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Q Condensor
QD
QF
QLn+1
QW
Q reboiling
BT
CT2
DT3
CH3COOH
P-xylene
-18.944
-11.035
1.0971
1.515
-2.89E-03
-3.90E-03
2.93E-06
3.92E-06
H2O
N Butyl
Acetat
1.83E+01
4.72E-01
-1.34E-03
1.31E-06
122.827
6.59E-01
-1.84E-03
2.63E-06
cp L
BT
CT2
DT3
Komponen
BT
CT2
DT3
CH3COOH
P-xylene
4.84
-25.901
2.55E-01
6.04E-01
-1.75E-04
-3.37E-04
4.95E-08
6.82E-08
H2O
3.40E+01
13.62
-1.00E-02
5.49E-01
3.00E-05
-2.58E-04
-2.00E-08
1.10E-08
N Butyl Acetat
cp g =
(A
+
BT
Data temperatur dari hasil perhitungan :
Temperatur destilat
= 95 C = 368 K
Temperatur refluks
= 95 C
CT2
DT3
= 368 K
= 119.0871 C = 392.0871 K
= 25 C = 298 K
Menghitung V hV =
V = laju alir mol komponen fase uap
T Uap = 392.0871 K
= 940.871
Komponen
CH3COOH
H20
NBA
D
cpL
mol/h
J/jam
32.049811 9364.865233
342.42469 5267.154449
68.870523 16498.66447
3240017.567
Ln+1
cpL
Moll/h
J/jam
145.43933 9364.865
1553.8943 5267.154
312.52862 16498.66
14702925.92
Tekanan
Perhitungan
Cp L = ( A + BT + CT2 + DT3
Komponen
CH3COOH
P-Xylene
H20
cp L
massa
Mol
n cp L
J/mol
Kg/jam
74996.55773 1249.943 12568.712 15710168.38
957.6195 9.034146 19279.096 174170.1756
324.4023414 18.02235 6996.6763 126096.5657
H keluar
14050858 J/jam
Q Destilat + Q Bottom
Q Destilat
= 3240018 J/jam
Q bottom
= 16010435 J/jam
Q Condensation
= -6439314 J/jam
95 % reboiling
(H keluar + Q condensation ) -
95 % reboiling
-1239719
J /jam
Q reboiling
-1304968
J/jam
-65248.4
J/jam
Q loss
H masuk
Q out (joule/jam)
H masuk
14050858.03
H keluar
1925043
Q reboiling
-1304967.59
Q Condensation
-6439314
Q loss
65248
12745890
127475890
Tout
Cp dt =
( Cp
T = t ref
Tin
( Cp
T = t ref
Kebutuhan Steam
Q reboiler dari hasil perhitungan neraca energi unit 1 distilasi =
- 1304968 J/jam
Q Condensor
QD
QF
QLn+1
QW
Q reboiling
Komponen
Komposisi Distilate
laju mol
massa
XD
mol/jam
Kg/jam
CH3COOH
0.00747644
1.707709
102.4625
0.0074764
2.56398488
153.8391
H20
Butyl Asetat
0.9885071
0.00401645
225.7868
0.917406
4064.163
106.5659
0.9885071
0.0040165
339.0004468
1.377410468
6102.008
160
Untuk menghitung Vhf, Dhd dan Ln+1Hn+1 , dibuthkan data konstanta kapasitas panas
Untuk fase cair dan gas
(diolah dari Yaws Handbook
Thermodynamic)
BT
CT2
DT3
CH3COOH
P-xylene
-18.944
-11.035
1.0971
1.515
-2.89E-03
-3.90E-03
2.93E-06
3.92E-06
H2O
N Butyl
Acetat
1.83E+01
4.72E-01
-1.34E-03
1.31E-06
122.827
6.59E-01
-1.84E-03
2.63E-06
cp L
BT
CT2
DT3
Komponen
BT
CT2
DT3
CH3COOH
P-xylene
4.84
-25.901
2.55E-01
6.04E-01
-1.75E-04
-3.37E-04
4.95E-08
6.82E-08
H2O
3.40E+01
13.62
-1.00E-02
5.49E-01
3.00E-05
-2.58E-04
-2.00E-08
1.10E-08
N Butyl Acetat
cp g =
(A
BT
CT2
= 80 C = 353 K
Temperatur refluks
= 80 C
= 353 K
= 100.0325 C = 373.0325 K
= 25 C = 298 K
Menghitung V hV =
V = laju alir mol komponen fase uap
DT3
T Uap = 373.0325 K
( A + BT + CT + DT
V
mol/h
cp g
J/mol
D
mol/h
cpL
J/mol
Ln+1
Mol/h
cpL
J/mol
CH3COOH
4.27169372
10092.81
2.563985
7315.2693
1.707708844
7315.269
H20
Butyl Asetat
564.787294 2611.197
2.29481683
12686.1
1546996.577
339.0004 4131.8782
1.37741
12829.68
1437136.536
225.7868468 4131.878
0.917406361 12829.68
957186.1336
Tekanan
Cp L = ( A + BT + CT2 + DT3
Perhitungan
Komponen
massa
Kg/jam
Mol
cp L
J/mol
n cp L
CH3COOH
H20
Butyl Asetat
= 3240018
H keluar =
J/jam
Q Destilat + Q Bottom
Q Destilat
= 1437137
J/jam
Q bottom
= 1829195
J/jam
= -847326
J/jam
Q Condensation
(H keluar + Q condensation ) -
95 % reboiling
-821013
J /jam
Q reboiling
-864224
J/jam
-43211.2
J/jam
Q loss
H masuk
3240018
Q reboiling
-864224
Q out (joule/jam)
H keluar
Q Condensation
Q loss
2375793.76
3266331.046
-847326
-43211.2
2375793.76
Kebutuhan Steam
Q reboiler dari hasil perhitungan neraca energi unit 1 distilasi =
Steam yang digunakan adalah superheated steam pada
Kondisi T steam masuk
Kondisi Tsteam out
T in = 150 C dan H spesifik = 2776000 joule/kg
T out = 120 C dan H spesifik = 2706300 joule/kg
Massa steam = Q / H
H = 2776000 2875000 = -69700joule/kg
Maka Massa steam = -864223.8043 / -69700
= 12.3991937 Kg/jam
-864223.8043 J/jam