of NiTi Alloys".

3. N.El-Bagoury, Q. Mohsen, Sahar Fadallah, Rasha " Ni effect on the antibacterial inhibi
of oxidized surface of NiTi Alloys".

.Journal: Materials Science and Engineering A, 2008
.Journal: Alloys and Compounds, 2009
.Title: High strain rate superplasticity of TiNp/2014Al composite
22

Journal: Materials and Design, 2010.

Manuscript Number: JMAD-D-09-01728
Title: Failure analysis of bursting on the inner pipe of a jacketed pipe in a tubular heat exchanger.
Journal: Materials and Design, 2010.
Title: Metallurgical Characterization of Bainitic Steel by Eddy Current Method.

Journal: Materials and Design, 2010.

Ms. Ref. No.: JMAD-D-10-00899
Title: Corrosion Evaluation of One Dry Desulfurization Equipment-Circulating Fluidized Bed (CF
Boiler.

Journal: Phase Transition, 2011.

Manuscript ID: GPHT-2011-0032
Title: Investigation on the microstructure of a -Mg32(Al, Zn)49 strengthened M
Zn-Al alloy with relatively low Zn content

1.
Moustafa I. M., Nader El-Bagoury, Solidification Simulations of Thin Slab Cast
CMRDI Conference Proceedings of Challenges Facing Arab Steel Industry 20-22 Oct. 199
2.
Yuho Deguchi, Seong-Hun Kang, Nader El-Bagoury, Kaoru Yamamoto and Kei
Ogi, Redistribution of Alloy Elements during the Solidification of Inconel 718, 6th Pacific
International Conference Proceedings on Modeling of Casting and Solidification Proce
2004 Kaohsiung, Taiwan.
3.
Nader El-Bagoury, Kaoru Yamamoto, Hirofumi Miyahara, Keisaku Ogi, Influenc
Rhenium and Cooling Rate on the Solidification of Ni Base Superalloys, Inconel 7
Conference Proceedings of the 2nd Japan-Korean Workshop for Young Foundry Engineers
9 July, 2005, Jeju Island, Korea.
4.
Nader El-Bagoury, Kaoru Yamamoto, Keisaku Ogi, Rhenium Effect on Solidificatio
Inconel 718 Alloy conference of Japan Institute of Metals Conference No.134, 31 Marc
April 2004, Tokyo, Japan.
5.
Nader El-Bagoury, Kaoru Yamamoto, Keisaku Ogi, Solidification of Rhenium-Conta
Inconel 718 Alloy conference of Japan Institute of Metals Conference, Kyushu Branch, 4
2004, Kumamoto University, Kumamoto, Japan.
6.
Nader El-Bagoury, Kaoru Yamamoto, Hirofumi Miyahara, Keisaku Ogi, Cooling
Effect on the Solidification of Inconel 718 Alloy Fall Conference of Japan Foundry Engine
Society 12 October 2004, Kita Kyushu, Japan.
7.
Nader El-Bagoury, Kaoru Yamamoto, Hirofumi Miyahara, Keisaku Ogi, Solidificatio
3.5% Rhenium-Containing Inconel 718 under Different Cooling Rates BEST PAPER in
Spring Conference of Japan Foundry Engineering Society No 146, Tokyo, May 2005.
8.
Nader El-Bagoury Ni Base Superalloys as Advanced Materials, First Afro-A
Conference (AMSAT06), 13-16 Nov. 2006, Cairo Egypt.
9.
Nader El-Bagoury, Adel Nofal, Kauro Yamamoto, Hirofumi Miyahara and Kiesaku
"Development of Rhenium Alloyed Inconel 718 Alloy" Egyptian-German Workshop, 7-9
2007, CMRDI, Cairo, Egypt.
10.
Nader El-Bagoury, Adel Nofal, Kauro Yamamoto, Hirofumi Miyahara and Kiesaku
"Contribution to the Development of Rhenium Alloyed Inconel 718 Alloy", 12 th Internat
23

Conference on Aerospace Sciences and Aviation Technology, 29-31 May 2007, Military Tech
College, Cairo, Egypt.
11.
Nader El-Bagoury, Mohammed Waly, Adel Nofal, "Effect of Various Heat Treat
Conditions on Microstructure of IN738LC Alloy", International Conference on Metals Proces
and Manufacturing, 19-22 November 2007, Cairo, Egypt.
12.
Nader El-Bagoury, Mohammed Waly, Adel Nofal, The 9th Cairo University Internat
Conference, Mechanical Design & Production, 8-10 Jan. 2008.
13.
Nader El-Bagoury and Adel Nofal, Microstructure of Ni-base super cast Inconel
Alloy, ArabCast, 7-10 Nov, 2008.
14. Nader El-Bagoury, 1st Taif Univeristy scientific conference, Faculty of Science, 14-18
2009.
15. Mohamed A. Amin, N. El-Bagoury, International Conference on Materials Science an
Applications, Development and Innovation, 13-15 Feb 2012, TAIF University, KINGDOM
SAUDI ARBIA.

1. Nader El-Bagoury and Adel Nofal, "Investment Casting of Ni Base Superal

International Seminar on Recent Trends in Investment Casting, 12-13 Feb. 2007, CM
Cairo, Egypt.
2. Nader El-Bagoury, Adel Nofal, Kauro Yamamoto, Hirofumi Miyahara and Kiesaku Ogi
"Development of Rhenium Alloyed Inconel 718 Alloy" Egyptian-German workshop on Mate
Based Manufacturing Technology, Cairo-Egypt, 7-9 May, CMRDI, Cairo, Egypt.

1. Development and Protection of Materials Resistant Metal Dusting in Oil and

Industry.
2. Effect of Casting Variables on Microstructure and Properties of GTD-111 Alloy.
3. Influence of Heat Treatment Conditions on Microstructure, Mechanical Properties
Corrosion behaviors of Ni Base Superalloys.
4. Solidification and Phase Transformation of Shape Memory Alloys.
5. Synthesis of High Density Mullite- Based composites for High Temperature Applications.
6. Synthesis of Nano crystalline Ni-Mn Ferrites for Magnetic Applications in TV.
7. An Investigation on a failed turbocharger turbine blade. (Arabian-Britain for Eng
Company EGYPT)
8. Failure analysis of a petrochemical reactor. (SABIC Company Kingdom of Saudi Ara
9. High Temperature Corrosion of Coated Stainless Steel Alloys. (Aramco Kingdom
Saudi Arabia)
10. Aqueous Corrosion of Steel and Stainless Steel Alloys. (Aramco Kingdom of S
Arabia)

1. Best paper in Spring Conference of Japan Foundry Engineering Society No 146, Tokyo. (May 200
2. Chosen as an Ambassador for Kyushu University. (March 2006)
3. Chosen as a Reviewer in the Journal of Materials Science and Engineering A. (April 2008)
4. Chosen as a Reviewer in the Journal of Alloys and Compounds. (Jan. 2009)
5. Chosen as a Reviewer in the Journal of Materials Design. (Mar. 2010)
6. Chosen as a Reviewer in the Journal of Phase Transition. (Mar. 2011)
24

1997
TOEFL 2002
2003
2004
1994
1995

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- 1968 / 3 / 11:-
hessien@hotmail.com
&
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( 2003

-1
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28

 - -5
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2008 -2007 -9
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2008-2007
-2008 -11
2009
2009-2008- -12

1- Materials Science and Engineering B (Elsevier Publishing)
2- Applied Surface Science (Elsevier Publishing)
3- Materials Research Bulletin (Elsevier Publishing)
4- Journal of Alloys and Compounds (Elsevier Publishing)
5- Journal of Ironmaking and Steelmaking (Maney Publishing)
6- Journal of Magnetism and Magnetic materials (Elsevier Publishing)
7- Journal of Materials science (SpringerLink Publishing)
1234-

Transformation of silica fume secondary resources of ferrosilicon alloys to chemical mechanical
polishing (CMP) slurry for semiconductor applications, Junior Scientist, USA-Egypt Joint
Program, 2006-2008
Bioactive nano-magnetic Materials for Hyperthermia Treatment of Cancer and for Bone
Reconstruction Scaffolds, Principal Investigator, STFD, 2009, Egypt.
Hexagonal strontium and barium ferrites nanoparticles for microwave absorbance and magnetic
applications" Head of Group, STFD May 2009, Egypt.
CaSnO-materials for carbon monoxide sensing and catalysis, Co-principal Investigator ,
Swedish-Mena Program, May 2008.

( )

29

Insitu synthesis and sintering -1

10

10

10

of MoSi2/zirconia mullite
composite for high temperature
applications
Synthesis of molybdenum-2
silicide/mullite composites for
high temperature applications
Extension for the above-3
project
Fabrication of soft and hard -3
nanocrystalline ferrite from the
iron oxides by-product for
magnetic and electronic
applications
Synthesis of -4
nanocrystalline Ni-Mn
Ferrites for Magnetic
Applications in TV

Synthesis of magnetic -5
nanometer pigment Fe3O4 by
co-precipitation and
.combustion reaction
Synthesis of -6
nanocrystalline Magnseium
Ferrites from secondary iron
oxide (mill scale) for
Magnetic Applications

1.

M. M. Hessien, Z. I. Zaki, Q. Mohsen, " Synthesis of Nanocrystalline Magnesium Ferrites Powder

from Mill Scale", International Journal of Material Science IJMS Vol.1 Iss.1 (2011) 30-34

2.

M.M.Hessien, Q.Mohsen, A.El-Maghraby, " Synthesis of magnetic nanometer pigment Fe3O4 by

co-precipitation and gaseous reduction", Chemical Technology : An Indian Journal, In press 2012
3.

M.M.Hessien, Z.I.Zaki, Q.Mohsen," Synthesis of nanocrystalline Ni-Mn ferrites for magnetic

applications by oxalate precursor rout", Materials Science : An Indian Journal In press 2012
4. Z. I. Zaki, M. M. Hessien, Synthesis of molybdenum silicide/mullite composites for high
temperature applications International Journal of Self Propagating High Temperature Synthesis,
20, 2 (2011) 7281.
5. M.M. Hessien et. al., Structural properties of ferric pseudobrookite Fe2TiO5 powder by new
method International Journal of Nanoparticles, Vol. 4, No. 1, 2011
30

6. M.M. Rashad, M.M. Hessien, E.A. Abdel-Aal, K. El-Barawy, R.K. Singh, Transformation of silica
fume into Chemical Mechanical Polishing (CMP) nano-slurries for advanced semiconductor
manufacturing, Powder Technology, Volume 205, Issues 1-3, 10 January 2011, Pages 149-154
7. Said. M. El-Sheikh, Farid A. Harraz, Mamhoud M. Hessien , Magnetic behavior of cobalt ferrite
nanowires prepared by template-assisted technique Materials Chemistry and Physics, Volume
123, Issue 1, 1 September 2010, Pages 254-259
8. M.M. Rashad, M.M, Hessien, A. El-Midany, I.A. Ibrahim , Effect of synthesis conditions on the
preparation of YIG powders via co-precipitation method , Journal of Magnetism and Magnetic
Materials, Volume 321, Issue 22, November 2009, Pages 3752-3757
9. M.M. Hessien, M.M. Rashad, R.R. Zaky, E.A. Abdel-Aal, K.A. El-Barawy, Controlling the
synthesis conditions for silica nanosphere from semi-burned rice straw, Materials Science and
Engineering: B, Volume 162, Issue 1, 15 May 2009, Pages 14-21
10. N.M. Deraz, M.M. Hessien, "Structural and magnetic properties of pure and doped nanocrystalline
cadmium ferrite", Journal of Alloys and Compounds, Volume 475, Issues 1-2, 5 May 2009, Pages
832-839
11. M. M. Hessien, M. M. Rashad, M. S. Hassan, K. El-Barawy, "Synthesis and magnetic properties of
strontium hexaferrite from celestite ore", Journal of Alloys and compounds, Volume 476, Issues 1-2,
12 May 2009, Pages 373-378
12. Y.M.Z. Ahmed, M. M. Hessien, M.M. Rashad, I.A. Ibrahim, " Nano-crystalline copper ferrites from
secondary iron oxide (mill scale" J. Journal of Magnetism and Magnetic Materials, Volume 321,
Issue 3, February 2009, Pages 181-187
13. S. A. M. Abdel-Hameed, M. M. Hessein, M. A. Azooz, "Preparation and characterization of some
ferromagnetic glass- ceramics contains high quantity of magnetite",

Ceramics International,

Volume 35, Issue 4, May 2009, Pages 1539-1544

14. E. M. M. Ewais, M. M. Hessien, A. A. El-Geassy, " In-Situ synthesis of magnetic Mn-Zn ferrite
ceramic object by solid state reaction", J. Aust. Ceram. Soc. 44 [1] (2008) 57-62
15. M. M. Hessien, "Synthesis and characterization of lithium ferrite by oxalate precursor route",
Journal of Magnetism and Magnetic Materials, Journal of Magnetism and Magnetic Materials 320
(2008) 2800-2807.
16. R.R. Zaky , M.M. Hessien , A.A. El-Midany, M.H. Khedr , E.A. Abdel-Aal , K.A. El-Barawy;

31

"Preparation of silica nanoparticles from semi-burned rice straw ash", Powder Technology, 185
(2008) 31-35.
17. M. M. Hessien, M. M. Rashad, K. El-Barawy and I. A. Ibrahim; "Influence of manganese
substitution and annealing temperature on the formation, microstructure and magnetic properties of
Mn-Zn ferrites", Journal of Magnetism and Magnetic Materials 320 (2008) 16151621.
18. M. M. Rashad, R.S. Mohamed, M. M. Hessien, I. A. Ibrahim, A. T. Kandil "Synthesis and
Characterization of lead titanate nanopowders by organic acid precursor" J. Optoelectronic and
Advanced Materials, 10 (2008)1026-1031
19. M. M. Rashad, M. Radwan, M. M. Hessien Effect of Fe/Ba mole ratio and surface active agent on
the formation of barium hexaferrite Journal of Alloys and Compounds, Volume 453, Issues 1-2, 3
April 2008, Pages 304-308.
20. M. M. Hessien, M. M. Rashad, K. El-Baraway Controlling the structure and the magnetic
properties of strontium hexaferrite synthesized by co-precipitation method Journal of Magnetism
and Magnetic Materials 320 (2008) 336343
21. M. M Hessien, Y. kashiwaya, K. Ishii, M. I. Nasr, A. A. El-Geassy, "Effect of barite on
mineralogical composition and structure of iron ore sinter, Journal of Ironmaking & Steelmaking,
35, 3 (2008) 169-178.
22. M. M Hessien, Y. kashiwaya, K. Ishii, M. I. Nasr, A. A. El-Geassy, " Characterisation of iron ore
sinter and its behaviour during non-isothermal reduction conditions", Journal of Ironmaking &
Steelmaking, 35, 3 (2008) 183-190.
23. M. M Hessien, Y. kashiwaya, K. Ishii, M. I. Nasr, A. A. El-Geassy, " Sintering and heating
reduction processes of alumina containing iron ore samples, Journal of Ironmaking & Steelmaking,
35, 3 (2008) 191-204.
24. M. M Hessien and M. H. Khedr; Catalytic activity and magnetic properties of barium hexaferrite
prepared from barite ore, Materials Research Bulletin, Volume 42, Issue 7, 3 July (2007), 1242
25. M. Radwan, M.M. Rashad, M.M. Hessien, "Synthesis and characterization of barium hexaferrite
nanoparticles", Journal of Materials Processing Technology, 181(2007) 106-109.
26. M. M. Hessien, M. Radwan, M. M. Rashad, "Enhancement of magnetic properties for the barium
hexaferrite prepared through ceramic route", Journal of Analytical and Applied Pyrolysis, Volume
78, Issue 2, March 2007, 282-287.

32

27. M. Bahgat, M. Radwan, M.M. Hessien, "Reduction behavior of barium hexaferrite into metallic
iron nanocrystallites", Journal of Magnetism and Magnetic Materials, Volume 310 ( 2007, 107115>
28. M. I. Nasr, A. A. Omar, M. M. Hessien, A. A. El-Geassy; Carbon monoxide reduction and
accompanying swelling of iron oxide compacts; ISIJ International, Vol.36, (1996), P 164
171.
29. A. A. El-Geassy, M. I. Nasr, M. M. Hessien; Effect of reducing gas on the volume change
during reduction of iron oxide compacts; ISIJ International, Vol.36, (1996), P 640 -649.

33


1-

Family

)(Reviewer Record

Second
Third
Ramadan
Eid

First
Mohamed

Name

)Telephone No.) (Mobile) 0530786037
mrnais3@yahoo. Com
m.ramadan@uoh.edu.sa :
:
:
:
:
:
:
:
.

2-
) ( Reviewer Record

Family
Al-Axir

Third
Afifi

Second
Hassan

First
Mohamed

Name

): (Complete Mailing Address

34

 ): (.Telephone No
)Home) :
Work) : :
)0592859451
0592859451
Mobile) :
)0592859451
)E-Mail) : axir56@yahoo.com
) : ( Nationality
......................................................................................
.......
) : ( University
...................................................................................
....
): (College
....................................................................................
....................
) : (Department
) : (Academic Title
.................................................................................
) : ( Major Field .
):( Specialization and Research Activities

3-
) ( Reviewer Record

Family
Masseud

Third
Mohamed

Second
Ibrahim

First
Masseud

Name

): (Complete Mailing Address

35

 ): (.Telephone No
)Home) : 0563774476
)Work) : 0563774476
)Mobile) : 0563774476
)E-Mail) : Ibrahim_64@yahoo.com
) : ( Nationality
) : ( University

): (College

): (Department
) : (Academic Title
) : ( Major Field
):( Specialization and Research Activities
Stress Analysis - Fracture Mechanics Advanced materials

4-
) ( Reviewer Record

Family
Ghanem

Third
Mohamed

Second
Mosalam

First
Mohamed

)(Complete Mailing Address

): (.Telephone No

36

Name

Home) :)

Work) : 0597528337)
0597528337
Mobile) : 0597528337)
E-Mail) : ghanem105@yahoo.com)
: ( Nationality )
: ( University )

: (College)

: (Department)
: (Academic Title )
: ( Major Field )

:( Specialization and Research Activities)

Stress Analysis - Fracture Mechanics - Alloys design Advanced materials - Welding

37

 5-

Family

))Reviewer Record

Second
Third
Mohamed
Hafez

First
Khaled

Name

)(Telephone No.
: k.hafez@uoh.edu.sa

(Mobile) 0533408306

:
:
:
:
:
:
:
.

38